#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/59/2225917.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225917_Fobs loop_ _publ_author_name 'Wang, Zhi-Gang' 'Xia, Zong-Lin' 'Wang, Rong' 'Wang, Ming-Li' _publ_section_title ; 4-[6,8-Dibromo-2-(2-chloro-5-nitrophenyl)-1,2,3,4-tetrahydroquinazolin-3-yl]cyclohexanol ; _journal_coeditor_code LH5014 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1205 _journal_page_last o1206 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.764 _cell_angle_beta 73.309 _cell_angle_gamma 84.750 _cell_length_a 10.2614 _cell_length_b 13.1418 _cell_length_c 16.9315 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8044 _[local]_cod_data_source_file lh5014Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 20080829a_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 359.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2668.55 3012.12 55.62 o 2 0 0 4239.16 4881.94 62.46 o 3 0 0 1531.36 1631.30 25.72 o 4 0 0 28462.72 27984.76 338.16 o 5 0 0 3125.85 3282.46 49.93 o 6 0 0 941.76 872.08 23.87 o 7 0 0 347.27 363.33 18.49 o 8 0 0 70.69 79.98 16.15 o 9 0 0 281.23 358.87 40.03 o 10 0 0 208.38 227.86 40.99 o 11 0 0 120.32 123.10 48.42 o 12 0 0 16.01 -4.43 46.75 o -12 1 0 37.43 43.63 48.42 o -11 1 0 65.02 99.96 44.59 o -10 1 0 91.52 116.51 43.63 o -9 1 0 150.84 160.85 35.12 o -8 1 0 2172.11 2023.74 71.08 o -7 1 0 138.64 151.37 19.96 o -6 1 0 12883.63 12995.23 193.64 o -5 1 0 21.75 -7.18 10.91 o -4 1 0 993.43 1249.93 23.06 o -3 1 0 3549.88 3989.98 53.11 o -2 1 0 6873.48 7618.76 138.92 o -1 1 0 269.74 257.58 10.55 o 1 1 0 1755.96 1830.41 34.16 o 2 1 0 974.36 919.10 21.58 o 3 1 0 2335.68 2224.39 45.07 o 4 1 0 12815.88 12708.47 278.08 o 5 1 0 4308.66 4382.51 98.77 o 6 1 0 1615.94 1414.86 30.39 o 7 1 0 10.14 22.23 12.76 o 8 1 0 1098.74 1169.06 33.22 o 9 1 0 3556.79 3738.57 66.78 o 10 1 0 114.30 108.12 37.52 o 11 1 0 313.66 274.48 47.70 o 12 1 0 253.27 216.59 56.33 o -11 2 0 186.37 145.75 51.06 o -10 2 0 38.69 127.41 39.79 o -9 2 0 615.86 460.51 45.43 o -8 2 0 134.22 96.01 31.28 o -7 2 0 79.18 94.57 25.17 o -6 2 0 1325.42 1336.57 28.67 o -5 2 0 7.24 11.21 7.96 o -4 2 0 4373.04 4378.74 59.48 o -3 2 0 2342.81 2363.07 33.43 o -2 2 0 28372.47 29152.73 507.37 o -1 2 0 10710.28 10593.72 187.94 o 0 2 0 1419.02 1550.52 18.51 o 1 2 0 922.75 917.18 16.47 o 2 2 0 259.74 322.19 14.14 o 3 2 0 25915.36 25403.10 424.07 o 4 2 0 1860.49 1851.50 43.99 o 5 2 0 163.98 219.34 32.00 o 6 2 0 3990.22 4026.42 68.68 o 7 2 0 420.55 431.73 20.65 o 8 2 0 0.15 4.68 16.01 o 9 2 0 91.23 79.53 42.79 o 10 2 0 77.85 78.87 33.80 o 11 2 0 218.78 228.46 47.94 o 12 2 0 101.35 164.09 48.54 o -11 3 0 254.71 282.75 51.78 o -10 3 0 0.74 -13.66 38.48 o -9 3 0 356.78 256.86 41.11 o -8 3 0 236.93 305.05 37.64 o -7 3 0 888.22 955.18 49.50 o -6 3 0 481.73 572.70 37.40 o -5 3 0 11666.80 12084.26 366.48 o -4 3 0 4315.94 4705.62 124.96 o -3 3 0 443.12 367.02 20.98 o -2 3 0 2340.62 2398.19 53.10 o -1 3 0 270.21 150.18 11.33 o 0 3 0 383.89 521.84 9.74 o 1 3 0 21701.16 21640.42 260.43 o 2 3 0 8703.88 8306.02 109.43 o 3 3 0 2158.56 2143.84 47.70 o 4 3 0 940.83 912.27 30.32 o 5 3 0 8298.24 8803.71 161.09 o 6 3 0 4907.04 4793.49 72.04 o 7 3 0 1359.49 1202.07 33.03 o 8 3 0 465.52 444.00 24.32 o 9 3 0 0.22 3.27 19.38 o 10 3 0 373.40 452.66 29.75 o 11 3 0 147.78 130.05 44.47 o 12 3 0 217.04 261.90 55.14 o -11 4 0 162.34 105.12 49.74 o -10 4 0 553.74 588.40 59.69 o -9 4 0 229.63 233.49 41.59 o -8 4 0 94.77 128.85 36.08 o -7 4 0 2.69 16.06 27.69 o -6 4 0 669.42 694.24 39.43 o -5 4 0 164.72 227.62 23.73 o -4 4 0 2017.44 2259.87 59.57 o -3 4 0 2085.36 2049.27 53.34 o -2 4 0 162.88 135.32 13.06 o -1 4 0 120.61 120.98 5.64 o 0 4 0 148.49 250.70 8.62 o 1 4 0 349.69 381.67 11.01 o 2 4 0 2135.01 2158.60 37.09 o 3 4 0 4555.02 4901.50 94.69 o 4 4 0 13853.01 14033.27 245.84 o 5 4 0 1156.03 1039.92 38.72 o 6 4 0 1044.64 934.80 38.00 o 7 4 0 4140.16 3870.32 67.54 o 8 4 0 521.07 456.57 25.25 o 9 4 0 85.26 59.46 20.09 o 10 4 0 1.96 -2.34 21.91 o 11 4 0 61.62 1.14 36.86 o -11 5 0 10.44 -30.92 50.46 o -10 5 0 595.01 669.07 60.53 o -9 5 0 176.51 186.38 45.79 o -8 5 0 193.93 185.43 37.52 o -7 5 0 217.60 208.92 33.80 o -6 5 0 1410.25 1671.83 60.29 o -5 5 0 1493.14 1454.76 52.14 o -4 5 0 4372.10 4769.17 104.88 o -3 5 0 88.10 72.28 15.22 o -2 5 0 642.26 814.07 23.43 o -1 5 0 18508.69 17975.64 194.91 o 0 5 0 3001.48 3500.45 42.58 o 1 5 0 7512.81 7381.40 81.98 o 2 5 0 846.78 741.35 21.73 o 3 5 0 8116.02 8496.08 117.97 o 4 5 0 2661.50 2964.06 68.44 o 5 5 0 69.21 92.77 19.90 o 6 5 0 1253.67 1249.32 45.31 o 7 5 0 72.10 30.09 20.98 o 8 5 0 44.01 53.83 18.22 o 9 5 0 277.09 298.82 24.83 o 10 5 0 22.23 79.85 23.84 o 11 5 0 1.07 -24.36 26.91 o -11 6 0 2.08 81.63 50.46 o -10 6 0 43.39 -33.08 42.67 o -9 6 0 525.05 403.45 52.86 o -8 6 0 168.10 226.90 40.15 o -7 6 0 2297.71 2507.02 82.23 o -6 6 0 84.43 43.03 26.61 o -5 6 0 804.53 668.23 38.96 o -4 6 0 1500.16 1262.98 45.07 o -3 6 0 413.15 427.67 27.45 o -2 6 0 2880.91 3137.08 39.63 o -1 6 0 6798.38 7192.88 80.18 o 0 6 0 253.24 270.06 12.38 o 1 6 0 12667.96 13170.06 140.94 o 2 6 0 814.89 890.52 19.42 o 3 6 0 2608.52 2797.55 50.67 o 4 6 0 37.62 18.70 16.78 o 5 6 0 1913.53 2047.48 58.37 o 6 6 0 245.73 249.55 26.49 o 7 6 0 416.86 332.14 31.76 o 8 6 0 2203.29 2025.49 69.04 o 9 6 0 37.86 2.75 19.96 o 10 6 0 340.48 372.00 30.64 o 11 6 0 68.30 74.43 40.51 o -10 7 0 174.80 136.04 47.94 o -9 7 0 152.08 215.87 44.71 o -8 7 0 110.68 125.26 37.04 o -7 7 0 1418.07 1217.07 58.85 o -6 7 0 541.47 529.07 39.43 o -5 7 0 364.06 372.77 32.24 o -4 7 0 1210.40 1165.05 47.47 o -3 7 0 2802.67 2799.25 71.68 o -2 7 0 520.67 311.82 12.41 o -1 7 0 601.25 642.58 37.21 o 0 7 0 2873.44 3001.94 53.17 o 1 7 0 1885.08 1791.58 41.62 o 2 7 0 20902.12 21988.80 229.54 o 3 7 0 79.45 116.27 23.31 o 4 7 0 703.17 706.58 36.08 o 5 7 0 1259.78 1210.12 46.99 o 6 7 0 830.31 839.03 44.23 o 7 7 0 161.13 158.70 29.97 o 8 7 0 44.48 49.82 18.86 o 9 7 0 9.08 14.26 29.37 o 10 7 0 226.57 174.64 38.60 o 11 7 0 50.87 80.67 38.72 o -10 8 0 161.03 85.34 47.35 o -9 8 0 140.18 127.17 46.87 o -8 8 0 51.07 -9.71 33.56 o -7 8 0 8.96 -2.28 31.16 o -6 8 0 1530.63 1249.68 57.29 o -5 8 0 130.97 132.09 30.09 o -4 8 0 2170.63 1925.22 63.05 o -3 8 0 342.03 320.88 24.57 o -2 8 0 390.02 448.32 24.07 o -1 8 0 941.80 1022.29 33.19 o 0 8 0 728.28 863.71 21.41 o 1 8 0 79.56 66.35 10.78 o 2 8 0 174.39 205.61 13.46 o 3 8 0 46.49 21.74 15.61 o 4 8 0 1192.40 1218.32 37.85 o 5 8 0 1814.33 1810.39 60.29 o 6 8 0 309.67 315.60 32.84 o 7 8 0 816.86 843.47 48.66 o 8 8 0 414.36 411.84 42.79 o 9 8 0 24.52 30.09 33.80 o 10 8 0 85.35 95.77 38.24 o -9 9 0 115.14 130.53 45.67 o -8 9 0 18.97 9.11 34.64 o -7 9 0 23.40 10.55 36.68 o -6 9 0 789.67 767.71 50.34 o -5 9 0 66.14 30.68 26.85 o -4 9 0 318.24 268.51 25.02 o -3 9 0 334.45 395.63 25.34 o -2 9 0 21.51 16.06 15.87 o -1 9 0 2925.91 2567.13 39.69 o 0 9 0 2479.13 2577.41 40.36 o 1 9 0 352.21 327.24 16.29 o 2 9 0 144.03 98.00 13.59 o 3 9 0 1473.52 1694.90 108.12 o 4 9 0 348.56 292.38 41.11 o 5 9 0 1484.35 1556.76 59.93 o 6 9 0 174.45 141.20 29.85 o 7 9 0 17.67 1.20 29.73 o 8 9 0 87.56 123.58 34.76 o 9 9 0 44.91 95.89 38.24 o 10 9 0 120.80 106.08 40.63 o -9 10 0 94.96 30.09 48.42 o -8 10 0 23.60 -37.52 42.19 o -7 10 0 86.75 72.76 37.28 o -6 10 0 36.42 44.11 36.08 o -5 10 0 251.78 225.88 27.96 o -4 10 0 251.94 299.69 27.44 o -3 10 0 1158.61 1118.84 40.60 o -2 10 0 37.78 36.70 18.92 o -1 10 0 38.35 18.92 17.93 o 0 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129.21 42.43 o 0 12 0 2.52 11.39 39.19 o 1 12 0 388.17 383.64 36.56 o 2 12 0 32.32 43.56 23.61 o 3 12 0 12.39 27.48 24.81 o 4 12 0 281.06 214.86 28.36 o 5 12 0 269.49 350.83 43.27 o 6 12 0 0.96 1.68 35.00 o 7 12 0 50.44 37.04 40.87 o 8 12 0 171.60 178.11 45.07 o -6 13 0 2.07 10.91 52.86 o -5 13 0 366.67 400.34 61.49 o -4 13 0 37.57 -0.72 48.18 o -3 13 0 32.44 -0.48 42.79 o -2 13 0 6.90 9.95 42.55 o -1 13 0 96.86 64.13 47.11 o 0 13 0 40.06 -22.53 40.15 o 1 13 0 25.00 16.90 41.71 o 2 13 0 56.12 43.68 26.28 o 3 13 0 25.90 14.62 25.06 o 4 13 0 1.42 -7.90 29.01 o 5 13 0 6.66 12.59 38.48 o 6 13 0 31.13 62.33 46.03 o 7 13 0 8.67 59.33 45.31 o -5 14 0 43.59 42.67 56.69 o -4 14 0 36.98 3.84 48.66 o -3 14 0 53.12 101.04 52.02 o -2 14 0 187.25 183.75 53.46 o -1 14 0 308.48 384.40 59.69 o 0 14 0 189.73 190.82 51.30 o 1 14 0 0.18 35.24 45.19 o 2 14 0 14.38 74.19 47.70 o 3 14 0 213.84 201.50 34.67 o 4 14 0 250.57 269.66 36.20 o 5 14 0 73.33 82.17 33.90 o 6 14 0 0.96 3.72 44.47 o -3 15 0 58.42 111.47 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