#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/60/2226085.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226085_Fobs loop_ _publ_author_name 'Johnson, Magnus T.' 'Cetina, Mario' 'Rissanen, Kari' 'Wendt, Ola F.' _publ_section_title ; [2,6-Bis(di-tert-butylphosphinomethyl)phenyl-\k^3^P,C^1^,P'](trifluoroacetato)palladium(II) ; _journal_coeditor_code CV2705 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m675 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1239 _cell_length_b 15.7484 _cell_length_c 32.4400 _exptl_crystal_F_000 2544.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file cv2705Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mj1002 in P b c a; C26 H43 F3 O2 P2 Pd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 578.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8013.88 7266.67 197.39 o 4 0 0 989.68 1424.94 48.22 o 6 0 0 93836.27 89381.41 3473.76 o 8 0 0 4003.64 4700.88 248.01 o 10 0 0 3.26 -77.70 97.49 o 12 0 0 33145.49 31734.01 1500.75 o 2 1 0 51016.93 49482.82 933.39 o 4 1 0 2195.91 1843.83 44.80 o 6 1 0 1651.42 2187.99 73.88 o 8 1 0 1344.62 1916.39 74.38 o 10 1 0 5840.18 6236.36 234.63 o 12 1 0 1057.79 1011.08 104.39 o 0 2 0 259435.38 954.70 439.04 o 2 2 0 11151.17 14531.52 269.73 o 4 2 0 18766.63 21479.32 457.39 o 6 2 0 60430.56 62411.12 1436.35 o 8 2 0 6264.60 6324.44 188.17 o 10 2 0 1612.63 1427.15 98.95 o 12 2 0 25578.16 26443.87 948.23 o 2 3 0 51003.78 49594.18 877.79 o 4 3 0 33739.85 29388.51 639.14 o 6 3 0 31330.13 34291.56 754.31 o 8 3 0 11043.75 9763.99 265.77 o 10 3 0 8535.75 8813.69 305.66 o 12 3 0 1710.30 2019.67 150.81 o 0 4 0 21873.14 24610.44 717.40 o 2 4 0 3237.66 3562.51 64.76 o 4 4 0 1778.69 2316.09 63.55 o 6 4 0 34530.10 34402.36 853.57 o 8 4 0 2840.57 2993.50 174.75 o 10 4 0 495.40 281.73 81.37 o 12 4 0 4071.81 3623.65 284.42 o 2 5 0 32773.21 33940.52 654.65 o 4 5 0 62342.84 64343.93 1403.82 o 6 5 0 4097.96 4007.30 94.27 o 8 5 0 283.83 476.16 39.23 o 10 5 0 19813.42 20818.33 702.20 o 12 5 0 4545.81 4228.79 201.46 o 0 6 0 1139.18 1028.83 45.38 o 2 6 0 1013.71 1142.12 36.75 o 4 6 0 7007.81 6994.67 173.29 o 6 6 0 331.05 278.74 22.97 o 8 6 0 2324.05 2597.68 114.57 o 10 6 0 1134.99 927.36 68.41 o 12 6 0 1.55 -38.91 80.45 o 2 7 0 20796.51 20029.00 419.38 o 4 7 0 13049.93 11700.66 289.77 o 6 7 0 14549.84 14622.76 337.83 o 8 7 0 2518.15 2499.72 102.99 o 10 7 0 6673.27 6237.96 198.97 o 12 7 0 1361.67 1566.69 121.15 o 0 8 0 8805.79 9170.53 310.74 o 2 8 0 169.37 89.95 23.05 o 4 8 0 246.13 372.25 29.79 o 6 8 0 37862.19 37493.62 858.16 o 8 8 0 8405.64 7846.61 266.76 o 10 8 0 2079.73 1809.63 188.89 o 2 9 0 23.38 105.13 27.57 o 4 9 0 617.95 796.05 46.79 o 6 9 0 1730.34 1961.74 75.93 o 8 9 0 583.01 589.10 125.18 o 10 9 0 3129.89 3020.31 172.99 o 0 10 0 157466.00 156407.16 5747.45 o 2 10 0 5374.97 4540.26 123.22 o 4 10 0 5.12 14.38 39.49 o 6 10 0 25006.61 26458.28 739.42 o 8 10 0 1536.83 1520.48 102.60 o 10 10 0 1848.83 1999.88 122.00 o 2 11 0 537.26 788.76 45.98 o 4 11 0 1773.29 2045.34 76.60 o 6 11 0 0.15 -23.19 52.75 o 8 11 0 699.06 658.30 85.96 o 10 11 0 1011.68 1031.44 112.46 o 0 12 0 38192.88 40673.59 1544.90 o 2 12 0 3410.14 4070.01 120.63 o 4 12 0 469.07 433.99 46.40 o 6 12 0 3130.63 3172.04 168.49 o 8 12 0 3489.27 3416.19 184.95 o 10 12 0 2258.45 2115.06 157.11 o 2 13 0 20220.39 19562.80 465.27 o 4 13 0 19840.87 19431.17 538.16 o 6 13 0 4.14 15.21 55.28 o 8 13 0 8964.52 9163.73 317.13 o 0 14 0 3438.24 2796.87 147.32 o 2 14 0 1144.80 951.52 65.32 o 4 14 0 213.15 161.71 55.32 o 6 14 0 3433.77 2754.22 140.64 o 8 14 0 1965.08 2068.33 235.79 o 2 15 0 24425.90 25036.46 632.95 o 4 15 0 21655.82 22402.08 660.87 o 6 15 0 1925.71 1904.85 116.99 o 0 16 0 112.20 79.84 89.95 o 2 16 0 381.49 584.24 115.61 o 4 16 0 5.23 65.44 104.43 o 6 16 0 10.58 188.87 83.66 o 2 17 0 10919.48 10150.63 325.01 o 4 17 0 18163.10 16638.76 619.98 o 0 18 0 3742.94 3763.66 261.69 o 2 18 0 12.50 186.16 82.91 o 2 1 1 46.46 70.90 6.52 o 3 1 1 2455.90 2673.04 36.28 o 4 1 1 21634.23 21067.67 310.44 o 5 1 1 16705.53 17146.32 266.83 o 6 1 1 73.22 212.28 14.99 o 7 1 1 24744.24 23978.66 463.99 o 8 1 1 1419.96 1483.53 54.42 o 9 1 1 702.49 739.00 45.67 o 10 1 1 13577.16 13759.99 331.08 o 11 1 1 4579.67 4620.50 138.95 o 12 1 1 3088.02 3621.26 197.97 o 13 1 1 4732.22 4477.06 152.98 o 0 2 1 23052.14 13439.90 1067.62 o 1 2 1 22032.58 19904.28 264.54 o 2 2 1 18412.81 20172.06 258.29 o 3 2 1 10107.42 9776.88 122.14 o 4 2 1 5395.50 6254.39 98.63 o 5 2 1 7737.74 7444.46 125.38 o 6 2 1 20744.35 20081.77 315.47 o 7 2 1 3019.10 3445.08 75.87 o 8 2 1 476.67 477.22 28.95 o 9 2 1 2328.95 2624.65 68.12 o 10 2 1 541.75 575.64 64.51 o 11 2 1 1421.97 1755.57 83.00 o 12 2 1 3573.51 3877.71 131.15 o 13 2 1 174.25 179.49 67.92 o 1 3 1 28573.57 26783.71 346.06 o 2 3 1 23369.78 25307.09 303.34 o 3 3 1 344.41 469.16 12.52 o 4 3 1 7404.32 7571.75 116.07 o 5 3 1 17628.39 18219.68 282.76 o 6 3 1 1929.47 1938.50 44.90 o 7 3 1 12525.83 12342.15 212.27 o 8 3 1 27.19 65.82 22.36 o 9 3 1 239.42 233.57 30.23 o 10 3 1 1671.48 1716.33 77.69 o 11 3 1 1146.29 1376.90 71.78 o 12 3 1 1813.46 1834.00 88.18 o 13 3 1 2783.54 2584.26 116.82 o 0 4 1 9226.42 7287.59 143.46 o 1 4 1 16794.50 17404.63 235.29 o 2 4 1 3087.40 2629.21 37.51 o 3 4 1 596.71 430.43 15.16 o 4 4 1 2565.37 2836.45 47.28 o 5 4 1 59552.70 63095.30 1032.34 o 6 4 1 47337.27 48953.09 823.29 o 7 4 1 1117.28 879.84 52.92 o 8 4 1 3350.75 3254.22 82.47 o 9 4 1 3917.48 3548.14 92.77 o 10 4 1 336.11 365.10 50.59 o 11 4 1 7233.54 7337.50 207.35 o 12 4 1 10653.43 11117.04 361.36 o 1 5 1 2400.70 2895.25 50.69 o 2 5 1 2114.23 2390.41 37.89 o 3 5 1 630.66 812.49 18.43 o 4 5 1 1698.52 2039.19 40.36 o 5 5 1 249.63 198.74 14.49 o 6 5 1 334.75 454.67 22.56 o 7 5 1 3244.60 3058.60 57.12 o 8 5 1 3647.72 3401.05 85.72 o 9 5 1 45.86 34.94 31.25 o 10 5 1 33.64 94.24 48.28 o 11 5 1 51.59 162.79 52.96 o 12 5 1 403.28 457.60 71.18 o 0 6 1 39257.16 38786.00 814.64 o 1 6 1 2041.70 1972.96 38.77 o 2 6 1 2974.06 3296.27 50.42 o 3 6 1 50.31 257.98 16.93 o 4 6 1 2185.33 1928.51 49.05 o 5 6 1 31961.33 30635.03 467.57 o 6 6 1 57959.95 57858.01 835.63 o 7 6 1 3651.45 4068.04 70.34 o 8 6 1 7664.19 7698.00 158.33 o 9 6 1 4379.44 4724.01 108.49 o 10 6 1 15.56 -24.63 37.76 o 11 6 1 10755.92 11143.54 258.24 o 12 6 1 7501.43 7217.19 200.23 o 1 7 1 18476.60 19592.50 326.35 o 2 7 1 25804.56 26136.77 404.83 o 3 7 1 13.56 49.91 14.55 o 4 7 1 19179.92 19413.64 337.21 o 5 7 1 4924.38 4944.18 89.91 o 6 7 1 865.91 947.42 37.17 o 7 7 1 1306.49 1442.96 50.00 o 8 7 1 3498.68 3721.20 131.91 o 9 7 1 3415.13 3371.53 96.54 o 10 7 1 5372.75 5488.09 126.92 o 11 7 1 58.08 45.00 75.77 o 12 7 1 11.23 14.43 73.50 o 0 8 1 14579.96 13130.35 308.28 o 1 8 1 8414.48 9016.26 157.30 o 2 8 1 8954.50 8841.29 141.60 o 3 8 1 8386.88 8421.71 138.27 o 4 8 1 475.09 595.55 23.37 o 5 8 1 22201.72 23746.61 396.75 o 6 8 1 31490.05 32680.19 548.42 o 7 8 1 1715.08 1476.82 51.69 o 8 8 1 1668.89 1496.86 75.27 o 9 8 1 75.20 100.00 37.63 o 10 8 1 222.81 303.47 42.07 o 11 8 1 2811.52 2863.65 106.66 o 1 9 1 2352.78 2092.14 61.44 o 2 9 1 27214.57 28078.42 462.44 o 3 9 1 150.40 125.20 18.46 o 4 9 1 20340.45 21085.89 344.03 o 5 9 1 7477.48 7355.35 135.20 o 6 9 1 55.13 36.62 31.51 o 7 9 1 2403.56 2527.22 69.89 o 8 9 1 3511.78 3251.94 91.23 o 9 9 1 2819.34 2645.25 81.56 o 10 9 1 10951.56 10730.81 251.42 o 11 9 1 1385.21 1154.82 89.37 o 0 10 1 11933.27 12459.73 314.23 o 1 10 1 14.49 34.77 18.38 o 2 10 1 291.16 384.72 31.03 o 3 10 1 4099.95 4185.00 82.63 o 4 10 1 39.36 23.23 20.22 o 5 10 1 700.01 632.14 30.65 o 6 10 1 4636.21 4829.05 113.32 o 7 10 1 991.58 997.91 56.41 o 8 10 1 127.11 119.68 41.26 o 9 10 1 360.48 253.93 49.35 o 10 10 1 2369.54 2437.05 99.03 o 11 10 1 42.03 -34.21 65.41 o 1 11 1 19112.72 20094.14 388.83 o 2 11 1 7553.78 7724.19 139.66 o 3 11 1 1273.20 995.67 38.18 o 4 11 1 15309.12 14897.29 263.97 o 5 11 1 6930.95 6952.92 137.01 o 6 11 1 225.54 90.26 36.46 o 7 11 1 6191.58 6182.31 139.13 o 8 11 1 3643.85 3882.36 110.80 o 9 11 1 1287.31 1232.21 68.52 o 10 11 1 10872.59 10943.48 268.06 o 0 12 1 227.57 243.05 54.34 o 1 12 1 1671.55 1649.52 50.00 o 2 12 1 11.44 28.62 21.59 o 3 12 1 6608.47 6696.26 126.17 o 4 12 1 1792.65 1673.54 57.08 o 5 12 1 488.69 600.59 48.74 o 6 12 1 2695.29 2907.03 96.94 o 7 12 1 539.86 652.86 52.69 o 8 12 1 19.07 19.13 53.97 o 9 12 1 919.84 1113.76 74.06 o 10 12 1 1068.30 1060.56 71.30 o 1 13 1 8556.37 9100.78 177.75 o 2 13 1 3962.45 3998.43 119.29 o 3 13 1 0.50 49.09 28.72 o 4 13 1 4388.79 4332.33 97.39 o 5 13 1 933.90 1013.02 54.42 o 6 13 1 807.43 803.54 51.58 o 7 13 1 2245.24 2202.36 71.26 o 8 13 1 2652.43 2577.64 101.07 o 9 13 1 447.79 272.14 68.76 o 0 14 1 4064.83 4162.27 149.18 o 1 14 1 5335.07 5001.46 112.07 o 2 14 1 1280.13 1479.48 53.33 o 3 14 1 5711.58 5732.21 126.72 o 4 14 1 518.61 404.42 48.61 o 5 14 1 6478.72 6411.90 176.78 o 6 14 1 6028.97 5898.83 149.36 o 7 14 1 3137.77 2973.34 121.40 o 8 14 1 382.39 305.79 72.60 o 1 15 1 49.46 61.22 36.65 o 2 15 1 446.92 354.61 43.62 o 3 15 1 589.04 810.23 58.97 o 4 15 1 181.96 341.05 57.33 o 5 15 1 32.72 32.61 53.87 o 6 15 1 5.51 -41.53 55.98 o 7 15 1 170.85 242.44 75.66 o 0 16 1 4795.46 4440.46 189.00 o 1 16 1 4806.83 4647.17 126.71 o 2 16 1 22.35 40.21 46.43 o 3 16 1 5455.16 5685.27 150.05 o 4 16 1 169.99 301.49 58.18 o 5 16 1 10176.78 9965.68 285.83 o 6 16 1 5651.05 5246.26 161.82 o 1 17 1 252.89 188.32 61.55 o 2 17 1 611.21 623.83 67.13 o 3 17 1 0.67 22.85 60.69 o 4 17 1 2978.85 2626.70 104.47 o 5 17 1 163.55 135.13 70.85 o 0 18 1 3010.58 2659.96 145.26 o 1 18 1 1444.52 1168.16 116.66 o 2 18 1 97.70 196.65 56.71 o 3 18 1 1964.50 1729.05 91.93 o 0 0 2 245.36 -6.19 4.13 o 1 0 2 47775.90 -9.30 6.20 o 2 0 2 380.21 463.09 15.45 o 3 0 2 19114.10 19415.92 365.97 o 4 0 2 3256.51 3929.71 84.51 o 5 0 2 7206.75 6078.52 154.85 o 6 0 2 217.56 301.56 39.62 o 7 0 2 5023.28 6455.79 181.87 o 8 0 2 1478.49 1267.57 70.38 o 9 0 2 3529.18 4869.98 186.65 o 10 0 2 333.51 605.29 108.37 o 11 0 2 38104.75 37533.96 1242.97 o 12 0 2 1587.97 1792.42 189.25 o 13 0 2 646.61 643.94 114.46 o 2 1 2 4108.25 3216.93 41.13 o 3 1 2 12630.16 14547.41 184.94 o 4 1 2 2722.49 1618.41 31.71 o 5 1 2 475.15 1087.68 24.68 o 6 1 2 4855.83 5867.64 97.69 o 7 1 2 7360.18 7754.29 139.05 o 8 1 2 578.11 410.40 40.11 o 9 1 2 124.02 203.59 45.26 o 10 1 2 1019.78 1107.35 82.96 o 11 1 2 2546.62 2547.92 100.70 o 12 1 2 7.42 -5.62 54.45 o 13 1 2 1829.02 1771.68 124.58 o 0 2 2 23816.56 27080.54 617.69 o 1 2 2 43691.23 44540.84 611.41 o 2 2 2 22818.05 24740.61 312.07 o 3 2 2 51629.48 50528.89 643.14 o 4 2 2 0.74 12.39 9.41 o 5 2 2 39609.02 41003.01 650.81 o 6 2 2 1711.17 1489.61 35.02 o 7 2 2 1753.88 1374.51 35.11 o 8 2 2 3227.49 3373.18 85.55 o 9 2 2 746.44 684.57 43.28 o 10 2 2 4504.13 4118.11 156.16 o 11 2 2 17716.52 17862.46 429.95 o 12 2 2 13.74 116.29 60.64 o 13 2 2 37.32 -23.45 60.09 o 1 3 2 7957.12 6315.13 86.64 o 2 3 2 25289.93 24507.34 307.88 o 3 3 2 945.94 1552.09 26.79 o 4 3 2 2920.19 4049.62 66.20 o 5 3 2 15521.68 16192.01 244.74 o 6 3 2 1228.61 1420.27 35.77 o 7 3 2 35560.92 36913.94 662.03 o 8 3 2 1807.24 1452.50 56.76 o 9 3 2 7928.63 7899.60 179.82 o 10 3 2 137.37 101.17 43.82 o 11 3 2 5675.18 6559.59 187.87 o 12 3 2 90.09 -26.95 63.14 o 13 3 2 7975.66 7866.61 246.91 o 0 4 2 53599.45 60788.72 1219.25 o 1 4 2 173.47 292.49 13.26 o 2 4 2 23131.82 23690.74 302.79 o 3 4 2 3.89 -15.58 10.39 o 4 4 2 20.23 36.43 18.70 o 5 4 2 2008.14 1907.42 40.36 o 6 4 2 210.88 251.66 15.99 o 7 4 2 4.65 24.38 16.44 o 8 4 2 239.39 184.39 29.98 o 9 4 2 205.68 256.57 36.36 o 10 4 2 1960.46 1940.11 86.00 o 11 4 2 4943.10 5447.60 164.06 o 12 4 2 0.09 98.61 61.61 o 1 5 2 115836.52 116884.79 1907.46 o 2 5 2 1171.60 781.08 28.19 o 3 5 2 1112.98 1064.47 22.33 o 4 5 2 456.35 404.80 23.83 o 5 5 2 41751.89 40283.47 667.30 o 6 5 2 689.56 593.96 19.49 o 7 5 2 28470.21 28990.00 454.23 o 8 5 2 27.15 115.70 33.95 o 9 5 2 2883.36 3116.84 83.38 o 10 5 2 68.21 77.82 42.71 o 11 5 2 5189.02 4846.48 153.69 o 12 5 2 119.26 263.44 63.33 o 0 6 2 1619.41 1850.65 70.50 o 1 6 2 7125.32 7618.34 116.83 o 2 6 2 34.63 34.69 12.91 o 3 6 2 6301.96 6659.13 108.41 o 4 6 2 157.50 140.53 21.35 o 5 6 2 9027.11 9568.05 160.39 o 6 6 2 864.07 941.75 41.23 o 7 6 2 9326.42 9530.04 166.01 o 8 6 2 366.34 417.89 34.88 o 9 6 2 2659.61 3075.67 95.25 o 10 6 2 294.80 253.34 52.58 o 11 6 2 2320.34 2404.25 110.89 o 12 6 2 37.57 104.59 73.75 o 1 7 2 35312.29 35740.09 557.40 o 2 7 2 46.98 179.61 17.26 o 3 7 2 326.85 384.38 19.03 o 4 7 2 694.27 583.59 31.46 o 5 7 2 54972.16 55254.09 924.33 o 6 7 2 8.81 42.24 20.41 o 7 7 2 32262.06 32033.45 524.46 o 8 7 2 177.91 140.80 34.10 o 9 7 2 4102.33 3859.19 101.20 o 10 7 2 129.56 158.68 39.94 o 11 7 2 3535.25 3789.54 128.31 o 12 7 2 0.23 73.91 66.60 o 0 8 2 5291.00 5505.46 144.74 o 1 8 2 24683.77 23536.29 411.44 o 2 8 2 17.02 55.88 20.63 o 3 8 2 21625.85 20379.88 323.70 o 4 8 2 3572.76 3228.51 67.24 o 5 8 2 29601.97 29775.12 518.44 o 6 8 2 2.05 62.52 23.48 o 7 8 2 10606.03 11058.57 201.18 o 8 8 2 4.45 8.10 31.08 o 9 8 2 6292.50 6395.94 151.88 o 10 8 2 183.22 309.72 42.48 o 11 8 2 10619.71 10294.25 252.43 o 1 9 2 14815.95 13334.50 236.77 o 2 9 2 80.18 34.92 20.24 o 3 9 2 5963.04 5778.67 99.44 o 4 9 2 0.25 37.14 17.05 o 5 9 2 7153.57 7322.58 135.66 o 6 9 2 635.34 657.86 38.65 o 7 9 2 7918.89 7780.44 148.11 o 8 9 2 66.75 111.43 36.67 o 9 9 2 381.80 358.51 45.01 o 10 9 2 129.18 182.72 47.03 o 11 9 2 7113.73 6853.08 199.17 o 0 10 2 5.92 88.30 28.73 o 1 10 2 33634.58 35211.64 605.27 o 2 10 2 29.79 91.90 20.68 o 3 10 2 24328.62 25994.76 437.11 o 4 10 2 9.43 18.66 20.43 o 5 10 2 16219.61 17228.11 305.05 o 6 10 2 602.92 718.73 45.80 o 7 10 2 2321.18 2299.62 83.16 o 8 10 2 428.06 397.09 48.87 o 9 10 2 5013.63 4951.87 118.68 o 10 10 2 97.82 74.66 44.03 o 11 10 2 19904.37 19162.49 488.93 o 1 11 2 41.69 28.20 20.70 o 2 11 2 1887.85 1464.15 42.21 o 3 11 2 22.60 48.69 25.17 o 4 11 2 36.73 85.06 22.95 o 5 11 2 83.28 67.11 28.28 o 6 11 2 5.37 66.95 34.31 o 7 11 2 388.95 613.33 51.95 o 8 11 2 995.73 1222.66 84.05 o 9 11 2 13.09 36.76 51.19 o 10 11 2 5.94 -8.42 49.36 o 0 12 2 801.82 945.92 51.62 o 1 12 2 25637.81 24180.40 440.03 o 2 12 2 1017.57 782.44 36.94 o 3 12 2 15699.23 15766.70 270.42 o 4 12 2 2353.08 2382.51 57.95 o 5 12 2 10788.53 11004.32 220.30 o 6 12 2 1653.27 1692.74 65.06 o 7 12 2 2540.14 2645.58 85.43 o 8 12 2 462.64 461.37 53.54 o 9 12 2 6256.53 5504.53 164.04 o 10 12 2 71.18 55.36 54.63 o 1 13 2 769.04 1056.90 39.95 o 2 13 2 1366.93 1445.74 47.25 o 3 13 2 3343.83 3320.24 73.27 o 4 13 2 76.87 152.98 32.38 o 5 13 2 865.78 764.51 69.68 o 6 13 2 855.15 868.08 59.26 o 7 13 2 3614.25 3293.83 94.76 o 8 13 2 21.65 -89.38 64.88 o 9 13 2 3889.98 3676.53 132.27 o 0 14 2 787.55 756.62 67.39 o 1 14 2 1155.42 1188.50 60.20 o 2 14 2 1028.48 1211.29 49.52 o 3 14 2 1184.16 1342.51 50.69 o 4 14 2 78.40 103.07 43.44 o 5 14 2 3988.66 4143.29 108.56 o 6 14 2 612.08 557.38 67.61 o 7 14 2 200.68 343.85 56.89 o 8 14 2 202.72 275.57 74.07 o 1 15 2 10507.38 10840.24 228.89 o 2 15 2 1894.13 1518.20 65.10 o 3 15 2 647.43 750.85 49.05 o 4 15 2 713.99 643.15 64.71 o 5 15 2 5119.71 4639.05 131.90 o 6 15 2 110.45 7.12 57.75 o 7 15 2 5413.46 4847.46 161.29 o 0 16 2 16.31 38.70 61.12 o 1 16 2 21.38 0.89 46.97 o 2 16 2 70.69 24.45 47.46 o 3 16 2 177.31 339.96 52.00 o 4 16 2 19.77 7.18 54.01 o 5 16 2 259.39 252.11 60.13 o 6 16 2 6.40 13.57 58.89 o 1 17 2 4833.26 4556.86 122.68 o 2 17 2 589.93 739.98 66.67 o 3 17 2 110.34 93.63 55.91 o 4 17 2 474.79 602.71 63.89 o 5 17 2 6221.78 6793.87 226.43 o 0 18 2 65.60 111.33 66.63 o 1 18 2 1668.50 1432.10 78.88 o 2 18 2 165.11 180.66 56.23 o 3 18 2 3013.64 2587.92 99.18 o 2 1 3 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840.45 43.04 o 6 10 9 708.85 879.86 55.24 o 7 10 9 841.88 929.35 46.90 o 8 10 9 1875.37 2012.41 84.20 o 9 10 9 2751.26 2610.47 103.84 o 10 10 9 250.91 251.62 65.92 o 1 11 9 7586.67 7611.92 151.62 o 2 11 9 13382.34 13490.55 264.08 o 3 11 9 3515.91 3141.90 82.14 o 4 11 9 16912.31 16632.44 297.02 o 5 11 9 7665.59 7740.09 162.06 o 6 11 9 1827.45 1621.19 69.42 o 7 11 9 2685.58 2924.24 100.12 o 8 11 9 2111.54 2234.72 98.48 o 9 11 9 940.06 857.87 72.06 o 10 11 9 4462.62 4113.43 164.00 o 0 12 9 2193.36 2399.03 94.83 o 1 12 9 547.97 673.67 50.18 o 2 12 9 6048.75 5988.36 127.30 o 3 12 9 1785.54 1589.10 54.66 o 4 12 9 5635.99 6150.83 139.06 o 5 12 9 421.51 549.10 46.29 o 6 12 9 1907.68 1892.50 74.56 o 7 12 9 1.66 144.76 63.15 o 8 12 9 3781.70 3607.72 133.38 o 9 12 9 636.41 466.91 87.77 o 1 13 9 1523.19 1673.76 61.04 o 2 13 9 10447.80 10526.24 205.54 o 3 13 9 922.40 1057.66 58.36 o 4 13 9 7577.38 7824.91 158.84 o 5 13 9 995.32 652.49 51.17 o 6 13 9 584.34 891.10 60.16 o 7 13 9 1258.40 949.90 65.37 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10 368.50 78.29 24.17 o 3 0 10 66262.39 68203.73 1545.59 o 4 0 10 28252.95 28562.66 728.36 o 5 0 10 9369.27 9049.79 233.82 o 6 0 10 14267.85 14800.66 381.14 o 7 0 10 7031.22 6230.38 152.40 o 8 0 10 6328.51 6491.34 221.07 o 9 0 10 35872.73 35750.61 901.08 o 10 0 10 4278.31 3788.33 132.39 o 11 0 10 12744.39 12558.54 401.32 o 12 0 10 86.26 18.47 110.61 o 1 1 10 11249.16 11639.64 187.99 o 2 1 10 199.52 152.80 21.73 o 3 1 10 10678.29 10836.26 186.16 o 4 1 10 1873.34 2103.30 45.12 o 5 1 10 316.01 478.01 29.51 o 6 1 10 502.59 449.83 27.42 o 7 1 10 5962.96 6014.74 124.12 o 8 1 10 1676.71 1900.25 51.84 o 9 1 10 390.08 385.84 35.44 o 10 1 10 7.47 37.77 39.90 o 11 1 10 66.79 120.96 52.87 o 12 1 10 82.30 121.02 56.63 o 0 2 10 1285.75 2083.29 58.29 o 1 2 10 20473.94 19797.16 339.77 o 2 2 10 10952.24 12483.52 218.37 o 3 2 10 143239.34 141612.98 2734.89 o 4 2 10 398.99 279.00 30.68 o 5 2 10 12453.59 11454.39 194.17 o 6 2 10 78.23 52.01 17.33 o 7 2 10 414.38 498.90 29.44 o 8 2 10 4987.59 4683.14 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8 10 1912.54 2173.71 90.12 o 1 8 10 297.08 310.07 18.47 o 2 8 10 293.94 202.04 24.14 o 3 8 10 20772.62 20537.55 340.67 o 4 8 10 166.03 308.57 30.03 o 5 8 10 3975.13 4380.88 88.41 o 6 8 10 1555.35 1188.77 83.91 o 7 8 10 727.12 684.42 41.00 o 8 8 10 2511.74 2351.65 85.56 o 9 8 10 4866.18 4906.53 150.94 o 10 8 10 11.87 90.60 61.72 o 11 8 10 2378.15 2386.19 170.49 o 1 9 10 756.45 897.31 36.41 o 2 9 10 1161.44 1322.02 47.63 o 3 9 10 3363.09 3465.91 92.47 o 4 9 10 4.67 11.03 19.68 o 5 9 10 407.28 343.93 29.25 o 6 9 10 347.06 259.20 30.17 o 7 9 10 1949.69 2476.72 93.74 o 8 9 10 214.43 88.53 47.55 o 9 9 10 1517.73 1458.22 80.30 o 10 9 10 10.01 7.33 57.42 o 11 9 10 162.25 196.64 67.36 o 0 10 10 4316.17 4131.33 125.07 o 1 10 10 3085.24 2893.10 70.15 o 2 10 10 1994.46 2151.72 72.48 o 3 10 10 22408.71 22770.31 428.41 o 4 10 10 6375.47 5477.51 119.54 o 5 10 10 5439.92 5153.13 103.89 o 6 10 10 316.02 278.29 36.15 o 7 10 10 1322.21 1135.17 69.76 o 8 10 10 4530.99 4665.71 134.89 o 9 10 10 10512.39 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639.81 552.91 85.66 o 3 12 28 1177.93 921.99 96.78 o 1 1 29 3429.97 2922.86 133.88 o 2 1 29 16915.45 16876.37 342.91 o 3 1 29 483.78 437.86 48.41 o 4 1 29 12941.30 12395.17 269.49 o 5 1 29 1827.04 1814.33 71.91 o 6 1 29 1588.72 1580.28 72.02 o 7 1 29 1149.71 1040.55 85.80 o 8 1 29 1538.24 1461.14 90.80 o 0 2 29 12341.53 12753.45 387.77 o 1 2 29 15.43 19.19 52.51 o 2 2 29 111.20 129.53 38.83 o 3 2 29 0.37 67.51 42.62 o 4 2 29 589.65 563.82 52.70 o 5 2 29 31.02 27.04 44.52 o 6 2 29 4594.91 4632.17 148.45 o 7 2 29 502.72 524.09 52.24 o 8 2 29 1470.77 1604.82 85.70 o 1 3 29 4874.09 4724.65 130.36 o 2 3 29 4154.34 4091.40 108.06 o 3 3 29 1268.33 1278.68 62.85 o 4 3 29 4038.11 4344.28 109.70 o 5 3 29 12.96 -15.01 40.64 o 6 3 29 502.70 529.90 55.25 o 7 3 29 397.65 402.77 60.35 o 8 3 29 27.86 97.25 58.81 o 0 4 29 28309.30 28657.46 878.94 o 1 4 29 9.47 -28.43 34.08 o 2 4 29 2259.91 2143.95 96.24 o 3 4 29 483.57 474.09 49.76 o 4 4 29 85.59 105.67 40.62 o 5 4 29 159.86 93.21 38.26 o 6 4 29 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78.00 63.42 o 2 6 30 0.45 40.28 57.13 o 3 6 30 551.44 502.39 58.32 o 4 6 30 117.92 74.80 52.23 o 5 6 30 197.87 229.97 54.42 o 6 6 30 25.25 -82.04 54.69 o 7 6 30 0.41 68.34 59.27 o 1 7 30 1917.89 2183.55 122.35 o 2 7 30 1405.26 1717.27 94.07 o 3 7 30 70.04 64.61 58.25 o 4 7 30 2950.99 2854.01 98.13 o 5 7 30 1160.78 1439.96 95.38 o 6 7 30 1464.25 1500.78 104.37 o 0 8 30 9065.69 9004.52 658.30 o 1 8 30 3843.03 3640.34 205.51 o 2 8 30 1877.73 1934.83 100.64 o 3 8 30 223.40 216.74 55.46 o 4 8 30 79.77 81.48 61.69 o 5 8 30 3806.99 3446.15 124.19 o 6 8 30 1291.69 1307.54 80.99 o 1 9 30 660.60 661.34 82.90 o 2 9 30 555.13 460.79 75.61 o 3 9 30 763.07 835.19 78.12 o 4 9 30 788.26 783.92 85.55 o 5 9 30 39.65 3.76 67.53 o 0 10 30 3779.97 4194.64 251.63 o 1 10 30 2895.99 3340.35 149.03 o 2 10 30 258.46 475.30 88.34 o 3 10 30 379.83 425.40 78.82 o 4 10 30 786.57 483.33 77.54 o 1 11 30 1050.20 1018.29 96.45 o 2 11 30 1787.45 1695.89 112.05 o 1 1 31 15043.97 15097.99 346.25 o 2 1 31 1.41 29.46 42.23 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174.63 61.50 o 1 7 33 82.32 147.19 56.49 o 2 7 33 1016.52 1094.87 96.14 o 3 7 33 16.20 -78.85 62.37 o 4 7 33 1485.91 1380.18 83.59 o 0 8 33 5232.11 5504.49 344.90 o 1 8 33 262.70 193.40 67.95 o 2 8 33 220.96 239.32 139.65 o 3 8 33 340.10 388.42 71.56 o 1 9 33 2.62 41.48 68.01 o 2 9 33 4250.59 4408.06 161.57 o 0 0 34 5884.69 5530.23 587.35 o 1 0 34 13860.32 14464.05 438.33 o 2 0 34 1480.43 1608.15 132.11 o 3 0 34 538.22 828.98 95.77 o 4 0 34 3133.83 3093.09 163.84 o 5 0 34 8306.75 7807.68 277.44 o 6 0 34 4384.26 4508.60 186.88 o 1 1 34 196.38 197.27 53.52 o 2 1 34 523.11 460.71 97.33 o 3 1 34 189.69 175.92 52.45 o 4 1 34 1760.41 1771.37 85.34 o 5 1 34 17.47 90.93 55.59 o 6 1 34 48.11 120.05 58.63 o 0 2 34 6301.80 6632.25 438.13 o 1 2 34 4162.02 4350.54 135.63 o 2 2 34 2071.01 2021.93 89.62 o 3 2 34 1575.95 1763.01 81.74 o 4 2 34 532.40 324.50 61.83 o 5 2 34 5273.66 5036.87 140.75 o 6 2 34 2997.39 2584.89 91.06 o 1 3 34 1161.55 976.47 63.98 o 2 3 34 3258.16 3192.42 107.55 o 3 3 34 26.40 48.32 49.20 o 4 3 34 6636.05 7050.74 173.99 o 5 3 34 1269.63 1241.42 80.87 o 0 4 34 525.19 635.88 118.52 o 1 4 34 1333.58 1309.72 72.73 o 2 4 34 377.26 488.07 57.10 o 3 4 34 2695.02 2365.91 109.72 o 4 4 34 89.10 106.14 50.05 o 5 4 34 1639.84 1640.49 84.28 o 1 5 34 745.62 919.43 79.07 o 2 5 34 6793.57 6246.74 194.40 o 3 5 34 269.17 219.71 56.83 o 4 5 34 7967.43 7312.45 223.56 o 5 5 34 945.89 874.07 70.77 o 0 6 34 142.21 233.89 92.21 o 1 6 34 61.12 101.80 63.94 o 2 6 34 555.67 452.98 78.60 o 3 6 34 205.05 241.00 104.39 o 4 6 34 188.19 99.47 66.74 o 1 7 34 951.96 775.98 83.15 o 2 7 34 2832.54 3217.14 134.38 o 3 7 34 0.92 64.06 70.58 o 0 8 34 3293.61 2646.48 201.79 o 1 8 34 1035.62 1041.87 138.14 o 2 8 34 5158.27 5115.73 180.87 o 1 1 35 4534.57 4632.44 160.63 o 2 1 35 825.96 972.09 71.91 o 3 1 35 1005.21 1150.45 69.04 o 4 1 35 62.20 101.76 56.70 o 5 1 35 1419.56 1447.50 90.04 o 0 2 35 81.83 81.63 113.21 o 1 2 35 2661.89 2720.24 97.02 o 2 2 35 1017.94 945.83 64.98 o 3 2 35 5220.73 5478.79 168.65 o 4 2 35 512.53 471.74 65.97 o 5 2 35 830.36 796.29 71.76 o 1 3 35 925.15 1045.20 88.50 o 2 3 35 4.77 190.03 62.10 o 3 3 35 348.05 326.75 55.49 o 4 3 35 387.51 372.70 61.45 o 5 3 35 3.08 33.46 55.80 o 0 4 35 100.08 45.79 86.66 o 1 4 35 5048.71 5034.94 193.97 o 2 4 35 4092.98 3874.10 122.10 o 3 4 35 16397.61 16222.80 386.52 o 4 4 35 1370.45 1231.59 76.66 o 1 5 35 0.01 72.76 65.75 o 2 5 35 370.94 388.91 73.60 o 3 5 35 208.81 146.96 56.50 o 4 5 35 83.12 142.68 60.91 o 0 6 35 92.92 50.00 83.73 o 1 6 35 2773.80 2939.18 117.88 o 2 6 35 3155.11 3100.21 121.21 o 3 6 35 11558.74 11769.81 336.80 o 1 7 35 4480.31 4584.50 155.57 o 2 7 35 393.43 457.61 68.04 o 0 0 36 4446.18 3787.12 338.89 o 1 0 36 1419.35 1498.98 135.62 o 2 0 36 139.04 246.78 84.80 o 3 0 36 14198.58 13895.07 457.89 o 4 0 36 3294.32 3461.51 181.20 o 1 1 36 234.61 345.52 60.99 o 2 1 36 1375.22 1321.50 71.11 o 3 1 36 4.02 96.06 58.69 o 4 1 36 9.73 -36.76 58.70 o 0 2 36 2291.52 2031.89 144.23 o 1 2 36 471.87 389.26 59.95 o 2 2 36 106.56 193.14 53.57 o 3 2 36 16497.63 17248.09 409.83 o 4 2 36 627.47 856.87 72.46 o 1 3 36 2854.04 2859.35 108.04 o 2 3 36 3248.58 3136.01 133.87 o 3 3 36 178.21 133.72 59.95 o 4 3 36 1152.57 980.17 90.51 o 0 4 36 561.78 505.81 108.56 o 1 4 36 0.92 77.43 61.82 o 2 4 36 320.53 398.45 82.19 o 3 4 36 5829.60 5324.29 156.39 o 1 5 36 6334.47 6500.22 189.17 o 2 5 36 1965.11 1722.05 106.88 o 3 5 36 0.55 -56.78 66.99 o 0 6 36 872.49 759.78 107.07 o 1 6 36 18.78 5.98 65.85 o 2 6 36 147.30 287.96 70.86 o 1 1 37 333.49 349.17 66.51 o 2 1 37 5331.58 5096.51 216.41 o 3 1 37 4.65 5.12 60.77 o 0 2 37 3136.48 2856.38 194.45 o 1 2 37 1.87 89.21 58.03 o 2 2 37 482.49 808.17 83.52 o 3 2 37 2711.97 2644.18 115.26 o 1 3 37 370.67 290.87 67.08 o 2 3 37 7066.74 7160.79 221.28 o 3 3 37 0.02 36.87 61.79 o 0 4 37 8248.28 7834.68 316.92 o 1 4 37 126.40 187.98 68.74 o 2 4 37 1426.31 1567.18 96.63 o 1 5 37 40.78 53.96 66.24 o 0 0 38 596.93 633.75 144.51 o 1 0 38 1419.40 1615.23 124.76 o 2 0 38 4877.64 4816.17 204.32 o 1 1 38 274.44 275.46 67.27 o 2 1 38 804.17 824.69 65.31 o 0 2 38 360.66 607.91 102.95 o 1 2 38 485.25 341.88 76.80 o