#------------------------------------------------------------------------------ #$Date: 2010-10-08 09:13:40 +0300 (Fri, 08 Oct 2010) $ #$Revision: 1452 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226070.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226070_Fobs loop_ _publ_author_name 'Aridoss, G.' 'Sundaramoorthy, S.' 'Velmurugan, D.' 'Park, K. S.' 'Jeong, Y. T.' _publ_section_title ; 1-(2-Bromoacetyl)-3-methyl-2,6-diphenylpiperidin-4-one ; _journal_coeditor_code BT5275 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1479 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 125.368 _cell_angle_gamma 90.000 _cell_length_a 21.4006 _cell_length_b 14.5873 _cell_length_c 13.8107 _exptl_crystal_F_000 1584.00 _reflns_d_resolution_high 0.7456 _[local]_cod_data_source_file bt5275Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SSHARI1_0m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 375.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 287.26 533.08 21.14 o 6 0 0 49983.23 50403.45 826.05 o 8 0 0 8618.07 5836.60 115.69 o 10 0 0 1824.71 1602.74 52.03 o 12 0 0 3574.73 4006.06 76.83 o 14 0 0 4728.91 4006.01 79.13 o 16 0 0 4238.07 4376.36 104.61 o 18 0 0 1993.69 2023.32 108.61 o 20 0 0 822.55 856.24 57.37 o 22 0 0 1420.23 1563.03 114.91 o 1 1 0 9180.57 10215.31 155.13 o 3 1 0 32767.92 34634.38 362.99 o 5 1 0 17160.53 18027.06 189.79 o 7 1 0 53.86 215.72 7.84 o 9 1 0 1219.12 1056.01 19.22 o 11 1 0 13033.47 12206.04 148.25 o 13 1 0 1319.01 1213.93 25.34 o 15 1 0 111.75 107.10 16.51 o 17 1 0 89.34 69.36 20.29 o 19 1 0 718.48 819.14 38.55 o 21 1 0 107.43 110.97 74.77 o 23 1 0 35.17 71.82 77.13 o 0 2 0 58298.87 67391.78 1114.02 o 2 2 0 7858.63 11710.34 130.49 o 4 2 0 23679.94 30731.62 359.07 o 6 2 0 7612.77 8227.86 93.40 o 8 2 0 10221.53 10491.29 126.72 o 10 2 0 15.43 -5.34 8.12 o 12 2 0 750.59 716.83 18.22 o 14 2 0 46.19 10.77 14.13 o 16 2 0 1983.96 1908.48 41.91 o 18 2 0 0.91 11.65 26.47 o 20 2 0 25.89 64.51 32.24 o 22 2 0 283.05 170.00 58.99 o 1 3 0 5456.11 5230.23 73.16 o 3 3 0 45251.00 44518.64 492.04 o 5 3 0 44943.79 45234.32 527.62 o 7 3 0 409.31 284.81 11.30 o 9 3 0 10097.18 9446.63 117.65 o 11 3 0 16630.82 15073.05 181.93 o 13 3 0 3220.45 2948.66 51.21 o 15 3 0 142.86 201.00 22.34 o 17 3 0 3217.86 3195.05 58.90 o 19 3 0 3953.55 3781.74 84.74 o 21 3 0 645.76 683.43 72.41 o 23 3 0 39.21 39.24 57.45 o 0 4 0 85497.08 97331.98 1865.17 o 2 4 0 7866.26 7574.20 116.40 o 4 4 0 10865.66 13282.33 160.22 o 6 4 0 11929.21 11013.73 153.56 o 8 4 0 6462.62 5372.64 91.10 o 10 4 0 1021.75 935.11 25.43 o 12 4 0 27.92 -4.43 14.03 o 14 4 0 6020.66 5569.62 86.48 o 16 4 0 1469.97 1495.47 40.71 o 18 4 0 2672.47 2509.26 72.51 o 20 4 0 754.25 837.15 50.13 o 22 4 0 330.35 326.26 59.35 o 1 5 0 15.94 52.45 7.39 o 3 5 0 1108.85 1838.36 27.80 o 5 5 0 1054.05 1210.48 24.40 o 7 5 0 160.13 201.40 9.32 o 9 5 0 5.66 39.85 8.15 o 11 5 0 146.48 197.39 15.24 o 13 5 0 24.25 15.63 18.07 o 15 5 0 758.27 755.37 27.36 o 17 5 0 943.96 926.94 39.89 o 19 5 0 243.88 259.78 33.85 o 21 5 0 90.19 57.73 49.52 o 0 6 0 26323.33 25244.09 488.33 o 2 6 0 11528.37 11180.74 155.78 o 4 6 0 11110.94 13799.99 211.62 o 6 6 0 7941.59 6957.17 100.93 o 8 6 0 12018.32 11286.02 146.32 o 10 6 0 2790.24 3017.10 51.12 o 12 6 0 95.91 63.61 16.02 o 14 6 0 1787.80 1818.13 45.29 o 16 6 0 2969.23 2943.08 56.72 o 18 6 0 545.51 548.05 29.78 o 20 6 0 1470.83 1423.33 48.28 o 22 6 0 844.88 966.90 74.55 o 1 7 0 1099.31 1890.32 32.84 o 3 7 0 26545.12 27523.87 377.03 o 5 7 0 15897.21 16357.45 227.96 o 7 7 0 186.43 190.78 16.40 o 9 7 0 4114.93 3952.07 61.56 o 11 7 0 4348.56 4014.49 65.70 o 13 7 0 2570.75 2624.51 50.51 o 15 7 0 43.39 56.57 21.14 o 17 7 0 1477.10 1477.23 41.77 o 19 7 0 431.01 527.62 42.06 o 21 7 0 791.17 864.03 61.25 o 0 8 0 2599.09 3208.02 71.28 o 2 8 0 641.49 730.97 20.01 o 4 8 0 37.71 31.14 10.76 o 6 8 0 612.77 884.97 24.76 o 8 8 0 1029.15 1082.39 36.26 o 10 8 0 433.72 515.56 34.08 o 12 8 0 956.81 1057.82 40.12 o 14 8 0 249.18 237.81 22.69 o 16 8 0 238.22 239.36 25.61 o 18 8 0 7.13 42.07 36.48 o 20 8 0 17.52 -37.81 37.81 o 1 9 0 327.19 297.12 15.25 o 3 9 0 4537.68 4197.61 70.63 o 5 9 0 8277.00 8938.39 164.74 o 7 9 0 20.16 5.09 14.28 o 9 9 0 543.94 541.01 25.96 o 11 9 0 4017.90 4207.77 77.07 o 13 9 0 534.52 569.30 29.31 o 15 9 0 8.02 -12.83 22.97 o 17 9 0 980.94 1018.19 45.60 o 19 9 0 42.32 87.11 38.27 o 0 10 0 12808.92 12836.25 255.93 o 2 10 0 990.00 1037.30 27.45 o 4 10 0 1017.35 1243.72 33.20 o 6 10 0 7493.38 7249.20 120.03 o 8 10 0 2058.92 2063.68 76.56 o 10 10 0 918.54 1029.65 57.48 o 12 10 0 52.98 8.78 22.13 o 14 10 0 578.94 589.70 32.64 o 16 10 0 1759.79 1845.75 60.63 o 18 10 0 2.25 23.60 38.01 o 20 10 0 258.46 230.96 64.86 o 1 11 0 2314.20 2563.50 46.50 o 3 11 0 2220.73 2397.52 44.95 o 5 11 0 359.59 383.60 22.51 o 7 11 0 373.13 327.66 35.34 o 9 11 0 38.02 33.53 21.73 o 11 11 0 185.47 179.11 27.93 o 13 11 0 297.74 313.41 28.73 o 15 11 0 110.08 104.64 34.44 o 17 11 0 5.66 -21.34 36.39 o 19 11 0 48.47 -40.93 40.93 o 0 12 0 504.05 539.78 31.32 o 2 12 0 389.78 396.87 26.48 o 4 12 0 420.09 406.82 21.21 o 6 12 0 411.40 414.26 24.95 o 8 12 0 170.33 206.93 47.92 o 10 12 0 109.54 134.65 25.72 o 12 12 0 385.78 349.71 29.60 o 14 12 0 395.19 462.47 39.65 o 16 12 0 149.32 186.90 45.38 o 18 12 0 10.47 -48.37 63.64 o 1 13 0 155.33 190.11 20.09 o 3 13 0 2613.87 2867.82 63.59 o 5 13 0 402.04 500.11 31.42 o 7 13 0 171.45 208.08 33.85 o 9 13 0 194.96 155.19 35.47 o 11 13 0 999.43 1199.43 55.67 o 13 13 0 485.01 551.06 47.75 o 15 13 0 163.52 36.26 48.61 o 17 13 0 103.00 158.43 65.77 o 0 14 0 20.43 -1.90 36.63 o 2 14 0 705.06 749.14 35.11 o 4 14 0 971.80 863.10 55.60 o 6 14 0 25.70 18.21 32.14 o 8 14 0 611.40 580.51 41.83 o 10 14 0 2.17 -15.84 37.85 o 12 14 0 9.66 -4.47 38.72 o 14 14 0 11.87 20.98 43.94 o 16 14 0 268.58 433.48 130.65 o 1 15 0 123.67 80.03 29.11 o 3 15 0 167.59 221.64 47.24 o 5 15 0 2.52 6.03 59.03 o 7 15 0 13.74 28.45 48.32 o 9 15 0 7.83 42.55 55.88 o 11 15 0 127.41 136.19 57.00 o 13 15 0 41.75 35.23 59.07 o 0 16 0 258.51 304.79 49.54 o 2 16 0 1058.62 1097.06 98.38 o 4 16 0 303.59 244.28 73.19 o 6 16 0 3.61 20.84 53.22 o 8 16 0 435.86 479.57 60.86 o 10 16 0 308.58 175.34 59.33 o 12 16 0 21.26 -88.15 110.18 o 1 17 0 68.53 74.84 68.47 o 3 17 0 231.70 132.84 55.18 o 5 17 0 9.14 44.91 55.18 o 7 17 0 8.65 73.78 54.82 o 9 17 0 99.02 99.33 59.97 o 11 17 0 19.98 -107.04 108.61 o 2 18 0 19.07 89.67 55.60 o 4 18 0 111.01 24.62 55.90 o 6 18 0 98.64 49.86 127.50 o 8 18 0 36.73 105.46 111.76 o 3 19 0 7.51 91.24 70.05 o 5 19 0 31.67 88.39 63.73 o -23 1 1 2.22 4.82 51.67 o -21 1 1 1287.98 1315.81 56.61 o -19 1 1 879.19 890.52 38.41 o -17 1 1 1345.36 1324.27 35.30 o -15 1 1 662.85 573.67 25.35 o -13 1 1 12282.89 11021.14 143.13 o -11 1 1 1753.01 1132.14 21.96 o -9 1 1 1983.66 2448.09 33.47 o -7 1 1 21332.20 21211.15 250.84 o -5 1 1 23371.72 20519.25 196.74 o -1 1 1 896.68 815.30 13.44 o 3 1 1 75602.97 83281.63 1119.57 o 5 1 1 2041.57 1542.39 26.36 o 7 1 1 1694.06 1555.45 23.75 o 9 1 1 10095.52 8722.14 107.10 o 11 1 1 11891.38 11091.68 135.86 o 13 1 1 554.39 601.73 18.63 o 15 1 1 2270.61 2267.95 46.30 o 17 1 1 2282.27 2137.72 57.20 o 19 1 1 448.53 518.66 34.49 o 21 1 1 46.22 3.73 62.96 o -24 2 1 319.25 478.30 67.87 o -22 2 1 1316.59 1211.54 72.90 o -20 2 1 10.95 -33.17 33.17 o -18 2 1 745.58 758.16 31.60 o -16 2 1 2507.92 2154.75 43.12 o -14 2 1 5517.55 5124.83 67.58 o -12 2 1 2056.02 1949.82 30.55 o -10 2 1 20930.37 19717.90 234.70 o -8 2 1 31164.24 30231.56 383.08 o -6 2 1 160.77 49.34 5.75 o -4 2 1 78.27 420.19 18.00 o -2 2 1 33303.01 30236.01 379.37 o 0 2 1 3215.04 1375.11 22.71 o 2 2 1 19733.91 27401.70 407.68 o 4 2 1 18094.10 18234.09 247.30 o 6 2 1 22721.18 19530.82 218.21 o 8 2 1 8012.97 8019.19 98.49 o 10 2 1 619.13 835.03 32.64 o 12 2 1 8908.68 8296.57 104.31 o 14 2 1 5394.83 4907.42 77.54 o 16 2 1 30.81 28.00 19.47 o 18 2 1 172.00 201.71 30.03 o 20 2 1 968.17 990.11 60.47 o 22 2 1 615.48 672.21 117.27 o -23 3 1 47.43 -35.40 54.23 o -21 3 1 77.93 113.67 38.15 o -19 3 1 62.67 22.89 25.63 o -17 3 1 712.82 658.22 26.06 o -15 3 1 280.18 350.44 19.41 o -13 3 1 964.35 893.32 20.23 o -11 3 1 1508.71 1587.25 25.86 o -9 3 1 4.25 7.04 6.02 o -7 3 1 17778.10 21441.48 271.21 o -5 3 1 9059.39 13732.41 174.39 o -3 3 1 5907.93 7218.61 86.28 o -1 3 1 47024.79 63066.89 902.82 o 1 3 1 5679.69 5989.64 77.46 o 3 3 1 29.96 49.01 6.25 o 5 3 1 994.02 1323.74 28.05 o 7 3 1 3420.29 4587.47 58.31 o 9 3 1 39.82 132.60 10.24 o 11 3 1 1030.26 947.15 31.98 o 13 3 1 55.14 59.48 16.10 o 15 3 1 13.79 7.27 18.83 o 17 3 1 212.00 191.31 23.30 o 19 3 1 341.29 341.97 41.94 o 21 3 1 1.79 -4.08 55.62 o -22 4 1 346.11 283.00 58.96 o -20 4 1 13.25 6.24 37.49 o -18 4 1 818.36 822.36 30.18 o -16 4 1 5782.27 5772.93 90.45 o -14 4 1 73.47 42.57 16.46 o -12 4 1 1385.12 1520.89 32.85 o -10 4 1 16595.94 15687.67 202.52 o -6 4 1 4161.23 4485.72 66.12 o -4 4 1 18845.63 21284.54 268.96 o -2 4 1 14003.66 12669.13 174.32 o 0 4 1 25998.00 26953.73 367.11 o 2 4 1 34344.63 43149.98 543.90 o 4 4 1 19828.82 20267.24 303.25 o 6 4 1 1142.44 455.75 13.41 o 8 4 1 1935.67 1455.74 24.11 o 10 4 1 3150.01 3283.90 45.70 o 12 4 1 796.46 691.81 23.49 o 14 4 1 5096.48 4936.17 79.62 o 16 4 1 538.87 514.98 25.89 o 18 4 1 5.77 3.88 24.57 o 20 4 1 585.64 657.53 48.81 o -23 5 1 2.79 11.48 62.18 o -21 5 1 323.47 402.23 42.54 o -19 5 1 339.18 401.69 28.21 o -17 5 1 1798.02 1751.46 44.93 o -15 5 1 5236.26 5181.03 82.40 o -13 5 1 4482.69 3768.17 62.29 o -11 5 1 12922.37 12899.22 181.68 o -9 5 1 223.97 275.53 14.51 o -7 5 1 25964.45 27757.26 378.83 o -5 5 1 33259.89 31719.88 567.62 o -3 5 1 607.22 250.46 15.40 o -1 5 1 716.30 1116.97 20.49 o 1 5 1 7833.50 5497.07 78.58 o 3 5 1 4632.06 3025.55 46.59 o 5 5 1 2228.71 1969.35 40.74 o 7 5 1 5951.46 5859.36 84.87 o 9 5 1 9144.36 8237.19 132.72 o 11 5 1 4426.99 4173.75 67.01 o 13 5 1 582.60 629.31 24.13 o 15 5 1 3826.87 3690.72 65.34 o 17 5 1 577.74 683.67 30.57 o 19 5 1 1068.16 1163.86 50.73 o 21 5 1 509.92 415.41 60.47 o -22 6 1 6.00 -3.94 55.65 o -20 6 1 33.95 51.32 29.74 o -18 6 1 141.65 130.82 22.61 o -16 6 1 113.67 79.35 20.65 o -14 6 1 168.55 189.66 18.77 o -12 6 1 9.56 13.73 15.07 o -10 6 1 973.98 712.41 27.03 o -8 6 1 2708.94 2674.25 45.58 o -6 6 1 1365.84 1526.41 37.11 o -4 6 1 5813.14 7159.56 101.68 o -2 6 1 7825.52 7818.44 110.13 o 0 6 1 1293.04 1119.17 22.08 o 2 6 1 338.32 560.97 17.88 o 4 6 1 3346.22 5380.82 87.47 o 6 6 1 1289.53 1168.88 32.15 o 8 6 1 1912.00 1916.40 36.84 o 10 6 1 25.67 41.33 14.97 o 12 6 1 740.07 742.83 24.85 o 14 6 1 233.78 265.17 21.88 o 16 6 1 210.50 242.24 27.22 o 18 6 1 1146.40 1028.67 47.60 o 20 6 1 369.73 315.34 53.24 o -21 7 1 146.48 160.42 38.17 o -19 7 1 674.79 759.02 36.65 o -17 7 1 782.83 658.34 29.04 o -15 7 1 1387.20 1427.85 38.13 o -13 7 1 46.91 32.52 16.57 o -11 7 1 830.79 752.64 22.01 o -9 7 1 364.55 368.57 19.44 o -7 7 1 1425.98 1421.26 35.55 o -5 7 1 1812.28 1528.22 28.93 o -3 7 1 136.92 38.56 9.34 o -1 7 1 4535.07 5220.08 76.31 o 1 7 1 46.28 82.21 9.97 o 3 7 1 20300.27 22903.71 315.32 o 5 7 1 249.42 238.94 15.55 o 7 7 1 770.21 894.20 67.93 o 9 7 1 3570.18 3296.30 61.05 o 11 7 1 51.89 36.20 16.77 o 13 7 1 433.98 458.69 30.95 o 15 7 1 1601.51 1587.61 42.78 o 17 7 1 25.10 -13.18 34.17 o 19 7 1 205.20 206.22 39.48 o -22 8 1 22.76 42.77 65.36 o -20 8 1 4.21 -47.15 48.96 o -18 8 1 1325.27 1430.75 47.87 o -16 8 1 1121.60 1277.77 37.21 o -14 8 1 500.55 474.60 23.88 o -12 8 1 18.96 17.45 17.09 o -10 8 1 2188.79 1963.70 40.30 o -8 8 1 3520.93 2893.52 49.53 o -6 8 1 2353.42 2589.60 43.30 o -4 8 1 4299.23 4760.51 71.32 o -2 8 1 5115.54 4387.84 66.41 o 0 8 1 9962.37 9332.01 132.40 o 2 8 1 250.30 243.72 13.27 o 4 8 1 4100.22 3686.19 58.71 o 6 8 1 7697.15 6721.62 125.88 o 8 8 1 5892.79 6244.69 119.96 o 10 8 1 2773.63 2817.06 64.14 o 12 8 1 2248.27 2128.85 45.62 o 14 8 1 3081.80 3126.05 59.95 o 16 8 1 656.05 735.72 36.28 o 18 8 1 758.47 716.69 46.89 o 20 8 1 42.80 -5.85 42.71 o -21 9 1 6.40 32.25 49.76 o -19 9 1 204.38 207.33 38.77 o -17 9 1 0.51 -23.61 25.16 o -15 9 1 86.11 68.30 25.33 o -13 9 1 880.28 849.65 34.60 o -11 9 1 575.30 481.03 22.92 o -9 9 1 132.13 120.55 19.24 o -7 9 1 1409.29 1354.12 39.19 o -5 9 1 1596.62 1611.09 38.49 o -3 9 1 95.55 204.56 13.70 o -1 9 1 87.53 84.58 12.33 o 1 9 1 3199.04 3210.26 52.04 o 3 9 1 1932.09 1721.55 38.80 o 5 9 1 251.38 275.46 16.56 o 7 9 1 51.12 8.32 14.28 o 9 9 1 1006.83 975.24 36.44 o 11 9 1 1806.25 1830.42 46.39 o 13 9 1 117.13 67.38 28.30 o 15 9 1 5.71 -25.18 27.02 o 17 9 1 1279.35 1220.06 51.94 o 19 9 1 62.59 44.70 39.85 o -20 10 1 2.38 -23.47 38.94 o -18 10 1 3.74 -35.05 35.05 o -16 10 1 98.02 103.13 28.20 o -14 10 1 9.19 16.52 28.89 o -12 10 1 7.50 15.41 20.35 o -10 10 1 1348.06 1382.65 38.91 o -8 10 1 5.03 14.31 25.99 o -6 10 1 241.28 290.75 16.84 o -4 10 1 39.88 67.35 17.60 o -2 10 1 40.08 66.20 13.68 o 0 10 1 2638.21 2556.72 45.14 o 2 10 1 651.38 662.32 34.90 o 4 10 1 4207.22 4423.45 70.52 o 6 10 1 233.80 261.33 18.48 o 8 10 1 1839.09 2048.72 68.06 o 10 10 1 266.30 263.67 28.11 o 12 10 1 162.91 152.55 25.41 o 14 10 1 15.29 -27.36 27.36 o 16 10 1 0.11 -21.36 34.82 o 18 10 1 27.54 35.21 41.60 o -19 11 1 171.73 163.96 41.14 o -17 11 1 7.66 -23.78 34.45 o -15 11 1 8.85 -2.04 33.42 o -13 11 1 1857.05 1981.44 58.37 o -11 11 1 596.47 586.46 29.89 o -9 11 1 503.07 441.22 25.86 o -7 11 1 4821.60 4709.27 94.28 o -5 11 1 1602.57 1565.96 35.20 o -3 11 1 970.70 937.73 26.46 o -1 11 1 39.95 30.61 15.40 o 1 11 1 4154.99 3948.05 64.46 o 3 11 1 314.06 379.77 22.82 o 5 11 1 235.46 336.55 24.48 o 7 11 1 56.19 23.34 20.96 o 9 11 1 1436.71 1533.88 57.83 o 11 11 1 1905.05 2080.28 68.84 o 13 11 1 127.98 59.61 29.61 o 15 11 1 60.57 46.10 34.53 o 17 11 1 578.37 722.82 57.01 o -18 12 1 234.09 268.72 41.35 o -16 12 1 15.26 6.22 34.30 o -14 12 1 198.16 163.08 28.39 o -12 12 1 9.86 3.83 23.85 o -10 12 1 564.01 579.10 32.73 o -8 12 1 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267.71 29.32 o -12 12 5 11.94 -19.99 26.61 o -10 12 5 9.62 -5.19 25.33 o -8 12 5 2015.98 1994.15 85.37 o -6 12 5 219.99 248.27 47.03 o -4 12 5 701.77 837.19 36.86 o -2 12 5 5025.73 4719.74 97.71 o 0 12 5 923.70 859.02 37.38 o 2 12 5 431.10 277.80 29.34 o 4 12 5 41.99 93.07 35.94 o 6 12 5 352.57 310.67 40.41 o 8 12 5 192.49 279.92 47.23 o 10 12 5 5.50 39.72 47.26 o 12 12 5 3.06 -33.07 68.17 o -19 13 5 36.67 78.24 53.52 o -17 13 5 163.10 125.45 40.36 o -15 13 5 21.64 1.70 28.76 o -13 13 5 27.31 16.27 30.62 o -11 13 5 51.25 39.90 28.21 o -9 13 5 1.41 -3.45 26.59 o -7 13 5 0.07 -23.12 45.94 o -5 13 5 207.23 174.92 29.99 o -3 13 5 215.77 198.86 39.91 o -1 13 5 49.55 46.81 33.96 o 1 13 5 161.49 174.03 30.21 o 3 13 5 300.34 222.21 40.01 o 5 13 5 51.59 37.45 39.85 o 7 13 5 310.87 207.74 57.87 o 9 13 5 44.12 69.94 47.39 o 11 13 5 19.66 15.53 68.47 o -18 14 5 25.87 66.60 41.24 o -16 14 5 510.10 511.74 44.17 o -14 14 5 186.71 263.62 33.34 o -12 14 5 192.57 217.01 35.02 o -10 14 5 164.04 122.62 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