#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/61/2226111.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226111_Fobs loop_ _publ_author_name 'Khan, F. Nawaz' 'Manivel, P.' 'Roopan, S. Mohana' 'Hathwar, Venkatesha R.' 'Akkurt, Mehmet' _publ_section_title ; 3-tert-Butyl-1H-isochromene-1-thione ; _journal_coeditor_code FJ2306 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1470 _journal_volume 66 _journal_year 2010 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-R 3' _symmetry_space_group_name_H-M 'R -3 :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 43.2799 _cell_length_b 43.2799 _cell_length_c 6.9025 _exptl_crystal_F_000 4176.00 _reflns_d_resolution_high 0.7569 _[local]_cod_data_source_file fj2306Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vh-2a in R-3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1167.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 3 0 196186.72 197053.14 3607.98 o -2 4 0 16554.14 15286.06 87.77 o -4 5 0 212581.14 240984.59 1683.46 o -1 5 0 162800.98 169386.36 554.95 o -3 6 0 139.13 174.62 96.16 o 0 6 0 70234.55 70009.31 241.33 o -5 7 0 76.72 304.22 82.40 o -2 7 0 3.34 69.34 82.21 o -7 8 0 36722.27 38265.54 178.56 o -4 8 0 21161.26 23379.84 255.61 o -1 8 0 28745.95 34221.99 345.07 o -6 9 0 675.29 825.45 91.94 o -3 9 0 1920.64 1786.24 30.32 o 0 9 0 2136.96 2475.79 106.98 o -8 10 0 97791.07 100204.94 390.99 o -5 10 0 12016.47 14400.53 205.03 o -2 10 0 45850.75 47827.45 223.88 o -10 11 0 11838.82 12418.94 95.40 o -7 11 0 63479.84 71030.01 464.02 o -4 11 0 211095.00 234928.83 1069.89 o -1 11 0 32219.89 36316.45 288.43 o -9 12 0 2115.27 2154.86 163.83 o -6 12 0 54513.61 63856.02 436.16 o -3 12 0 4536.67 4663.60 70.55 o 0 12 0 33640.82 36158.70 186.89 o -11 13 0 5325.21 5463.18 125.45 o -8 13 0 3760.92 3650.77 79.99 o -5 13 0 20251.84 21500.85 135.88 o -2 13 0 9745.87 10170.95 153.83 o -13 14 0 74098.20 82297.30 365.59 o -10 14 0 8684.54 8411.77 70.44 o -7 14 0 50384.42 57666.26 436.94 o -4 14 0 7232.11 6341.45 71.50 o -1 14 0 1512.96 1544.63 80.48 o -12 15 0 5116.48 5147.82 116.11 o -9 15 0 871.61 942.39 82.11 o -6 15 0 12439.17 13238.36 114.22 o -3 15 0 30577.83 34205.50 194.53 o 0 15 0 9265.02 8020.62 142.12 o -14 16 0 1272.01 1181.79 74.80 o -11 16 0 45865.61 49518.95 343.41 o -8 16 0 15512.76 17206.67 158.59 o -5 16 0 17894.07 17025.58 214.39 o -2 16 0 1669.72 1507.95 76.49 o -16 17 0 349.12 351.26 53.52 o -13 17 0 17152.74 17814.32 203.60 o -10 17 0 46934.09 51466.12 310.66 o -7 17 0 1838.35 1706.97 89.41 o -4 17 0 6423.71 6384.68 73.32 o -1 17 0 12037.42 11407.19 163.98 o -15 18 0 3427.01 3792.86 67.81 o -12 18 0 6081.78 5891.11 121.59 o -9 18 0 625.60 1092.48 83.86 o -6 18 0 11943.78 12475.33 133.97 o -3 18 0 21859.19 22653.86 223.17 o 0 18 0 52982.09 54423.55 383.55 o -17 19 0 270.20 254.19 50.94 o -14 19 0 112481.58 129298.09 615.56 o -11 19 0 32102.89 35519.82 334.32 o -8 19 0 5850.00 6568.57 143.10 o -5 19 0 3380.47 3389.61 57.24 o -2 19 0 2457.07 2300.83 56.95 o -19 20 0 14258.44 14298.38 162.25 o -16 20 0 25144.37 26577.63 255.58 o -13 20 0 35390.40 39648.89 261.40 o -10 20 0 34257.75 38214.82 338.40 o -7 20 0 302.18 592.15 77.31 o -4 20 0 5161.70 4823.64 79.46 o -1 20 0 2048.10 2157.26 60.81 o -18 21 0 56.27 339.06 62.58 o -15 21 0 11653.03 13304.13 178.66 o -12 21 0 1598.73 1458.80 85.22 o -9 21 0 3591.85 3188.86 76.97 o -6 21 0 7820.01 8440.17 127.44 o -3 21 0 2632.37 2449.74 62.97 o 0 21 0 126.88 126.75 40.98 o -20 22 0 40.93 23.66 33.97 o -17 22 0 1793.33 1621.51 75.70 o -14 22 0 20512.13 23673.96 201.98 o -11 22 0 99700.24 107667.55 634.99 o -8 22 0 12021.10 11560.25 184.12 o -5 22 0 4490.63 4392.92 99.06 o -2 22 0 5000.00 5079.83 114.21 o -22 23 0 30558.66 28543.40 264.37 o -19 23 0 52.81 205.73 48.92 o -16 23 0 16863.20 21909.38 229.36 o -13 23 0 6.40 13.42 42.70 o -10 23 0 3839.28 4998.57 105.44 o -7 23 0 5042.34 3926.13 114.01 o -4 23 0 13179.60 12022.78 149.31 o -1 23 0 19016.23 18169.54 215.50 o -21 24 0 9613.38 9130.24 146.13 o -18 24 0 517.41 468.33 51.84 o -15 24 0 948.93 1024.53 60.85 o -12 24 0 244.03 380.68 56.71 o -9 24 0 2768.82 2359.37 77.10 o -6 24 0 2088.27 2001.40 73.62 o -3 24 0 875.88 715.59 48.44 o 0 24 0 1321.10 1398.86 80.94 o -23 25 0 1516.37 1591.54 76.84 o -20 25 0 152.55 315.23 49.95 o -17 25 0 12788.88 12422.16 159.92 o -14 25 0 6223.63 6758.23 151.62 o -11 25 0 72.39 169.70 40.04 o -8 25 0 5346.82 5296.01 117.15 o -5 25 0 5442.69 5345.82 158.04 o -2 25 0 12.87 72.83 51.51 o -25 26 0 8915.51 8017.85 183.43 o -22 26 0 3053.16 2690.55 94.37 o -19 26 0 3504.39 2852.85 96.17 o -16 26 0 235.19 257.91 56.39 o -13 26 0 748.18 1191.31 64.91 o -10 26 0 20026.33 20063.95 285.04 o -7 26 0 425.69 364.05 59.84 o -4 26 0 782.25 900.34 73.66 o -1 26 0 118.98 135.19 58.51 o -24 27 0 205.75 239.70 57.62 o -21 27 0 30.86 70.10 47.00 o -18 27 0 14582.92 13816.64 220.10 o -15 27 0 15412.24 15995.56 221.35 o -12 27 0 29620.83 29590.76 367.92 o -9 27 0 2879.39 3228.72 131.64 o -6 27 0 101.15 183.42 59.60 o -3 27 0 4299.48 4356.80 149.99 o 0 27 0 763.62 794.05 80.23 o -26 28 0 326.76 452.27 69.67 o -23 28 0 1906.64 1954.07 103.41 o -20 28 0 599.74 813.08 71.05 o -17 28 0 420.42 418.70 56.71 o -14 28 0 2612.45 2277.19 103.73 o -11 28 0 295.53 360.90 60.89 o -8 28 0 3671.90 3423.34 137.76 o -5 28 0 2518.54 2578.39 117.57 o -2 28 0 5755.31 5517.59 171.01 o -28 29 0 3142.48 3051.08 142.20 o -25 29 0 2308.87 2160.20 124.27 o -22 29 0 509.93 466.81 62.53 o -19 29 0 747.72 675.52 67.39 o -16 29 0 3425.00 2901.14 125.64 o -13 29 0 2608.61 2805.76 126.06 o -10 29 0 6679.15 5630.57 161.63 o -7 29 0 54034.61 53951.14 531.71 o -4 29 0 9747.84 9777.91 218.83 o -1 29 0 45.94 83.28 64.38 o -27 30 0 0.47 62.76 59.21 o -24 30 0 1287.34 1344.03 104.92 o -21 30 0 214.40 236.73 54.60 o -18 30 0 7013.88 7186.86 180.30 o -15 30 0 1516.27 1552.33 92.85 o -12 30 0 292.81 343.17 69.46 o -9 30 0 1069.66 1202.95 92.10 o -6 30 0 13082.50 12874.24 255.23 o -3 30 0 23983.57 23647.78 351.08 o 0 30 0 496.50 648.57 93.79 o -29 31 0 6235.04 6003.19 207.91 o -26 31 0 717.60 859.54 88.69 o -23 31 0 78.46 102.79 57.26 o -20 31 0 449.46 370.77 66.58 o -17 31 0 3278.77 2833.80 121.23 o -14 31 0 646.22 692.62 82.56 o -11 31 0 182.14 191.03 65.06 o -8 31 0 31443.97 32141.50 411.36 o -5 31 0 53992.24 51812.19 542.56 o -2 31 0 244.56 280.14 80.94 o -31 32 0 8883.08 8350.83 245.59 o -28 32 0 1843.24 1805.62 125.66 o -25 32 0 2008.81 2010.11 137.85 o -22 32 0 614.30 561.88 80.23 o -19 32 0 47.33 114.11 58.83 o -16 32 0 1187.60 1109.51 92.48 o -13 32 0 630.49 426.29 72.91 o -10 32 0 1098.12 1035.68 101.17 o -7 32 0 9675.28 9692.10 241.35 o -4 32 0 8422.69 8332.48 219.61 o -1 32 0 6172.98 5531.00 210.30 o -30 33 0 438.52 353.42 83.41 o -27 33 0 1588.18 1600.58 135.35 o -24 33 0 3333.64 3057.87 149.49 o -21 33 0 6392.13 6629.15 184.89 o -18 33 0 5288.71 5095.77 170.76 o -15 33 0 3477.50 3219.42 137.28 o -12 33 0 2552.05 2610.83 132.18 o -9 33 0 1119.38 1492.50 109.08 o -6 33 0 79598.73 77915.54 700.16 o -3 33 0 26942.89 26004.85 547.04 o 0 33 0 172.87 191.92 78.13 o -32 34 0 272.00 324.77 83.74 o -29 34 0 1265.84 1474.24 131.23 o -26 34 0 4258.81 3528.79 183.68 o -23 34 0 879.02 896.19 92.40 o -20 34 0 779.63 579.43 74.26 o -17 34 0 1351.34 1557.38 107.85 o -14 34 0 6155.48 5704.28 185.90 o -11 34 0 12076.30 10872.07 254.55 o -8 34 0 7373.09 7476.30 218.62 o -5 34 0 3657.65 3552.86 172.48 o -2 34 0 1.66 27.36 69.62 o -34 35 0 0.26 101.07 73.85 o -31 35 0 18.86 17.03 74.91 o -28 35 0 3908.61 3796.46 220.89 o -25 35 0 223.46 386.96 95.86 o -22 35 0 538.43 601.01 90.04 o -19 35 0 221.52 239.10 66.59 o -16 35 0 3705.78 4039.72 158.00 o -13 35 0 2307.25 2208.08 127.29 o -10 35 0 20276.68 20055.81 346.48 o -7 35 0 11787.34 10945.86 260.27 o -4 35 0 11496.25 10687.30 290.19 o -1 35 0 1310.22 1396.80 151.92 o -33 36 0 0.57 84.72 78.19 o -30 36 0 55.24 132.70 79.90 o -27 36 0 622.57 732.47 133.19 o -24 36 0 7954.81 7029.61 225.12 o -21 36 0 1110.80 906.80 101.99 o -18 36 0 484.23 627.79 84.19 o -15 36 0 2399.00 2455.06 132.33 o -12 36 0 32.86 89.37 69.04 o -9 36 0 11357.42 10549.97 261.00 o -6 36 0 7647.88 7651.59 286.23 o -3 36 0 3921.11 3785.13 182.19 o 0 36 0 19.01 98.60 75.44 o -35 37 0 56.07 64.35 69.56 o -32 37 0 1594.20 1618.24 144.17 o -29 37 0 313.37 363.02 110.44 o -26 37 0 58.04 136.59 84.59 o -23 37 0 523.77 721.70 91.32 o -20 37 0 505.45 343.64 79.31 o -17 37 0 159.66 37.34 61.11 o -14 37 0 5232.17 5264.42 184.34 o -11 37 0 9510.51 9284.66 245.11 o -8 37 0 474.93 405.74 92.08 o -5 37 0 45.84 123.09 74.61 o -2 37 0 81.52 126.42 77.70 o -37 38 0 353.39 419.67 118.14 o -34 38 0 6233.91 6264.19 260.85 o -31 38 0 65.28 122.48 81.66 o -28 38 0 4883.94 4603.47 221.37 o -25 38 0 878.41 1176.82 125.31 o -22 38 0 584.83 548.68 96.20 o -19 38 0 461.32 483.39 91.95 o -16 38 0 1164.02 1313.24 109.62 o -13 38 0 953.35 1189.98 104.50 o -10 38 0 7884.13 7064.09 221.57 o -7 38 0 219.92 256.30 80.31 o -4 38 0 3678.25 4160.12 189.04 o -1 38 0 332.74 374.88 96.51 o -36 39 0 450.74 556.54 100.29 o -33 39 0 84.19 98.27 80.36 o -30 39 0 1071.53 949.49 121.06 o -27 39 0 1164.22 1061.26 127.05 o -24 39 0 55.86 201.08 77.00 o -21 39 0 361.27 730.28 94.56 o -18 39 0 1655.19 1751.84 118.13 o -15 39 0 189.34 192.96 72.12 o -12 39 0 1.11 143.86 67.85 o -9 39 0 13.32 72.32 65.29 o -6 39 0 475.54 570.60 104.89 o -3 39 0 128.44 135.18 87.13 o 0 39 0 42.15 77.26 80.62 o -38 40 0 0.21 145.36 82.65 o -35 40 0 31.05 91.91 87.73 o -32 40 0 48.34 124.05 88.44 o -29 40 0 5773.79 5280.04 258.20 o -26 40 0 2964.26 2565.11 182.95 o -23 40 0 85.90 78.85 65.55 o -20 40 0 499.31 617.48 90.50 o -17 40 0 986.10 1034.69 100.64 o -14 40 0 2002.43 2011.44 127.78 o -11 40 0 82.75 214.38 77.42 o -8 40 0 1915.25 1651.57 138.17 o -5 40 0 60.11 132.09 78.85 o -2 40 0 1567.87 1578.33 163.21 o -40 41 0 524.73 504.51 112.52 o -37 41 0 1061.26 904.22 124.30 o -34 41 0 53.91 187.69 93.33 o -31 41 0 2277.52 2077.87 164.33 o -28 41 0 2694.85 2111.34 163.55 o -25 41 0 60.11 136.15 77.56 o -22 41 0 1775.62 2128.87 142.81 o -19 41 0 81.32 127.49 78.31 o -16 41 0 2.19 124.01 71.18 o -13 41 0 163.05 135.80 73.41 o -10 41 0 126.20 127.29 75.37 o -7 41 0 387.06 363.49 91.36 o -4 41 0 3721.98 3564.76 207.24 o -1 41 0 8.03 71.54 84.46 o -39 42 0 72.58 196.45 96.40 o -36 42 0 282.40 330.50 98.60 o -33 42 0 227.88 279.08 148.87 o -30 42 0 303.10 594.84 111.57 o -27 42 0 4711.76 4380.85 225.06 o -24 42 0 67.04 70.84 75.03 o -21 42 0 1345.77 1342.81 155.28 o -18 42 0 1919.33 1773.28 136.16 o -15 42 0 1854.49 1817.35 128.68 o -12 42 0 24.07 65.34 71.43 o -9 42 0 73.19 70.41 74.15 o -6 42 0 672.29 924.17 173.48 o -3 42 0 2.54 119.66 84.22 o 0 42 0 102.26 56.25 80.34 o -41 43 0 50.46 116.90 91.55 o -38 43 0 8.89 139.40 87.84 o -35 43 0 17.82 194.34 100.70 o -32 43 0 111.87 174.67 83.68 o -29 43 0 547.65 541.72 108.01 o -26 43 0 2.91 58.97 80.06 o -23 43 0 2364.84 2516.57 156.21 o -20 43 0 724.89 707.79 105.26 o -17 43 0 309.42 228.58 79.86 o -14 43 0 46.02 179.31 73.17 o -11 43 0 148.56 202.63 119.93 o -8 43 0 5.28 108.79 78.46 o -5 43 0 303.72 392.03 103.40 o -2 43 0 6.57 72.12 86.91 o -43 44 0 116.15 348.87 107.93 o -40 44 0 794.88 1129.15 138.29 o -37 44 0 1203.04 1069.77 135.18 o -34 44 0 478.07 503.96 116.09 o -31 44 0 601.30 514.21 115.27 o -28 44 0 25.48 119.96 94.68 o -25 44 0 49.10 174.14 90.63 o -22 44 0 107.26 232.60 84.26 o -19 44 0 91.95 185.19 82.38 o -16 44 0 8.85 116.34 68.95 o -13 44 0 911.28 924.08 108.12 o -10 44 0 1072.98 844.78 109.96 o -7 44 0 891.25 842.32 115.73 o -4 44 0 270.54 352.19 120.12 o -1 44 0 278.56 465.16 117.18 o -42 45 0 87.87 186.64 126.82 o -39 45 0 39.68 147.72 97.70 o -36 45 0 1612.55 1750.91 166.34 o -33 45 0 1156.61 1451.40 151.22 o -30 45 0 121.82 489.94 108.77 o -27 45 0 620.52 592.09 130.07 o -24 45 0 237.95 306.69 100.05 o -21 45 0 118.92 134.77 85.56 o -18 45 0 284.74 184.34 90.54 o -15 45 0 568.81 544.78 100.19 o -12 45 0 1921.01 2185.71 150.84 o -9 45 0 158.98 255.45 112.20 o -6 45 0 547.74 618.98 190.85 o -3 45 0 3686.20 3900.48 224.77 o 0 45 0 445.42 508.55 132.69 o -44 46 0 1.78 141.26 116.78 o -41 46 0 53.94 78.51 98.53 o -38 46 0 2.20 147.67 97.03 o -35 46 0 495.30 295.59 104.72 o -32 46 0 434.61 403.26 114.38 o -29 46 0 22.43 229.94 100.94 o -26 46 0 0.97 24.13 84.22 o -23 46 0 14.02 94.87 78.81 o -20 46 0 195.53 440.63 93.90 o -17 46 0 291.40 259.06 88.84 o -14 46 0 2.69 11.80 75.38 o -11 46 0 2139.40 2370.63 215.78 o -8 46 0 612.98 679.83 131.62 o -5 46 0 342.90 435.26 112.02 o -2 46 0 16.60 92.80 125.77 o -46 47 0 237.74 397.00 141.93 o -43 47 0 1249.27 1454.35 184.75 o -40 47 0 428.79 554.19 142.68 o -37 47 0 89.37 112.71 102.17 o -34 47 0 1100.62 1295.46 141.29 o -31 47 0 779.86 701.99 149.14 o -28 47 0 318.40 232.51 103.61 o -25 47 0 612.46 689.74 118.44 o -22 47 0 73.40 211.55 90.93 o -19 47 0 11.13 113.47 81.55 o -16 47 0 331.16 480.86 111.98 o -13 47 0 6.26 96.61 84.97 o -10 47 0 77.64 112.65 83.45 o -7 47 0 742.73 975.21 211.35 o -4 47 0 570.44 808.34 168.70 o -1 47 0 119.50 484.58 157.59 o -45 48 0 707.50 622.52 245.30 o -42 48 0 91.72 121.78 106.37 o -39 48 0 452.32 673.30 137.78 o -36 48 0 849.16 927.94 138.50 o -33 48 0 211.70 101.96 104.95 o -30 48 0 808.35 1013.85 138.75 o -27 48 0 814.00 667.52 118.24 o -24 48 0 90.15 301.09 106.58 o -21 48 0 483.25 640.80 114.45 o -18 48 0 20.60 62.05 91.34 o -15 48 0 380.23 399.88 104.63 o -12 48 0 8.35 59.74 86.94 o -9 48 0 169.94 213.99 103.49 o -6 48 0 127.26 195.14 119.16 o -3 48 0 39.99 54.20 120.42 o 0 48 0 0.15 80.50 126.29 o -47 49 0 715.43 925.09 164.15 o -44 49 0 86.39 179.82 143.80 o -41 49 0 681.85 767.76 159.64 o -38 49 0 5.05 98.25 115.07 o -35 49 0 88.39 105.13 90.01 o -32 49 0 3.98 61.16 88.29 o -29 49 0 1959.08 2336.71 206.97 o -26 49 0 1535.65 1988.14 218.15 o -23 49 0 2207.43 2276.07 182.63 o -20 49 0 92.73 250.95 127.21 o -17 49 0 28.11 198.04 103.39 o -14 49 0 180.81 284.48 156.82 o -11 49 0 21.01 113.96 94.08 o -8 49 0 0.39 56.62 102.01 o -5 49 0 140.79 426.24 136.50 o -2 49 0 164.83 169.38 137.70 o -46 50 0 17.76 86.86 122.17 o -43 50 0 615.44 789.27 158.15 o -40 50 0 0.45 67.30 104.96 o -37 50 0 0.14 89.64 113.30 o -34 50 0 20.16 231.53 122.82 o -31 50 0 44.84 274.29 111.14 o -28 50 0 8.15 62.52 92.74 o -25 50 0 45.08 200.00 113.11 o -22 50 0 138.17 221.14 96.75 o -19 50 0 592.55 823.73 141.22 o -16 50 0 294.86 438.85 130.56 o -13 50 0 383.80 482.57 113.63 o -10 50 0 3.42 186.57 119.75 o -7 50 0 131.13 160.89 114.40 o -4 50 0 324.70 367.77 142.03 o -1 50 0 26.88 0.00 282.03 o -45 51 0 96.60 472.49 171.84 o -42 51 0 5.85 82.78 134.33 o -39 51 0 193.52 171.01 122.08 o -36 51 0 570.26 482.32 148.98 o -33 51 0 103.46 199.96 114.99 o -30 51 0 12.21 332.83 108.95 o -27 51 0 83.96 283.46 106.67 o -24 51 0 84.98 238.12 118.09 o -21 51 0 339.28 465.87 120.22 o -18 51 0 358.17 760.22 124.08 o -15 51 0 11.34 159.28 107.81 o -12 51 0 12.14 124.97 105.99 o -9 51 0 514.11 695.46 149.77 o -6 51 0 38.05 53.60 122.11 o -44 52 0 10.14 284.83 156.62 o -41 52 0 750.45 548.13 196.41 o -38 52 0 20.23 149.15 124.70 o -35 52 0 40.59 153.52 127.33 o -32 52 0 85.55 353.07 183.19 o -29 52 0 500.98 584.33 125.10 o -26 52 0 109.35 172.31 114.91 o -23 52 0 19.91 33.12 115.90 o -20 52 0 301.75 203.33 112.98 o -17 52 0 60.30 214.64 108.87 o -14 52 0 212.34 337.56 139.53 o -11 52 0 322.16 388.58 142.22 o -8 52 0 0.55 169.96 158.11 o -43 53 0 30.41 42.84 173.65 o -40 53 0 830.18 595.19 153.87 o -37 53 0 375.05 509.38 170.43 o -34 53 0 137.92 226.91 147.30 o -31 53 0 0.11 2.48 116.85 o -28 53 0 8.55 73.17 120.97 o -25 53 0 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