#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:38:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181182 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/61/2226107.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226107_Fobs loop_ _publ_author_name 'Manjunath, H. R.' 'Shreenivasa, M. T.' 'Mahendra, M.' 'Mohan Kumar, T. M.' 'Kumara Swamy, B. E.' 'Sridhar, M. A.' _publ_section_title ; 4-Nitro-2-phenoxyaniline ; _journal_coeditor_code FJ2288 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1255 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.406 _cell_angle_gamma 90.000 _cell_length_a 10.4100 _cell_length_b 15.6570 _cell_length_c 6.9600 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file fj2288Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aniline' _shelx_refln_list_code 4 _shelx_f_calc_maximum 70.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 395.76 342.66 7.30 o 4 0 0 321.12 313.57 7.33 o 5 0 0 985.32 942.05 15.35 o 6 0 0 372.92 404.90 7.55 o 7 0 0 382.06 404.51 6.58 o 9 0 0 8.35 7.20 0.67 o 10 0 0 7.13 5.51 1.08 o 11 0 0 3.41 4.83 0.85 o 12 0 0 0.28 -1.04 1.04 o 1 1 0 111.39 0.02 0.07 o 2 1 0 487.20 376.40 11.96 o 3 1 0 223.65 206.50 3.62 o 4 1 0 307.10 286.82 4.39 o 5 1 0 35.21 39.19 1.11 o 6 1 0 3.41 1.74 0.32 o 7 1 0 28.31 31.99 0.77 o 8 1 0 0.37 0.61 0.37 o 9 1 0 1.99 1.56 0.51 o 10 1 0 13.12 14.23 1.56 o 11 1 0 2.89 3.49 0.46 o 12 1 0 7.75 8.66 2.23 o 1 2 0 662.21 618.22 10.52 o 2 2 0 1853.09 1841.14 49.94 o 3 2 0 279.79 284.00 4.29 o 4 2 0 201.83 189.63 3.03 o 5 2 0 619.45 678.24 9.29 o 6 2 0 383.15 389.04 5.90 o 7 2 0 2.85 3.71 0.43 o 8 2 0 9.65 12.12 1.23 o 9 2 0 4.03 2.53 0.71 o 10 2 0 9.26 10.24 1.62 o 11 2 0 0.53 1.69 0.57 o 1 3 0 34.46 41.01 2.70 o 2 3 0 1209.77 1217.42 26.21 o 3 3 0 10.14 7.18 0.31 o 4 3 0 62.40 76.21 4.29 o 5 3 0 2.70 3.39 0.59 o 6 3 0 154.90 168.39 4.49 o 7 3 0 42.56 47.50 1.39 o 8 3 0 2.91 2.93 0.36 o 9 3 0 20.55 21.60 1.13 o 10 3 0 0.52 0.69 0.82 o 11 3 0 2.79 0.93 0.64 o 0 4 0 22.64 24.10 0.57 o 1 4 0 3221.17 3300.71 71.29 o 2 4 0 660.61 614.51 46.26 o 3 4 0 694.81 683.17 20.27 o 4 4 0 28.81 26.33 0.62 o 5 4 0 462.31 466.92 8.82 o 6 4 0 12.39 15.25 0.57 o 7 4 0 8.19 6.79 0.43 o 8 4 0 13.23 14.14 0.59 o 9 4 0 1.53 1.31 0.38 o 10 4 0 38.48 34.81 2.36 o 11 4 0 9.89 9.91 2.41 o 1 5 0 465.10 426.03 11.22 o 2 5 0 323.60 308.38 13.73 o 3 5 0 95.91 117.32 2.24 o 4 5 0 45.54 50.48 0.82 o 5 5 0 3.93 2.36 0.24 o 6 5 0 3.07 3.01 0.43 o 7 5 0 202.95 239.62 4.77 o 9 5 0 5.74 8.04 2.70 o 10 5 0 50.28 43.23 2.06 o 11 5 0 13.10 11.82 1.10 o 0 6 0 11.38 17.98 0.47 o 1 6 0 737.57 723.32 27.60 o 2 6 0 124.05 130.09 4.10 o 3 6 0 446.98 464.93 7.57 o 4 6 0 6.15 7.54 1.19 o 5 6 0 36.23 31.59 1.89 o 6 6 0 5.46 5.53 0.49 o 7 6 0 6.87 9.61 3.17 o 8 6 0 1.98 3.24 0.53 o 9 6 0 4.50 5.80 0.55 o 11 6 0 4.15 4.02 1.35 o 1 7 0 290.18 271.72 4.15 o 2 7 0 919.90 972.11 22.19 o 3 7 0 736.89 738.87 20.13 o 4 7 0 69.81 65.64 3.50 o 5 7 0 160.11 183.54 4.56 o 6 7 0 7.27 9.28 0.43 o 7 7 0 0.23 1.14 0.56 o 8 7 0 2.98 4.70 0.54 o 9 7 0 54.07 62.66 1.67 o 11 7 0 2.19 2.90 1.28 o 0 8 0 105.44 118.97 3.57 o 1 8 0 17.69 23.53 0.70 o 3 8 0 3.41 3.27 0.84 o 4 8 0 280.96 316.64 11.13 o 5 8 0 62.13 58.28 5.60 o 6 8 0 2.17 0.44 0.77 o 8 8 0 26.69 25.57 1.22 o 9 8 0 14.62 15.46 2.80 o 10 8 0 4.90 4.36 1.68 o 1 9 0 0.02 0.37 0.17 o 2 9 0 3.57 2.71 0.24 o 3 9 0 14.08 12.38 0.34 o 4 9 0 3.89 5.92 0.44 o 5 9 0 5.49 4.56 0.73 o 6 9 0 151.02 148.05 2.94 o 7 9 0 40.49 34.37 1.69 o 9 9 0 3.84 3.49 0.51 o 10 9 0 0.02 0.74 0.38 o 0 10 0 101.33 95.87 3.49 o 1 10 0 28.20 26.71 0.76 o 2 10 0 0.40 0.15 0.24 o 3 10 0 84.30 84.59 2.53 o 4 10 0 4.74 8.15 0.93 o 5 10 0 17.84 18.48 0.79 o 6 10 0 2.80 2.44 0.54 o 7 10 0 117.51 125.88 2.63 o 8 10 0 19.97 25.88 4.65 o 9 10 0 4.77 5.55 0.47 o 10 10 0 5.69 6.21 0.78 o 1 11 0 24.12 25.18 1.87 o 2 11 0 16.50 16.88 0.45 o 3 11 0 52.42 55.24 1.11 o 4 11 0 7.93 7.86 0.81 o 5 11 0 14.22 19.05 0.59 o 6 11 0 27.18 22.35 2.70 o 7 11 0 1.05 2.04 0.42 o 8 11 0 10.50 8.30 0.80 o 9 11 0 8.29 8.31 0.62 o 0 12 0 256.25 262.83 6.71 o 1 12 0 823.14 845.19 16.78 o 3 12 0 0.79 0.74 0.52 o 4 12 0 58.02 55.66 2.20 o 6 12 0 0.79 0.96 0.27 o 7 12 0 44.29 37.70 2.08 o 8 12 0 3.65 2.90 0.91 o 9 12 0 14.19 11.13 1.11 o 1 13 0 190.24 190.38 5.18 o 2 13 0 9.31 7.97 0.79 o 3 13 0 23.50 23.88 1.25 o 4 13 0 6.98 3.87 0.67 o 5 13 0 21.11 16.95 0.56 o 6 13 0 9.70 8.58 0.69 o 7 13 0 5.73 3.10 0.42 o 0 14 0 31.57 30.80 0.85 o 1 14 0 43.33 44.07 1.23 o 2 14 0 17.17 17.11 1.03 o 3 14 0 65.13 62.66 2.13 o 4 14 0 11.22 9.68 0.39 o 5 14 0 0.37 1.38 0.41 o 6 14 0 0.23 0.04 0.15 o 7 14 0 2.15 0.70 0.52 o 1 15 0 4.88 3.44 0.29 o 2 15 0 8.29 6.77 0.60 o 3 15 0 39.24 35.68 1.21 o 4 15 0 27.49 19.42 1.96 o 5 15 0 4.03 2.89 0.51 o 6 15 0 0.16 0.13 0.33 o 7 15 0 0.00 1.33 0.52 o 0 16 0 9.43 10.95 0.64 o 1 16 0 10.90 10.04 0.78 o 2 16 0 0.89 1.69 0.41 o 3 16 0 0.02 -0.16 0.29 o 4 16 0 11.98 8.10 1.26 o 5 16 0 0.84 2.04 0.63 o 6 16 0 0.84 0.90 0.62 o 1 17 0 0.09 0.19 0.16 o 2 17 0 0.56 -0.09 0.32 o 3 17 0 8.41 6.59 0.52 o 4 17 0 2.79 2.74 0.76 o 1 18 0 0.10 -0.21 0.21 o 2 18 0 1.66 1.06 0.43 o -12 1 1 1.26 0.47 1.57 o -11 1 1 5.47 4.75 1.11 o -10 1 1 6.22 3.92 0.60 o -9 1 1 0.04 1.09 0.42 o -7 1 1 424.08 449.85 18.42 o -6 1 1 7.51 8.54 1.61 o -5 1 1 206.94 195.91 3.98 o -4 1 1 324.14 306.01 7.84 o 1 1 1 1987.13 1878.05 39.60 o 2 1 1 212.29 197.78 2.94 o 3 1 1 196.62 200.90 7.65 o 4 1 1 293.81 301.48 4.77 o 5 1 1 1053.93 1128.08 13.82 o 6 1 1 37.37 40.76 0.99 o 7 1 1 0.77 0.83 0.33 o 8 1 1 1.73 0.88 0.42 o 9 1 1 5.75 6.04 0.49 o 10 1 1 7.07 6.86 0.63 o 11 1 1 2.38 1.83 0.66 o -12 2 1 0.20 0.72 0.97 o -11 2 1 2.68 2.70 1.30 o -10 2 1 1.03 1.13 0.51 o -9 2 1 3.71 4.04 0.62 o -8 2 1 10.46 10.35 0.73 o -7 2 1 51.42 59.03 4.37 o -6 2 1 5.59 5.51 0.68 o -5 2 1 16.85 17.48 1.51 o -4 2 1 500.49 457.22 14.60 o -3 2 1 526.88 461.20 14.06 o -2 2 1 381.26 393.37 9.73 o 0 2 1 24.30 19.27 0.42 o 1 2 1 4990.08 4892.49 159.45 o 2 2 1 95.04 65.73 2.99 o 3 2 1 6.61 5.79 0.40 o 4 2 1 39.36 33.48 0.69 o 5 2 1 285.50 319.62 6.20 o 6 2 1 2.43 2.52 0.33 o 7 2 1 1.42 2.13 0.40 o 8 2 1 0.96 0.88 0.64 o 9 2 1 7.10 6.50 0.87 o 10 2 1 13.08 13.93 1.38 o 11 2 1 0.01 0.46 0.60 o -12 3 1 2.97 4.68 0.82 o -11 3 1 0.12 0.46 0.79 o -10 3 1 17.79 17.45 2.89 o -9 3 1 2.54 2.16 0.60 o -8 3 1 0.07 0.66 1.07 o -7 3 1 0.24 0.07 0.31 o -6 3 1 3.16 3.69 0.57 o -5 3 1 37.53 37.34 1.40 o -4 3 1 454.67 434.66 5.93 o -3 3 1 370.39 329.83 28.51 o -2 3 1 121.69 130.97 3.55 o -1 3 1 623.02 606.15 15.13 o 1 3 1 3533.26 3404.29 103.82 o 3 3 1 191.76 200.80 3.14 o 4 3 1 356.52 344.88 4.66 o 5 3 1 132.27 148.28 2.07 o 6 3 1 120.71 115.02 1.75 o 7 3 1 2.40 2.42 0.63 o 8 3 1 21.13 20.50 0.87 o 9 3 1 6.39 7.14 0.87 o 10 3 1 38.59 38.06 1.07 o 11 3 1 0.00 -0.12 0.50 o -11 4 1 15.05 14.98 1.09 o -9 4 1 34.91 33.63 1.63 o -8 4 1 20.02 24.87 0.96 o -7 4 1 1.77 2.34 0.33 o -6 4 1 55.10 56.01 1.55 o -5 4 1 1.18 1.09 0.30 o -4 4 1 10.97 9.91 0.75 o -2 4 1 1010.38 944.57 60.63 o 0 4 1 4633.06 4185.73 79.30 o 1 4 1 589.68 582.90 9.98 o 2 4 1 1115.00 981.77 18.29 o 4 4 1 30.60 32.78 0.77 o 5 4 1 34.63 33.79 1.09 o 6 4 1 156.85 141.36 2.79 o 7 4 1 44.90 55.86 2.06 o 8 4 1 240.86 273.55 5.20 o 9 4 1 8.70 10.23 0.68 o 10 4 1 11.07 10.66 1.16 o 11 4 1 0.43 0.53 0.61 o -11 5 1 0.97 1.19 1.26 o -10 5 1 71.94 67.29 2.45 o -9 5 1 15.28 15.41 0.95 o -8 5 1 11.47 12.22 0.87 o -7 5 1 5.46 7.78 0.56 o -6 5 1 0.62 -0.25 0.44 o -5 5 1 62.83 58.37 1.10 o -4 5 1 21.43 24.48 1.64 o -3 5 1 1617.91 1514.14 35.56 o -2 5 1 75.38 70.11 4.41 o -1 5 1 0.12 0.30 0.32 o 0 5 1 527.03 491.43 13.37 o 1 5 1 1812.97 1854.15 46.11 o 2 5 1 215.56 233.52 3.39 o 3 5 1 233.50 252.42 5.42 o 4 5 1 158.50 168.49 2.16 o 5 5 1 9.74 10.85 0.46 o 6 5 1 269.60 265.33 12.84 o 7 5 1 14.72 14.47 0.77 o 8 5 1 503.86 584.28 9.37 o 9 5 1 1.55 2.07 1.43 o 10 5 1 2.01 2.03 1.04 o 11 5 1 0.44 0.51 0.40 o -11 6 1 1.62 0.13 0.35 o -10 6 1 4.25 2.62 0.58 o -9 6 1 15.76 18.58 3.45 o -8 6 1 4.35 5.29 0.48 o -7 6 1 2.64 2.46 0.29 o -6 6 1 218.77 239.35 13.91 o -5 6 1 552.36 543.81 13.72 o -4 6 1 525.67 575.52 15.83 o -3 6 1 186.91 160.47 3.29 o -2 6 1 52.00 44.80 3.74 o -1 6 1 309.05 257.71 8.03 o 0 6 1 12.97 7.15 0.57 o 1 6 1 8.77 12.20 0.33 o 2 6 1 920.30 924.93 15.18 o 3 6 1 947.19 992.24 19.95 o 4 6 1 95.93 88.15 2.44 o 5 6 1 14.79 11.63 0.59 o 6 6 1 7.01 6.54 0.86 o 7 6 1 29.90 29.80 0.85 o 8 6 1 71.90 66.58 1.39 o 9 6 1 10.06 9.11 0.99 o 10 6 1 15.73 14.65 0.97 o -11 7 1 0.14 1.08 0.46 o -10 7 1 0.59 0.22 0.37 o -8 7 1 4.52 5.41 0.46 o -7 7 1 22.39 25.68 1.00 o -6 7 1 6.01 5.44 0.80 o -5 7 1 64.93 72.66 1.71 o -4 7 1 45.49 49.80 5.63 o -2 7 1 267.29 267.85 7.87 o -1 7 1 123.79 117.27 2.45 o 0 7 1 926.84 930.78 26.34 o 1 7 1 248.29 274.98 5.58 o 2 7 1 130.58 121.80 1.64 o 3 7 1 224.53 266.16 22.79 o 4 7 1 15.24 17.02 1.44 o 5 7 1 0.44 0.10 0.31 o 6 7 1 49.64 52.69 1.87 o 7 7 1 304.01 303.56 12.40 o 8 7 1 1.22 1.58 0.59 o 9 7 1 12.67 11.34 0.83 o 10 7 1 3.30 3.76 0.55 o -11 8 1 2.34 1.02 0.60 o -9 8 1 116.60 131.81 14.75 o -8 8 1 4.49 5.85 0.88 o -7 8 1 0.74 1.42 0.25 o -6 8 1 8.20 7.80 0.93 o -5 8 1 9.32 7.00 0.62 o -4 8 1 41.54 48.23 1.80 o -3 8 1 294.85 405.67 14.92 o -2 8 1 305.57 306.45 7.41 o -1 8 1 292.74 305.42 5.04 o 0 8 1 131.44 147.06 7.35 o 1 8 1 562.08 577.54 10.17 o 2 8 1 276.85 324.21 5.02 o 3 8 1 5.54 3.82 0.39 o 4 8 1 9.89 9.93 0.54 o 5 8 1 7.41 6.56 0.58 o 6 8 1 11.97 15.34 1.42 o 7 8 1 337.06 356.81 13.08 o 8 8 1 44.44 46.91 4.38 o 9 8 1 4.47 4.83 0.72 o 10 8 1 0.03 0.54 0.41 o -10 9 1 9.46 8.08 0.97 o -9 9 1 46.23 40.82 1.95 o -8 9 1 15.72 15.02 0.71 o -7 9 1 0.25 0.56 0.46 o -6 9 1 5.00 4.64 0.87 o -5 9 1 5.08 5.57 0.96 o -4 9 1 225.95 248.46 4.18 o -3 9 1 1.17 0.41 0.40 o -1 9 1 0.58 0.42 0.16 o 0 9 1 136.74 153.60 3.34 o 1 9 1 566.39 543.59 21.70 o 2 9 1 4.95 3.08 0.46 o 3 9 1 75.68 87.39 8.93 o 4 9 1 5.04 5.27 0.42 o 5 9 1 271.78 302.28 14.29 o 6 9 1 22.58 19.17 0.73 o 7 9 1 11.06 12.51 1.56 o 8 9 1 0.59 2.07 0.63 o 9 9 1 0.21 0.19 0.36 o 10 9 1 8.52 8.74 1.09 o -10 10 1 1.71 0.67 0.42 o -9 10 1 0.62 -0.22 0.88 o -8 10 1 7.79 6.72 0.70 o -7 10 1 0.00 2.04 0.91 o -6 10 1 4.50 3.88 0.60 o -5 10 1 20.71 19.03 0.50 o -4 10 1 45.55 45.18 3.14 o -3 10 1 0.32 0.14 0.53 o -2 10 1 6.98 7.59 0.71 o -1 10 1 2.99 2.03 0.13 o 0 10 1 1.55 1.65 0.19 o 1 10 1 11.21 11.04 0.45 o 2 10 1 96.43 105.36 6.69 o 4 10 1 0.39 1.30 0.56 o 5 10 1 1.55 0.55 0.37 o 6 10 1 31.01 45.13 8.68 o 7 10 1 18.40 23.54 0.86 o 8 10 1 9.60 14.15 4.80 o 9 10 1 0.02 -0.63 0.63 o -9 11 1 0.31 0.16 0.53 o -8 11 1 18.98 24.77 3.36 o -7 11 1 0.04 0.49 0.61 o -6 11 1 29.91 37.18 2.22 o -5 11 1 54.36 54.30 1.56 o -4 11 1 5.40 4.93 0.54 o -3 11 1 80.10 79.97 1.85 o -2 11 1 28.23 25.07 1.78 o 0 11 1 47.34 53.96 1.15 o 1 11 1 1.50 0.79 0.17 o 2 11 1 96.82 86.54 2.92 o 3 11 1 110.17 121.92 4.02 o 4 11 1 76.28 92.79 2.04 o 5 11 1 3.81 4.38 0.36 o 6 11 1 25.29 17.82 0.95 o 7 11 1 21.43 19.71 1.51 o 8 11 1 2.34 3.21 0.51 o 9 11 1 0.89 1.07 0.46 o -9 12 1 1.73 2.42 0.67 o -7 12 1 1.24 1.13 0.55 o -6 12 1 25.42 26.32 1.08 o -5 12 1 3.26 5.46 0.64 o -4 12 1 117.69 128.26 2.76 o -3 12 1 66.84 78.56 3.07 o -2 12 1 63.10 69.79 2.33 o -1 12 1 79.21 70.12 7.74 o 0 12 1 34.87 31.81 0.83 o 1 12 1 67.92 68.71 2.30 o 2 12 1 13.18 12.96 1.20 o 3 12 1 23.88 27.44 1.91 o 4 12 1 0.97 0.37 0.22 o 5 12 1 15.72 13.04 0.49 o 6 12 1 25.29 27.73 0.86 o 7 12 1 6.68 8.08 0.68 o 8 12 1 0.52 0.94 0.85 o -8 13 1 4.60 3.75 1.43 o -7 13 1 3.96 3.04 0.56 o -6 13 1 38.12 35.45 1.83 o -5 13 1 4.67 7.05 0.89 o -4 13 1 44.63 45.25 2.23 o -3 13 1 366.98 384.84 13.69 o -2 13 1 195.43 205.43 11.66 o -1 13 1 5.54 5.40 0.71 o 1 13 1 293.88 292.81 10.46 o 2 13 1 4.90 3.69 0.40 o 3 13 1 1.37 0.69 0.25 o 4 13 1 90.43 78.54 5.58 o 5 13 1 28.29 24.60 0.99 o 6 13 1 0.51 0.95 0.45 o 7 13 1 0.05 0.21 0.32 o 8 13 1 1.83 0.46 0.28 o -8 14 1 0.18 0.34 0.45 o -7 14 1 3.95 2.52 0.84 o -6 14 1 21.94 24.10 1.10 o -5 14 1 3.26 1.58 0.74 o -4 14 1 30.36 23.27 1.35 o -3 14 1 122.18 130.45 4.62 o -2 14 1 60.81 62.40 4.38 o -1 14 1 7.10 6.52 0.74 o 0 14 1 192.91 257.56 6.33 o 1 14 1 190.55 181.37 8.49 o 2 14 1 54.99 42.88 1.73 o 3 14 1 14.08 11.66 0.89 o 4 14 1 13.96 10.00 0.38 o 5 14 1 8.80 7.28 0.50 o 6 14 1 8.11 6.28 0.43 o 7 14 1 0.61 0.09 0.21 o -7 15 1 2.17 1.97 0.59 o -6 15 1 3.20 3.15 0.66 o -5 15 1 1.88 2.53 0.51 o -4 15 1 16.73 16.09 1.20 o -3 15 1 7.39 5.81 0.74 o -2 15 1 10.64 11.72 0.89 o -1 15 1 0.01 1.28 0.76 o 1 15 1 15.73 14.38 2.27 o 2 15 1 38.57 36.90 4.51 o 3 15 1 0.14 0.29 0.17 o 4 15 1 0.28 0.11 0.58 o 5 15 1 4.75 3.49 0.50 o 6 15 1 0.00 0.18 0.23 o -6 16 1 0.00 -0.17 0.60 o -5 16 1 15.74 16.01 1.39 o -4 16 1 0.13 0.44 0.43 o -3 16 1 2.42 1.64 0.53 o -2 16 1 1.55 0.87 0.43 o -1 16 1 80.69 97.51 2.56 o 0 16 1 1.10 0.49 0.19 o 1 16 1 2.06 1.39 0.25 o 3 16 1 17.79 26.18 1.13 o 4 16 1 4.41 3.55 0.36 o 5 16 1 1.77 1.32 0.35 o -5 17 1 1.12 0.79 0.40 o -4 17 1 0.07 0.13 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