#------------------------------------------------------------------------------ #$Date: 2010-10-08 09:13:40 +0300 (Fri, 08 Oct 2010) $ #$Revision: 1452 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226177.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226177_Fobs loop_ _publ_author_name 'Schulz, Stefan' 'Drexler, Hans-Joachim' 'Heller, Detlef' _publ_section_title ; (+)-{1,2-Bis[(2R,5R)-2,5-dimethylphospholan-1-yl]ethane-\k^2^P,P'}(\h^4^-cycloocta-1,5-diene)rhodium(I) tetrafluoridoborate ; _journal_coeditor_code IM2198 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m721 _journal_page_last m722 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.2243 _cell_length_b 14.7707 _cell_length_c 50.1580 _exptl_crystal_F_000 3456.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file im2198Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ks1020a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 598.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5517.31 6399.53 550.31 o 4 0 0 44.61 478.31 410.01 o 6 0 0 53003.55 53797.59 1670.63 o 8 0 0 20631.64 20632.63 549.44 o 10 0 0 18235.14 17623.27 502.50 o 12 0 0 16.32 -28.66 464.78 o 1 1 0 193.09 358.96 338.95 o 2 1 0 78268.50 84143.73 872.51 o 3 1 0 244.46 269.00 287.21 o 4 1 0 67883.03 67515.93 562.89 o 5 1 0 5987.30 6140.96 272.93 o 6 1 0 18945.40 17928.69 344.13 o 7 1 0 7719.28 7788.58 303.40 o 8 1 0 192.29 352.72 283.23 o 9 1 0 1825.95 1896.86 289.32 o 10 1 0 8307.71 8184.17 323.72 o 11 1 0 1177.69 1425.03 326.90 o 12 1 0 2677.12 2544.21 369.36 o 0 2 0 3143.73 3460.55 665.38 o 1 2 0 5213.69 5271.64 428.17 o 2 2 0 605.21 430.79 359.55 o 3 2 0 18525.05 16801.53 432.01 o 4 2 0 315.24 452.04 233.20 o 5 2 0 50461.81 50151.58 465.29 o 6 2 0 1321.98 1147.98 252.69 o 7 2 0 8431.08 7891.41 286.98 o 8 2 0 557.23 658.89 281.49 o 9 2 0 4445.62 4406.89 302.34 o 10 2 0 4472.59 4742.68 330.59 o 11 2 0 5916.53 5537.78 360.09 o 12 2 0 163.68 339.55 332.96 o 1 3 0 304964.22 312289.63 2834.37 o 2 3 0 3789.14 3574.32 405.84 o 3 3 0 13052.05 12832.55 374.76 o 4 3 0 4044.81 3942.55 321.66 o 5 3 0 48994.07 48402.74 439.92 o 6 3 0 429.93 384.97 274.06 o 7 3 0 39174.14 37997.60 418.15 o 8 3 0 570.87 597.57 267.82 o 9 3 0 33588.79 34293.45 682.51 o 10 3 0 371.05 490.50 332.23 o 11 3 0 37.23 100.90 306.44 o 0 4 0 532.77 626.49 753.00 o 1 4 0 2880.20 2993.13 428.23 o 2 4 0 1541.68 1928.59 340.32 o 3 4 0 58436.55 58494.64 691.35 o 4 4 0 11276.42 11950.30 535.07 o 5 4 0 27685.32 26735.84 358.48 o 6 4 0 20.02 -25.59 237.69 o 7 4 0 1312.09 1506.78 258.05 o 8 4 0 5023.12 4354.72 341.62 o 9 4 0 5101.91 5166.07 383.40 o 10 4 0 2094.82 2387.57 319.34 o 11 4 0 2455.26 2288.68 359.17 o 1 5 0 7332.54 7416.53 406.19 o 2 5 0 18347.52 18675.32 410.41 o 3 5 0 115.78 363.33 287.31 o 4 5 0 74459.27 71624.46 794.72 o 5 5 0 3054.47 3308.28 306.76 o 6 5 0 23833.23 21969.04 391.06 o 7 5 0 253.71 126.85 282.84 o 8 5 0 1196.93 1245.93 289.40 o 9 5 0 450.34 286.82 300.31 o 10 5 0 3706.01 3473.41 346.15 o 11 5 0 511.80 607.26 331.83 o 0 6 0 231716.70 231042.33 1615.83 o 1 6 0 7672.96 7177.54 394.66 o 2 6 0 16345.02 15322.97 402.60 o 3 6 0 18499.95 17856.69 393.47 o 4 6 0 266.19 217.19 313.77 o 5 6 0 199.70 368.00 287.49 o 6 6 0 44457.49 42931.59 462.16 o 7 6 0 100.04 86.97 292.44 o 8 6 0 20440.33 20982.92 379.69 o 9 6 0 46.33 206.75 322.03 o 10 6 0 2924.04 2922.34 338.23 o 11 6 0 43.03 221.40 384.93 o 1 7 0 888.70 997.00 322.55 o 2 7 0 31892.36 30661.43 466.41 o 3 7 0 14228.85 13768.40 340.11 o 4 7 0 19464.04 19289.85 423.97 o 5 7 0 3160.91 3118.65 305.20 o 6 7 0 1654.71 1770.01 308.59 o 7 7 0 1824.14 1874.73 274.07 o 8 7 0 2100.14 2120.43 304.20 o 9 7 0 2627.56 2540.72 324.21 o 10 7 0 955.83 855.73 327.99 o 11 7 0 522.86 595.61 366.93 o 0 8 0 18871.66 19034.42 580.67 o 1 8 0 251.55 339.60 331.46 o 2 8 0 3371.55 3626.50 383.35 o 3 8 0 8181.35 8098.82 375.14 o 4 8 0 946.68 1101.66 364.40 o 5 8 0 17715.50 16788.08 406.93 o 6 8 0 1701.65 1412.65 319.76 o 7 8 0 2911.26 2574.13 300.00 o 8 8 0 0.53 21.05 268.48 o 9 8 0 395.81 396.33 320.69 o 10 8 0 0.97 -32.72 361.48 o 1 9 0 45430.93 43906.86 543.14 o 2 9 0 3615.99 3895.02 359.21 o 3 9 0 1896.38 2555.21 340.24 o 4 9 0 4966.24 4332.27 349.86 o 5 9 0 5525.96 5861.78 425.01 o 6 9 0 12.56 223.98 306.18 o 7 9 0 11804.06 12400.96 319.52 o 8 9 0 1.23 100.69 294.81 o 9 9 0 4958.38 5439.09 350.52 o 10 9 0 11.19 169.27 341.17 o 0 10 0 4222.13 4793.27 466.07 o 1 10 0 4480.37 4336.28 327.43 o 2 10 0 279.23 105.57 366.71 o 3 10 0 19743.71 19090.46 431.10 o 4 10 0 499.98 758.46 347.79 o 5 10 0 1029.59 1182.12 389.28 o 6 10 0 591.07 750.85 307.97 o 7 10 0 102.16 77.53 293.95 o 8 10 0 37.50 101.13 308.38 o 9 10 0 1017.20 844.50 365.66 o 1 11 0 10.17 75.73 347.72 o 2 11 0 1469.93 1501.10 352.01 o 3 11 0 283.17 275.54 317.36 o 4 11 0 2095.53 2260.61 356.51 o 5 11 0 1491.99 1607.82 311.00 o 6 11 0 6577.02 6895.03 389.90 o 7 11 0 966.57 841.97 311.13 o 8 11 0 520.79 361.22 320.09 o 9 11 0 109.14 167.07 338.60 o 0 12 0 11858.17 12004.67 544.62 o 1 12 0 784.48 933.51 327.42 o 2 12 0 4536.27 4771.80 352.59 o 3 12 0 2154.84 2092.41 281.51 o 4 12 0 1093.99 1188.92 318.19 o 5 12 0 833.52 758.92 327.92 o 6 12 0 2989.56 3381.21 343.67 o 7 12 0 3.83 221.64 319.76 o 8 12 0 3228.18 3360.05 354.14 o 1 13 0 64.29 240.02 346.90 o 2 13 0 1744.06 1755.88 333.16 o 3 13 0 25.00 -20.91 327.08 o 4 13 0 2507.84 2967.40 344.32 o 5 13 0 46.79 132.94 363.09 o 6 13 0 29.53 -53.74 428.27 o 7 13 0 876.48 876.01 337.59 o 8 13 0 1611.56 1428.38 360.79 o 0 14 0 1044.84 1212.52 486.07 o 1 14 0 115.17 81.60 334.13 o 2 14 0 685.84 603.17 368.16 o 3 14 0 660.63 518.09 365.47 o 4 14 0 127.07 400.73 373.07 o 5 14 0 1256.94 1617.04 396.46 o 6 14 0 544.65 506.15 441.47 o 7 14 0 428.04 515.68 369.69 o 1 15 0 3629.17 3857.12 355.57 o 2 15 0 2411.41 2192.79 361.81 o 3 15 0 8.26 -21.15 321.77 o 4 15 0 490.88 364.82 362.26 o 5 15 0 336.52 570.71 392.87 o 6 15 0 0.82 57.08 377.23 o 0 16 0 63.03 229.45 496.43 o 1 16 0 146.37 260.77 391.15 o 2 16 0 76.96 129.13 360.64 o 3 16 0 1392.49 1071.96 402.42 o 4 16 0 6.33 -61.24 370.70 o 5 16 0 1079.65 1259.40 384.98 o 1 17 0 44.07 -11.79 406.94 o 2 17 0 569.67 668.33 375.02 o 3 17 0 789.29 681.43 394.08 o 1 0 1 355.89 462.19 344.13 o 2 0 1 1010.22 1189.92 355.70 o 3 0 1 7483.60 7386.02 370.04 o 4 0 1 976.85 1278.76 292.32 o 5 0 1 16209.14 16795.30 417.91 o 6 0 1 1253.32 1223.85 314.52 o 7 0 1 7011.39 7231.37 301.76 o 8 0 1 267.68 429.30 268.69 o 9 0 1 263.69 505.29 267.54 o 10 0 1 176.20 340.19 284.21 o 11 0 1 153.34 298.71 330.29 o 12 0 1 25.24 147.27 326.60 o -12 1 1 1099.01 1069.59 331.67 o -11 1 1 277.80 565.84 324.03 o -10 1 1 5162.27 5330.27 336.27 o -9 1 1 4937.40 5340.49 303.87 o -8 1 1 3787.09 3673.64 279.74 o -7 1 1 2501.06 2124.23 325.62 o -6 1 1 5426.26 5214.27 280.34 o -5 1 1 690.35 508.00 229.98 o -4 1 1 77190.91 78337.23 676.84 o -3 1 1 6713.77 6244.32 324.23 o -2 1 1 123078.55 132042.06 965.43 o -1 1 1 7908.51 8421.66 493.68 o 0 1 1 1108.82 1480.17 459.41 o 1 1 1 7823.47 8478.79 495.55 o 2 1 1 122517.20 132034.44 1046.51 o 3 1 1 6993.81 6654.81 346.71 o 4 1 1 77040.06 78118.46 688.56 o 5 1 1 722.99 643.20 256.11 o 6 1 1 5585.71 4977.51 297.06 o 7 1 1 2401.96 2374.21 268.79 o 8 1 1 3945.34 3818.88 305.56 o 9 1 1 4904.31 5291.08 308.05 o 10 1 1 5209.42 5577.15 306.20 o 11 1 1 291.57 291.92 324.25 o 12 1 1 1038.28 1036.23 357.55 o -12 2 1 78.54 35.26 335.09 o -11 2 1 2325.92 2146.57 347.46 o -10 2 1 1031.05 1060.77 293.75 o -9 2 1 9123.12 8798.74 331.00 o -8 2 1 7705.51 7598.72 325.39 o -7 2 1 68.70 176.12 251.15 o -6 2 1 2338.32 2666.06 247.22 o -5 2 1 56446.89 56129.42 486.72 o -4 2 1 131.39 152.92 236.77 o -3 2 1 24833.49 24780.27 423.11 o -2 2 1 26151.13 27232.11 553.54 o -1 2 1 5070.12 5375.83 430.91 o 0 2 1 81333.38 86825.70 1191.07 o 1 2 1 4885.79 5123.90 471.41 o 2 2 1 25146.20 26098.30 578.31 o 3 2 1 24677.76 24631.64 455.87 o 4 2 1 108.74 165.71 235.80 o 5 2 1 56072.70 55680.75 477.41 o 6 2 1 2226.01 2476.98 263.74 o 7 2 1 75.23 39.98 257.89 o 8 2 1 8048.82 8334.62 329.76 o 9 2 1 8882.78 9494.11 326.34 o 10 2 1 1017.95 1429.10 284.18 o 11 2 1 2361.93 2334.33 336.12 o 12 2 1 85.92 234.69 356.47 o -11 3 1 54.49 154.09 306.29 o -10 3 1 1224.04 1441.11 337.45 o -9 3 1 1463.35 1346.60 325.78 o -8 3 1 4740.64 4906.65 286.46 o -7 3 1 446.65 504.06 250.36 o -6 3 1 5161.74 4993.43 272.88 o -5 3 1 3762.38 3540.89 254.08 o -4 3 1 7933.48 7867.31 340.77 o -3 3 1 154.40 54.18 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