#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/61/2226178.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226178_Fobs loop_ _publ_author_name 'Zhao, Min Min' 'Shi, Ping Ping' _publ_section_title ; Bis(4-fluoroanilinium) tetrachloridocuprate(II) ; _journal_coeditor_code IM2199 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m656 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.917 _cell_angle_gamma 90.000 _cell_length_a 15.6026 _cell_length_b 7.3893 _cell_length_c 7.1238 _exptl_crystal_F_000 430.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file im2199Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 179.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1874.97 1892.62 32.41 o 4 0 0 2481.61 2384.41 29.83 o 5 0 0 3495.61 3534.07 42.65 o 6 0 0 11139.40 10994.06 132.12 o 7 0 0 10573.75 10987.82 222.30 o 8 0 0 15307.75 16157.80 348.11 o 9 0 0 4.36 12.47 3.57 o 10 0 0 249.25 212.10 18.15 o 11 0 0 41.84 50.59 9.58 o 12 0 0 891.51 926.78 42.51 o 13 0 0 910.64 1016.36 48.72 o 14 0 0 2367.01 2441.96 98.41 o 15 0 0 158.36 196.08 22.59 o 16 0 0 15.90 14.88 13.82 o 17 0 0 49.02 75.23 20.56 o 18 0 0 4.59 12.48 15.08 o 19 0 0 4.49 13.03 16.64 o 1 1 0 31.42 24.51 1.17 o 2 1 0 32.20 25.69 1.18 o 3 1 0 99.23 129.66 2.94 o 4 1 0 1034.79 1067.78 15.38 o 5 1 0 1711.05 1746.77 18.85 o 6 1 0 1827.61 2025.15 31.03 o 7 1 0 684.12 722.82 18.76 o 8 1 0 70.08 67.68 6.32 o 9 1 0 550.43 575.73 22.67 o 10 1 0 337.10 371.72 11.60 o 11 1 0 287.34 347.37 12.44 o 12 1 0 799.34 864.06 22.11 o 13 1 0 491.56 566.24 24.55 o 14 1 0 31.38 52.32 10.18 o 15 1 0 75.25 91.98 13.09 o 16 1 0 21.30 55.61 11.41 o 17 1 0 30.48 55.34 13.53 o 18 1 0 34.82 40.28 15.07 o 19 1 0 31.05 54.23 14.78 o 0 2 0 16820.73 16508.82 140.50 o 1 2 0 132.15 105.45 10.01 o 2 2 0 13.04 10.28 1.59 o 3 2 0 5151.38 5664.34 47.30 o 4 2 0 300.10 335.42 5.83 o 5 2 0 4.00 7.67 2.88 o 6 2 0 2113.34 2062.53 24.91 o 7 2 0 2303.33 2423.48 114.73 o 8 2 0 3575.40 3771.59 45.53 o 9 2 0 3.47 25.59 7.03 o 10 2 0 35.76 31.30 8.70 o 11 2 0 271.08 264.70 13.34 o 12 2 0 1013.28 1094.19 27.80 o 13 2 0 1080.35 1203.31 35.58 o 14 2 0 1715.72 1857.54 49.53 o 15 2 0 375.60 425.78 22.97 o 16 2 0 151.36 219.14 17.81 o 17 2 0 13.79 16.39 10.09 o 18 2 0 43.61 58.18 13.88 o 19 2 0 88.89 107.49 21.53 o 1 3 0 1133.22 1178.82 15.71 o 2 3 0 1589.96 1642.79 43.72 o 3 3 0 635.45 602.22 25.88 o 4 3 0 0.77 1.93 1.69 o 5 3 0 367.19 407.54 7.90 o 6 3 0 0.53 -2.16 2.46 o 7 3 0 290.41 327.03 8.96 o 8 3 0 1402.73 1461.29 23.70 o 9 3 0 851.82 937.40 50.55 o 10 3 0 450.75 420.58 15.70 o 11 3 0 66.01 99.89 8.83 o 12 3 0 77.54 73.88 8.55 o 13 3 0 17.36 27.89 7.63 o 14 3 0 326.73 341.79 19.60 o 15 3 0 167.97 202.96 16.39 o 16 3 0 198.37 219.32 21.12 o 17 3 0 31.90 30.98 11.82 o 18 3 0 0.18 -1.30 9.25 o 0 4 0 5603.21 5640.03 171.26 o 1 4 0 5055.04 5219.11 63.35 o 2 4 0 4065.25 4281.95 58.31 o 3 4 0 13.88 6.63 3.29 o 4 4 0 1555.29 1622.03 59.53 o 5 4 0 2208.40 2271.24 38.48 o 6 4 0 2667.88 2573.65 42.99 o 7 4 0 2249.13 2204.98 44.89 o 8 4 0 1783.53 1740.19 38.31 o 9 4 0 887.14 866.57 18.53 o 10 4 0 207.09 177.72 8.40 o 11 4 0 50.35 56.15 7.85 o 12 4 0 972.92 1099.03 37.62 o 13 4 0 590.45 608.08 22.81 o 14 4 0 374.08 415.85 19.86 o 15 4 0 137.42 131.53 12.87 o 16 4 0 42.96 31.76 11.78 o 17 4 0 13.28 3.24 12.68 o 18 4 0 4.67 11.36 14.73 o 1 5 0 549.27 540.76 24.23 o 2 5 0 691.96 719.96 16.19 o 3 5 0 12.52 22.76 5.59 o 4 5 0 251.13 246.21 10.11 o 5 5 0 913.33 942.13 26.66 o 6 5 0 362.14 370.48 14.09 o 7 5 0 17.48 8.40 5.22 o 8 5 0 78.78 91.00 8.80 o 9 5 0 320.37 374.08 15.64 o 10 5 0 3.36 8.18 5.57 o 11 5 0 371.24 377.45 20.28 o 12 5 0 284.89 311.00 20.45 o 13 5 0 177.85 199.76 16.95 o 14 5 0 0.38 1.14 8.29 o 15 5 0 46.88 67.48 15.29 o 16 5 0 59.51 46.58 18.00 o 17 5 0 0.08 7.80 14.03 o 0 6 0 907.50 959.86 42.65 o 1 6 0 564.15 589.68 22.47 o 2 6 0 385.17 412.35 19.24 o 3 6 0 162.55 154.02 11.16 o 4 6 0 454.96 482.04 15.78 o 5 6 0 470.81 471.80 16.26 o 6 6 0 341.32 313.40 17.04 o 7 6 0 312.17 293.13 13.83 o 8 6 0 360.63 328.40 15.82 o 9 6 0 354.37 354.69 18.14 o 10 6 0 96.94 70.81 10.83 o 11 6 0 36.20 57.35 11.59 o 12 6 0 331.11 342.17 22.41 o 13 6 0 154.31 147.36 20.31 o 14 6 0 117.24 135.15 16.96 o 15 6 0 50.53 46.91 16.59 o 1 7 0 188.95 209.54 15.34 o 2 7 0 345.24 391.52 20.53 o 3 7 0 3.20 -4.93 6.75 o 4 7 0 104.52 115.80 12.12 o 5 7 0 242.81 263.38 16.85 o 6 7 0 170.31 187.44 21.88 o 7 7 0 2.75 7.41 7.92 o 8 7 0 56.04 51.05 9.45 o 9 7 0 165.67 174.81 16.04 o 10 7 0 4.54 -4.29 8.52 o 11 7 0 143.71 147.40 16.28 o 12 7 0 99.17 104.61 15.29 o 13 7 0 49.69 59.10 17.39 o 0 8 0 191.45 199.04 35.15 o 1 8 0 16.90 39.49 16.45 o 2 8 0 15.10 9.47 9.31 o 3 8 0 227.61 261.78 19.28 o 4 8 0 229.62 242.49 18.85 o 5 8 0 89.29 113.80 15.02 o 6 8 0 16.21 0.92 8.64 o 7 8 0 40.43 47.18 11.70 o 8 8 0 103.99 123.60 16.02 o 9 8 0 74.43 76.62 16.66 o 10 8 0 110.04 102.99 20.79 o 11 8 0 141.27 151.14 27.62 o 1 9 0 59.40 59.54 21.46 o 2 9 0 108.76 122.54 26.37 o 3 9 0 12.33 2.73 10.64 o 4 9 0 0.51 5.49 9.66 o 5 9 0 6.78 33.50 17.95 o 6 9 0 3.05 -0.79 9.06 o -20 1 1 148.68 148.47 20.78 o -19 1 1 76.91 71.01 15.34 o -18 1 1 1.25 6.26 9.27 o -17 1 1 3.78 1.02 7.44 o -16 1 1 196.91 221.27 17.91 o -15 1 1 497.69 505.62 24.94 o -14 1 1 1200.74 1189.18 31.69 o -13 1 1 227.74 271.93 19.68 o -12 1 1 318.61 317.84 25.38 o -11 1 1 43.61 49.89 7.66 o -10 1 1 131.00 202.95 11.80 o -9 1 1 637.06 643.09 14.06 o -8 1 1 1271.49 1205.65 18.93 o -7 1 1 4626.95 4834.48 56.33 o -6 1 1 3037.85 3017.75 34.58 o -5 1 1 82.85 95.37 5.39 o -4 1 1 400.19 323.85 9.56 o -3 1 1 178.74 141.79 7.37 o -2 1 1 16369.42 15648.03 90.51 o -1 1 1 1330.59 1360.50 22.34 o 0 1 1 1227.92 1274.84 29.21 o 1 1 1 13475.85 13582.38 97.59 o 2 1 1 568.37 434.06 5.03 o 3 1 1 416.02 336.09 7.84 o 4 1 1 1270.28 1039.48 16.74 o 5 1 1 4888.49 4969.30 57.30 o 6 1 1 9562.69 9326.24 110.17 o 7 1 1 1290.35 1161.48 24.54 o 8 1 1 1340.55 1193.28 23.91 o 9 1 1 635.05 709.62 44.41 o 10 1 1 128.09 105.73 6.86 o 11 1 1 612.89 654.10 24.75 o 12 1 1 1482.73 1259.12 38.35 o 13 1 1 1226.87 1272.07 41.27 o 14 1 1 695.91 700.85 29.90 o 15 1 1 441.49 434.44 23.90 o 16 1 1 1.98 3.20 8.42 o 17 1 1 1.34 14.63 10.45 o 18 1 1 99.20 108.15 17.92 o 19 1 1 245.84 256.25 25.49 o -19 2 1 15.42 5.05 10.42 o -18 2 1 0.01 11.15 11.81 o -17 2 1 26.72 30.01 11.05 o -16 2 1 128.75 118.91 14.13 o -15 2 1 10.87 23.26 7.39 o -14 2 1 95.59 70.64 8.68 o -13 2 1 53.72 67.05 10.71 o -12 2 1 164.65 145.71 9.86 o -11 2 1 231.13 196.32 15.11 o -10 2 1 174.87 185.90 7.56 o -9 2 1 92.92 101.96 9.33 o -8 2 1 373.26 369.08 9.22 o -7 2 1 34.59 55.10 5.09 o -6 2 1 880.68 816.20 13.82 o -5 2 1 161.55 151.77 4.54 o -4 2 1 1525.49 1564.64 23.96 o -3 2 1 220.94 268.13 11.17 o -2 2 1 667.53 700.89 17.25 o -1 2 1 1091.76 1170.63 90.49 o 0 2 1 4467.87 4556.20 37.19 o 1 2 1 41.63 103.74 11.88 o 2 2 1 2178.03 2276.19 24.86 o 3 2 1 349.34 399.45 17.53 o 4 2 1 15.83 20.65 3.44 o 5 2 1 53.87 107.57 4.72 o 6 2 1 61.39 49.78 3.13 o 7 2 1 197.18 199.70 14.55 o 8 2 1 392.78 349.67 13.03 o 9 2 1 2.52 18.30 8.78 o 10 2 1 7.24 1.69 5.10 o 11 2 1 151.47 157.98 10.69 o 12 2 1 15.22 15.41 5.70 o 13 2 1 44.67 54.68 9.77 o 14 2 1 6.52 2.58 7.40 o 15 2 1 16.62 18.01 9.17 o 16 2 1 1.28 1.98 8.41 o 17 2 1 24.44 26.01 11.21 o 18 2 1 49.98 57.72 16.87 o 19 2 1 34.80 36.37 14.02 o -19 3 1 146.48 131.56 23.46 o -18 3 1 38.40 49.64 14.16 o -17 3 1 48.32 84.01 13.80 o -16 3 1 393.37 383.29 23.80 o -15 3 1 703.76 714.07 27.38 o -14 3 1 1279.48 1279.43 36.83 o -13 3 1 626.26 591.58 21.42 o -12 3 1 896.44 814.45 23.79 o -11 3 1 894.86 892.67 22.10 o -10 3 1 703.57 732.59 17.11 o -9 3 1 1579.28 1526.92 28.20 o -8 3 1 2288.90 2145.16 33.20 o -7 3 1 4652.18 4438.90 63.24 o -6 3 1 3269.51 3056.52 49.40 o -5 3 1 439.66 309.69 7.23 o -4 3 1 1988.42 1898.85 22.33 o -3 3 1 1591.70 1491.68 40.79 o -2 3 1 2581.28 2419.69 26.90 o -1 3 1 3043.23 3092.09 51.16 o 0 3 1 2744.83 2614.48 31.51 o 1 3 1 551.08 612.52 22.35 o 2 3 1 628.95 671.82 14.53 o 3 3 1 440.96 492.78 17.58 o 4 3 1 16.48 18.62 3.23 o 5 3 1 829.07 929.62 22.81 o 6 3 1 1508.18 1685.93 30.52 o 7 3 1 664.09 667.36 20.54 o 8 3 1 134.65 230.09 12.59 o 9 3 1 212.46 235.08 11.36 o 10 3 1 212.39 262.62 11.94 o 11 3 1 126.39 177.56 12.13 o 12 3 1 18.28 40.55 18.77 o 13 3 1 455.58 485.53 32.59 o 14 3 1 251.89 239.98 22.11 o 15 3 1 41.38 71.50 12.65 o 16 3 1 3.35 -6.23 8.61 o 17 3 1 2.06 1.67 9.17 o 18 3 1 92.66 107.01 16.78 o -18 4 1 25.77 46.85 17.10 o -17 4 1 5.36 16.49 13.61 o -16 4 1 35.63 44.48 12.56 o -15 4 1 17.58 35.56 9.28 o -14 4 1 44.41 56.71 10.02 o -13 4 1 30.20 58.71 11.36 o -12 4 1 79.46 100.02 10.26 o -11 4 1 6.39 7.06 4.47 o -10 4 1 156.13 144.21 7.98 o -9 4 1 736.78 666.56 16.33 o -8 4 1 272.02 247.07 8.88 o -7 4 1 102.93 97.23 9.23 o -6 4 1 4.88 119.94 11.05 o -5 4 1 191.26 206.09 14.81 o -4 4 1 372.25 350.32 18.89 o -3 4 1 2281.94 2101.82 108.39 o -2 4 1 1724.96 1763.38 28.30 o -1 4 1 1503.11 1479.32 23.87 o 0 4 1 152.52 284.78 7.93 o 1 4 1 294.97 388.96 21.76 o 2 4 1 6.49 58.20 16.82 o 3 4 1 905.36 769.02 39.97 o 4 4 1 969.67 966.47 19.50 o 5 4 1 1396.36 1235.89 19.22 o 6 4 1 270.36 276.40 8.04 o 7 4 1 0.21 5.37 3.45 o 8 4 1 104.98 132.41 7.30 o 9 4 1 8.36 15.17 8.37 o 10 4 1 0.46 0.09 4.47 o 11 4 1 237.43 220.36 12.44 o 12 4 1 28.94 26.25 7.08 o 13 4 1 3.52 7.62 6.72 o 14 4 1 82.62 90.00 10.99 o 15 4 1 137.60 140.83 14.57 o 16 4 1 58.91 78.31 17.74 o 17 4 1 0.24 -10.67 13.16 o -17 5 1 0.70 -8.27 14.60 o -16 5 1 25.80 38.95 16.08 o -15 5 1 18.44 29.21 11.79 o -14 5 1 42.90 81.08 13.28 o -13 5 1 5.47 15.48 8.95 o -12 5 1 12.80 57.76 16.47 o -11 5 1 85.56 219.31 36.02 o -10 5 1 1.61 12.50 7.85 o -9 5 1 8.57 84.66 26.98 o -8 5 1 96.67 237.24 21.39 o -7 5 1 256.56 445.38 29.04 o -6 5 1 231.98 333.32 16.83 o -5 5 1 53.99 101.08 10.21 o -4 5 1 395.87 473.00 29.34 o -3 5 1 659.68 758.71 18.60 o -2 5 1 631.60 644.54 16.09 o -1 5 1 974.55 1001.34 27.31 o 0 5 1 1349.57 1285.60 28.06 o 1 5 1 773.56 764.74 22.26 o 2 5 1 1633.20 1522.69 54.44 o 3 5 1 1955.10 1894.27 33.70 o 4 5 1 943.33 861.58 21.25 o 5 5 1 1785.60 1747.87 42.76 o 6 5 1 2339.53 2196.36 43.94 o 7 5 1 1692.58 1612.20 35.60 o 8 5 1 964.68 926.31 29.67 o 9 5 1 371.51 373.88 23.66 o 10 5 1 1768.78 1772.34 50.58 o 11 5 1 846.26 805.81 31.04 o 12 5 1 307.97 297.24 20.65 o 13 5 1 735.93 687.18 44.09 o 14 5 1 451.10 418.07 26.40 o 15 5 1 212.03 247.55 25.70 o 16 5 1 82.97 120.27 27.57 o -15 6 1 48.70 59.95 14.76 o -14 6 1 0.64 26.01 13.59 o -13 6 1 145.62 158.88 21.44 o -12 6 1 82.48 126.06 14.74 o -11 6 1 4.62 -4.02 6.35 o -10 6 1 49.31 41.98 8.46 o -9 6 1 6.99 35.91 10.34 o -8 6 1 0.46 18.20 7.91 o -7 6 1 239.56 246.62 16.68 o -6 6 1 840.92 795.09 26.45 o -5 6 1 872.90 872.77 23.86 o -4 6 1 177.63 159.17 9.59 o -3 6 1 25.19 95.24 8.19 o -2 6 1 368.50 464.07 20.64 o -1 6 1 112.15 159.94 12.92 o 0 6 1 671.31 714.51 24.80 o 1 6 1 1222.18 1352.33 38.03 o 2 6 1 846.92 866.45 27.60 o 3 6 1 131.97 123.30 13.06 o 4 6 1 30.04 88.60 12.25 o 5 6 1 0.94 87.90 9.72 o 6 6 1 51.54 46.94 11.58 o 7 6 1 192.29 186.44 12.46 o 8 6 1 289.98 256.61 13.54 o 9 6 1 33.55 40.58 7.95 o 10 6 1 0.30 2.13 7.01 o 11 6 1 107.44 125.45 14.16 o 12 6 1 56.21 83.13 15.02 o 13 6 1 20.93 11.76 10.17 o 14 6 1 5.44 1.05 10.51 o 15 6 1 8.07 -2.64 11.29 o -13 7 1 227.04 188.84 19.68 o -12 7 1 393.86 384.26 25.99 o -11 7 1 691.96 632.02 38.86 o -10 7 1 522.20 473.30 22.60 o -9 7 1 381.67 383.90 19.24 o -8 7 1 385.97 354.87 18.16 o -7 7 1 537.75 506.42 24.67 o -6 7 1 616.52 540.66 26.03 o -5 7 1 603.05 539.62 26.23 o -4 7 1 547.89 544.89 23.92 o -3 7 1 632.16 683.67 56.27 o -2 7 1 614.65 654.52 27.55 o -1 7 1 82.14 93.83 11.29 o 0 7 1 52.42 60.32 17.08 o 1 7 1 269.86 329.99 19.51 o 2 7 1 224.14 247.42 16.22 o 3 7 1 121.96 164.66 13.49 o 4 7 1 43.61 66.34 10.47 o 5 7 1 44.41 99.82 22.17 o 6 7 1 28.19 53.07 11.08 o 7 7 1 9.27 43.54 18.85 o 8 7 1 1.50 31.27 14.18 o 9 7 1 18.09 22.72 14.14 o 10 7 1 44.96 88.87 18.09 o 11 7 1 9.30 3.11 8.93 o 12 7 1 6.31 13.76 13.35 o 13 7 1 0.68 33.11 19.71 o -11 8 1 13.40 7.28 14.66 o -10 8 1 14.41 13.10 13.28 o -9 8 1 88.14 87.59 14.49 o -8 8 1 118.87 144.07 16.87 o -7 8 1 47.15 30.74 11.51 o -6 8 1 9.73 16.67 11.68 o -5 8 1 18.38 25.34 9.98 o -4 8 1 205.98 196.83 17.77 o -3 8 1 322.84 384.17 23.90 o -2 8 1 208.09 249.07 19.26 o -1 8 1 286.53 343.25 22.15 o 0 8 1 97.36 132.89 15.38 o 1 8 1 52.64 63.47 12.31 o 2 8 1 62.26 77.45 12.81 o 3 8 1 119.41 129.27 14.66 o 4 8 1 247.67 258.42 19.05 o 5 8 1 172.95 151.16 15.40 o 6 8 1 40.59 60.34 21.74 o 7 8 1 5.89 10.99 12.19 o 8 8 1 5.83 -0.55 9.98 o 9 8 1 1.34 -11.67 13.21 o 10 8 1 19.71 51.59 23.09 o -6 9 1 39.22 42.54 14.03 o -5 9 1 64.47 59.64 13.92 o -4 9 1 105.65 129.05 17.14 o -3 9 1 154.12 210.91 37.78 o -2 9 1 176.14 184.09 24.79 o -1 9 1 22.43 19.81 18.05 o 0 9 1 22.82 28.73 31.86 o 1 9 1 269.10 302.04 23.59 o 2 9 1 341.46 363.94 25.67 o 3 9 1 264.93 283.38 23.25 o 4 9 1 250.29 216.70 20.93 o 5 9 1 244.38 224.11 31.72 o 6 9 1 167.81 138.53 20.51 o -20 0 2 74.72 58.20 20.94 o -19 0 2 10.77 14.04 15.97 o -18 0 2 1.69 16.62 14.28 o -17 0 2 108.92 142.18 27.94 o -16 0 2 524.63 541.09 37.99 o -15 0 2 1017.77 984.24 50.58 o -14 0 2 1158.25 1213.82 62.46 o -13 0 2 1337.56 1408.16 42.85 o -12 0 2 837.64 811.21 27.48 o -11 0 2 27.53 27.28 7.73 o -10 0 2 2.39 9.61 7.04 o -9 0 2 2101.08 1984.07 45.42 o -8 0 2 1953.34 1810.93 39.73 o -7 0 2 2072.50 1966.17 47.65 o -6 0 2 27.31 29.31 5.45 o -5 0 2 689.71 649.41 13.48 o -4 0 2 7297.00 7541.83 88.31 o -3 0 2 97.10 118.95 5.39 o -2 0 2 8.99 23.10 4.70 o -1 0 2 17241.67 16591.45 99.43 o 0 0 2 217.24 208.97 6.11 o 1 0 2 16.19 6.98 4.61 o 2 0 2 5474.22 5181.24 82.43 o 3 0 2 533.77 500.30 20.04 o 4 0 2 22.32 27.00 3.53 o 5 0 2 2311.86 1984.15 31.85 o 6 0 2 2727.29 2582.02 43.00 o 7 0 2 6139.77 5905.79 137.73 o 8 0 2 23.73 88.61 29.15 o 9 0 2 52.78 41.80 11.28 o 10 0 2 54.83 51.59 11.78 o 11 0 2 856.10 906.57 45.72 o 12 0 2 1023.31 1095.60 52.68 o 13 0 2 3216.14 3218.73 143.35 o 14 0 2 400.61 494.52 63.25 o 15 0 2 181.73 249.32 27.41 o 16 0 2 19.22 23.62 16.48 o 17 0 2 73.90 68.53 19.55 o 18 0 2 137.28 178.38 28.19 o -20 1 2 1.74 6.81 10.74 o -19 1 2 15.60 28.50 11.97 o -18 1 2 49.21 59.38 13.33 o -17 1 2 124.41 162.57 16.11 o -16 1 2 126.90 138.63 14.18 o -15 1 2 309.38 334.88 16.94 o -14 1 2 57.15 65.81 7.30 o -13 1 2 13.06 23.91 5.91 o -12 1 2 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