#------------------------------------------------------------------------------ #$Date: 2010-10-08 09:13:40 +0300 (Fri, 08 Oct 2010) $ #$Revision: 1452 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226091.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226091_Fobs loop_ _publ_author_name 'Ovchynnikov, Vladimir A.' _publ_section_title ; N-[Bis(benzylamino)phosphoryl]-2,2,2-trichloroacetamide ; _journal_coeditor_code DN2554 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1425 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.320 _cell_angle_beta 67.762 _cell_angle_gamma 86.469 _cell_length_a 9.1165 _cell_length_b 10.3586 _cell_length_c 11.7713 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file dn2554Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c300 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4597.50 4712.47 129.51 o 2 0 0 9.56 10.92 0.42 o 3 0 0 1321.38 1301.19 35.90 o 4 0 0 0.31 2.79 0.31 o 5 0 0 13.70 18.20 0.80 o 6 0 0 1027.69 1097.67 30.49 o 7 0 0 5.48 5.60 0.64 o 8 0 0 24.16 22.29 1.07 o 9 0 0 217.79 214.27 6.41 o -9 1 0 309.25 299.30 8.75 o -8 1 0 194.26 195.11 5.85 o -7 1 0 228.38 200.03 5.87 o -6 1 0 543.72 514.39 14.47 o -5 1 0 319.89 291.97 8.30 o -4 1 0 934.65 887.43 17.38 o -3 1 0 122.92 107.04 2.20 o -2 1 0 2421.41 2403.95 66.15 o -1 1 0 189.58 218.26 18.56 o 0 1 0 45.00 58.45 1.20 o 1 1 0 16.23 22.83 0.51 o 2 1 0 2201.93 2389.60 48.05 o 3 1 0 61.91 41.87 1.31 o 4 1 0 70.86 75.46 2.28 o 5 1 0 30.74 28.45 1.07 o 6 1 0 87.78 77.56 2.46 o 7 1 0 97.43 98.98 3.10 o 8 1 0 25.02 28.87 2.53 o 9 1 0 90.94 94.03 3.17 o -9 2 0 86.45 87.16 2.96 o -8 2 0 19.02 19.12 1.02 o -7 2 0 178.78 152.21 4.57 o -6 2 0 301.30 291.94 8.39 o -5 2 0 51.86 56.42 1.44 o -4 2 0 1161.13 1077.13 21.09 o -3 2 0 2469.49 2341.15 45.60 o -2 2 0 1903.42 2018.46 72.38 o -1 2 0 25.40 19.13 0.73 o 0 2 0 2404.08 2259.24 45.41 o 1 2 0 227.78 196.27 4.01 o 2 2 0 4591.36 4533.71 105.83 o 3 2 0 235.35 216.90 4.48 o 4 2 0 899.87 968.53 27.16 o 5 2 0 0.07 0.86 0.23 o 6 2 0 794.07 758.91 15.49 o 7 2 0 0.18 0.45 0.31 o 8 2 0 12.28 12.19 1.23 o 9 2 0 0.23 0.00 0.56 o -9 3 0 93.03 95.22 3.20 o -8 3 0 129.74 132.90 4.13 o -7 3 0 10.17 7.67 0.67 o -6 3 0 82.33 81.39 1.85 o -5 3 0 98.40 114.13 2.44 o -4 3 0 608.05 663.81 13.08 o -3 3 0 260.47 268.13 5.54 o -2 3 0 147.04 182.67 10.23 o -1 3 0 1087.17 1051.47 21.20 o 0 3 0 87.23 92.37 1.94 o 1 3 0 599.51 602.03 12.18 o 2 3 0 689.92 690.51 13.98 o 3 3 0 4.46 6.00 0.31 o 4 3 0 528.01 573.41 11.69 o 5 3 0 0.02 0.86 0.32 o 6 3 0 22.40 23.48 0.79 o 7 3 0 119.86 114.40 2.61 o 8 3 0 9.15 9.77 0.62 o 9 3 0 2.60 3.13 0.79 o -8 4 0 1.21 0.35 0.49 o -7 4 0 86.54 82.23 1.92 o -6 4 0 0.50 0.43 0.27 o -5 4 0 277.66 268.80 5.46 o -4 4 0 265.26 277.26 5.77 o -3 4 0 490.50 510.63 10.42 o -2 4 0 1701.30 1780.26 35.88 o -1 4 0 225.34 239.95 7.67 o 0 4 0 572.56 620.62 12.58 o 1 4 0 1318.50 1346.55 27.15 o 2 4 0 156.02 177.45 3.70 o 3 4 0 583.82 590.64 12.02 o 4 4 0 24.53 20.92 1.08 o 5 4 0 284.55 301.68 6.31 o 6 4 0 63.70 61.36 1.53 o 7 4 0 776.68 769.41 15.77 o 8 4 0 9.97 8.39 1.00 o 9 4 0 1.64 2.00 0.81 o -8 5 0 60.71 58.18 1.51 o -7 5 0 35.24 36.94 1.07 o -6 5 0 625.71 548.70 10.93 o -5 5 0 10.01 12.37 0.55 o -4 5 0 728.87 688.30 22.69 o -3 5 0 89.06 92.57 2.75 o -2 5 0 101.04 130.18 2.80 o -1 5 0 6.62 10.19 0.93 o 0 5 0 97.46 127.95 3.29 o 1 5 0 1567.35 1707.79 34.43 o 2 5 0 577.58 637.01 12.96 o 3 5 0 1233.13 1202.54 24.34 o 4 5 0 613.70 634.52 12.97 o 5 5 0 396.14 393.36 8.16 o 6 5 0 246.93 243.46 12.83 o 7 5 0 37.60 42.68 1.96 o 8 5 0 90.28 95.80 3.55 o -8 6 0 238.61 234.91 5.16 o -7 6 0 3.43 4.05 0.84 o -6 6 0 4.25 4.97 0.45 o -5 6 0 70.21 60.64 4.10 o -4 6 0 197.79 211.22 6.63 o -3 6 0 665.46 629.29 12.86 o -2 6 0 2473.79 2429.50 48.98 o -1 6 0 1734.30 1734.77 88.49 o 0 6 0 4.55 3.39 0.38 o 1 6 0 394.85 393.21 8.08 o 2 6 0 397.20 409.46 8.42 o 3 6 0 378.20 375.76 7.77 o 4 6 0 209.55 194.54 4.16 o 5 6 0 68.67 80.98 2.98 o 6 6 0 146.55 162.03 5.39 o 7 6 0 132.05 137.12 4.72 o 8 6 0 12.35 10.59 1.21 o -8 7 0 58.24 72.84 1.87 o -7 7 0 23.25 20.52 0.80 o -6 7 0 25.59 17.94 0.71 o -5 7 0 13.09 11.99 0.59 o -4 7 0 246.73 259.42 5.49 o -3 7 0 276.18 289.65 6.08 o -2 7 0 658.14 657.70 13.45 o -1 7 0 14.06 18.08 0.63 o 0 7 0 729.18 670.59 13.68 o 1 7 0 78.51 80.32 1.84 o 2 7 0 3.93 5.49 0.38 o 3 7 0 75.15 81.26 4.02 o 4 7 0 1.97 6.84 0.74 o 5 7 0 193.52 228.02 7.29 o 6 7 0 444.33 470.85 14.48 o 7 7 0 10.76 15.23 1.24 o -7 8 0 6.71 6.05 0.57 o -6 8 0 95.12 98.03 4.63 o -5 8 0 350.67 369.52 7.77 o -4 8 0 47.28 47.71 1.31 o -3 8 0 694.24 704.24 19.77 o -2 8 0 1195.01 1171.02 23.79 o -1 8 0 175.03 166.07 3.60 o 0 8 0 157.99 150.57 3.29 o 1 8 0 123.47 130.31 2.89 o 2 8 0 345.82 332.60 10.24 o 3 8 0 90.41 79.40 2.86 o 4 8 0 32.36 43.15 1.83 o 5 8 0 12.50 8.40 1.01 o 6 8 0 57.68 60.17 2.55 o -6 9 0 125.06 127.56 3.76 o -5 9 0 12.57 13.02 0.73 o -4 9 0 23.46 26.19 0.92 o -3 9 0 259.36 263.55 6.59 o -2 9 0 249.09 261.17 6.94 o -1 9 0 3.85 2.07 0.72 o 0 9 0 149.85 138.12 3.08 o 1 9 0 90.00 80.76 2.88 o 2 9 0 39.34 40.42 1.77 o 3 9 0 102.75 111.27 3.83 o 4 9 0 0.41 1.68 0.75 o 5 9 0 8.79 13.92 1.20 o -5 10 0 0.00 0.02 0.68 o -4 10 0 21.95 20.22 0.86 o -3 10 0 170.92 175.71 7.26 o -2 10 0 2.10 5.18 0.53 o -1 10 0 245.31 232.60 7.40 o 0 10 0 10.61 11.72 1.02 o 1 10 0 4.14 0.92 0.61 o 2 10 0 5.68 1.63 0.75 o 3 10 0 2.12 0.00 0.61 o 4 10 0 31.40 23.70 1.46 o -3 11 0 30.11 28.34 1.61 o -2 11 0 3.97 1.86 0.83 o -1 11 0 155.08 157.52 5.31 o 0 11 0 199.07 201.17 6.54 o 1 11 0 22.54 16.61 1.22 o 0 -11 1 102.45 98.62 3.62 o 1 -11 1 10.42 20.37 1.41 o 2 -11 1 208.89 226.39 7.40 o -3 -10 1 120.32 122.93 4.37 o -2 -10 1 18.40 22.67 1.53 o -1 -10 1 28.00 25.09 1.43 o 0 -10 1 8.18 11.83 1.00 o 1 -10 1 150.17 152.80 5.12 o 2 -10 1 281.28 315.11 9.90 o 3 -10 1 100.14 107.52 3.84 o 4 -10 1 11.51 15.54 1.24 o 5 -10 1 11.71 12.31 1.09 o -4 -9 1 7.02 4.92 0.90 o -3 -9 1 22.89 21.23 1.27 o -2 -9 1 24.35 23.75 1.33 o -1 -9 1 1.01 0.00 0.52 o 0 -9 1 165.44 156.64 5.17 o 1 -9 1 90.90 87.19 3.08 o 2 -9 1 17.35 17.00 1.16 o 3 -9 1 28.78 30.03 0.99 o 4 -9 1 200.84 192.56 10.82 o 5 -9 1 124.28 121.12 15.43 o 6 -9 1 18.89 21.70 0.72 o -5 -8 1 113.09 131.69 4.60 o -4 -8 1 184.45 170.20 5.63 o -3 -8 1 0.06 0.51 0.52 o -2 -8 1 90.65 82.51 2.96 o -1 -8 1 948.79 937.08 28.07 o 0 -8 1 14.16 11.00 0.86 o 1 -8 1 46.90 47.36 1.25 o 2 -8 1 143.37 145.18 3.49 o 3 -8 1 8.92 8.98 0.53 o 4 -8 1 107.86 113.43 2.62 o 5 -8 1 6.48 6.01 1.53 o 6 -8 1 37.00 33.74 2.35 o 7 -8 1 65.34 65.19 1.67 o -6 -7 1 3.14 3.50 0.84 o -5 -7 1 9.38 9.22 0.96 o -4 -7 1 67.08 52.52 2.10 o -3 -7 1 60.40 62.90 2.37 o -2 -7 1 6.20 9.17 0.78 o -1 -7 1 199.62 208.36 4.42 o 0 -7 1 62.85 68.73 1.61 o 1 -7 1 544.37 524.43 15.68 o 2 -7 1 809.00 781.64 15.94 o 3 -7 1 4.61 5.00 1.01 o 4 -7 1 96.35 94.75 3.44 o 5 -7 1 60.17 60.08 1.96 o 6 -7 1 0.46 0.00 0.30 o 7 -7 1 7.33 11.65 0.62 o 8 -7 1 10.92 6.02 0.82 o -7 -6 1 2.89 2.91 0.89 o -5 -6 1 59.27 57.66 2.31 o -4 -6 1 249.46 230.44 7.27 o -3 -6 1 114.84 123.01 4.06 o -2 -6 1 98.08 106.49 2.35 o -1 -6 1 376.48 382.36 7.87 o 0 -6 1 352.79 334.91 6.92 o 1 -6 1 14.88 16.52 0.75 o 2 -6 1 65.11 60.50 1.51 o 3 -6 1 1764.80 1796.74 36.30 o 4 -6 1 102.94 106.81 2.42 o 5 -6 1 85.33 85.76 2.87 o 6 -6 1 74.15 73.97 1.77 o 7 -6 1 1.32 0.31 0.88 o 8 -6 1 0.51 0.38 0.34 o 9 -6 1 72.03 76.29 2.82 o -8 -5 1 163.63 134.89 4.66 o -7 -5 1 0.27 0.84 0.76 o -6 -5 1 89.18 95.47 3.42 o -5 -5 1 170.85 185.08 5.96 o -4 -5 1 67.22 69.94 1.67 o -3 -5 1 0.02 0.28 0.51 o -2 -5 1 812.40 824.97 22.15 o -1 -5 1 196.02 240.54 4.99 o 0 -5 1 1834.05 1926.09 38.82 o 1 -5 1 516.43 519.62 10.59 o 2 -5 1 1636.84 1677.91 51.99 o 3 -5 1 48.37 46.40 1.82 o 4 -5 1 121.43 119.17 4.64 o 5 -5 1 234.43 219.31 3.80 o 6 -5 1 891.86 826.74 16.35 o 7 -5 1 87.37 81.96 1.92 o 8 -5 1 18.93 19.64 0.77 o 9 -5 1 256.23 255.92 7.64 o -8 -4 1 15.88 17.93 1.35 o -7 -4 1 499.31 525.45 16.08 o -6 -4 1 24.23 23.03 1.33 o -5 -4 1 73.85 66.93 4.34 o -4 -4 1 1133.61 1081.02 21.91 o -3 -4 1 1211.47 1219.90 24.67 o -2 -4 1 517.52 577.17 11.74 o -1 -4 1 106.14 98.09 5.51 o 0 -4 1 365.69 303.54 6.22 o 1 -4 1 1096.27 1008.46 20.38 o 2 -4 1 1109.20 1039.81 24.25 o 3 -4 1 1222.57 1204.91 62.62 o 4 -4 1 436.40 439.35 7.30 o 5 -4 1 11.12 6.76 0.37 o 6 -4 1 196.42 192.83 4.02 o 7 -4 1 21.47 18.29 0.69 o 8 -4 1 1.74 1.41 0.55 o 9 -4 1 147.11 143.07 4.53 o -8 -3 1 42.76 54.93 2.31 o -7 -3 1 121.05 111.17 5.38 o -6 -3 1 71.36 63.40 1.57 o -5 -3 1 951.50 898.78 18.28 o -4 -3 1 37.01 38.32 0.97 o 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1 0.03 0.00 0.32 o -7 -1 1 86.14 82.75 1.98 o -6 -1 1 45.37 47.51 1.23 o -5 -1 1 99.46 78.15 2.39 o -4 -1 1 145.36 168.74 4.84 o -3 -1 1 3290.76 3242.99 65.23 o -2 -1 1 169.36 187.73 3.86 o -1 -1 1 13010.36 13583.16 399.58 o 0 -1 1 856.55 854.78 17.19 o 1 -1 1 163.05 207.92 3.46 o 2 -1 1 193.11 196.05 3.24 o 3 -1 1 259.02 232.31 6.44 o 4 -1 1 386.37 427.09 11.97 o 5 -1 1 1566.20 1496.74 41.37 o 6 -1 1 174.26 171.49 5.05 o 7 -1 1 466.15 435.65 12.36 o 9 -1 1 38.04 38.54 1.68 o 10 -1 1 29.78 28.01 1.45 o -9 0 1 7.65 10.46 0.68 o -8 0 1 12.35 11.23 0.74 o -7 0 1 141.36 135.39 4.10 o -6 0 1 155.82 145.19 4.30 o -5 0 1 12.11 9.23 0.53 o -4 0 1 1379.82 1494.75 41.27 o -3 0 1 350.72 382.30 10.65 o -2 0 1 3388.25 3276.78 63.71 o -1 0 1 229.34 233.98 3.83 o 0 0 1 475.87 501.22 10.08 o 1 0 1 1734.87 1864.24 32.20 o 2 0 1 12452.11 10710.62 294.30 o 3 0 1 2.62 2.99 0.28 o 4 0 1 1.76 5.09 0.37 o 5 0 1 681.07 627.09 17.46 o 6 0 1 137.74 133.00 3.98 o 7 0 1 23.35 24.82 1.11 o 8 0 1 87.43 78.66 2.58 o 9 0 1 18.82 17.71 1.06 o 10 0 1 0.79 0.96 0.71 o -9 1 1 3.24 1.84 0.63 o -8 1 1 13.25 14.34 0.96 o -7 1 1 115.11 103.27 3.22 o -6 1 1 44.66 43.36 1.56 o -5 1 1 3.56 4.71 0.47 o -4 1 1 205.11 226.26 4.55 o -3 1 1 7.63 7.76 0.29 o -2 1 1 12064.39 11372.34 220.96 o -1 1 1 865.27 987.78 27.22 o 0 1 1 134.43 165.06 2.67 o 1 1 1 4.90 5.35 0.23 o 2 1 1 403.28 380.76 10.56 o 3 1 1 1747.80 1762.45 48.56 o 4 1 1 2036.71 1990.31 54.88 o 5 1 1 89.33 87.76 2.68 o 6 1 1 314.10 304.00 8.67 o 7 1 1 894.76 854.95 23.86 o 8 1 1 75.67 72.61 2.47 o 9 1 1 250.19 285.18 8.39 o 10 1 1 24.81 26.56 1.78 o -9 2 1 13.70 9.99 0.90 o -8 2 1 53.70 49.32 1.85 o -7 2 1 75.43 68.57 2.29 o -6 2 1 257.36 243.67 7.05 o -5 2 1 1799.07 1672.30 32.69 o -4 2 1 164.40 165.31 3.38 o -3 2 1 5.90 1.23 0.24 o -2 2 1 13526.72 15068.26 414.07 o -1 2 1 113.29 112.35 1.85 o 1 2 1 4283.56 4224.34 84.86 o 2 2 1 3369.98 3282.75 65.97 o 3 2 1 773.41 779.47 15.76 o 4 2 1 1157.80 1115.38 22.55 o 5 2 1 335.79 335.99 6.94 o 6 2 1 23.01 29.82 0.87 o 7 2 1 288.12 290.64 6.13 o 8 2 1 0.01 0.00 0.81 o 9 2 1 0.40 0.00 0.41 o 10 2 1 3.88 2.82 0.71 o -9 3 1 8.53 5.74 0.82 o -8 3 1 12.09 11.62 0.86 o -7 3 1 4.73 5.07 0.62 o -6 3 1 44.64 45.59 1.17 o -5 3 1 3.08 2.50 0.28 o -4 3 1 2162.62 2157.25 42.10 o -3 3 1 3088.13 3177.15 87.50 o -2 3 1 1538.84 1604.18 35.68 o -1 3 1 77.06 67.51 1.19 o 0 3 1 1031.77 980.35 19.76 o 1 3 1 715.39 655.27 13.23 o 2 3 1 126.49 94.09 2.00 o 3 3 1 695.39 610.41 12.39 o 4 3 1 622.34 616.72 16.03 o 5 3 1 309.56 312.15 6.48 o 6 3 1 880.04 855.14 21.52 o 7 3 1 286.13 269.63 10.83 o 8 3 1 0.06 0.15 0.49 o 9 3 1 99.68 93.84 4.43 o -9 4 1 313.69 326.42 9.53 o -8 4 1 125.69 134.61 4.25 o -7 4 1 28.99 33.45 0.99 o -6 4 1 337.00 302.10 6.16 o -5 4 1 471.75 411.05 8.23 o -4 4 1 24.00 21.76 0.93 o -3 4 1 352.22 370.96 10.16 o -2 4 1 5.27 8.56 0.51 o -1 4 1 439.09 521.50 13.51 o 0 4 1 4553.59 4680.50 94.07 o 1 4 1 5272.60 5528.75 111.10 o 2 4 1 89.40 110.27 2.35 o 3 4 1 2.67 2.05 0.27 o 4 4 1 64.32 64.78 2.61 o 5 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39.50 1.94 o 0 6 12 5.88 2.26 0.80 o 1 6 12 38.37 32.69 1.59 o 2 6 12 413.03 414.25 11.76 o 3 6 12 94.48 89.26 3.06 o 4 6 12 24.88 19.49 0.92 o 5 6 12 105.34 110.24 7.84 o 6 6 12 138.88 109.02 2.56 o 7 6 12 268.36 248.73 5.25 o 8 6 12 280.00 290.81 8.63 o -1 7 12 53.13 47.49 2.14 o 0 7 12 51.00 56.12 2.25 o 1 7 12 184.93 177.27 5.44 o 2 7 12 55.92 49.98 1.74 o 3 7 12 25.59 24.95 0.93 o 4 7 12 179.30 173.50 3.76 o 5 7 12 23.39 30.01 1.04 o 6 7 12 14.63 15.08 1.18 o 7 7 12 256.01 255.93 7.68 o 0 8 12 12.70 11.75 1.09 o 1 8 12 120.65 119.00 4.58 o 2 8 12 31.08 31.11 1.06 o 3 8 12 33.05 34.04 2.44 o 4 8 12 172.81 184.80 4.02 o 5 8 12 178.27 182.02 3.97 o 6 8 12 0.19 0.00 0.66 o 1 9 12 165.69 173.57 5.41 o 2 9 12 0.19 0.00 0.52 o 3 9 12 6.17 6.87 0.65 o 4 9 12 116.39 114.56 3.55 o 5 9 12 31.53 34.71 1.69 o 4 0 13 13.48 15.85 1.27 o 2 1 13 0.96 0.11 0.75 o 3 1 13 12.31 13.12 1.16 o 4 1 13 89.84 95.12 3.31 o 5 1 13 12.58 19.05 1.29 o 6 1 13 3.18 4.04 0.88 o 1 2 13 0.89 0.42 0.89 o 2 2 13 194.45 201.95 6.22 o 3 2 13 142.11 153.71 4.87 o 4 2 13 162.45 169.84 5.29 o 5 2 13 75.13 90.23 3.22 o 6 2 13 44.81 45.01 2.01 o 7 2 13 17.38 13.31 1.25 o 2 3 13 13.08 14.92 1.25 o 3 3 13 40.85 34.98 1.76 o 4 3 13 210.05 233.04 6.99 o 6 3 13 94.06 88.50 3.12 o 7 3 13 449.22 456.90 12.99 o 1 4 13 112.63 114.30 3.88 o 2 4 13 55.19 53.95 2.29 o 3 4 13 29.69 27.98 1.57 o 4 4 13 112.90 129.48 4.31 o 5 4 13 278.81 279.38 8.20 o 1 5 13 390.50 420.20 12.06 o 2 5 13 74.66 86.42 3.09 o 3 5 13 24.16 35.05 1.72 o 4 5 13 82.88 85.88 3.05 o 5 5 13 0.95 0.00 0.67 o 6 5 13 1.04 1.39 0.82 o 7 5 13 43.65 41.38 2.01 o 1 6 13 8.86 14.07 1.19 o 2 6 13 24.98 28.02 1.58 o 3 6 13 2.71 1.99 0.79 o 4 6 13 19.12 18.90 1.33 o 5 6 13 17.97 24.94 1.47 o 6 6 13 2.14 2.83 1.04 o 7 6 13 5.38 4.51 0.67 o 1 7 13 5.03 1.80 0.86 o 2 7 13 38.57 33.03 1.71 o 3 7 13 4.16 1.76 0.78 o 4 7 13 0.47 0.27 0.74 o 5 7 13 164.70 144.55 3.26 o 6 7 13 16.66 21.72 2.27 o 2 8 13 36.07 36.35 1.83 o 3 8 13 186.26 175.80 3.86 o 4 8 13 0.38 0.22 0.48 o 5 8 13 0.17 0.15 0.52 o