#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/59/2225925.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225925_Fobs loop_ _publ_author_name 'Jenkinson, Sarah F.' 'Crabtree, Elizabeth V.' 'Glawar, Andreas F. G.' 'Butters, Terry D.' 'Fleet, George W. J.' 'Watkin, David J.' _publ_section_title ; 2-Acetamido-N-benzyl-1,4-imino-1,2,4-trideoxy-L-xylitol (N-benzyl-L-XYLNAc) ; _journal_coeditor_code LH5029 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1147 _journal_page_last o1148 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 10-03-31 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 4.97310(10) _cell_length_b 10.0145(3) _cell_length_c 26.9297(7) _[local]_cod_data_source_file lh5029Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 494.90 560.11 20.10 o 4 0 0 64.80 69.74 3.70 o 6 0 0 34.40 33.35 3.70 o 2 1 0 259.40 253.38 5.40 o 3 1 0 0.50 0.34 0.85 o 4 1 0 1.20 0.17 0.70 o 5 1 0 6.50 5.66 1.10 o 6 1 0 -1.60 0.44 1.90 o 1 2 0 3627.60 3828.99 117.30 o 2 2 0 308.30 267.67 6.70 o 3 2 0 10.10 9.26 1.00 o 4 2 0 287.20 276.06 11.40 o 5 2 0 23.60 23.26 1.40 o 6 2 0 8.40 9.34 3.10 o 1 3 0 48.00 53.72 1.00 o 2 3 0 36.40 27.88 1.30 o 3 3 0 65.40 74.39 2.10 o 4 3 0 4.60 2.64 1.90 o 5 3 0 129.70 110.45 4.20 o 6 3 0 3.20 11.00 2.80 o 0 4 0 10.80 11.07 0.60 o 1 4 0 70.70 68.64 1.30 o 2 4 0 2.80 2.96 0.50 o 3 4 0 55.60 67.90 1.80 o 4 4 0 71.60 68.90 2.70 o 5 4 0 23.00 25.96 1.90 o 6 4 0 -1.10 0.06 2.90 o 1 5 0 442.20 389.06 9.30 o 2 5 0 170.40 172.58 4.50 o 3 5 0 51.40 46.63 2.30 o 4 5 0 38.70 38.84 1.90 o 5 5 0 0.00 0.02 0.01 o 0 6 0 32.20 34.19 1.50 o 1 6 0 29.80 30.28 1.00 o 2 6 0 54.60 48.09 2.20 o 3 6 0 30.70 39.19 1.50 o 4 6 0 89.70 86.75 2.90 o 5 6 0 7.80 3.07 2.40 o 1 7 0 10.30 8.85 0.70 o 2 7 0 2.50 4.80 1.00 o 3 7 0 55.00 58.49 3.30 o 4 7 0 2.60 5.63 1.60 o 5 7 0 3.70 6.02 2.60 o 0 8 0 25.40 21.89 2.90 o 1 8 0 1.90 2.24 0.60 o 2 8 0 128.30 120.26 5.60 o 3 8 0 35.60 34.52 2.70 o 4 8 0 2.80 5.81 1.50 o 5 8 0 3.80 4.21 3.00 o 1 9 0 7.20 7.68 1.60 o 2 9 0 -0.40 0.00 2.15 o 3 9 0 2.80 6.29 2.10 o 4 9 0 8.70 11.91 4.20 o 0 10 0 4.00 5.42 1.80 o 1 10 0 26.10 20.74 2.80 o 2 10 0 0.10 0.00 1.39 o 3 10 0 7.10 8.28 3.00 o 4 10 0 13.80 20.19 4.20 o 1 11 0 2.90 5.27 1.70 o 2 11 0 0.40 0.77 2.66 o 3 11 0 4.50 2.14 4.80 o 1 12 0 2.50 0.19 2.90 o 2 12 0 13.40 13.91 3.90 o 2 0 1 1004.40 991.87 22.40 o 3 0 1 262.30 255.26 7.60 o 4 0 1 1.40 0.38 1.10 o 5 0 1 245.20 217.08 5.90 o 6 0 1 2.70 6.89 2.10 o 2 1 1 80.90 77.22 1.31 o 3 1 1 73.40 54.30 1.71 o 4 1 1 21.55 21.32 0.85 o 5 1 1 39.80 40.92 1.56 o 6 1 1 14.85 22.88 2.04 o 1 2 1 1160.95 1222.07 15.67 o 2 2 1 12.75 11.75 0.49 o 3 2 1 56.85 52.00 1.56 o 4 2 1 29.20 30.63 1.61 o 5 2 1 86.65 85.33 2.11 o 6 2 1 19.90 21.71 3.30 o 0 3 1 0.30 0.21 0.22 o 1 3 1 47.90 51.89 0.64 o 2 3 1 26.70 23.05 0.81 o 3 3 1 39.75 41.92 1.25 o 4 3 1 80.95 76.79 1.84 o 5 3 1 38.70 37.12 1.52 o 6 3 1 3.35 8.77 2.97 o 0 4 1 159.60 174.17 2.50 o 1 4 1 590.75 572.19 6.91 o 2 4 1 3.65 8.13 0.43 o 3 4 1 80.70 86.62 1.70 o 4 4 1 54.80 58.17 1.49 o 5 4 1 14.95 17.36 1.54 o 6 4 1 9.00 14.07 2.62 o 0 5 1 5.50 7.24 0.50 o 1 5 1 11.10 12.14 0.50 o 2 5 1 9.15 9.71 0.68 o 3 5 1 574.05 526.31 9.94 o 4 5 1 163.95 156.65 3.92 o 5 5 1 14.70 14.65 1.49 o 0 6 1 395.50 367.20 6.80 o 1 6 1 39.65 35.25 0.93 o 2 6 1 26.85 26.62 1.03 o 3 6 1 64.85 71.62 1.98 o 4 6 1 29.05 28.51 1.13 o 5 6 1 4.95 6.43 1.70 o 0 7 1 517.10 501.43 10.40 o 1 7 1 135.75 133.12 2.23 o 2 7 1 92.05 88.34 2.54 o 3 7 1 25.00 26.79 1.36 o 4 7 1 11.55 13.42 1.27 o 5 7 1 10.65 7.46 1.88 o 0 8 1 3.90 5.77 1.10 o 1 8 1 40.40 44.05 1.49 o 2 8 1 12.70 13.59 1.13 o 3 8 1 7.40 9.48 1.29 o 4 8 1 2.25 3.85 1.06 o 5 8 1 11.70 10.43 1.94 o 0 9 1 145.20 134.41 5.40 o 1 9 1 136.30 120.54 4.36 o 2 9 1 11.35 12.29 1.38 o 3 9 1 0.30 2.03 1.53 o 4 9 1 23.15 21.55 2.43 o 0 10 1 2.20 0.39 1.90 o 1 10 1 3.55 4.09 1.24 o 2 10 1 7.90 8.98 1.56 o 3 10 1 13.10 8.75 3.16 o 4 10 1 22.00 19.36 6.20 o 0 11 1 8.80 8.29 2.20 o 1 11 1 20.60 19.18 2.51 o 2 11 1 8.90 6.83 2.94 o 3 11 1 7.20 7.75 2.34 o 2 12 1 23.60 16.69 3.59 o 2 0 2 81.60 72.72 1.80 o 3 0 2 45.40 55.77 1.60 o 4 0 2 28.00 33.20 1.30 o 5 0 2 15.60 16.23 1.50 o 6 0 2 29.40 30.69 3.30 o 2 1 2 39.05 33.57 0.78 o 3 1 2 19.70 20.09 0.67 o 4 1 2 6.70 14.20 0.74 o 5 1 2 40.20 43.93 1.90 o 6 1 2 9.80 12.64 2.48 o 1 2 2 311.05 319.88 3.89 o 2 2 2 68.40 67.52 1.24 o 3 2 2 49.75 51.27 1.65 o 4 2 2 37.95 35.88 1.86 o 5 2 2 78.05 71.28 1.81 o 6 2 2 11.15 10.02 2.59 o 0 3 2 6.50 4.47 0.30 o 1 3 2 1373.80 1390.37 13.90 o 2 3 2 426.65 376.87 6.26 o 3 3 2 100.10 111.36 2.59 o 4 3 2 67.85 61.96 1.63 o 5 3 2 33.70 31.27 1.49 o 6 3 2 8.15 5.81 2.93 o 0 4 2 53.60 59.10 1.00 o 1 4 2 572.35 542.01 6.63 o 2 4 2 28.30 34.96 0.74 o 3 4 2 8.05 11.47 0.71 o 4 4 2 64.25 70.18 1.79 o 5 4 2 28.45 28.56 1.56 o 6 4 2 10.20 10.76 3.39 o 0 5 2 1244.40 1171.14 21.30 o 1 5 2 857.90 804.71 11.88 o 2 5 2 61.80 69.48 1.59 o 3 5 2 32.85 28.35 1.10 o 4 5 2 34.30 38.96 1.38 o 5 5 2 18.75 14.44 1.88 o 0 6 2 67.00 68.11 1.60 o 1 6 2 83.50 79.92 1.46 o 2 6 2 84.95 87.25 2.09 o 3 6 2 90.65 90.14 2.54 o 4 6 2 10.10 13.33 0.92 o 5 6 2 1.50 2.35 1.66 o 0 7 2 17.70 21.91 1.10 o 1 7 2 29.85 32.95 1.10 o 2 7 2 129.65 117.28 3.34 o 3 7 2 42.95 42.95 1.71 o 4 7 2 48.10 44.57 1.67 o 5 7 2 4.85 3.21 1.87 o 0 8 2 26.60 29.74 1.60 o 1 8 2 11.80 15.56 0.92 o 2 8 2 22.40 23.84 1.45 o 3 8 2 17.10 16.07 1.48 o 4 8 2 2.00 0.81 1.25 o 5 8 2 18.95 21.08 2.45 o 0 9 2 21.00 22.14 1.60 o 1 9 2 58.90 60.14 1.92 o 2 9 2 36.65 39.13 2.02 o 3 9 2 32.80 27.80 3.00 o 4 9 2 5.55 5.73 2.39 o 0 10 2 258.60 214.08 10.50 o 1 10 2 1.15 1.35 1.64 o 2 10 2 0.30 2.06 1.32 o 3 10 2 4.10 4.22 2.10 o 4 10 2 42.70 36.95 5.60 o 0 11 2 2.10 8.77 2.20 o 1 11 2 12.25 15.24 2.16 o 2 11 2 4.55 9.32 2.11 o 3 11 2 11.75 10.88 3.22 o 0 12 2 3.20 5.98 2.70 o 2 0 3 48.20 51.33 1.10 o 3 0 3 374.70 351.23 8.50 o 4 0 3 103.50 94.87 3.00 o 5 0 3 13.90 16.25 1.60 o 6 0 3 4.00 4.26 2.20 o 1 1 3 135.10 205.56 4.09 o 2 1 3 81.55 86.45 1.27 o 3 1 3 4.95 4.32 0.51 o 4 1 3 46.60 49.61 1.38 o 5 1 3 38.45 39.58 1.70 o 6 1 3 96.60 87.68 4.92 o 1 2 3 1539.85 1558.27 18.60 o 2 2 3 213.65 209.83 4.19 o 3 2 3 49.15 48.14 2.20 o 4 2 3 36.85 35.32 1.24 o 5 2 3 20.30 22.56 1.35 o 6 2 3 56.05 55.86 3.82 o 0 3 3 173.80 189.44 3.40 o 1 3 3 2.35 1.74 0.18 o 2 3 3 463.40 459.08 6.38 o 3 3 3 5.55 10.30 0.64 o 4 3 3 17.50 16.79 0.88 o 5 3 3 89.30 79.02 2.41 o 6 3 3 3.80 7.57 2.55 o 0 4 3 185.40 196.91 3.00 o 1 4 3 124.30 144.90 1.77 o 2 4 3 585.75 542.93 8.86 o 3 4 3 0.95 1.14 0.84 o 4 4 3 9.05 9.40 0.78 o 5 4 3 30.90 32.08 1.60 o 6 4 3 18.25 18.73 3.32 o 0 5 3 19.60 18.20 0.80 o 1 5 3 479.30 467.07 6.56 o 2 5 3 58.75 61.32 1.31 o 3 5 3 131.55 122.35 3.09 o 4 5 3 9.70 10.59 0.85 o 5 5 3 1.80 0.91 1.72 o 0 6 3 163.70 167.62 3.30 o 1 6 3 38.65 39.52 0.96 o 2 6 3 8.80 9.76 0.67 o 3 6 3 11.80 10.66 0.85 o 4 6 3 73.45 74.97 2.52 o 5 6 3 11.85 12.89 1.84 o 0 7 3 21.40 24.39 1.20 o 1 7 3 5.60 6.64 0.57 o 2 7 3 71.40 58.46 2.10 o 3 7 3 14.60 18.68 1.21 o 4 7 3 2.15 2.91 1.20 o 5 7 3 13.60 15.46 2.46 o 0 8 3 24.30 29.52 1.50 o 1 8 3 18.65 19.06 1.07 o 2 8 3 9.45 8.36 1.24 o 3 8 3 20.70 23.66 1.66 o 4 8 3 3.40 3.77 1.28 o 5 8 3 13.25 14.23 2.15 o 0 9 3 8.30 11.14 1.40 o 1 9 3 17.10 22.15 1.63 o 2 9 3 15.85 18.83 1.49 o 3 9 3 16.05 16.74 2.33 o 4 9 3 16.70 11.25 2.36 o 0 10 3 94.80 91.23 4.40 o 1 10 3 4.50 5.86 1.50 o 2 10 3 13.05 15.73 2.25 o 3 10 3 10.10 13.64 2.70 o 4 10 3 5.20 3.67 2.93 o 1 11 3 19.55 18.65 2.58 o 2 11 3 7.40 4.44 2.46 o 3 11 3 7.70 4.73 3.60 o 0 12 3 142.70 140.49 12.00 o 1 12 3 25.80 29.11 4.40 o 2 12 3 11.60 14.27 4.40 o 1 0 4 953.10 1392.94 36.30 o 2 0 4 120.20 121.53 2.70 o 3 0 4 33.70 38.09 1.50 o 4 0 4 5.80 3.61 0.80 o 5 0 4 9.40 15.44 1.30 o 6 0 4 -1.10 2.11 2.30 o 1 1 4 1618.10 1782.67 20.58 o 2 1 4 114.70 114.23 1.77 o 3 1 4 17.90 13.93 0.68 o 4 1 4 17.35 15.77 0.86 o 5 1 4 20.35 26.50 1.35 o 6 1 4 17.50 18.56 3.18 o 1 2 4 86.55 91.84 1.17 o 2 2 4 66.40 70.19 1.27 o 3 2 4 290.15 258.11 5.62 o 4 2 4 33.20 32.19 1.13 o 5 2 4 66.60 58.03 2.39 o 6 2 4 12.60 14.78 2.51 o 0 3 4 586.40 614.28 9.10 o 1 3 4 1.50 2.25 0.18 o 2 3 4 584.65 541.84 7.80 o 3 3 4 10.25 7.36 0.71 o 4 3 4 103.60 101.43 2.62 o 5 3 4 26.70 23.28 1.49 o 6 3 4 4.65 1.77 2.97 o 0 4 4 3.70 4.26 0.40 o 1 4 4 191.55 192.38 2.69 o 2 4 4 228.20 203.41 3.85 o 3 4 4 53.35 56.31 1.46 o 4 4 4 62.05 62.58 1.56 o 5 4 4 5.20 4.62 1.10 o 6 4 4 2.00 7.30 3.24 o 0 5 4 139.00 148.19 2.70 o 1 5 4 16.15 15.55 0.54 o 2 5 4 91.65 80.68 1.88 o 3 5 4 6.65 3.95 0.71 o 4 5 4 1.50 1.26 0.86 o 5 5 4 6.45 9.14 1.31 o 0 6 4 195.90 178.60 3.70 o 1 6 4 122.80 114.85 2.06 o 2 6 4 140.60 149.53 3.43 o 3 6 4 5.05 6.02 0.78 o 4 6 4 2.50 2.27 0.88 o 5 6 4 9.60 9.77 1.70 o 0 7 4 29.90 31.38 1.30 o 1 7 4 9.25 11.79 0.68 o 2 7 4 94.15 93.66 2.55 o 3 7 4 92.55 95.56 2.98 o 4 7 4 84.25 83.53 2.73 o 5 7 4 -0.25 1.47 2.54 o 0 8 4 24.30 23.14 1.60 o 1 8 4 49.75 57.37 1.51 o 2 8 4 2.95 5.37 1.03 o 3 8 4 45.55 46.90 2.79 o 4 8 4 11.80 12.10 1.31 o 5 8 4 -1.75 0.63 2.34 o 0 9 4 13.60 15.06 1.50 o 1 9 4 11.55 17.64 1.84 o 2 9 4 53.35 53.90 2.33 o 3 9 4 30.95 32.95 2.60 o 4 9 4 61.80 57.62 4.50 o 0 10 4 19.10 21.45 1.70 o 1 10 4 4.00 3.76 1.28 o 2 10 4 11.15 14.75 2.26 o 3 10 4 1.40 2.46 3.40 o 4 10 4 15.40 11.86 3.60 o 0 11 4 0.10 0.90 1.20 o 1 11 4 17.35 17.63 1.67 o 2 11 4 13.10 7.55 2.84 o 3 11 4 31.80 31.44 5.90 o 1 12 4 10.05 6.71 3.23 o 2 12 4 2.40 0.03 5.00 o 1 0 5 61.10 70.86 1.20 o 2 0 5 127.80 138.66 2.80 o 3 0 5 255.00 229.92 7.80 o 4 0 5 31.10 32.18 1.60 o 5 0 5 32.00 33.26 2.10 o 6 0 5 0.30 1.16 2.96 o 1 1 5 1737.50 1860.38 19.81 o 2 1 5 52.30 56.63 0.88 o 3 1 5 28.75 28.14 0.82 o 4 1 5 24.90 26.17 1.06 o 5 1 5 1.05 2.76 1.13 o 6 1 5 13.90 11.05 2.78 o 0 2 5 210.90 211.65 3.50 o 1 2 5 441.65 418.97 4.94 o 2 2 5 76.20 71.51 1.42 o 3 2 5 77.85 83.84 1.78 o 4 2 5 16.55 16.75 0.85 o 5 2 5 195.30 179.23 6.28 o 6 2 5 16.00 13.94 2.31 o 0 3 5 297.10 313.22 4.90 o 1 3 5 568.70 572.43 6.43 o 2 3 5 32.25 26.30 0.82 o 3 3 5 113.95 115.23 2.41 o 4 3 5 0.45 1.47 0.89 o 5 3 5 28.90 26.71 1.56 o 6 3 5 -1.70 0.74 2.76 o 0 4 5 579.10 538.09 8.90 o 1 4 5 356.95 347.04 4.40 o 2 4 5 303.60 294.82 4.87 o 3 4 5 64.25 64.45 1.85 o 4 4 5 149.10 144.47 3.75 o 5 4 5 11.35 13.92 1.34 o 6 4 5 0.80 0.23 2.32 o 0 5 5 297.30 296.85 5.40 o 1 5 5 50.45 50.15 1.08 o 2 5 5 20.75 23.95 0.88 o 3 5 5 62.45 64.52 1.83 o 4 5 5 64.85 63.62 2.16 o 5 5 5 3.25 3.60 1.17 o 0 6 5 1.50 1.83 0.50 o 1 6 5 8.25 10.67 0.60 o 2 6 5 57.45 60.45 1.73 o 3 6 5 26.35 28.14 1.13 o 4 6 5 81.50 75.43 2.30 o 5 6 5 19.85 21.79 1.77 o 0 7 5 2.80 3.85 0.70 o 1 7 5 376.70 370.86 6.41 o 2 7 5 3.10 0.85 0.74 o 3 7 5 43.70 44.60 2.39 o 4 7 5 1.60 1.21 1.23 o 5 7 5 5.60 7.10 1.64 o 0 8 5 7.80 8.79 1.50 o 1 8 5 442.55 417.80 9.34 o 2 8 5 44.25 44.40 1.88 o 3 8 5 42.90 36.60 2.76 o 4 8 5 5.55 5.63 1.21 o 5 8 5 2.40 2.33 2.23 o 0 9 5 17.40 20.19 2.90 o 1 9 5 174.35 165.17 5.60 o 2 9 5 14.40 12.98 1.52 o 3 9 5 19.20 17.28 2.24 o 4 9 5 9.60 9.85 2.40 o 0 10 5 19.90 21.23 2.50 o 1 10 5 8.35 7.66 1.38 o 2 10 5 6.15 5.39 2.31 o 3 10 5 25.45 21.21 2.60 o 4 10 5 1.60 0.22 2.50 o 0 11 5 22.10 20.03 4.00 o 1 11 5 0.35 1.79 1.71 o 2 11 5 11.35 12.76 3.18 o 3 11 5 11.60 9.50 2.90 o 1 12 5 1.60 0.76 2.70 o 2 12 5 3.50 5.42 2.19 o 1 0 6 275.40 302.82 4.10 o 2 0 6 11.90 13.15 0.60 o 3 0 6 101.90 103.30 2.90 o 4 0 6 3.30 4.91 0.70 o 5 0 6 28.90 29.59 2.20 o 6 0 6 9.50 9.38 3.30 o 1 1 6 722.50 783.05 7.32 o 2 1 6 1085.75 1055.27 14.47 o 3 1 6 33.60 31.37 1.14 o 4 1 6 219.20 215.89 5.73 o 5 1 6 27.20 30.57 1.67 o 6 1 6 3.85 6.24 1.78 o 0 2 6 1046.30 1045.13 18.00 o 1 2 6 471.60 466.05 5.69 o 2 2 6 186.55 185.48 3.29 o 3 2 6 5.90 6.78 0.58 o 4 2 6 219.35 203.10 3.98 o 5 2 6 8.90 8.06 1.22 o 6 2 6 2.45 7.76 2.76 o 0 3 6 4.10 9.74 0.30 o 1 3 6 87.30 94.14 1.20 o 2 3 6 381.10 359.17 6.35 o 3 3 6 384.55 363.62 9.14 o 4 3 6 259.90 251.18 4.70 o 5 3 6 78.35 71.72 2.97 o 6 3 6 5.85 11.64 2.57 o 0 4 6 228.10 235.59 4.20 o 1 4 6 51.00 50.53 0.92 o 2 4 6 53.70 51.65 1.17 o 3 4 6 19.95 19.66 0.96 o 4 4 6 161.35 149.98 4.23 o 5 4 6 98.40 92.08 3.32 o 6 4 6 5.35 2.89 2.57 o 0 5 6 22.30 23.44 1.00 o 1 5 6 57.75 57.10 1.17 o 2 5 6 154.30 155.64 3.40 o 3 5 6 50.50 48.08 1.61 o 4 5 6 7.70 9.01 1.37 o 5 5 6 12.90 13.74 1.52 o 0 6 6 138.50 141.27 3.00 o 1 6 6 17.85 25.68 0.76 o 2 6 6 8.80 11.09 0.67 o 3 6 6 73.20 70.83 2.20 o 4 6 6 19.85 19.82 1.90 o 5 6 6 29.10 22.16 2.39 o 0 7 6 211.10 202.37 5.70 o 1 7 6 57.65 63.27 1.71 o 2 7 6 87.95 89.15 2.19 o 3 7 6 43.50 40.95 2.29 o 4 7 6 4.15 4.34 1.03 o 5 7 6 0.85 1.81 1.87 o 0 8 6 94.90 95.52 5.30 o 1 8 6 80.70 71.28 2.32 o 2 8 6 18.35 18.70 1.75 o 3 8 6 26.60 30.32 2.14 o 4 8 6 0.90 3.22 1.77 o 1 9 6 59.45 55.37 2.40 o 2 9 6 34.00 34.48 2.59 o 3 9 6 0.55 2.31 3.40 o 4 9 6 2.70 1.60 1.74 o 0 10 6 -0.30 1.83 2.85 o 1 10 6 4.00 7.27 1.70 o 2 10 6 -0.65 2.71 3.47 o 3 10 6 7.70 9.35 1.93 o 0 11 6 5.80 3.54 3.80 o 1 11 6 8.25 7.15 2.44 o 2 11 6 10.20 12.92 3.30 o 3 11 6 3.40 0.89 3.09 o 1 12 6 2.15 2.68 2.33 o 2 12 6 17.00 14.05 3.56 o 1 0 7 42.90 50.85 0.90 o 2 0 7 0.80 0.17 0.72 o 3 0 7 1.80 2.93 0.50 o 4 0 7 1.10 0.61 0.80 o 5 0 7 21.50 25.67 2.10 o 6 0 7 3.30 0.68 2.10 o 0 1 7 255.90 261.50 5.00 o 1 1 7 68.40 73.82 0.85 o 2 1 7 38.00 34.16 0.78 o 3 1 7 354.85 325.27 7.47 o 4 1 7 139.95 140.01 3.78 o 5 1 7 6.50 7.20 1.54 o 6 1 7 6.60 4.73 2.51 o 0 2 7 2242.60 2293.69 41.90 o 1 2 7 267.50 231.56 3.42 o 2 2 7 53.10 51.17 1.31 o 3 2 7 115.30 113.65 2.37 o 4 2 7 109.00 110.07 2.94 o 5 2 7 9.15 8.48 1.20 o 6 2 7 2.55 3.26 2.05 o 0 3 7 4.00 4.83 0.30 o 1 3 7 526.95 521.49 6.93 o 2 3 7 78.25 89.46 1.73 o 3 3 7 125.05 130.17 3.00 o 4 3 7 111.00 113.78 2.91 o 5 3 7 44.75 41.98 1.95 o 6 3 7 7.35 8.62 2.26 o 0 4 7 597.80 634.15 10.50 o 1 4 7 53.75 53.78 0.85 o 2 4 7 140.70 147.42 2.24 o 3 4 7 44.85 53.54 1.39 o 4 4 7 35.70 34.05 1.66 o 5 4 7 2.40 3.22 1.17 o 6 4 7 11.10 13.36 2.65 o 0 5 7 77.50 63.36 2.20 o 1 5 7 199.65 198.91 2.98 o 2 5 7 169.50 161.33 2.91 o 3 5 7 308.55 291.23 6.96 o 4 5 7 66.90 65.14 3.19 o 5 5 7 9.85 8.50 1.97 o 0 6 7 462.00 422.55 9.60 o 1 6 7 122.05 128.62 2.45 o 2 6 7 110.05 94.19 2.64 o 3 6 7 30.75 29.02 1.35 o 4 6 7 33.80 31.47 1.74 o 5 6 7 21.70 19.57 2.42 o 0 7 7 1.90 1.77 0.70 o 1 7 7 80.75 74.89 2.18 o 2 7 7 142.65 148.65 3.08 o 3 7 7 1.70 2.12 1.03 o 4 7 7 21.00 18.85 1.42 o 5 7 7 12.65 13.56 2.37 o 0 8 7 2.50 3.48 1.10 o 1 8 7 157.55 148.38 3.89 o 2 8 7 123.75 129.06 4.67 o 3 8 7 38.45 36.19 2.58 o 4 8 7 26.75 24.17 2.82 o 0 9 7 447.90 406.39 14.40 o 1 9 7 8.20 7.00 1.70 o 2 9 7 99.10 84.12 4.44 o 3 9 7 16.90 14.90 2.83 o 4 9 7 6.75 4.83 2.16 o 0 10 7 8.90 5.88 3.10 o 1 10 7 3.05 1.43 1.63 o 2 10 7 37.55 33.24 3.05 o 3 10 7 3.10 4.86 2.25 o 1 11 7 17.85 18.53 3.01 o 2 11 7 2.40 1.61 2.60 o 3 11 7 25.95 25.14 3.82 o 1 12 7 5.40 7.32 2.63 o 2 12 7 2.15 5.04 2.41 o 0 0 8 2591.60 2432.03 139.60 o 1 0 8 335.30 374.19 5.40 o 2 0 8 83.40 89.09 2.80 o 3 0 8 0.20 0.86 0.36 o 4 0 8 70.00 65.52 2.50 o 5 0 8 4.10 4.98 1.70 o 6 0 8 9.90 7.20 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1.31 o 2 5 26 0.40 1.04 1.52 o 3 5 26 12.80 12.16 2.84 o 0 6 26 30.80 32.48 2.20 o 1 6 26 5.45 7.98 1.46 o 2 6 26 39.25 35.25 3.49 o 3 6 26 2.50 6.71 2.95 o 0 7 26 22.10 22.41 2.70 o 1 7 26 16.25 18.96 2.16 o 2 7 26 12.45 9.70 2.71 o 0 8 26 82.70 73.33 10.30 o 1 8 26 7.55 14.31 2.30 o 1 0 27 45.00 49.92 2.60 o 2 0 27 12.90 15.06 1.90 o 3 0 27 -1.60 0.05 3.80 o 0 1 27 1.10 0.00 0.70 o 1 1 27 24.00 25.46 1.41 o 2 1 27 7.45 7.24 1.43 o 3 1 27 29.90 26.82 3.58 o 4 1 27 21.30 13.54 4.40 o 0 2 27 42.90 41.34 1.90 o 1 2 27 8.95 8.70 0.99 o 2 2 27 7.40 8.09 1.34 o 3 2 27 0.40 3.44 2.73 o 0 3 27 6.50 7.69 1.10 o 1 3 27 6.20 7.75 1.04 o 2 3 27 1.00 0.53 1.60 o 3 3 27 6.00 2.65 2.03 o 0 4 27 23.20 24.79 1.60 o 1 4 27 0.50 0.05 1.12 o 2 4 27 2.75 6.50 1.72 o 3 4 27 2.90 3.50 2.49 o 0 5 27 5.00 8.25 1.20 o 1 5 27 2.60 5.13 1.24 o 2 5 27 -0.65 0.63 3.49 o 3 5 27 5.35 6.39 2.55 o 0 6 27 10.00 12.81 2.10 o 1 6 27 9.80 9.36 1.49 o 2 6 27 33.05 32.68 3.59 o 0 7 27 0.30 0.10 2.30 o 1 7 27 25.45 24.42 2.37 o 2 7 27 -1.30 3.54 2.25 o 0 8 27 -0.10 1.13 2.78 o 1 8 27 12.70 18.28 2.73 o 0 0 28 105.30 92.76 4.30 o 1 0 28 16.60 20.88 1.80 o 2 0 28 3.50 2.93 1.50 o 3 0 28 6.70 5.20 3.20 o 0 1 28 8.90 7.84 1.10 o 1 1 28 7.75 10.10 1.03 o 2 1 28 10.70 12.13 1.56 o 3 1 28 12.05 8.39 2.80 o 0 2 28 3.80 3.47 1.00 o 1 2 28 11.90 13.23 1.20 o 2 2 28 2.95 5.09 1.46 o 3 2 28 5.20 6.24 3.70 o 0 3 28 136.00 122.28 4.20 o 1 3 28 33.05 28.98 1.91 o 2 3 28 17.95 16.67 1.90 o 3 3 28 1.80 5.57 1.87 o 0 4 28 6.50 8.87 1.20 o 1 4 28 6.70 9.47 1.03 o 2 4 28 12.60 13.38 2.36 o 3 4 28 11.45 17.46 3.11 o 0 5 28 28.90 31.20 2.50 o 1 5 28 48.20 40.26 3.80 o 2 5 28 17.80 14.99 2.90 o 0 6 28 135.40 121.96 6.90 o 1 6 28 10.55 10.52 1.77 o 2 6 28 6.40 8.10 2.21 o 0 7 28 0.60 0.00 2.94 o 1 7 28 18.25 21.32 2.16 o 1 0 29 -0.20 0.00 1.16 o 2 0 29 -0.40 0.14 1.77 o 3 0 29 5.70 9.18 3.00 o 0 1 29 14.40 16.43 1.40 o 1 1 29 10.75 11.66 1.03 o 2 1 29 4.15 3.76 1.50 o 3 1 29 20.90 21.83 3.54 o 0 2 29 142.30 138.58 4.70 o 1 2 29 53.85 52.46 2.02 o 2 2 29 -0.05 0.01 1.43 o 3 2 29 11.95 9.79 2.93 o 0 3 29 24.30 25.34 1.80 o 1 3 29 26.10 25.60 1.84 o 2 3 29 1.10 0.38 1.50 o 3 3 29 1.45 3.46 2.85 o 0 4 29 0.00 0.18 0.01 o 1 4 29 36.15 38.67 2.70 o 2 4 29 -0.45 1.05 2.19 o 3 4 29 4.70 2.55 3.30 o 0 5 29 2.50 1.82 3.70 o 1 5 29 27.60 30.36 2.61 o 2 5 29 1.20 3.77 2.07 o 0 6 29 1.40 0.01 2.60 o 1 6 29 3.95 1.96 2.14 o 2 6 29 14.25 15.97 3.21 o 0 7 29 35.60 28.82 4.30 o 0 0 30 35.10 36.77 4.70 o 1 0 30 -1.20 0.73 1.30 o 2 0 30 10.90 9.86 2.20 o 3 0 30 20.10 20.96 5.30 o 0 1 30 24.30 23.68 2.10 o 1 1 30 33.70 33.31 2.00 o 2 1 30 9.00 12.37 1.60 o 3 1 30 21.70 14.45 5.10 o 0 2 30 2.40 4.89 1.30 o 1 2 30 36.75 39.17 1.84 o 2 2 30 9.25 9.93 1.71 o 3 2 30 13.10 19.75 4.40 o 0 3 30 3.60 5.25 1.40 o 1 3 30 1.65 1.33 1.20 o 2 3 30 39.45 41.01 3.99 o 0 4 30 33.10 30.59 2.50 o 1 4 30 9.40 10.60 2.12 o 2 4 30 8.05 9.52 2.68 o 0 5 30 13.70 10.65 3.00 o 1 5 30 1.10 0.29 1.26 o 2 5 30 4.55 7.38 2.06 o 0 6 30 0.80 0.74 3.40 o 1 6 30 11.55 9.56 2.47 o 1 0 31 3.30 1.64 2.40 o 2 0 31 1.20 3.22 1.80 o 0 1 31 0.00 1.36 0.01 o 1 1 31 74.45 68.05 3.49 o 2 1 31 11.85 9.72 2.10 o 0 2 31 4.00 5.65 1.70 o 1 2 31 2.10 4.73 1.06 o 2 2 31 5.25 6.11 2.33 o 0 3 31 20.60 21.85 1.90 o 1 3 31 4.10 6.31 1.31 o 2 3 31 11.35 17.15 2.16 o 0 4 31 15.10 16.81 2.30 o 1 4 31 -0.70 1.63 1.12 o 2 4 31 -1.45 1.85 2.71 o 0 5 31 1.50 0.57 2.80 o 1 5 31 3.15 3.30 1.78 o 0 6 31 25.60 32.50 6.70 o 0 0 32 3.60 4.13 3.70 o 1 0 32 1.30 0.00 1.40 o 2 0 32 27.30 25.37 2.90 o 0 1 32 0.80 1.41 2.86 o 1 1 32 1.35 1.85 1.78 o 2 1 32 34.85 34.50 2.95 o 0 2 32 3.60 0.86 1.80 o 1 2 32 31.60 29.98 2.02 o 2 2 32 2.70 6.14 1.80 o 0 3 32 -1.00 0.03 4.00 o 1 3 32 10.20 12.63 1.38 o 2 3 32 3.10 4.77 4.37 o 0 4 32 4.70 5.96 2.00 o 1 4 32 8.85 9.88 1.88 o 0 5 32 -0.50 0.98 3.54 o 1 0 33 0.50 1.56 2.69 o 2 0 33 10.80 15.55 2.40 o 0 1 33 1.20 0.86 2.10 o 1 1 33 6.15 6.48 1.63 o 2 1 33 6.40 6.41 2.03 o 0 2 33 21.20 24.34 4.80 o 1 2 33 36.35 39.86 2.44 o 0 3 33 0.00 0.03 0.01 o 1 3 33 0.70 0.35 1.67 o 0 4 33 64.50 57.06 5.90 o 0 0 34 25.40 26.39 4.40 o 1 0 34 6.10 8.51 2.40 o 0 1 34 1.60 2.04 2.40 o 1 1 34 6.90 9.06 1.45 o 0 2 34 4.30 2.66 3.50 o 1 2 34 16.80 19.74 2.09 o 0 3 34 8.20 12.62 3.40 o