#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:38:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181182 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/61/2226167.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226167_Fobs loop_ _publ_author_name 'Garden, Simon J.' 'Pinto, Angelo C.' 'da Cunha, Fernanda R.' 'Fontes, Silvia P.' 'Lima, A. S.' 'Tiekink, Edward R. T.' _publ_section_title ; (2E)-N-(3,5-Dibromo-4-methoxyphenyl)-2-(hydroxyimino)acetamide ; _journal_coeditor_code HG2689 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1436 _journal_page_last o1437 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.356 _cell_angle_gamma 90.000 _cell_length_a 10.3841 _cell_length_b 8.8535 _cell_length_c 13.0164 _exptl_crystal_F_000 679.87 _reflns_d_resolution_high 0.7699 _cod_data_source_file hg2689Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0538' _shelx_refln_list_code 4 _shelx_f_calc_maximum 208.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24395.05 23685.47 543.50 o 4 0 0 2459.32 2389.59 46.95 o 6 0 0 4.99 -2.41 5.86 o 8 0 0 0.17 8.43 8.10 o 10 0 0 568.97 645.11 24.49 o 12 0 0 1033.68 1087.08 103.16 o 1 1 0 884.20 893.15 17.82 o 2 1 0 570.40 648.06 13.26 o 3 1 0 3191.28 3044.71 40.17 o 4 1 0 689.06 639.26 11.35 o 5 1 0 15355.11 16149.61 192.79 o 6 1 0 794.42 855.94 15.27 o 7 1 0 7223.67 7654.67 100.71 o 8 1 0 630.53 684.09 15.38 o 9 1 0 915.29 993.08 21.97 o 10 1 0 508.10 583.39 18.03 o 11 1 0 105.80 98.18 10.52 o 12 1 0 68.37 82.10 13.86 o 0 2 0 8218.32 8044.04 101.57 o 1 2 0 8497.47 8026.11 103.77 o 2 2 0 8331.43 8234.86 108.48 o 3 2 0 2263.38 2231.43 32.96 o 4 2 0 6366.35 6238.17 78.66 o 5 2 0 6198.73 6410.81 80.02 o 6 2 0 3303.68 3473.50 48.72 o 7 2 0 6.64 4.75 4.10 o 8 2 0 1364.74 1476.61 26.69 o 9 2 0 1503.14 1609.17 32.48 o 10 2 0 832.25 932.64 36.46 o 11 2 0 500.35 526.37 24.43 o 12 2 0 249.94 230.22 22.94 o 1 3 0 43674.36 42162.49 609.05 o 2 3 0 1834.10 1922.39 28.84 o 3 3 0 9532.34 9572.24 150.70 o 4 3 0 750.31 759.28 14.66 o 5 3 0 2933.61 3176.16 47.77 o 6 3 0 174.09 162.81 6.96 o 7 3 0 9.04 2.49 3.79 o 8 3 0 10.78 21.41 5.55 o 9 3 0 773.58 764.10 20.44 o 10 3 0 584.65 604.51 21.18 o 11 3 0 404.73 413.97 29.44 o 12 3 0 211.87 178.86 19.19 o 0 4 0 4645.44 4846.60 96.00 o 1 4 0 2061.50 2141.53 25.79 o 2 4 0 61.92 50.22 5.53 o 3 4 0 1.05 9.06 3.55 o 4 4 0 7979.92 8066.22 110.71 o 5 4 0 244.18 263.08 11.10 o 6 4 0 11849.92 12815.00 180.56 o 7 4 0 0.17 0.19 6.45 o 8 4 0 3706.08 4177.38 77.30 o 9 4 0 26.96 35.59 10.39 o 10 4 0 78.63 82.58 13.05 o 11 4 0 122.23 110.77 35.89 o 12 4 0 45.60 43.14 23.44 o 1 5 0 17583.44 17698.63 207.67 o 2 5 0 1923.48 1864.03 25.96 o 3 5 0 4088.72 4034.83 59.06 o 4 5 0 902.22 849.69 20.00 o 5 5 0 255.76 256.76 10.17 o 6 5 0 872.98 886.21 20.94 o 7 5 0 179.12 187.17 9.26 o 8 5 0 551.51 565.74 18.59 o 9 5 0 179.51 169.01 12.69 o 10 5 0 141.83 148.70 16.37 o 11 5 0 337.33 344.44 29.41 o 0 6 0 7308.13 7079.20 153.72 o 1 6 0 275.12 274.87 5.98 o 2 6 0 4409.14 4662.71 56.42 o 3 6 0 4977.22 5028.31 61.80 o 4 6 0 5096.02 5092.36 109.08 o 5 6 0 1863.43 1953.43 51.31 o 6 6 0 804.76 831.15 23.20 o 7 6 0 16.48 8.22 9.08 o 8 6 0 268.75 249.92 17.17 o 9 6 0 1334.01 1439.40 71.31 o 10 6 0 91.20 73.90 20.12 o 11 6 0 466.58 430.63 52.93 o 1 7 0 132.43 130.25 5.35 o 2 7 0 918.11 960.41 13.63 o 3 7 0 3376.01 3444.08 48.77 o 4 7 0 1201.80 1232.96 19.62 o 5 7 0 1567.62 1586.96 30.91 o 6 7 0 845.81 858.38 22.26 o 7 7 0 1526.85 1581.62 45.75 o 8 7 0 2.63 -0.69 16.90 o 9 7 0 358.42 394.02 25.42 o 10 7 0 258.12 264.04 32.56 o 0 8 0 6269.80 6466.81 198.62 o 1 8 0 359.67 369.42 19.14 o 2 8 0 7464.86 7679.57 117.27 o 3 8 0 1.72 10.32 4.00 o 4 8 0 56.08 59.49 4.41 o 5 8 0 357.91 381.56 12.01 o 6 8 0 174.79 187.20 11.77 o 7 8 0 74.29 79.11 12.67 o 8 8 0 34.00 25.53 15.21 o 9 8 0 15.53 -1.56 13.69 o 1 9 0 33.76 33.80 10.31 o 2 9 0 756.50 739.74 30.75 o 3 9 0 782.20 833.13 22.87 o 4 9 0 822.55 801.13 24.48 o 5 9 0 933.01 974.01 27.76 o 6 9 0 147.80 148.34 14.59 o 7 9 0 947.62 953.02 45.16 o 8 9 0 229.75 227.37 24.47 o 0 10 0 17.20 28.20 39.81 o 1 10 0 332.97 339.81 18.03 o 2 10 0 592.25 570.71 27.03 o 3 10 0 2447.75 2573.15 85.59 o 4 10 0 113.95 119.31 20.09 o 5 10 0 500.75 507.76 39.01 o 6 10 0 192.61 217.42 26.29 o 1 11 0 1661.43 1607.19 64.67 o 2 11 0 31.65 13.80 17.78 o 3 11 0 432.88 492.44 38.25 o -13 0 1 23.29 33.98 22.40 o -11 0 1 0.04 12.41 16.10 o -9 0 1 124.56 126.37 12.69 o -7 0 1 2454.36 2592.74 56.52 o -5 0 1 14804.01 15429.24 268.55 o 1 0 1 3.72 5.32 5.22 o 3 0 1 4927.53 4977.01 90.11 o 5 0 1 1599.77 1575.17 32.39 o 7 0 1 919.64 924.83 23.03 o 9 0 1 2713.58 2988.63 75.67 o 11 0 1 353.41 362.97 31.92 o -13 1 1 97.21 121.42 39.50 o -12 1 1 390.12 415.85 24.29 o -11 1 1 85.87 75.31 13.71 o -10 1 1 2093.48 2333.11 50.18 o -9 1 1 622.26 683.55 19.23 o -8 1 1 3617.68 4016.02 59.42 o -7 1 1 1199.76 1202.44 20.87 o -6 1 1 546.63 530.91 11.22 o -5 1 1 379.52 340.69 8.17 o -4 1 1 527.48 562.38 10.16 o -3 1 1 1.74 3.31 2.98 o -2 1 1 19.45 30.01 4.99 o -1 1 1 615.89 618.20 15.82 o 1 1 1 31.50 40.95 2.70 o 2 1 1 23887.50 23037.37 265.46 o 3 1 1 26.30 24.01 2.80 o 4 1 1 8787.25 8499.97 105.21 o 5 1 1 3936.80 4042.72 53.37 o 6 1 1 173.05 163.74 6.11 o 7 1 1 1550.15 1653.12 27.75 o 8 1 1 109.49 106.53 6.87 o 9 1 1 141.89 157.55 8.24 o 10 1 1 577.63 572.99 19.23 o 11 1 1 76.63 73.45 12.75 o 12 1 1 196.67 183.81 16.82 o -12 2 1 380.15 371.25 31.16 o -11 2 1 365.97 371.48 20.05 o -10 2 1 43.81 45.72 7.93 o -9 2 1 925.14 1045.96 24.42 o -8 2 1 3192.98 3492.45 58.90 o -7 2 1 1840.39 1894.23 32.84 o -6 2 1 1781.02 1783.99 32.69 o -5 2 1 2991.08 2960.09 44.30 o -4 2 1 1516.16 1543.40 24.69 o -3 2 1 3342.55 3382.29 61.04 o -2 2 1 20389.81 19571.73 532.97 o -1 2 1 4015.51 3943.59 49.06 o 0 2 1 3232.03 3178.63 52.53 o 1 2 1 4385.13 4131.38 52.37 o 2 2 1 4970.04 4921.02 61.74 o 3 2 1 2301.70 2287.79 31.45 o 4 2 1 1967.57 2014.80 28.49 o 5 2 1 899.85 855.05 14.77 o 6 2 1 4611.57 4885.97 66.65 o 7 2 1 430.74 501.85 11.76 o 8 2 1 711.29 747.94 17.27 o 9 2 1 41.67 53.37 7.31 o 10 2 1 17.60 21.17 7.52 o 11 2 1 57.54 42.62 9.38 o 12 2 1 77.73 89.82 22.50 o -12 3 1 168.66 152.44 22.45 o -11 3 1 103.61 83.09 20.16 o -10 3 1 52.07 33.23 9.11 o -9 3 1 310.22 307.59 16.83 o -8 3 1 1758.72 1847.33 35.66 o -7 3 1 1394.63 1456.30 31.08 o -6 3 1 4064.52 4304.08 70.95 o -5 3 1 2018.52 2030.13 36.07 o -4 3 1 18778.73 18906.12 261.53 o -3 3 1 6.19 5.15 4.24 o -2 3 1 21799.66 20941.63 374.29 o -1 3 1 1255.13 1299.89 16.56 o 0 3 1 5391.85 5530.86 65.20 o 1 3 1 11.71 21.68 3.48 o 2 3 1 906.01 923.47 14.82 o 3 3 1 113.83 116.45 4.22 o 4 3 1 1836.60 1817.43 26.65 o 5 3 1 596.38 566.65 11.28 o 6 3 1 388.45 398.17 9.83 o 7 3 1 3129.43 3289.80 47.07 o 8 3 1 513.90 541.98 14.07 o 9 3 1 640.26 644.72 15.85 o 10 3 1 567.75 589.73 20.74 o 11 3 1 9.04 -9.85 14.86 o 12 3 1 64.12 73.61 16.93 o -12 4 1 7.30 -6.24 15.83 o -11 4 1 1386.45 1409.20 111.05 o -10 4 1 29.81 22.61 12.12 o -9 4 1 3145.32 3372.19 75.11 o -8 4 1 29.47 35.43 7.55 o -7 4 1 1616.81 1722.11 34.82 o -6 4 1 610.65 674.45 22.34 o -5 4 1 95.91 115.53 6.61 o -4 4 1 2073.60 2115.70 43.56 o -3 4 1 3615.24 3811.95 53.94 o -2 4 1 723.25 789.87 19.03 o -1 4 1 94.66 91.42 4.37 o 0 4 1 1022.68 1001.74 15.70 o 1 4 1 9268.42 9375.38 107.10 o 2 4 1 2456.86 2528.07 39.33 o 3 4 1 16189.50 16104.95 206.11 o 4 4 1 397.55 424.50 14.19 o 5 4 1 3858.98 3990.27 59.77 o 6 4 1 585.06 616.09 13.06 o 7 4 1 272.92 273.98 11.41 o 8 4 1 543.65 596.26 18.19 o 9 4 1 1172.97 1231.92 36.95 o 10 4 1 5.48 12.58 10.55 o 11 4 1 417.43 406.11 43.34 o -11 5 1 282.47 282.09 25.44 o -10 5 1 109.44 120.29 16.40 o -9 5 1 303.24 313.88 19.35 o -8 5 1 202.98 216.93 12.34 o -7 5 1 307.27 312.53 12.86 o -6 5 1 2209.43 2285.92 42.21 o -5 5 1 357.33 361.98 10.20 o -4 5 1 9281.19 9796.91 148.59 o -3 5 1 1072.20 1096.54 17.83 o -2 5 1 9975.70 10158.39 150.29 o -1 5 1 5153.67 4910.69 63.67 o 0 5 1 1226.24 1121.16 20.95 o 1 5 1 2067.41 1938.34 25.12 o 2 5 1 170.03 200.71 5.11 o 3 5 1 832.53 924.24 16.92 o 4 5 1 54.54 46.97 3.06 o 5 5 1 1470.03 1544.88 29.22 o 6 5 1 13.19 7.43 6.03 o 7 5 1 38.29 45.82 8.07 o 8 5 1 466.44 443.96 16.98 o 9 5 1 0.28 -1.11 8.89 o 10 5 1 283.68 301.02 20.35 o 11 5 1 126.62 106.76 20.53 o -11 6 1 123.79 123.13 21.85 o -10 6 1 190.74 200.30 19.99 o -9 6 1 607.82 577.90 27.07 o -8 6 1 2725.90 2902.73 63.74 o -7 6 1 2613.03 2829.46 59.49 o -6 6 1 4800.74 4947.39 82.81 o -5 6 1 1754.02 1877.03 45.00 o -4 6 1 260.09 240.06 9.85 o -3 6 1 3557.37 3626.65 51.09 o -2 6 1 189.26 182.60 8.17 o -1 6 1 2161.17 2224.05 34.39 o 0 6 1 3114.70 3099.51 62.59 o 1 6 1 3216.80 3171.78 48.09 o 2 6 1 48.05 57.49 2.89 o 3 6 1 47.73 58.92 4.25 o 4 6 1 2579.90 2659.94 37.84 o 5 6 1 3.21 8.46 5.81 o 6 6 1 5974.46 6308.73 105.34 o 7 6 1 3.34 4.38 7.35 o 8 6 1 1599.61 1647.05 53.23 o 9 6 1 7.25 29.00 16.57 o 10 6 1 84.14 81.52 17.79 o -10 7 1 379.41 412.53 35.68 o -9 7 1 162.62 146.84 18.76 o -8 7 1 442.81 441.15 25.85 o -7 7 1 78.70 85.10 9.73 o -6 7 1 1375.75 1374.40 36.96 o -5 7 1 1.09 -2.89 5.23 o -4 7 1 297.69 328.39 9.65 o -3 7 1 1043.58 1104.27 24.67 o -2 7 1 83.87 85.31 5.06 o -1 7 1 3859.28 3838.08 63.89 o 0 7 1 2835.92 2808.70 48.35 o 1 7 1 3715.53 3763.10 62.59 o 2 7 1 977.58 951.71 16.32 o 3 7 1 2078.47 2167.37 32.13 o 4 7 1 1994.70 2082.02 31.83 o 5 7 1 14.92 17.47 6.16 o 6 7 1 204.84 202.23 12.27 o 7 7 1 323.25 305.03 15.30 o 8 7 1 214.34 229.20 17.64 o 9 7 1 5.32 -0.43 13.75 o 10 7 1 334.09 283.61 24.54 o -9 8 1 18.31 20.97 20.76 o -8 8 1 28.03 20.11 18.10 o -7 8 1 175.42 165.61 13.39 o -6 8 1 133.54 128.17 11.07 o -5 8 1 4569.12 4826.22 76.47 o -4 8 1 32.00 36.25 5.57 o -3 8 1 3447.24 3632.54 66.18 o -2 8 1 1907.69 1977.49 40.42 o -1 8 1 4591.56 4729.99 78.95 o 0 8 1 379.02 393.06 10.57 o 1 8 1 303.34 316.17 10.18 o 2 8 1 1230.80 1276.42 26.00 o 3 8 1 1159.93 1248.34 20.24 o 4 8 1 266.99 251.72 7.37 o 5 8 1 16.41 32.19 6.07 o 6 8 1 8.53 12.67 7.13 o 7 8 1 294.78 247.12 21.30 o 8 8 1 56.19 43.57 19.65 o 9 8 1 127.56 120.20 19.44 o -8 9 1 310.87 289.07 23.06 o -7 9 1 1381.84 1396.77 61.38 o -6 9 1 270.87 256.02 13.55 o -5 9 1 1185.05 1136.93 35.02 o -4 9 1 1.63 1.85 3.09 o -3 9 1 42.57 45.57 4.58 o -2 9 1 3.86 6.32 4.98 o -1 9 1 261.96 237.68 22.46 o 0 9 1 661.57 659.12 24.30 o 1 9 1 48.09 42.76 14.14 o 2 9 1 926.77 1017.40 35.54 o 3 9 1 320.35 335.94 12.21 o 4 9 1 1064.46 1053.07 27.84 o 5 9 1 2175.77 2200.70 54.27 o 6 9 1 256.55 244.49 27.13 o 7 9 1 1776.47 1856.92 95.09 o -6 10 1 674.52 633.58 61.25 o -5 10 1 351.71 349.90 21.37 o -4 10 1 109.52 145.36 43.43 o -3 10 1 7.52 11.50 19.56 o -2 10 1 2145.03 2325.65 85.07 o -1 10 1 426.04 412.25 23.34 o 0 10 1 4791.43 5167.04 120.35 o 1 10 1 16.54 5.91 13.44 o 2 10 1 956.77 1060.63 96.65 o 3 10 1 159.05 159.87 13.06 o 4 10 1 14.83 36.80 9.72 o 5 10 1 79.42 96.32 16.54 o 6 10 1 209.53 192.08 20.84 o -3 11 1 131.24 146.74 28.34 o -2 11 1 965.52 920.21 53.08 o -1 11 1 22.22 25.82 14.17 o 0 11 1 131.66 143.70 16.04 o 1 11 1 114.19 137.07 14.78 o 2 11 1 132.65 105.72 22.59 o 3 11 1 177.55 188.34 39.36 o -12 0 2 0.78 41.84 31.22 o -10 0 2 556.87 549.23 26.85 o -8 0 2 4220.67 4459.78 106.33 o -6 0 2 29847.55 31811.81 718.16 o -4 0 2 12782.84 12922.24 252.54 o -2 0 2 11187.06 8597.52 213.06 o 0 0 2 24762.04 -5.43 3.62 o 2 0 2 13909.34 12963.43 217.94 o 4 0 2 3.09 0.34 4.73 o 6 0 2 1757.35 1773.93 37.67 o 8 0 2 0.27 11.50 8.32 o 10 0 2 94.65 106.38 13.28 o 12 0 2 1147.20 1200.64 67.57 o -13 1 2 270.97 265.72 41.52 o -12 1 2 182.14 171.54 14.87 o -11 1 2 241.07 218.71 14.94 o -10 1 2 388.35 422.63 22.40 o -9 1 2 163.14 174.88 9.98 o -8 1 2 317.91 323.72 10.92 o -7 1 2 299.77 303.89 10.25 o -6 1 2 104.19 133.24 8.90 o -5 1 2 588.93 588.25 13.76 o -4 1 2 73.15 120.11 5.19 o -3 1 2 70.90 77.77 5.26 o -2 1 2 639.85 477.54 12.03 o -1 1 2 7975.05 7932.15 110.17 o 0 1 2 202.61 220.19 4.80 o 1 1 2 394.86 378.22 6.26 o 2 1 2 15348.20 14541.26 172.34 o 3 1 2 2853.65 2829.91 35.56 o 4 1 2 3267.74 3266.80 43.66 o 5 1 2 3877.26 3853.78 51.10 o 6 1 2 49.07 36.05 5.01 o 7 1 2 5260.87 5524.20 76.94 o 8 1 2 467.11 468.35 13.30 o 9 1 2 1685.51 1798.95 35.97 o 10 1 2 137.57 143.60 10.32 o 11 1 2 11.48 19.96 10.45 o 12 1 2 21.80 23.12 20.51 o -13 2 2 47.78 35.46 33.48 o -12 2 2 36.66 45.81 22.31 o -11 2 2 824.21 827.67 32.14 o -10 2 2 53.94 37.44 9.31 o -9 2 2 418.44 406.76 15.72 o -8 2 2 49.57 55.48 6.38 o -7 2 2 198.11 207.40 8.41 o -6 2 2 18.42 23.21 5.07 o -5 2 2 10074.13 10009.37 144.73 o -4 2 2 11.68 7.74 3.39 o -3 2 2 3468.73 3355.96 120.15 o -2 2 2 0.36 0.19 2.36 o -1 2 2 3388.44 3399.14 49.97 o 0 2 2 469.93 475.91 7.55 o 1 2 2 12765.97 12294.71 146.57 o 2 2 2 596.58 676.89 9.80 o 3 2 2 12957.15 12822.15 153.25 o 4 2 2 451.46 421.21 8.63 o 5 2 2 670.50 689.02 11.54 o 6 2 2 980.49 999.90 16.77 o 7 2 2 510.14 532.68 12.71 o 8 2 2 1604.82 1723.04 32.79 o 9 2 2 684.38 736.41 19.09 o 10 2 2 713.45 687.47 22.94 o 11 2 2 374.08 385.58 22.86 o 12 2 2 131.82 146.01 23.11 o -12 3 2 83.05 37.08 19.49 o -11 3 2 288.01 252.42 22.48 o -10 3 2 562.77 580.35 21.29 o -9 3 2 638.29 662.68 19.32 o -8 3 2 781.13 822.53 22.59 o -7 3 2 2904.01 3053.08 61.44 o -6 3 2 4.58 6.65 5.63 o -5 3 2 911.12 946.96 28.64 o -4 3 2 658.77 629.23 26.55 o -3 3 2 618.26 583.33 28.06 o -2 3 2 23.30 42.86 4.06 o -1 3 2 2185.04 2176.38 27.63 o 0 3 2 657.57 595.23 8.82 o 1 3 2 12963.69 12456.69 148.57 o 2 3 2 3198.44 3019.84 37.78 o 3 3 2 370.51 342.65 8.06 o 4 3 2 9083.96 9349.69 117.66 o 5 3 2 156.01 191.07 6.21 o 6 3 2 728.86 771.38 14.77 o 7 3 2 52.88 54.83 5.44 o 8 3 2 41.72 49.19 5.35 o 9 3 2 61.39 56.23 6.96 o 10 3 2 114.45 100.45 7.76 o 11 3 2 592.52 588.97 37.10 o -12 4 2 378.10 324.36 29.80 o -11 4 2 39.82 38.70 15.41 o -10 4 2 1.70 24.69 11.64 o -9 4 2 503.95 484.51 25.38 o -8 4 2 1169.61 1246.57 32.89 o -7 4 2 958.15 975.05 25.07 o -6 4 2 2599.68 2620.55 51.06 o -5 4 2 115.79 120.25 7.68 o -4 4 2 40.28 45.80 5.59 o -3 4 2 1727.02 1686.65 42.45 o -2 4 2 4136.28 4148.50 94.33 o -1 4 2 3134.64 3420.75 48.06 o 0 4 2 6487.42 6677.64 74.96 o 1 4 2 1023.77 1023.29 15.89 o 2 4 2 17.74 29.81 5.73 o 3 4 2 2207.28 2176.93 29.05 o 4 4 2 5617.99 5838.51 76.90 o 5 4 2 1085.96 1192.16 20.46 o 6 4 2 6516.56 6647.96 90.40 o 7 4 2 4.60 9.50 4.90 o 8 4 2 2730.69 2887.22 52.67 o 9 4 2 50.11 31.57 9.05 o 10 4 2 182.35 182.49 15.06 o 11 4 2 28.04 42.45 18.50 o -12 5 2 58.09 83.25 35.29 o -11 5 2 2.41 41.42 19.36 o -10 5 2 26.11 31.54 13.41 o -9 5 2 323.63 355.21 18.76 o -8 5 2 115.11 104.64 9.33 o -7 5 2 1738.57 1805.81 39.16 o -6 5 2 1020.92 1055.70 24.39 o -5 5 2 1037.94 1068.50 28.39 o -4 5 2 4620.38 4572.17 134.03 o -3 5 2 691.18 714.00 18.79 o -2 5 2 2128.60 2084.92 31.81 o -1 5 2 4061.28 4148.54 52.31 o 0 5 2 357.44 419.96 8.56 o 1 5 2 2243.51 2242.85 28.21 o 2 5 2 4154.22 4124.80 60.24 o 3 5 2 776.24 799.97 13.39 o 4 5 2 35.62 30.68 5.33 o 5 5 2 19.46 22.62 4.23 o 6 5 2 112.40 101.92 5.22 o 7 5 2 21.02 18.87 3.88 o 8 5 2 812.93 889.11 29.46 o 9 5 2 56.86 52.19 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