#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/59/2225931.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2225931_Fobs
loop_
_publ_author_name
'Tursina, Anna I.'
'Cherviakov, Sergei G.'
'No\"el, Henri'
'Chernyshev, Vladimir V.'
'Seropegin, Yuri D.'
_publ_section_title
;
 Lanthanum ruthenium indide, La~21~Ru~9+<i>x~</i>In~5-<i>x~</i>
 (<i>x</i> = 1.2)
;
_journal_coeditor_code           MG2098
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i40
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           140
_symmetry_space_group_name_Hall  '-I 4 2c'
_symmetry_space_group_name_H-M   'I 4/m c m'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   12.1298
_cell_length_b                   12.1298
_cell_length_c                   25.9820
_exptl_crystal_F_000             7328.80
_reflns_d_resolution_high        0.7698
_[local]_cod_data_source_file    mg2098Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  import in I 4/m c m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            2816.48
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, -z+1/2'
'-x, -y, z'
'-x, y, -z+1/2'
'y, x, -z+1/2'
'y, -x, z'
'-y, x, z'
'-y, -x, -z+1/2'
'x+1/2, y+1/2, z+1/2'
'x+1/2, -y+1/2, -z+1'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1'
'y+1/2, x+1/2, -z+1'
'y+1/2, -x+1/2, z+1/2'
'-y+1/2, x+1/2, z+1/2'
'-y+1/2, -x+1/2, -z+1'
'-x, -y, -z'
'-x, y, z-1/2'
'x, y, -z'
'x, -y, z-1/2'
'-y, -x, z-1/2'
'-y, x, -z'
'y, -x, -z'
'y, x, z-1/2'
'-x+1/2, -y+1/2, -z+1/2'
'-x+1/2, y+1/2, z'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z'
'-y+1/2, -x+1/2, z'
'-y+1/2, x+1/2, -z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'y+1/2, x+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 2 0 41327.42 37539.39 1587.11 o
1 3 0 7287.86 7455.78 965.96 o
3 3 0 2103942.00 2059348.75 18358.44 o
0 4 0 53707.06 45775.76 1941.10 o
2 4 0 4017552.75 3912945.50 20036.46 o
4 4 0 1306919.88 1292295.50 14495.82 o
1 5 0 800508.31 790425.56 5483.91 o
3 5 0 1532843.38 1465986.63 10074.59 o
5 5 0 4425273.50 4454184.50 38283.35 o
0 6 0 365197.97 358050.16 5143.64 o
2 6 0 1863423.88 1870608.00 11065.10 o
4 6 0 10943.84 9572.28 1685.92 o
6 6 0 1641898.88 1659423.63 18283.41 o
1 7 0 1800852.50 1846572.00 11199.60 o
3 7 0 1288967.13 1334537.00 9768.20 o
5 7 0 10526.55 10148.25 1624.12 o
7 7 0 843236.00 828507.94 12373.08 o
0 8 0 481157.47 468733.53 6809.71 o
2 8 0 1240605.63 1280709.38 8832.26 o
4 8 0 206608.30 207909.78 3970.30 o
6 8 0 706611.00 747190.38 7940.78 o
8 8 0 1419278.00 1471989.13 18595.80 o
1 9 0 464221.94 466283.28 5065.85 o
3 9 0 34842.71 36211.78 2379.30 o
5 9 0 63260.88 63166.36 2904.14 o
7 9 0 23989.93 24187.59 3111.08 o
9 9 0 226614.09 218894.41 7655.62 o
0 10 0 1477436.25 1472663.75 15340.34 o
2 10 0 744351.06 765077.13 6990.14 o
4 10 0 324040.13 320296.34 5712.65 o
6 10 0 230344.80 220538.86 4636.27 o
8 10 0 34524.53 30506.77 3904.80 o
10 10 0 904706.50 977385.81 17814.42 o
1 11 0 4287.12 5326.26 1988.53 o
3 11 0 62541.11 58754.82 3001.66 o
5 11 0 205044.08 196617.08 4918.30 o
7 11 0 1127.85 620.97 3646.11 o
9 11 0 55805.25 36767.96 5150.64 o
11 11 0 33875.40 42417.26 9316.59 o
0 12 0 405703.91 397294.34 8606.67 o
2 12 0 179701.06 170238.47 3712.71 o
4 12 0 396621.41 411983.06 7163.88 o
6 12 0 1053110.38 1105244.75 11685.91 o
8 12 0 113785.38 90425.24 5563.54 o
10 12 0 138794.52 137479.09 7887.59 o
1 13 0 18210.44 12350.96 2493.01 o
3 13 0 5262.60 5752.32 3420.27 o
5 13 0 504394.22 537189.63 8240.42 o
7 13 0 189997.52 187292.06 6481.77 o
0 14 0 1193151.75 1240303.63 22107.00 o
2 14 0 36698.30 15162.59 4595.73 o
4 14 0 58708.05 42701.88 4414.00 o
6 14 0 5577.74 -3610.39 6122.16 o
1 15 0 226502.84 230455.09 6344.05 o
3 15 0 9434.42 3803.32 4872.32 o
1 2 1 8.98 2923.62 579.37 o
2 3 1 26369.78 26458.30 766.02 o
1 4 1 979973.19 962885.31 4153.94 o
3 4 1 11498.93 10299.48 900.84 o
2 5 1 59870.89 63705.72 1489.66 o
4 5 1 20098.79 18731.49 984.61 o
1 6 1 64419.91 59986.41 1110.43 o
3 6 1 115135.16 121119.28 1670.41 o
5 6 1 57427.77 57062.87 1558.86 o
2 7 1 60482.54 61351.36 1243.02 o
4 7 1 3939.16 2126.09 1052.47 o
6 7 1 2168.40 2057.96 1659.06 o
1 8 1 46580.59 46594.21 1342.60 o
3 8 1 29668.23 32414.15 1335.43 o
5 8 1 33825.48 30214.52 1772.08 o
7 8 1 215.99 10807.13 2018.58 o
2 9 1 15315.56 14530.04 1137.62 o
4 9 1 251056.58 258631.73 3232.58 o
6 9 1 139360.73 142386.34 2559.77 o
8 9 1 12538.59 11230.79 2368.95 o
1 10 1 65758.98 57855.78 1683.22 o
3 10 1 2921.62 4130.46 1460.95 o
5 10 1 33306.89 24351.39 2368.15 o
7 10 1 5266.27 3103.33 2352.26 o
9 10 1 24104.46 28477.79 3113.40 o
2 11 1 96432.12 88635.16 2064.26 o
4 11 1 11106.13 10501.74 2218.36 o
6 11 1 4219.32 5118.61 2117.54 o
8 11 1 44969.40 47656.94 3316.50 o
10 11 1 2793.93 6246.82 3442.94 o
1 12 1 1376.15 -570.83 1646.51 o
3 12 1 55024.64 58752.00 2445.73 o
5 12 1 2746.76 4040.61 2836.76 o
7 12 1 25403.95 25012.53 3274.14 o
9 12 1 8955.10 15509.08 4159.78 o
2 13 1 2736.61 3921.96 1935.74 o
4 13 1 15176.75 17988.85 2879.59 o
6 13 1 13231.44 11745.34 3048.34 o
8 13 1 4124.47 6442.97 3959.30 o
1 14 1 33946.75 30726.68 2219.79 o
3 14 1 585.03 7757.67 2901.20 o
5 14 1 4754.25 1780.65 3800.42 o
7 14 1 84.53 747.04 4366.65 o
2 15 1 2902.39 5521.86 3908.85 o
4 15 1 38188.74 50739.50 4338.38 o
0 2 2 487.78 2773.80 752.88 o
2 2 2 1446.37 4648.45 973.23 o
1 3 2 64364.20 62779.32 872.64 o
3 3 2 1880.07 532.60 1040.41 o
0 4 2 47261.74 45724.68 1184.07 o
2 4 2 27301.70 27172.57 928.11 o
4 4 2 14022.53 10219.42 1587.77 o
1 5 2 56331.45 55077.54 1012.03 o
3 5 2 5253.78 4173.51 853.34 o
5 5 2 5858.56 2546.55 1584.19 o
0 6 2 62793.56 59783.77 1560.22 o
2 6 2 24817.82 24830.58 967.41 o
4 6 2 18312.63 17741.26 1157.19 o
6 6 2 36231.20 37421.36 2472.79 o
1 7 2 17931.61 19714.58 903.19 o
3 7 2 1740.48 2827.88 1101.51 o
5 7 2 660.64 1479.23 1089.38 o
7 7 2 3508.06 3294.92 2677.99 o
0 8 2 18398.11 13667.95 1680.48 o
2 8 2 1125.76 1139.66 849.93 o
4 8 2 15601.15 16899.45 1359.41 o
6 8 2 245.50 520.39 1384.26 o
8 8 2 703.36 838.85 3621.68 o
1 9 2 3545.17 3170.46 1190.89 o
3 9 2 10920.25 7888.38 1878.08 o
5 9 2 394.68 -40.14 1516.55 o
7 9 2 784.82 495.52 2167.23 o
9 9 2 554.72 -599.70 4080.94 o
0 10 2 8718.70 11816.99 1993.10 o
2 10 2 483.21 959.51 1213.06 o
4 10 2 1448.17 1890.79 1613.52 o
6 10 2 2557.03 5254.42 1842.30 o
8 10 2 5.12 3052.89 2643.89 o
10 10 2 6661.24 7588.40 4705.05 o
1 11 2 17214.93 14977.39 1641.19 o
3 11 2 64.63 -1449.93 1779.07 o
5 11 2 10039.76 12530.92 2082.43 o
7 11 2 17669.24 15852.57 2711.16 o
9 11 2 2174.77 6293.49 3489.25 o
11 11 2 27121.06 34350.65 6330.56 o
0 12 2 1103.52 -2571.93 2787.32 o
2 12 2 3563.93 3941.43 2078.81 o
4 12 2 1238.30 589.90 2298.13 o
6 12 2 8793.88 9246.28 3070.23 o
8 12 2 4971.94 4422.61 3138.53 o
10 12 2 5321.63 7739.94 4526.25 o
1 13 2 2038.11 1906.89 1923.52 o
3 13 2 1660.04 2408.26 2539.42 o
5 13 2 222.80 -27.71 2819.22 o
7 13 2 4409.09 8759.43 3658.10 o
0 14 2 5662.86 5876.47 3259.36 o
2 14 2 77.92 176.58 2508.30 o
4 14 2 33.95 6112.00 3220.80 o
6 14 2 170.21 3331.38 3489.89 o
1 15 2 14.23 3825.61 3835.84 o
3 15 2 773.60 1881.40 3377.79 o
1 2 3 1402.76 4292.51 958.32 o
2 3 3 780455.56 790758.94 4090.52 o
1 4 3 1790250.13 1771692.50 7543.89 o
3 4 3 323219.94 320008.31 2368.95 o
2 5 3 321891.97 327188.94 2549.39 o
4 5 3 1113.34 2691.53 904.95 o
1 6 3 23099.31 23735.85 963.01 o
3 6 3 471966.72 471911.91 3275.85 o
5 6 3 361433.06 365904.22 3528.35 o
2 7 3 853.31 1866.62 928.07 o
4 7 3 12.63 -346.28 1208.10 o
6 7 3 138971.06 139807.80 2445.46 o
1 8 3 579409.69 565955.06 3690.55 o
3 8 3 99070.04 93910.57 1804.58 o
5 8 3 397021.81 400347.03 3722.65 o
7 8 3 78008.85 83390.55 2624.82 o
2 9 3 341789.31 348324.88 3119.94 o
4 9 3 183678.38 175180.31 2685.45 o
6 9 3 199024.27 198942.06 3011.37 o
8 9 3 32679.21 27277.89 2537.99 o
1 10 3 156743.20 161669.47 2361.96 o
3 10 3 13011.24 11013.69 1781.12 o
5 10 3 31360.61 27153.84 1908.21 o
7 10 3 2813.10 4853.97 2265.26 o
9 10 3 99477.20 100945.96 3603.68 o
2 11 3 673851.38 709424.81 5149.12 o
4 11 3 24654.20 29162.04 2180.16 o
6 11 3 13789.14 14793.27 2225.61 o
8 11 3 8977.27 4155.17 2737.24 o
10 11 3 34302.77 35869.68 3737.49 o
1 12 3 54023.18 49319.80 2017.08 o
3 12 3 17437.94 14772.44 1994.46 o
5 12 3 117176.04 107912.60 3155.39 o
7 12 3 8021.88 9088.72 2921.44 o
9 12 3 34137.55 30355.79 4099.71 o
2 13 3 9017.32 6827.24 2070.72 o
4 13 3 8493.77 8799.33 2510.20 o
6 13 3 22320.20 19101.59 3191.02 o
8 13 3 8531.31 7077.08 4091.36 o
1 14 3 1129.94 3340.35 2348.30 o
3 14 3 12146.05 18015.28 2898.70 o
5 14 3 88784.15 76242.71 3648.22 o
7 14 3 23028.33 22900.07 4481.97 o
2 15 3 57490.80 60979.64 3759.39 o
4 15 3 159487.80 151325.67 4772.29 o
1 1 4 18866.71 16500.69 1048.42 o
0 2 4 85165.50 74691.66 1208.69 o
2 2 4 46883.27 42791.75 1357.65 o
1 3 4 101641.12 104084.58 1176.19 o
3 3 4 69612.04 60857.36 1759.52 o
0 4 4 405291.63 398431.84 3597.62 o
2 4 4 29546.88 31386.63 980.20 o
4 4 4 47741.68 53912.21 1705.78 o
1 5 4 195303.95 187165.50 1800.35 o
3 5 4 77348.20 73555.54 1516.54 o
5 5 4 131047.80 126704.48 2925.33 o
0 6 4 60888.55 60189.86 1613.43 o
2 6 4 26988.80 27546.11 1211.48 o
4 6 4 8812.20 10971.96 999.94 o
6 6 4 588.78 1926.17 1686.20 o
1 7 4 18736.51 24254.97 1130.71 o
3 7 4 165366.00 159672.84 2063.66 o
5 7 4 59.23 3280.25 1209.22 o
7 7 4 21977.39 23224.12 3094.96 o
0 8 4 127706.11 124639.68 2507.99 o
2 8 4 123213.52 117131.92 1745.09 o
4 8 4 36725.46 38559.60 1629.28 o
6 8 4 2041.97 4489.94 1590.97 o
8 8 4 63916.45 64409.61 3871.18 o
1 9 4 848.43 2536.00 1110.32 o
3 9 4 17199.70 23167.23 1484.07 o
5 9 4 49962.66 51540.09 1949.15 o
7 9 4 53806.57 50694.45 2347.22 o
9 9 4 10388.80 8155.38 3908.26 o
0 10 4 139666.50 140141.88 3457.28 o
2 10 4 4709.78 3936.81 1354.49 o
4 10 4 3187.02 4692.28 1748.65 o
6 10 4 97712.89 98937.58 2535.37 o
8 10 4 152.01 5862.88 2581.86 o
10 10 4 1055.47 6595.43 5376.75 o
1 11 4 31992.77 38302.90 1952.57 o
3 11 4 5489.10 40.00 1513.28 o
5 11 4 63229.14 67579.50 3057.70 o
7 11 4 48180.11 45732.88 2762.15 o
9 11 4 5501.33 6148.89 3393.97 o
11 11 4 3851.46 -3604.95 7711.42 o
0 12 4 14.21 -1501.20 2896.39 o
2 12 4 278.89 2313.21 1922.05 o
4 12 4 25847.86 27047.60 2482.49 o
6 12 4 33520.63 34768.38 2523.45 o
8 12 4 7839.14 4582.83 3195.27 o
10 12 4 2212.92 4349.16 4810.80 o
1 13 4 180.45 1117.73 2001.83 o
3 13 4 101381.24 105640.59 3058.02 o
5 13 4 1378.19 7526.31 2945.86 o
7 13 4 4394.37 14341.97 3460.26 o
0 14 4 1438.94 11342.03 4394.52 o
2 14 4 23400.35 31517.30 3333.57 o
4 14 4 20700.95 24815.15 3032.71 o
6 14 4 16586.76 13799.45 3725.40 o
1 15 4 8750.39 14290.78 3387.30 o
3 15 4 4979.44 7595.46 4507.78 o
1 2 5 1293.16 2968.94 638.53 o
2 3 5 1838057.00 1854085.50 8275.06 o
1 4 5 3608737.75 3477899.00 13961.10 o
3 4 5 450.69 664.99 754.23 o
2 5 5 3770.37 5593.74 801.19 o
4 5 5 123591.27 120261.28 1773.15 o
1 6 5 216974.23 201401.23 2024.14 o
3 6 5 615949.88 619053.75 4249.49 o
5 6 5 142460.27 139519.42 2053.50 o
2 7 5 47512.48 49258.93 1295.68 o
4 7 5 214793.25 202999.89 2384.43 o
6 7 5 1795.82 1535.29 1765.77 o
1 8 5 68802.05 66411.91 1501.35 o
3 8 5 1059299.38 1078660.38 7112.85 o
5 8 5 157958.27 154332.48 2466.64 o
7 8 5 271561.75 274901.78 3602.10 o
2 9 5 16599.89 16496.44 1204.18 o
4 9 5 1162682.50 1167685.75 6686.32 o
6 9 5 260501.11 270779.59 3520.41 o
8 9 5 29973.02 24361.00 2702.98 o
1 10 5 171286.30 172537.42 2389.80 o
3 10 5 27088.57 23145.43 1699.84 o
5 10 5 152181.42 136660.45 2711.11 o
7 10 5 764.97 888.06 1959.43 o
9 10 5 126968.49 118513.14 3646.50 o
2 11 5 416755.94 435075.44 3947.79 o
4 11 5 4827.70 2445.89 1978.75 o
6 11 5 118710.45 104639.36 3013.56 o
8 11 5 132312.14 128407.84 3750.23 o
10 11 5 79477.24 76411.68 4776.55 o
1 12 5 123970.25 135430.45 2681.89 o
3 12 5 401.23 4009.08 2101.61 o
5 12 5 1373.39 2169.66 2475.61 o
7 12 5 24.31 829.95 2947.30 o
9 12 5 43661.31 47241.04 3808.06 o
2 13 5 294656.22 276836.47 3802.05 o
4 13 5 45294.35 54825.26 2923.65 o
6 13 5 4374.32 -2025.10 2550.43 o
8 13 5 28742.33 23029.72 4190.08 o
1 14 5 66680.05 62150.53 3128.68 o
3 14 5 37.63 1441.85 2832.03 o
5 14 5 39968.71 39041.12 3493.70 o
2 15 5 244.16 3913.85 3594.93 o
4 15 5 93614.07 75597.53 4118.38 o
0 0 6 8174.04 10049.47 1828.55 o
1 1 6 762.31 2174.05 980.21 o
0 2 6 75365.33 79624.70 1636.78 o
2 2 6 7421.49 4673.04 1268.53 o
1 3 6 898901.56 898589.56 4893.40 o
3 3 6 282.31 -20.86 1120.54 o
0 4 6 1252313.63 1253016.63 8979.62 o
2 4 6 123999.70 129437.16 1613.97 o
4 4 6 104769.92 100934.86 2399.49 o
1 5 6 196555.41 195612.47 1879.37 o
3 5 6 4278.37 4897.76 972.34 o
5 5 6 235097.67 242296.86 3356.16 o
0 6 6 41237.67 36563.32 1639.14 o
2 6 6 295574.47 301404.69 2655.21 o
4 6 6 103492.73 104166.92 1770.38 o
6 6 6 16681.91 14774.82 2822.25 o
1 7 6 88989.16 92569.59 1772.77 o
3 7 6 411548.09 419577.06 3565.98 o
5 7 6 14061.62 16691.39 1313.24 o
7 7 6 224476.88 222001.81 4550.55 o
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2 8 6 142354.31 142317.84 1975.38 o
4 8 6 37445.47 35468.31 1513.08 o
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8 8 6 45998.42 47773.65 3644.49 o
1 9 6 21570.55 21880.05 1480.21 o
3 9 6 2988.98 5499.75 1574.39 o
5 9 6 205173.28 208800.48 3013.27 o
7 9 6 207795.09 212282.95 3323.15 o
9 9 6 455.54 3095.80 3642.98 o
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4 10 6 5669.32 3574.41 1358.86 o
6 10 6 131719.41 132488.16 2841.25 o
8 10 6 110.83 1607.02 2677.48 o
10 10 6 32116.41 25913.66 6222.95 o
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3 11 6 675.89 -1724.02 1724.02 o
5 11 6 17942.19 17395.05 2079.08 o
7 11 6 71291.48 63244.97 2737.48 o
9 11 6 9368.30 11006.29 3107.95 o
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2 12 6 3644.51 5003.68 1889.27 o
4 12 6 107422.83 111944.05 2933.18 o
6 12 6 16708.69 17526.80 2861.39 o
8 12 6 17710.17 18574.75 3469.36 o
1 13 6 6929.59 9278.23 2144.46 o
3 13 6 224327.66 217313.48 3508.14 o
5 13 6 3991.43 1799.29 2751.73 o
7 13 6 1279.85 7472.36 3441.13 o
0 14 6 28231.45 18470.16 4883.97 o
2 14 6 19138.02 15891.36 2663.08 o
4 14 6 23016.44 12163.70 3232.50 o
6 14 6 55137.55 62837.32 4559.97 o
1 15 6 8225.10 11792.24 3429.15 o
3 15 6 1512.03 3391.26 3380.75 o
1 2 7 273882.78 280433.28 2347.54 o
2 3 7 196218.41 191628.61 2240.12 o
1 4 7 58.41 -830.73 830.73 o
3 4 7 26552.99 26998.57 979.24 o
2 5 7 189801.20 196858.19 2119.37 o
4 5 7 222403.22 229122.63 2763.72 o
1 6 7 25239.12 26217.14 1143.48 o
3 6 7 106381.54 108783.33 1710.05 o
5 6 7 3829.46 3593.39 1589.65 o
2 7 7 99739.18 94632.66 1704.37 o
4 7 7 1004.47 503.10 1072.11 o
6 7 7 618.29 834.24 1407.13 o
1 8 7 92750.21 92480.06 1723.64 o
3 8 7 359744.63 361802.75 3402.21 o
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2 9 7 85981.17 85951.78 1819.19 o
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