#------------------------------------------------------------------------------ #$Date: 2010-06-08 21:54:03 +0300 (Tue, 08 Jun 2010) $ #$Revision: 1208 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2225950.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225950_Fobs loop_ _publ_author_name 'Rouchal, Michal' 'Ne\N,N-dimethyl-9H-purin-6-amine ; _journal_coeditor_code PK2238 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1016 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.965 _cell_angle_gamma 90.000 _cell_length_a 12.0483 _cell_length_b 8.7689 _cell_length_c 11.5538 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.8413 _[local]_cod_data_source_file pk2238Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10557.22 10371.49 53.38 o 3 0 0 5550.71 5280.34 25.51 o 4 0 0 7133.90 6776.63 41.68 o 5 0 0 1246.36 1178.39 5.95 o 6 0 0 1195.36 1226.17 6.67 o 7 0 0 2276.12 2241.65 11.28 o 8 0 0 527.10 532.06 6.20 o 9 0 0 1477.02 1525.75 10.81 o 10 0 0 597.02 576.56 8.26 o 11 0 0 70.17 69.73 4.03 o 12 0 0 0.41 3.13 3.17 o 13 0 0 157.55 177.09 8.65 o 1 1 0 0.29 1.79 0.89 o 2 1 0 2781.25 2836.61 5.46 o 3 1 0 107.41 118.53 1.60 o 4 1 0 838.16 801.08 3.26 o 5 1 0 420.75 432.49 2.77 o 6 1 0 123.06 96.23 1.65 o 7 1 0 83.33 86.30 1.99 o 8 1 0 784.32 792.38 5.23 o 9 1 0 195.23 217.39 3.47 o 10 1 0 130.95 122.56 2.99 o 11 1 0 48.35 52.68 2.67 o 12 1 0 2.67 4.67 2.95 o 13 1 0 147.50 159.73 6.10 o 0 2 0 1594.14 1599.72 5.61 o 1 2 0 163.90 183.30 1.44 o 2 2 0 60.32 50.14 1.08 o 3 2 0 874.74 873.03 3.63 o 4 2 0 685.35 661.72 3.11 o 5 2 0 206.91 183.00 1.98 o 6 2 0 109.92 105.96 1.82 o 7 2 0 637.10 645.52 4.77 o 8 2 0 77.89 81.42 2.35 o 9 2 0 294.19 294.06 3.92 o 10 2 0 66.42 67.97 3.76 o 11 2 0 48.80 46.30 3.51 o 12 2 0 2.27 4.51 3.10 o 13 2 0 2.15 0.53 3.64 o 1 3 0 0.05 0.24 0.82 o 2 3 0 256.87 261.06 1.97 o 3 3 0 252.40 296.45 2.32 o 4 3 0 10.64 21.51 0.90 o 5 3 0 16.89 19.34 0.98 o 6 3 0 2.46 3.63 1.41 o 7 3 0 108.64 110.01 2.45 o 8 3 0 2.06 5.26 2.83 o 9 3 0 695.12 695.08 8.60 o 10 3 0 191.93 192.65 5.32 o 11 3 0 298.74 306.93 6.75 o 12 3 0 49.44 48.17 3.91 o 0 4 0 2047.06 2123.62 17.48 o 1 4 0 1032.74 1088.49 3.98 o 2 4 0 407.57 414.53 2.73 o 3 4 0 1467.60 1502.80 5.49 o 4 4 0 248.39 258.88 2.55 o 5 4 0 279.82 317.11 3.24 o 6 4 0 40.22 35.13 2.56 o 7 4 0 16.69 18.29 2.83 o 8 4 0 74.98 80.12 4.17 o 9 4 0 715.27 697.01 8.98 o 10 4 0 14.97 12.66 3.19 o 11 4 0 6.34 4.11 3.36 o 12 4 0 0.03 0.72 3.42 o 1 5 0 2580.98 2689.16 9.15 o 2 5 0 67.22 70.22 1.52 o 3 5 0 515.77 534.17 3.51 o 4 5 0 1917.37 1967.92 9.53 o 5 5 0 8.77 11.15 1.95 o 6 5 0 223.31 211.97 4.41 o 7 5 0 842.87 821.30 8.19 o 8 5 0 69.22 74.69 3.95 o 9 5 0 67.37 70.69 3.83 o 10 5 0 65.06 67.07 4.03 o 11 5 0 19.53 21.88 3.59 o 0 6 0 445.42 388.24 5.40 o 1 6 0 50.67 47.85 1.86 o 2 6 0 3.15 7.58 1.90 o 3 6 0 103.33 104.16 2.80 o 4 6 0 26.95 27.04 2.22 o 5 6 0 79.60 78.39 2.90 o 6 6 0 0.15 0.50 2.48 o 7 6 0 13.14 17.33 2.70 o 8 6 0 580.63 560.38 7.55 o 9 6 0 292.61 284.95 6.12 o 10 6 0 141.56 133.30 4.84 o 11 6 0 79.56 80.46 4.34 o 1 7 0 520.71 506.74 6.33 o 2 7 0 88.41 93.91 3.51 o 3 7 0 579.65 578.20 7.23 o 4 7 0 810.16 773.67 8.55 o 5 7 0 340.79 332.64 6.14 o 6 7 0 545.92 550.13 7.18 o 7 7 0 2.18 1.15 2.76 o 8 7 0 458.63 454.03 7.24 o 9 7 0 41.35 52.07 3.80 o 0 8 0 232.11 210.16 11.98 o 1 8 0 21.79 19.15 5.09 o 2 8 0 138.60 138.28 7.48 o 3 8 0 96.94 110.64 4.11 o 4 8 0 62.50 60.94 3.56 o 5 8 0 22.14 24.50 3.18 o 6 8 0 13.07 12.19 3.22 o 7 8 0 284.70 283.75 6.64 o 8 8 0 57.09 65.15 4.23 o 1 9 0 1440.02 1394.59 20.69 o 2 9 0 124.64 140.88 8.33 o 3 9 0 290.52 285.27 10.59 o 4 9 0 211.59 209.17 9.46 o 5 9 0 1.64 0.00 2.94 o 6 9 0 161.77 176.81 5.69 o 0 10 0 26.19 26.61 9.02 o 1 10 0 2.64 5.38 5.72 o 2 10 0 77.15 81.30 7.58 o 3 10 0 54.66 60.60 7.23 o -13 1 1 3.41 7.77 3.43 o -12 1 1 12.61 15.83 2.98 o -11 1 1 23.65 25.31 2.77 o -10 1 1 41.94 46.31 2.24 o -9 1 1 265.42 285.39 3.48 o -8 1 1 268.35 257.43 3.10 o -7 1 1 1556.35 1582.23 6.49 o -6 1 1 778.94 787.68 4.25 o -5 1 1 584.58 611.13 3.39 o -4 1 1 34.13 26.16 1.04 o -3 1 1 107.49 121.37 1.30 o -2 1 1 340.11 332.55 5.72 o -1 1 1 1803.73 1841.99 6.82 o 0 1 1 6778.45 6640.96 109.67 o 1 1 1 607.44 604.74 2.28 o 2 1 1 13988.07 13561.39 43.85 o 3 1 1 865.25 856.04 3.79 o 4 1 1 2253.04 2330.50 6.85 o 5 1 1 322.17 321.33 2.62 o 6 1 1 464.91 432.26 3.26 o 7 1 1 12.80 16.05 1.53 o 8 1 1 48.10 46.87 2.16 o 9 1 1 330.19 314.46 4.19 o 10 1 1 1.38 1.69 2.00 o 11 1 1 0.74 1.64 2.15 o 12 1 1 139.70 134.79 4.87 o 13 1 1 1.13 3.01 3.51 o -13 2 1 20.84 18.53 3.42 o -12 2 1 414.77 414.01 7.51 o -11 2 1 182.52 179.62 5.08 o -10 2 1 26.34 28.28 2.66 o -9 2 1 1.08 1.27 2.25 o -8 2 1 0.93 2.19 1.47 o -7 2 1 191.28 169.50 2.38 o -6 2 1 26.24 21.79 1.20 o -5 2 1 19.44 17.60 0.88 o -4 2 1 28.18 18.02 0.73 o -3 2 1 499.87 499.83 2.13 o -2 2 1 7855.14 7681.78 23.81 o -1 2 1 1957.75 2018.10 9.01 o 0 2 1 47.15 68.17 1.00 o 1 2 1 1666.00 1609.70 4.09 o 2 2 1 14649.73 14472.95 61.97 o 3 2 1 71.07 96.61 1.49 o 4 2 1 410.45 431.10 3.10 o 5 2 1 62.50 51.11 1.35 o 6 2 1 8.90 9.36 1.32 o 7 2 1 377.61 375.71 3.88 o 8 2 1 1142.14 1137.27 7.02 o 9 2 1 158.16 164.81 3.49 o 10 2 1 247.21 254.35 5.19 o 11 2 1 1025.18 1069.39 11.46 o 12 2 1 41.90 50.18 4.58 o -13 3 1 0.40 0.36 3.47 o -12 3 1 73.78 78.56 4.05 o -11 3 1 6.51 3.04 3.03 o -10 3 1 25.09 30.19 3.34 o -9 3 1 137.41 123.58 4.23 o -8 3 1 1293.57 1214.59 10.28 o -7 3 1 228.67 238.15 4.78 o -6 3 1 1272.46 1295.11 5.33 o -5 3 1 1218.62 1205.41 4.90 o -4 3 1 238.38 215.56 1.83 o -3 3 1 659.32 630.27 2.83 o -2 3 1 79.80 73.13 1.08 o -1 3 1 367.18 344.36 2.15 o 0 3 1 1667.17 1729.30 4.69 o 1 3 1 674.18 672.06 3.25 o 2 3 1 5072.63 5118.63 10.55 o 3 3 1 566.15 596.16 3.50 o 4 3 1 117.64 101.81 1.63 o 5 3 1 166.51 166.73 2.22 o 6 3 1 589.37 573.46 4.69 o 7 3 1 157.29 167.05 3.34 o 8 3 1 123.25 115.59 2.89 o 9 3 1 788.81 794.99 9.36 o 10 3 1 332.36 341.23 6.86 o 11 3 1 400.49 414.78 7.85 o 12 3 1 3.32 2.42 3.50 o -12 4 1 91.68 90.81 4.79 o -11 4 1 343.28 347.19 7.18 o -10 4 1 14.19 11.85 3.25 o -9 4 1 1358.57 1376.94 12.08 o -8 4 1 393.15 383.45 6.49 o -7 4 1 1740.83 1641.88 10.74 o -6 4 1 42.59 45.17 2.68 o -5 4 1 239.30 230.42 3.43 o -4 4 1 822.51 747.31 6.01 o -3 4 1 80.46 79.38 1.45 o -2 4 1 933.42 871.82 4.37 o -1 4 1 1099.17 1216.76 4.14 o 0 4 1 1166.62 1133.95 4.86 o 1 4 1 1834.36 1893.76 6.00 o 2 4 1 109.63 98.27 1.64 o 3 4 1 753.87 710.43 4.13 o 4 4 1 35.18 25.38 1.40 o 5 4 1 1062.40 1114.37 5.71 o 6 4 1 747.17 722.40 5.73 o 7 4 1 91.51 84.58 4.13 o 8 4 1 225.25 224.91 5.98 o 9 4 1 488.66 480.33 8.68 o 10 4 1 703.27 724.12 9.85 o 11 4 1 22.92 21.61 3.61 o 12 4 1 33.77 30.44 3.84 o -12 5 1 319.73 338.62 7.08 o -11 5 1 251.52 267.57 6.21 o -10 5 1 248.22 250.15 5.77 o -9 5 1 91.73 80.42 3.83 o -8 5 1 2018.51 2017.92 13.15 o -7 5 1 52.59 53.73 3.11 o -6 5 1 306.55 310.08 5.04 o -5 5 1 511.67 500.67 5.79 o -4 5 1 337.71 345.33 4.66 o -3 5 1 231.39 232.76 3.21 o -2 5 1 1.27 2.19 0.89 o -1 5 1 1713.24 1709.99 5.96 o 0 5 1 287.79 346.46 2.65 o 1 5 1 447.59 417.24 3.25 o 2 5 1 217.91 178.69 2.24 o 3 5 1 276.32 268.46 2.77 o 4 5 1 134.05 117.98 2.43 o 5 5 1 51.27 54.37 2.50 o 6 5 1 327.23 295.71 5.09 o 7 5 1 2.85 3.11 2.47 o 8 5 1 1.09 2.60 2.89 o 9 5 1 110.26 114.88 4.64 o 10 5 1 29.29 29.91 3.41 o 11 5 1 136.15 149.53 5.12 o -11 6 1 56.52 52.01 3.92 o -10 6 1 4.83 6.07 2.95 o -9 6 1 0.47 1.16 2.96 o -8 6 1 4.51 5.06 2.54 o -7 6 1 14.17 10.71 2.55 o -6 6 1 0.58 1.87 2.49 o -5 6 1 11.63 10.93 2.33 o -4 6 1 374.94 386.29 5.21 o -3 6 1 38.62 36.37 2.73 o -2 6 1 10.51 7.58 2.17 o -1 6 1 8.09 16.98 2.26 o 0 6 1 570.34 539.39 3.84 o 1 6 1 15.03 14.54 1.51 o 2 6 1 146.48 144.23 2.31 o 3 6 1 303.04 277.81 3.78 o 4 6 1 22.92 17.18 2.12 o 5 6 1 202.67 202.81 3.95 o 6 6 1 258.48 251.93 5.00 o 7 6 1 242.88 235.84 5.09 o 8 6 1 0.15 0.00 3.12 o 9 6 1 82.98 79.50 4.28 o 10 6 1 400.24 413.90 7.57 o -10 7 1 46.30 54.73 3.95 o -9 7 1 35.01 31.19 3.31 o -8 7 1 9.76 5.54 2.81 o -7 7 1 1.00 0.00 2.68 o -6 7 1 47.90 49.40 3.18 o -5 7 1 253.74 235.10 5.39 o -4 7 1 25.59 23.01 2.83 o -3 7 1 150.00 139.50 4.13 o -2 7 1 452.04 446.57 6.30 o -1 7 1 252.45 248.46 3.98 o 0 7 1 98.92 95.68 2.77 o 1 7 1 105.11 108.33 4.73 o 2 7 1 46.59 46.58 2.63 o 3 7 1 2.26 2.43 2.23 o 4 7 1 3.16 2.19 2.27 o 5 7 1 2.08 3.66 2.20 o 6 7 1 1.60 0.83 2.51 o 7 7 1 44.85 40.65 3.18 o 8 7 1 11.61 12.37 2.93 o 9 7 1 11.34 15.85 3.47 o -8 8 1 69.73 80.89 4.23 o -7 8 1 54.16 59.20 4.13 o -6 8 1 262.51 238.18 5.98 o -5 8 1 7.34 5.94 2.85 o -4 8 1 147.94 135.71 4.55 o -3 8 1 28.80 28.51 3.01 o -2 8 1 104.73 109.26 3.89 o -1 8 1 89.58 95.79 6.56 o 0 8 1 58.08 60.73 5.92 o 1 8 1 0.27 1.36 4.45 o 2 8 1 0.99 3.60 4.69 o 3 8 1 337.48 304.57 6.60 o 4 8 1 18.07 23.28 3.00 o 5 8 1 4.40 3.87 3.07 o 6 8 1 18.54 16.30 3.10 o 7 8 1 0.83 1.36 3.25 o 8 8 1 1.66 2.33 3.03 o -7 9 1 2.12 4.68 3.10 o -6 9 1 475.78 496.99 8.51 o -5 9 1 48.03 49.04 3.72 o -4 9 1 92.73 95.66 4.33 o -3 9 1 20.82 20.66 5.58 o -2 9 1 16.92 12.04 5.39 o -1 9 1 50.57 54.56 6.27 o 0 9 1 119.48 109.73 7.61 o 1 9 1 213.36 203.10 9.08 o 2 9 1 423.79 427.02 12.22 o 3 9 1 57.21 45.59 6.41 o 4 9 1 175.55 168.11 9.03 o 5 9 1 0.03 0.12 3.22 o 6 9 1 50.88 48.36 4.17 o -4 10 1 306.01 301.46 11.66 o -3 10 1 3.17 1.59 5.49 o -2 10 1 55.66 61.81 7.15 o -1 10 1 166.99 169.14 9.25 o 0 10 1 93.66 100.02 7.91 o 1 10 1 439.29 428.11 13.11 o 2 10 1 62.65 64.39 6.83 o 3 10 1 209.69 219.03 10.05 o -14 0 2 555.91 578.70 20.85 o -13 0 2 579.99 608.72 20.17 o -12 0 2 23.60 32.15 7.43 o -11 0 2 209.69 210.72 4.82 o -10 0 2 4.28 3.38 2.23 o -9 0 2 238.95 211.10 4.28 o -8 0 2 139.05 123.55 3.23 o -7 0 2 1034.01 1099.39 7.49 o -6 0 2 3025.72 2940.76 14.29 o -5 0 2 28.21 33.54 1.63 o -4 0 2 4588.87 4774.09 16.37 o -3 0 2 8398.40 8307.11 36.07 o -2 0 2 59.94 73.23 1.44 o -1 0 2 4310.17 4277.73 8.56 o 0 0 2 31.07 40.59 1.34 o 1 0 2 527.03 572.85 4.23 o 2 0 2 1943.77 2052.37 7.78 o 3 0 2 1115.27 1054.49 6.28 o 4 0 2 535.90 582.55 4.76 o 5 0 2 438.95 416.39 4.49 o 6 0 2 958.35 987.56 7.76 o 7 0 2 125.46 127.76 3.31 o 8 0 2 13.14 10.98 2.79 o 9 0 2 48.63 48.53 3.57 o 10 0 2 1056.64 1074.76 11.94 o 11 0 2 5.75 7.40 3.32 o 12 0 2 110.82 114.36 5.52 o -13 1 2 16.20 19.07 3.16 o -12 1 2 2.02 4.86 2.48 o -11 1 2 25.58 21.41 2.64 o -10 1 2 375.23 371.73 4.98 o -9 1 2 136.95 127.13 2.50 o -8 1 2 290.35 284.70 3.14 o -7 1 2 1288.56 1311.33 5.76 o -6 1 2 222.59 194.35 2.21 o -5 1 2 2314.09 2363.31 6.26 o -4 1 2 532.80 591.52 2.94 o -3 1 2 187.82 178.19 2.08 o -2 1 2 3690.37 3687.77 14.35 o -1 1 2 2113.37 2083.32 6.24 o 0 1 2 5271.79 5404.72 11.86 o 1 1 2 11190.43 10979.36 20.82 o 2 1 2 18017.56 17389.38 72.75 o 3 1 2 993.29 990.83 4.36 o 4 1 2 2166.44 2115.74 7.17 o 5 1 2 372.00 338.59 3.03 o 6 1 2 579.61 591.21 4.15 o 7 1 2 431.72 414.49 4.07 o 8 1 2 95.08 96.14 2.71 o 9 1 2 294.64 312.35 4.59 o 10 1 2 476.90 479.69 5.87 o 11 1 2 303.17 310.02 5.54 o 12 1 2 46.16 49.95 3.14 o -13 2 2 334.19 334.76 7.15 o -12 2 2 36.05 35.02 3.43 o -11 2 2 158.57 161.55 4.81 o -10 2 2 259.49 256.62 4.88 o -9 2 2 121.99 119.54 3.53 o -8 2 2 18.25 25.89 2.04 o -7 2 2 73.16 96.51 4.54 o -6 2 2 511.85 446.25 3.08 o -5 2 2 2657.43 2698.13 20.23 o -4 2 2 3.97 0.96 0.53 o -3 2 2 77.96 86.78 1.63 o -2 2 2 4928.54 4825.44 19.39 o -1 2 2 171.70 198.33 1.54 o 0 2 2 3164.50 3234.62 16.24 o 1 2 2 3025.26 3005.32 6.47 o 2 2 2 6443.44 6330.65 11.15 o 3 2 2 3018.67 3267.40 7.93 o 4 2 2 40.72 57.37 1.64 o 5 2 2 916.30 824.74 5.01 o 6 2 2 11.38 15.73 1.59 o 7 2 2 108.84 121.46 2.70 o 8 2 2 182.08 164.53 3.22 o 9 2 2 3.07 1.86 2.10 o 10 2 2 117.47 123.50 3.56 o 11 2 2 117.21 115.38 4.65 o 12 2 2 173.34 182.47 6.73 o -13 3 2 187.16 185.57 5.85 o -12 3 2 1.90 0.45 2.97 o -11 3 2 53.77 52.18 3.61 o -10 3 2 5.77 6.21 2.76 o -9 3 2 8.97 6.70 2.86 o -8 3 2 1.19 1.13 2.59 o -7 3 2 574.88 586.61 5.27 o -6 3 2 56.32 64.61 2.12 o -5 3 2 492.10 525.05 4.28 o -4 3 2 458.68 503.98 3.94 o -3 3 2 264.16 269.37 2.66 o -2 3 2 729.83 767.30 4.25 o -1 3 2 112.66 132.05 1.31 o 0 3 2 282.75 318.51 2.19 o 1 3 2 42.69 50.49 1.23 o 2 3 2 705.59 824.51 3.92 o 3 3 2 678.71 758.55 3.78 o 4 3 2 1779.61 1872.04 6.35 o 5 3 2 818.81 799.07 5.53 o 6 3 2 287.79 311.54 3.89 o 7 3 2 49.50 52.14 2.53 o 8 3 2 120.85 120.08 3.14 o 9 3 2 21.32 21.50 2.67 o 10 3 2 20.91 22.36 3.43 o 11 3 2 312.99 314.94 7.15 o 12 3 2 50.84 59.78 5.01 o -12 4 2 0.44 2.18 3.23 o -11 4 2 64.26 63.85 4.22 o -10 4 2 342.77 334.93 6.66 o -9 4 2 21.33 26.15 3.35 o -8 4 2 370.02 352.55 6.18 o -7 4 2 55.98 50.40 2.96 o -6 4 2 245.43 240.14 3.55 o -5 4 2 83.11 87.33 2.33 o -4 4 2 200.22 196.90 2.87 o -3 4 2 201.67 245.16 3.21 o -2 4 2 24.35 16.73 0.79 o -1 4 2 0.01 0.82 0.72 o 0 4 2 88.53 86.37 1.58 o 1 4 2 255.22 294.45 2.66 o 2 4 2 1539.14 1614.83 5.86 o 3 4 2 619.78 668.94 4.28 o 4 4 2 26.74 27.01 1.56 o 5 4 2 116.00 129.39 2.48 o 6 4 2 652.21 667.92 5.06 o 7 4 2 377.82 352.79 4.99 o 8 4 2 85.87 90.26 4.71 o 9 4 2 101.19 94.89 4.98 o 10 4 2 131.58 140.76 5.79 o 11 4 2 1.75 3.84 3.48 o -12 5 2 20.80 20.62 3.36 o -11 5 2 27.22 22.03 3.34 o -10 5 2 175.96 180.82 5.08 o -9 5 2 655.46 639.63 7.97 o -8 5 2 8.61 8.00 2.68 o -7 5 2 2660.19 2663.42 13.06 o -6 5 2 17.12 19.19 2.37 o -5 5 2 779.85 753.70 6.48 o -4 5 2 244.18 249.32 4.04 o -3 5 2 6.29 6.18 1.72 o -2 5 2 1.27 3.49 1.42 o -1 5 2 74.26 68.41 1.41 o 0 5 2 24.31 36.01 1.39 o 1 5 2 748.18 826.02 4.66 o 2 5 2 425.87 430.06 3.43 o 3 5 2 133.64 140.44 2.31 o 4 5 2 108.79 99.21 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