#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:39:19 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181183 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/62/2226206.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226206_Fobs loop_ _publ_author_name 'He, Wen-Jie' 'Pan, Xiao-Bo' 'Yao, Li-Hui' 'Yu, Bing-Ran' 'Wu, Jin-Cai' 'Tang, Ning' _publ_section_title ; Acetonitriletriaqua[3-ethoxy-1,8-(3,6,9-trioxaundecane-1,11-diyldioxy)-9H-xanthen-9-one]terbium(III) tris(perchlorate) ; _journal_coeditor_code KP2258 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m704 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.933 _cell_angle_beta 84.813 _cell_angle_gamma 77.363 _cell_length_a 10.2838 _cell_length_b 11.7932 _cell_length_c 15.4680 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7684 _cod_data_source_file kp2258Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Tb in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 304.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9153.54 9743.54 116.65 o 3 0 0 8373.63 9363.28 122.74 o 4 0 0 14351.40 14549.06 185.17 o 5 0 0 291.30 356.02 27.31 o 6 0 0 154.66 250.39 25.27 o 7 0 0 2787.83 2895.57 75.12 o 8 0 0 2416.24 2383.63 55.73 o 9 0 0 47.71 54.47 22.11 o 10 0 0 279.59 296.92 29.88 o 11 0 0 543.02 485.12 56.51 o 12 0 0 72.31 68.39 43.08 o 13 0 0 4.95 -39.95 39.95 o -12 1 0 152.38 210.66 51.49 o -11 1 0 8.81 -10.36 36.97 o -10 1 0 2026.44 1983.85 92.80 o -9 1 0 318.58 355.72 29.85 o -8 1 0 2772.37 3021.49 66.69 o -7 1 0 58.96 56.07 19.61 o -6 1 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