#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:38:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181182 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/61/2226172.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226172_Fobs loop_ _publ_author_name 'Wilseck, Zachary M.' 'LaDuca, Robert L.' _publ_section_title ; Poly[[\m~4~-bis(4-pyridylcarbonyl)piperazine-\k^4^N:N':O:O']bis(thiocyanato-\kN)cobalt(II)] ; _journal_coeditor_code HY2308 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m713 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.080 _cell_angle_beta 102.264 _cell_angle_gamma 119.136 _cell_length_a 7.7410 _cell_length_b 7.8943 _cell_length_c 9.8010 _exptl_crystal_F_000 275.00 _reflns_d_resolution_high 0.8319 _cod_data_source_file hy2308Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p1b in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 997.65 973.10 42.84 o 2 0 0 1033.08 1046.43 38.39 o 3 0 0 10.60 17.26 0.91 o 4 0 0 713.53 744.50 27.54 o 5 0 0 649.17 710.29 29.26 o 6 0 0 1.31 1.73 0.70 o 7 0 0 24.32 21.73 2.88 o -8 1 0 15.60 13.63 2.29 o -7 1 0 135.17 115.66 9.20 o -6 1 0 3.74 4.03 0.75 o -5 1 0 198.24 213.92 8.24 o -4 1 0 69.61 85.59 3.45 o -3 1 0 307.56 288.69 10.77 o -2 1 0 4021.26 3838.22 140.38 o -1 1 0 1041.26 1044.39 38.23 o 0 1 0 4580.49 3986.94 160.06 o 1 1 0 41.67 30.11 1.28 o 2 1 0 57.14 48.23 2.02 o 3 1 0 29.11 26.94 1.31 o 4 1 0 350.45 377.45 15.84 o 5 1 0 318.22 352.91 18.80 o 6 1 0 92.14 109.58 8.22 o 7 1 0 2.69 1.85 1.45 o -8 2 0 30.12 29.36 3.39 o -7 2 0 28.16 28.56 2.47 o -6 2 0 39.97 40.45 2.20 o -5 2 0 351.69 357.96 13.43 o -4 2 0 331.88 295.15 11.09 o -3 2 0 251.26 258.76 9.70 o -2 2 0 60.49 57.87 2.30 o -1 2 0 2387.98 2338.51 85.35 o 0 2 0 382.57 363.88 13.44 o 1 2 0 327.37 345.79 12.90 o 2 2 0 75.04 85.92 3.48 o 3 2 0 525.33 521.42 21.70 o 4 2 0 494.17 529.49 24.70 o 5 2 0 0.42 -0.19 0.49 o 6 2 0 10.38 12.91 2.22 o -8 3 0 5.85 6.03 1.13 o -7 3 0 175.89 197.87 9.80 o -6 3 0 230.89 242.35 10.30 o -5 3 0 0.36 0.43 0.34 o -4 3 0 105.15 145.04 5.63 o -3 3 0 1471.90 1478.54 59.19 o -2 3 0 340.22 328.72 12.28 o -1 3 0 49.14 52.36 2.19 o 0 3 0 6.89 8.77 0.62 o 1 3 0 335.98 340.28 12.72 o 2 3 0 240.51 246.66 10.57 o 3 3 0 16.05 17.61 1.27 o 4 3 0 85.58 85.74 4.79 o 5 3 0 39.86 47.07 3.14 o -9 4 0 58.39 55.07 5.17 o -8 4 0 90.71 98.31 5.47 o -7 4 0 0.38 0.58 0.47 o -6 4 0 35.50 37.54 2.38 o -5 4 0 312.05 312.32 11.82 o -4 4 0 166.55 159.93 6.21 o -3 4 0 74.15 80.11 3.27 o -2 4 0 125.07 110.04 4.35 o -1 4 0 519.50 515.55 19.21 o 0 4 0 7.98 7.94 0.65 o 1 4 0 79.50 86.32 3.61 o 2 4 0 26.78 29.18 1.81 o 3 4 0 121.12 124.02 10.13 o 4 4 0 6.98 5.90 1.15 o -9 5 0 3.16 4.06 1.08 o -8 5 0 25.72 35.35 2.60 o -7 5 0 129.52 155.86 7.93 o -6 5 0 64.07 68.01 4.31 o -5 5 0 7.37 7.01 0.64 o -4 5 0 1006.45 1109.49 43.87 o -3 5 0 718.93 757.44 28.09 o -2 5 0 11.11 10.47 0.75 o -1 5 0 0.37 0.28 0.33 o 0 5 0 69.75 71.62 3.42 o 1 5 0 682.03 749.36 34.50 o 2 5 0 24.13 21.49 3.22 o 3 5 0 14.46 13.02 1.63 o -9 6 0 7.21 11.76 1.62 o -8 6 0 0.31 0.63 0.49 o -7 6 0 72.10 79.00 8.14 o -6 6 0 615.81 705.98 48.44 o -5 6 0 11.40 11.43 0.86 o -4 6 0 131.72 145.52 7.25 o -3 6 0 89.36 98.20 4.99 o -2 6 0 398.19 419.34 19.10 o -1 6 0 208.13 237.31 12.03 o 0 6 0 60.06 66.77 6.55 o 1 6 0 24.98 19.78 2.41 o 2 6 0 46.72 46.25 4.38 o -8 7 0 66.51 62.25 5.45 o -7 7 0 119.42 100.41 7.84 o -6 7 0 135.20 110.46 8.24 o -5 7 0 4.07 3.95 0.84 o -4 7 0 315.45 321.81 18.96 o -3 7 0 111.65 114.46 5.88 o -2 7 0 4.73 3.43 0.72 o -1 7 0 6.13 6.46 1.40 o 0 7 0 66.81 60.00 7.26 o 1 7 0 28.04 28.48 3.24 o -8 8 0 0.99 0.61 0.71 o -7 8 0 76.44 64.66 5.66 o -6 8 0 167.15 142.12 14.30 o -5 8 0 26.44 30.57 3.50 o -4 8 0 0.15 0.01 0.43 o -3 8 0 4.95 6.14 0.93 o -2 8 0 144.37 138.23 10.11 o -1 8 0 8.78 8.39 1.66 o -6 9 0 3.34 4.79 1.30 o -5 9 0 19.30 24.10 2.30 o -4 9 0 53.95 63.87 3.85 o -3 9 0 3.43 7.45 1.29 o 3 -9 1 17.32 25.67 2.09 o 4 -9 1 3.23 3.61 0.77 o 5 -9 1 0.37 0.70 0.61 o 6 -9 1 67.49 69.72 6.07 o 1 -8 1 21.80 21.11 2.65 o 2 -8 1 1.78 1.02 0.56 o 3 -8 1 8.82 8.45 1.09 o 4 -8 1 131.26 144.58 13.98 o 5 -8 1 93.11 79.59 6.42 o 6 -8 1 0.29 0.39 0.63 o 7 -8 1 0.88 0.89 0.71 o 8 -8 1 26.94 20.61 2.68 o -1 -7 1 4.67 5.23 1.37 o 0 -7 1 9.98 7.55 1.46 o 1 -7 1 22.16 24.65 3.69 o 2 -7 1 366.71 351.45 19.19 o 3 -7 1 53.35 59.05 3.40 o 4 -7 1 14.42 15.85 1.33 o 5 -7 1 11.52 9.30 1.20 o 6 -7 1 150.16 136.13 9.90 o 7 -7 1 43.58 50.75 8.46 o 8 -7 1 2.49 1.14 0.68 o -2 -6 1 5.63 5.75 1.38 o -1 -6 1 73.11 61.69 5.29 o 0 -6 1 217.97 260.21 24.56 o 1 -6 1 150.69 177.21 8.54 o 2 -6 1 25.11 25.94 1.78 o 3 -6 1 108.72 115.93 5.37 o 4 -6 1 225.99 243.39 10.25 o 5 -6 1 0.34 0.34 0.40 o 6 -6 1 14.47 14.88 1.30 o 7 -6 1 133.87 123.54 14.48 o 8 -6 1 39.52 42.57 3.35 o -4 -5 1 0.84 1.07 0.73 o -3 -5 1 9.95 12.32 2.09 o -2 -5 1 83.23 80.06 9.28 o -1 -5 1 412.44 477.99 17.97 o 0 -5 1 82.02 97.03 4.05 o 1 -5 1 263.41 245.29 9.46 o 2 -5 1 418.06 430.78 16.21 o 3 -5 1 8.16 9.07 0.78 o 4 -5 1 131.78 150.18 6.84 o 5 -5 1 206.80 214.48 9.18 o 6 -5 1 100.88 110.65 5.06 o 7 -5 1 92.63 81.05 4.52 o 8 -5 1 19.72 22.79 1.90 o -4 -4 1 29.04 34.18 2.73 o -3 -4 1 5.15 4.41 0.87 o -2 -4 1 10.26 11.18 1.13 o -1 -4 1 1895.75 2013.26 73.85 o 0 -4 1 1153.11 1207.64 44.52 o 1 -4 1 249.09 298.65 11.25 o 2 -4 1 3.73 4.90 0.48 o 3 -4 1 854.72 817.94 32.94 o 4 -4 1 684.91 684.39 25.43 o 5 -4 1 214.22 231.73 9.78 o 6 -4 1 70.98 72.43 3.48 o 7 -4 1 343.28 328.85 24.25 o 8 -4 1 63.24 62.03 4.51 o -5 -3 1 1.65 1.34 0.64 o -4 -3 1 0.25 0.30 0.50 o -3 -3 1 235.86 247.53 11.90 o -2 -3 1 829.61 882.23 32.58 o -1 -3 1 242.92 253.45 9.62 o 0 -3 1 137.32 130.30 5.04 o 1 -3 1 5.04 11.42 0.66 o 2 -3 1 64.14 59.64 2.43 o 3 -3 1 1456.74 1535.16 56.32 o 4 -3 1 751.24 781.46 28.90 o 5 -3 1 1000.99 1016.63 41.11 o 6 -3 1 92.87 93.95 4.36 o 7 -3 1 1.06 0.92 0.50 o 8 -3 1 30.67 35.23 3.01 o -6 -2 1 9.45 11.84 1.63 o -5 -2 1 59.74 73.22 4.43 o -4 -2 1 29.92 29.29 2.02 o -3 -2 1 1.34 0.62 0.30 o -2 -2 1 1955.90 2034.90 74.68 o -1 -2 1 230.08 215.89 8.94 o 0 -2 1 1446.34 1522.48 55.74 o 1 -2 1 727.08 727.07 29.11 o 2 -2 1 3125.57 2897.57 106.01 o 3 -2 1 7536.47 7535.13 302.02 o 4 -2 1 78.93 84.64 3.41 o 5 -2 1 151.91 147.61 6.37 o 6 -2 1 60.14 62.44 3.56 o 7 -2 1 228.61 209.81 12.45 o 8 -2 1 42.30 40.49 4.31 o -7 -1 1 59.26 65.36 6.16 o -6 -1 1 3.58 4.29 0.97 o -5 -1 1 4.01 4.35 0.77 o -4 -1 1 477.37 526.88 19.69 o -3 -1 1 218.12 197.57 7.58 o -2 -1 1 24.15 24.71 1.15 o -1 -1 1 515.73 527.69 19.46 o 0 -1 1 936.89 942.94 37.61 o 1 -1 1 1212.60 1230.99 49.40 o 2 -1 1 352.05 334.51 13.61 o 3 -1 1 55.42 56.89 2.34 o 4 -1 1 116.88 104.19 4.15 o 5 -1 1 71.65 69.81 3.83 o 6 -1 1 0.25 0.32 0.44 o 7 -1 1 48.72 54.23 9.33 o -7 0 1 19.12 17.76 2.52 o -6 0 1 47.36 52.87 6.04 o -5 0 1 327.94 370.16 14.00 o -4 0 1 38.08 42.75 1.93 o -3 0 1 89.00 91.67 3.62 o -2 0 1 1494.53 1466.99 53.76 o -1 0 1 75.71 86.37 4.67 o 0 0 1 763.53 722.44 29.37 o 1 0 1 6.32 8.71 0.57 o 2 0 1 346.70 312.45 11.62 o 3 0 1 163.85 167.93 6.45 o 4 0 1 2.92 2.69 0.50 o 5 0 1 103.16 110.82 5.79 o 6 0 1 76.38 90.28 6.40 o 7 0 1 1.63 1.36 0.75 o -8 1 1 64.80 66.03 8.71 o -7 1 1 84.93 79.10 9.50 o -6 1 1 94.65 109.98 4.97 o -5 1 1 688.66 740.63 29.78 o -4 1 1 2590.14 2695.93 98.59 o -3 1 1 692.43 683.09 25.10 o -2 1 1 140.83 141.57 5.31 o -1 1 1 391.94 367.80 14.66 o 0 1 1 4044.78 3902.54 155.09 o 1 1 1 1491.61 1461.99 59.51 o 2 1 1 158.92 177.32 6.77 o 3 1 1 190.34 195.05 8.39 o 4 1 1 423.09 454.98 19.04 o 5 1 1 20.14 23.12 1.83 o 6 1 1 2.80 4.11 1.03 o -8 2 1 2.50 1.32 0.91 o -7 2 1 402.16 426.98 20.14 o -6 2 1 393.32 406.73 19.19 o -5 2 1 301.05 323.78 12.23 o -4 2 1 230.08 270.86 11.33 o -3 2 1 428.74 377.34 14.03 o -2 2 1 990.79 955.02 35.10 o -1 2 1 563.39 517.35 20.74 o 0 2 1 48.33 48.15 2.00 o 1 2 1 1651.10 1648.70 60.47 o 2 2 1 581.22 577.18 21.39 o 3 2 1 41.29 42.02 2.26 o 4 2 1 63.30 64.91 3.34 o 5 2 1 10.91 16.13 2.56 o 6 2 1 25.36 32.44 3.91 o -8 3 1 267.30 268.46 17.61 o -7 3 1 119.80 117.41 6.14 o -6 3 1 41.54 47.76 2.47 o -5 3 1 116.94 118.75 4.74 o -4 3 1 459.84 444.54 16.60 o -3 3 1 130.15 123.92 4.82 o -2 3 1 1.73 0.80 0.26 o -1 3 1 2918.35 2931.04 107.29 o 0 3 1 800.75 806.46 32.95 o 1 3 1 53.48 53.10 2.32 o 2 3 1 126.66 131.19 5.92 o 3 3 1 276.40 289.99 13.89 o 4 3 1 114.50 117.07 8.69 o 5 3 1 14.64 13.10 1.74 o -9 4 1 15.19 14.29 2.35 o -8 4 1 120.84 118.88 6.40 o -7 4 1 36.50 44.69 2.82 o -6 4 1 56.60 57.66 3.29 o -5 4 1 5.60 6.54 0.60 o -4 4 1 172.80 156.27 6.10 o -3 4 1 1298.57 1342.62 49.41 o -2 4 1 47.93 34.16 1.58 o -1 4 1 36.20 41.29 1.89 o 0 4 1 283.44 282.52 10.76 o 1 4 1 737.36 738.21 30.51 o 2 4 1 55.71 55.15 3.26 o 3 4 1 13.79 12.49 1.53 o 4 4 1 6.87 6.97 1.25 o -9 5 1 42.55 55.68 4.54 o -8 5 1 70.61 71.31 4.75 o -7 5 1 25.04 24.09 1.85 o -6 5 1 33.72 42.36 2.63 o -5 5 1 192.20 202.79 9.12 o -4 5 1 281.37 275.28 10.53 o -3 5 1 23.73 28.96 1.60 o -2 5 1 82.75 76.94 3.55 o -1 5 1 394.94 392.41 16.18 o 0 5 1 35.69 34.68 2.23 o 1 5 1 35.83 32.27 2.18 o 2 5 1 8.26 7.92 1.31 o 3 5 1 14.65 13.69 1.69 o -9 6 1 1.75 2.18 0.73 o -8 6 1 65.32 75.68 8.23 o -7 6 1 93.91 115.76 10.56 o -6 6 1 45.70 49.06 3.48 o -5 6 1 81.25 89.18 6.52 o -4 6 1 345.73 368.91 17.08 o -3 6 1 424.68 437.00 17.96 o -2 6 1 0.30 0.69 0.40 o -1 6 1 10.35 10.44 1.13 o 0 6 1 27.32 31.04 3.24 o 1 6 1 156.72 129.04 9.48 o 2 6 1 11.80 13.75 2.48 o -8 7 1 8.52 7.31 1.54 o -7 7 1 17.08 13.79 2.05 o -6 7 1 299.57 253.29 23.57 o -5 7 1 19.25 17.22 1.73 o -4 7 1 7.39 7.51 0.96 o -3 7 1 14.44 12.24 1.20 o -2 7 1 108.02 105.65 6.49 o -1 7 1 50.41 58.97 8.47 o 0 7 1 5.24 5.60 1.30 o -8 8 1 113.14 116.94 9.18 o -7 8 1 60.68 59.08 5.32 o -6 8 1 6.69 6.55 1.40 o -5 8 1 4.54 4.52 0.96 o -4 8 1 81.56 92.96 8.34 o -3 8 1 81.58 82.49 5.43 o -2 8 1 12.29 14.81 1.72 o -1 8 1 0.79 1.12 0.79 o -6 9 1 5.40 5.10 1.34 o -5 9 1 49.60 53.59 4.02 o -4 9 1 31.74 40.40 3.29 o 2 -9 2 0.30 -0.08 0.62 o 3 -9 2 0.38 0.67 0.65 o 4 -9 2 68.22 83.67 5.74 o 5 -9 2 71.95 77.71 11.17 o 6 -9 2 67.88 76.38 10.89 o 0 -8 2 10.53 8.45 1.73 o 1 -8 2 0.69 0.68 0.72 o 2 -8 2 100.28 90.69 5.74 o 3 -8 2 160.47 176.62 8.67 o 4 -8 2 40.15 43.69 5.05 o 5 -8 2 54.60 54.89 6.01 o 6 -8 2 69.53 66.04 8.56 o 7 -8 2 53.84 54.95 4.93 o -1 -7 2 11.82 8.81 1.66 o 0 -7 2 18.83 17.15 2.27 o 1 -7 2 93.18 93.84 9.32 o 2 -7 2 123.48 124.45 7.32 o 3 -7 2 101.01 105.19 5.41 o 4 -7 2 24.18 23.63 1.67 o 5 -7 2 264.82 240.70 13.65 o 6 -7 2 5.73 6.36 0.91 o 7 -7 2 24.39 29.72 4.16 o 8 -7 2 35.15 42.68 5.85 o -3 -6 2 23.67 27.16 3.19 o -2 -6 2 169.66 158.47 11.49 o -1 -6 2 13.43 10.65 1.74 o 0 -6 2 22.04 23.57 2.19 o 1 -6 2 102.47 115.41 5.23 o 2 -6 2 889.73 924.26 37.46 o 3 -6 2 304.49 316.69 13.21 o 4 -6 2 217.97 234.97 9.92 o 5 -6 2 33.37 37.02 2.69 o 6 -6 2 136.36 151.50 7.81 o 7 -6 2 98.93 103.65 7.25 o 8 -6 2 7.51 10.03 1.70 o -4 -5 2 63.66 68.96 6.25 o -3 -5 2 11.43 10.88 1.44 o -2 -5 2 0.35 0.85 0.62 o -1 -5 2 1.76 1.20 0.52 o 0 -5 2 446.68 460.90 18.95 o 1 -5 2 166.95 164.22 7.03 o 2 -5 2 94.42 106.57 4.70 o 3 -5 2 69.17 64.25 3.02 o 4 -5 2 12.77 10.92 0.82 o 5 -5 2 10.90 11.31 0.92 o 6 -5 2 12.48 18.57 1.31 o 7 -5 2 310.17 300.57 20.05 o 8 -5 2 45.18 45.96 4.22 o -5 -4 2 57.05 66.54 4.14 o -4 -4 2 11.77 13.05 1.39 o -3 -4 2 36.86 40.08 2.61 o -2 -4 2 76.76 79.57 3.76 o -1 -4 2 55.07 60.88 2.65 o 0 -4 2 589.50 642.10 23.87 o 1 -4 2 218.83 198.22 7.58 o 2 -4 2 227.07 214.61 8.16 o 3 -4 2 139.57 161.28 6.18 o 4 -4 2 10.35 8.14 0.73 o 5 -4 2 737.28 712.53 29.04 o 6 -4 2 160.25 178.51 8.26 o 7 -4 2 5.65 4.20 0.75 o 8 -4 2 7.77 7.52 1.26 o -6 -3 2 2.57 3.88 1.05 o -5 -3 2 245.61 274.83 13.34 o -4 -3 2 89.34 99.02 5.33 o -3 -3 2 1.02 1.26 0.53 o -2 -3 2 41.10 46.42 2.10 o -1 -3 2 976.25 1007.47 37.19 o 0 -3 2 1956.82 1927.06 77.60 o 1 -3 2 159.38 157.62 6.56 o 2 -3 2 151.64 150.12 5.72 o 3 -3 2 1537.11 1468.73 53.95 o 4 -3 2 330.03 302.08 12.49 o 5 -3 2 2.11 2.63 0.50 o 6 -3 2 29.68 29.12 2.03 o 7 -3 2 45.03 49.60 3.38 o 8 -3 2 23.29 22.17 2.30 o -6 -2 2 28.40 31.41 2.79 o -5 -2 2 38.05 43.81 2.79 o -4 -2 2 19.83 23.27 1.47 o -3 -2 2 195.04 194.06 8.19 o -2 -2 2 686.16 702.73 26.05 o -1 -2 2 151.28 163.01 6.20 o 0 -2 2 1056.81 1026.02 37.70 o 1 -2 2 3699.43 3542.79 141.34 o 2 -2 2 750.41 707.13 28.56 o 3 -2 2 129.97 132.29 5.66 o 4 -2 2 149.98 130.90 5.67 o 5 -2 2 12.41 10.74 1.02 o 6 -2 2 298.77 287.95 15.60 o 7 -2 2 23.30 22.45 2.80 o -7 -1 2 7.59 5.84 1.53 o -6 -1 2 78.95 80.74 12.79 o -5 -1 2 127.49 140.89 7.06 o -4 -1 2 4.83 4.68 0.59 o -3 -1 2 40.75 51.03 2.18 o -2 -1 2 2378.00 2368.70 86.89 o -1 -1 2 11215.26 10763.86 428.16 o 0 -1 2 0.75 0.85 0.18 o 1 -1 2 0.59 0.84 0.20 o 2 -1 2 478.26 426.04 17.35 o 3 -1 2 994.49 990.80 39.54 o 4 -1 2 332.61 313.83 14.88 o 5 -1 2 8.74 7.50 0.93 o 6 -1 2 328.14 313.99 15.04 o 7 -1 2 104.69 117.33 6.38 o -7 0 2 0.27 0.05 0.67 o -6 0 2 0.93 0.86 0.57 o -5 0 2 0.89 0.47 0.37 o -4 0 2 1101.28 1071.39 39.49 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156.93 139.25 10.97 o -3 1 8 22.98 20.02 1.81 o -2 1 8 48.45 59.92 5.57 o -1 1 8 408.53 461.31 21.38 o 0 1 8 72.35 82.14 7.04 o 1 1 8 8.74 9.48 1.39 o 2 1 8 12.30 13.37 1.73 o -7 2 8 80.12 76.95 6.23 o -6 2 8 179.80 156.83 11.32 o -5 2 8 20.91 14.96 1.56 o -4 2 8 3.48 3.11 0.65 o -3 2 8 321.61 377.30 20.11 o -2 2 8 372.14 405.16 25.19 o -1 2 8 2.60 3.38 0.72 o 0 2 8 15.70 16.44 1.52 o 1 2 8 98.82 79.06 6.79 o -7 3 8 0.19 -0.09 0.47 o -6 3 8 3.59 1.74 0.67 o -5 3 8 43.07 47.82 5.02 o -4 3 8 45.38 49.27 6.48 o -3 3 8 37.11 39.87 3.45 o -2 3 8 225.28 239.58 17.81 o -1 3 8 9.81 11.79 1.35 o 0 3 8 11.27 9.70 1.34 o -7 4 8 70.88 75.45 5.13 o -6 4 8 1.48 0.90 0.47 o -5 4 8 4.14 3.49 0.76 o -4 4 8 85.50 72.01 6.16 o -3 4 8 87.10 91.00 7.86 o -2 4 8 37.19 34.30 2.99 o -1 4 8 47.18 50.84 8.67 o -6 5 8 100.17 107.06 6.15 o -5 5 8 139.02 155.13 8.27 o -4 5 8 1.34 1.39 0.83 o -3 5 8 17.79 17.12 1.97 o 0 -7 9 70.91 72.05 6.76 o 1 -7 9 30.91 27.62 2.51 o 2 -7 9 31.39 27.28 3.00 o 3 -7 9 27.70 30.14 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