#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/62/2226244.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226244_Fobs loop_ _publ_author_name 'Xiao, Jing-mei' _publ_section_title ; 1-(2-Bromoethyl)-1,4-diazoniabicyclo[2.2.2]octane bromide tetrafluoroborate ; _journal_coeditor_code NK2032 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1344 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.9720 _cell_length_b 10.7818 _cell_length_c 21.1649 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file nk2032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 552.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10952.35 10917.40 196.09 o 4 0 0 115433.13 119477.20 2281.79 o 6 0 0 30832.57 31977.90 719.42 o 8 0 0 24.88 81.54 80.80 o 10 0 0 6546.95 5977.10 476.26 o 12 0 0 8437.82 8692.90 764.44 o 14 0 0 2573.59 2184.43 598.25 o 2 1 0 150.07 163.04 15.46 o 4 1 0 771.85 742.12 74.23 o 6 1 0 820.75 783.61 61.16 o 8 1 0 296.28 355.47 121.53 o 10 1 0 778.57 649.88 83.87 o 12 1 0 1.57 121.34 120.03 o 14 1 0 770.07 887.61 257.40 o 0 2 0 4939.92 5412.77 215.78 o 2 2 0 305282.16 293275.59 3172.65 o 4 2 0 46290.45 48173.31 1005.49 o 6 2 0 15661.17 15569.68 455.56 o 8 2 0 38.86 141.98 69.05 o 10 2 0 1998.97 1904.41 150.02 o 12 2 0 2676.00 2947.64 280.30 o 14 2 0 4986.37 4732.90 406.95 o 2 3 0 3197.66 2927.61 78.74 o 4 3 0 10.38 12.93 39.29 o 6 3 0 1943.31 1989.50 118.13 o 8 3 0 1138.40 1128.82 107.52 o 10 3 0 46.31 115.39 91.89 o 12 3 0 532.40 752.34 138.38 o 14 3 0 109.15 335.85 184.03 o 0 4 0 27720.18 28990.24 629.34 o 2 4 0 68121.33 70696.20 1160.58 o 4 4 0 28947.67 28844.91 488.93 o 6 4 0 1002.43 1119.72 84.14 o 8 4 0 165.82 360.67 100.18 o 10 4 0 177.26 257.63 113.76 o 12 4 0 2126.32 2184.96 195.88 o 14 4 0 881.82 1323.02 301.17 o 2 5 0 1965.35 1973.79 56.55 o 4 5 0 1270.19 1389.47 58.12 o 6 5 0 1169.72 1164.57 53.67 o 8 5 0 689.90 844.22 102.58 o 10 5 0 746.66 692.34 140.43 o 12 5 0 515.91 630.26 177.92 o 14 5 0 276.51 515.43 319.42 o 0 6 0 34172.61 35394.52 968.61 o 2 6 0 831.76 697.17 56.19 o 4 6 0 3727.07 3333.43 219.24 o 6 6 0 1026.84 855.69 75.19 o 8 6 0 753.24 705.28 93.67 o 10 6 0 484.51 598.22 180.14 o 12 6 0 320.67 390.44 166.18 o 14 6 0 161.89 109.80 193.65 o 2 7 0 4.73 22.27 37.96 o 4 7 0 549.40 678.64 179.51 o 6 7 0 1097.00 1092.17 114.49 o 8 7 0 120.06 482.45 134.88 o 10 7 0 287.18 179.61 139.70 o 12 7 0 176.19 255.06 174.41 o 0 8 0 1636.12 1722.27 131.19 o 2 8 0 106.26 172.70 74.24 o 4 8 0 47.88 611.07 182.07 o 6 8 0 204.43 141.05 73.46 o 8 8 0 140.79 311.75 146.75 o 10 8 0 110.17 89.20 147.67 o 12 8 0 47.24 45.01 150.14 o 2 9 0 13.09 30.33 67.59 o 4 9 0 29.45 -31.48 79.05 o 6 9 0 35.38 112.67 103.62 o 8 9 0 0.60 -32.00 170.32 o 10 9 0 9.38 202.19 171.65 o 0 10 0 2852.60 3091.25 363.95 o 2 10 0 2513.04 2255.30 184.67 o 4 10 0 1525.69 1896.03 194.70 o 6 10 0 44.14 121.78 135.14 o 8 10 0 15.56 65.66 137.43 o 10 10 0 229.62 321.47 244.62 o 2 11 0 239.69 307.23 140.05 o 4 11 0 37.15 151.72 106.29 o 6 11 0 692.54 814.88 201.63 o 8 11 0 57.80 109.93 156.32 o 0 12 0 1362.20 1498.86 363.30 o 2 12 0 3519.46 3067.87 317.83 o 4 12 0 286.33 441.37 179.85 o 6 12 0 208.64 268.70 190.93 o 8 12 0 75.22 -82.35 174.77 o 2 13 0 3.99 -34.25 148.04 o 4 13 0 263.48 353.34 237.10 o 0 14 0 2106.73 1770.29 433.92 o 2 1 1 3960.50 4049.16 77.15 o 3 1 1 14207.20 14641.44 190.07 o 4 1 1 27140.99 25985.25 308.97 o 5 1 1 32233.25 32135.69 356.02 o 6 1 1 20539.10 19025.79 281.29 o 7 1 1 15232.51 14819.29 212.56 o 8 1 1 16127.31 16406.49 314.85 o 9 1 1 10697.63 10348.10 230.55 o 10 1 1 7219.82 6766.39 211.52 o 11 1 1 4730.06 4882.81 225.98 o 12 1 1 2466.10 2450.82 188.80 o 13 1 1 525.64 511.68 128.21 o 14 1 1 512.46 567.63 156.39 o 15 1 1 24.34 104.10 144.83 o 0 2 1 2105.28 2441.74 46.11 o 1 2 1 9071.94 9945.78 131.25 o 2 2 1 9563.16 9973.95 127.11 o 3 2 1 1243.36 1366.34 30.00 o 4 2 1 627.80 785.42 38.16 o 5 2 1 3239.91 3337.78 69.32 o 6 2 1 3688.81 3544.07 90.83 o 7 2 1 498.71 570.25 46.85 o 8 2 1 4.93 7.72 38.14 o 9 2 1 515.31 528.12 64.53 o 10 2 1 140.29 77.56 55.52 o 11 2 1 253.34 384.87 84.75 o 12 2 1 215.16 201.90 96.15 o 13 2 1 264.50 415.36 113.61 o 14 2 1 218.93 290.87 124.83 o 15 2 1 256.72 347.26 153.68 o 1 3 1 5226.04 5236.69 72.80 o 2 3 1 6263.81 6009.33 74.02 o 3 3 1 14010.33 14256.39 150.10 o 4 3 1 10070.17 9316.54 106.75 o 5 3 1 19862.43 19975.77 336.47 o 6 3 1 9050.25 8658.03 183.95 o 7 3 1 21421.63 21485.32 430.51 o 8 3 1 8334.02 8059.58 204.73 o 9 3 1 6662.73 6262.06 190.24 o 10 3 1 5611.06 5634.96 196.11 o 11 3 1 2027.20 1908.86 126.79 o 12 3 1 1362.74 1211.59 128.50 o 13 3 1 591.85 470.11 130.99 o 14 3 1 197.39 130.59 108.31 o 15 3 1 4.73 95.68 164.40 o 0 4 1 35999.18 36318.09 555.54 o 1 4 1 14437.79 15569.01 168.49 o 2 4 1 13170.34 12941.29 134.82 o 3 4 1 51.66 95.47 18.77 o 4 4 1 18238.14 18941.80 232.15 o 5 4 1 1099.51 1053.21 32.97 o 6 4 1 626.27 495.45 40.22 o 7 4 1 2.14 93.08 37.68 o 8 4 1 167.05 326.63 61.65 o 9 4 1 1268.20 1330.01 103.22 o 10 4 1 158.91 253.91 64.57 o 11 4 1 464.75 335.18 80.32 o 12 4 1 281.59 383.66 94.51 o 13 4 1 344.77 326.17 117.51 o 14 4 1 308.62 472.83 157.39 o 1 5 1 681.70 779.55 34.39 o 2 5 1 384.18 453.78 30.35 o 3 5 1 5527.48 5570.33 119.88 o 4 5 1 1741.07 1764.42 71.72 o 5 5 1 1583.32 1395.68 66.32 o 6 5 1 4947.77 4373.26 106.65 o 7 5 1 3888.25 3600.00 110.40 o 8 5 1 1021.23 1106.03 77.93 o 9 5 1 4934.08 5032.95 179.97 o 10 5 1 120.19 298.92 93.61 o 11 5 1 862.62 984.09 115.36 o 12 5 1 212.94 183.17 96.93 o 13 5 1 220.40 339.47 150.79 o 14 5 1 41.14 53.86 145.53 o 0 6 1 14360.97 14969.41 308.34 o 1 6 1 2540.80 2555.72 61.34 o 2 6 1 14961.81 14067.17 189.65 o 3 6 1 10086.31 10420.54 196.73 o 4 6 1 5390.84 4996.65 109.51 o 5 6 1 11.07 42.22 29.39 o 6 6 1 2824.84 2726.29 78.66 o 7 6 1 64.39 33.38 45.87 o 8 6 1 731.73 633.15 75.42 o 9 6 1 82.61 171.64 81.23 o 10 6 1 150.51 317.03 100.05 o 11 6 1 988.79 900.20 131.27 o 12 6 1 548.42 458.04 121.30 o 13 6 1 333.60 373.28 150.44 o 14 6 1 309.43 95.41 141.48 o 1 7 1 2.08 23.13 39.31 o 2 7 1 241.14 244.00 36.25 o 3 7 1 31.32 37.90 54.37 o 4 7 1 954.03 955.41 71.93 o 5 7 1 1409.19 1329.62 82.69 o 6 7 1 451.82 412.41 55.65 o 7 7 1 351.80 372.80 105.99 o 8 7 1 0.62 128.41 82.60 o 9 7 1 55.39 -5.82 79.11 o 10 7 1 1.09 -31.60 86.58 o 11 7 1 201.15 306.59 113.69 o 12 7 1 3.07 -108.89 108.89 o 13 7 1 243.57 33.88 151.45 o 0 8 1 4891.84 4623.48 155.58 o 1 8 1 6425.26 6240.21 135.38 o 2 8 1 6291.56 6443.61 151.63 o 3 8 1 3387.90 3416.23 134.89 o 4 8 1 2037.04 2085.89 107.39 o 5 8 1 1129.51 1261.21 94.39 o 6 8 1 806.53 888.10 78.92 o 7 8 1 167.23 240.43 94.85 o 8 8 1 1.15 76.04 85.54 o 9 8 1 233.69 337.25 134.50 o 10 8 1 88.58 104.03 103.03 o 11 8 1 460.65 308.23 130.05 o 12 8 1 27.72 120.92 125.24 o 1 9 1 80.27 180.95 44.73 o 2 9 1 603.98 683.65 76.12 o 3 9 1 27.72 58.49 59.85 o 4 9 1 84.38 145.35 64.17 o 5 9 1 79.32 4.01 97.45 o 6 9 1 832.20 923.65 92.61 o 7 9 1 40.35 3.41 77.87 o 8 9 1 825.12 1045.38 147.58 o 9 9 1 21.29 93.68 103.21 o 10 9 1 286.37 248.74 121.24 o 11 9 1 109.95 249.66 135.60 o 0 10 1 1099.62 1207.45 160.15 o 1 10 1 2537.60 2520.43 130.31 o 2 10 1 378.31 425.69 77.43 o 3 10 1 1336.50 1136.65 98.74 o 4 10 1 743.62 909.36 98.82 o 5 10 1 532.06 683.89 101.77 o 6 10 1 125.54 88.09 89.68 o 7 10 1 51.10 156.23 116.84 o 8 10 1 14.12 45.19 98.43 o 9 10 1 73.70 60.95 104.34 o 10 10 1 0.64 102.78 119.29 o 1 11 1 13.27 -4.52 109.73 o 2 11 1 688.30 973.53 121.38 o 3 11 1 74.95 3.98 65.01 o 4 11 1 362.29 227.54 89.99 o 5 11 1 262.69 174.71 79.12 o 6 11 1 694.85 1068.32 151.18 o 7 11 1 44.79 -51.33 101.43 o 8 11 1 753.85 834.84 171.19 o 9 11 1 64.34 26.70 141.28 o 0 12 1 112.65 21.29 184.58 o 1 12 1 862.85 976.91 156.68 o 2 12 1 19.16 -9.72 86.68 o 3 12 1 208.67 323.89 169.65 o 4 12 1 0.17 30.41 88.64 o 5 12 1 195.55 -3.03 115.06 o 6 12 1 0.48 222.42 135.07 o 7 12 1 81.90 79.62 163.61 o 1 13 1 79.06 75.66 116.02 o 2 13 1 2.47 -119.46 119.46 o 3 13 1 209.64 156.75 129.52 o 4 13 1 531.52 614.65 207.84 o 5 13 1 103.18 39.52 131.96 o 2 0 2 0.29 99.83 18.97 o 3 0 2 30712.04 32165.20 367.58 o 4 0 2 2005.40 1838.46 46.93 o 5 0 2 14810.12 16021.23 258.01 o 6 0 2 714.79 673.18 42.97 o 7 0 2 1493.89 1504.78 63.68 o 8 0 2 1203.43 1193.84 58.45 o 9 0 2 211.02 220.70 37.36 o 10 0 2 1072.28 1262.01 158.96 o 11 0 2 362.53 249.55 125.66 o 12 0 2 2.80 171.21 143.22 o 13 0 2 265.94 137.97 156.98 o 14 0 2 139.32 234.70 170.30 o 15 0 2 1219.92 1411.04 288.56 o 1 1 2 4105.47 3181.09 45.87 o 2 1 2 2519.03 2417.19 47.42 o 3 1 2 3742.92 3799.04 45.48 o 4 1 2 2308.58 2346.07 58.37 o 5 1 2 2990.36 2907.86 42.21 o 6 1 2 4740.79 4609.87 64.94 o 7 1 2 337.23 357.88 37.76 o 8 1 2 1010.54 940.52 51.27 o 9 1 2 1120.45 1256.19 72.93 o 10 1 2 240.17 326.90 61.36 o 11 1 2 49.79 100.90 75.97 o 12 1 2 924.40 1137.13 137.17 o 13 1 2 68.81 70.60 96.48 o 14 1 2 8.67 -116.56 134.74 o 15 1 2 12.14 37.43 155.00 o 0 2 2 89.75 159.58 15.39 o 1 2 2 27302.51 28022.46 265.19 o 2 2 2 380.41 462.29 13.11 o 3 2 2 4898.57 5268.85 79.95 o 4 2 2 0.49 84.10 19.40 o 5 2 2 18.84 81.63 36.11 o 6 2 2 839.42 859.81 47.57 o 7 2 2 1918.49 1912.30 73.25 o 8 2 2 227.63 311.49 63.50 o 9 2 2 449.94 326.52 54.97 o 10 2 2 183.25 345.52 59.60 o 11 2 2 369.21 408.81 70.03 o 12 2 2 188.18 265.46 96.34 o 13 2 2 114.71 74.89 96.25 o 14 2 2 3.77 54.54 110.93 o 15 2 2 7.48 -122.01 134.97 o 1 3 2 5013.04 5143.21 72.57 o 2 3 2 9233.04 9254.56 192.18 o 3 3 2 394.43 425.00 27.57 o 4 3 2 22488.11 23426.05 332.61 o 5 3 2 738.50 861.46 35.48 o 6 3 2 17832.03 17610.96 249.49 o 7 3 2 1242.66 1256.76 76.01 o 8 3 2 10348.44 10317.47 245.74 o 9 3 2 96.92 116.94 53.08 o 10 3 2 8873.85 8692.17 267.32 o 11 3 2 194.04 162.28 68.78 o 12 3 2 773.30 856.71 137.85 o 13 3 2 139.98 174.51 98.25 o 14 3 2 175.78 161.61 112.06 o 15 3 2 39.49 93.24 164.05 o 0 4 2 285.81 251.30 26.76 o 1 4 2 2006.65 2073.29 50.45 o 2 4 2 896.26 852.64 38.37 o 3 4 2 38.03 102.07 19.80 o 4 4 2 714.05 699.62 28.10 o 5 4 2 1102.84 976.56 38.66 o 6 4 2 15.27 28.92 22.78 o 7 4 2 1243.89 1182.04 76.96 o 8 4 2 0.21 19.40 51.17 o 9 4 2 267.58 477.69 78.66 o 10 4 2 2.44 -7.31 77.42 o 11 4 2 71.95 67.06 67.73 o 12 4 2 63.67 -45.35 71.05 o 13 4 2 302.39 469.72 134.45 o 14 4 2 44.31 154.78 147.56 o 1 5 2 48.61 92.53 25.53 o 2 5 2 10452.42 11149.01 179.78 o 3 5 2 33.57 83.44 30.64 o 4 5 2 28516.75 28862.93 450.25 o 5 5 2 62.96 63.50 20.49 o 6 5 2 25136.15 23856.66 396.60 o 7 5 2 554.21 539.29 57.34 o 8 5 2 24933.44 23994.95 519.69 o 9 5 2 114.15 198.60 109.05 o 10 5 2 7088.41 6622.65 248.51 o 11 5 2 67.01 44.58 79.89 o 12 5 2 2605.96 2608.76 186.14 o 13 5 2 182.89 189.70 151.32 o 14 5 2 236.36 319.79 180.08 o 0 6 2 4108.76 4163.97 116.16 o 1 6 2 158.90 159.41 33.74 o 2 6 2 2594.47 2118.92 68.72 o 3 6 2 1058.45 1063.14 63.00 o 4 6 2 2107.71 1918.22 70.37 o 5 6 2 1536.47 1539.44 64.89 o 6 6 2 516.51 520.99 77.27 o 7 6 2 2540.96 2521.20 122.87 o 8 6 2 73.40 225.14 67.69 o 9 6 2 818.74 913.50 103.98 o 10 6 2 3.27 67.67 69.01 o 11 6 2 288.54 437.89 111.71 o 12 6 2 56.15 288.27 112.32 o 13 6 2 1.36 109.19 124.75 o 14 6 2 57.10 477.07 264.68 o 1 7 2 1.53 11.03 31.03 o 2 7 2 6668.41 6296.59 150.59 o 3 7 2 162.35 211.80 39.06 o 4 7 2 12769.41 12626.29 284.67 o 5 7 2 889.35 908.04 75.38 o 6 7 2 24752.38 24140.53 514.87 o 7 7 2 900.62 848.44 107.79 o 8 7 2 11462.34 11809.74 426.88 o 9 7 2 701.88 583.34 115.65 o 10 7 2 5754.23 5854.98 302.33 o 11 7 2 74.57 160.98 102.47 o 12 7 2 1795.85 1761.58 194.96 o 13 7 2 1.96 -24.51 161.31 o 0 8 2 3274.19 2745.35 145.56 o 1 8 2 13.51 38.68 44.53 o 2 8 2 3529.62 3499.97 106.85 o 3 8 2 125.78 158.71 46.12 o 4 8 2 1244.16 1263.14 90.14 o 5 8 2 1247.06 1410.96 137.19 o 6 8 2 1056.33 868.43 100.51 o 7 8 2 809.08 844.84 130.99 o 8 8 2 346.15 330.66 109.32 o 9 8 2 276.74 383.76 111.26 o 10 8 2 0.55 43.66 90.59 o 11 8 2 28.82 98.46 112.05 o 12 8 2 13.79 284.89 148.84 o 1 9 2 696.40 753.28 64.58 o 2 9 2 2601.69 2503.58 106.24 o 3 9 2 368.64 406.71 69.82 o 4 9 2 6302.81 6736.56 229.42 o 5 9 2 78.24 330.80 72.47 o 6 9 2 5161.12 5125.43 230.19 o 7 9 2 115.81 314.35 115.13 o 8 9 2 6273.91 6369.21 336.32 o 9 9 2 0.02 151.17 106.68 o 10 9 2 2661.14 3121.98 298.73 o 11 9 2 15.97 66.01 121.57 o 0 10 2 1694.85 1636.07 150.83 o 1 10 2 180.14 118.87 78.19 o 2 10 2 847.53 899.68 89.11 o 3 10 2 859.79 974.72 99.19 o 4 10 2 1291.71 1215.00 111.54 o 5 10 2 14.77 51.87 85.78 o 6 10 2 705.81 983.48 149.24 o 7 10 2 0.93 131.29 106.83 o 8 10 2 135.39 68.88 101.54 o 9 10 2 3.16 163.84 124.55 o 10 10 2 89.14 -9.56 102.79 o 1 11 2 245.10 453.20 117.46 o 2 11 2 265.86 599.47 149.57 o 3 11 2 91.65 95.27 73.36 o 4 11 2 1341.44 1401.22 120.65 o 5 11 2 37.62 54.05 70.68 o 6 11 2 2231.97 2565.78 218.82 o 7 11 2 1.30 -74.94 111.27 o 8 11 2 1033.44 1505.49 200.52 o 9 11 2 58.61 184.37 147.65 o 0 12 2 409.18 447.36 179.07 o 1 12 2 146.80 154.54 114.10 o 2 12 2 487.88 325.10 118.97 o 3 12 2 85.77 147.78 105.73 o 4 12 2 310.77 203.81 115.09 o 5 12 2 33.92 133.98 113.51 o 6 12 2 169.79 107.63 135.66 o 7 12 2 17.68 18.20 123.46 o 1 13 2 70.02 242.06 159.06 o 2 13 2 13.52 -67.00 114.26 o 3 13 2 152.33 32.70 94.21 o 4 13 2 268.17 489.27 194.04 o 5 13 2 20.96 160.59 166.85 o 1 1 3 203.16 289.86 13.68 o 2 1 3 3329.30 3526.72 68.17 o 3 1 3 6780.25 6968.23 86.12 o 4 1 3 4240.19 4169.58 60.86 o 5 1 3 7725.95 7869.42 105.81 o 6 1 3 7929.39 7583.27 106.09 o 7 1 3 4666.92 4538.98 83.03 o 8 1 3 6694.10 6147.05 164.00 o 9 1 3 2396.97 2474.32 102.95 o 10 1 3 1779.69 1850.91 91.70 o 11 1 3 212.04 125.68 79.77 o 12 1 3 1465.98 1555.90 146.37 o 13 1 3 8.04 88.91 94.35 o 14 1 3 397.60 385.12 138.34 o 15 1 3 12.97 -109.01 130.43 o 0 2 3 45418.68 47757.03 615.05 o 1 2 3 5811.55 6661.36 123.54 o 2 2 3 22491.49 22338.30 251.62 o 3 2 3 38034.89 38079.18 446.62 o 4 2 3 1982.54 2122.22 38.13 o 5 2 3 161.78 120.21 18.44 o 6 2 3 859.64 948.73 48.93 o 7 2 3 529.96 539.50 33.32 o 8 2 3 903.04 982.08 71.56 o 9 2 3 745.08 854.76 72.97 o 10 2 3 2526.77 2324.57 116.40 o 11 2 3 331.15 306.43 77.39 o 12 2 3 226.78 250.38 105.68 o 13 2 3 252.25 205.27 104.26 o 14 2 3 280.80 562.40 140.18 o 15 2 3 175.04 375.97 149.97 o 1 3 3 393.92 454.82 31.83 o 2 3 3 1282.55 1155.64 48.76 o 3 3 3 3143.71 3274.60 56.69 o 4 3 3 463.88 356.80 22.44 o 5 3 3 3804.01 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24 6.96 164.39 157.47 o 4 5 24 11.77 156.00 148.54 o 5 5 24 2.49 36.54 124.60 o 0 6 24 436.82 342.91 265.72 o 1 6 24 6.56 24.99 137.01 o 2 6 24 228.90 312.85 184.98 o 3 6 24 32.77 155.50 156.81 o 1 1 25 235.26 383.90 160.53 o 2 1 25 16.31 19.63 117.50 o 3 1 25 384.79 391.95 161.78 o 4 1 25 181.09 227.70 143.48 o 5 1 25 809.82 981.33 201.41 o 6 1 25 91.30 -39.85 137.67 o 0 2 25 43.46 -108.28 168.81 o 1 2 25 3.84 263.51 140.68 o 2 2 25 211.70 265.13 142.29 o 3 2 25 1.49 -17.32 116.28 o 4 2 25 48.90 140.34 136.64 o 5 2 25 20.53 85.14 134.10 o 6 2 25 22.66 -134.31 165.20 o 1 3 25 28.80 233.57 134.27 o 2 3 25 93.46 300.39 150.19 o 3 3 25 348.28 358.22 149.30 o 4 3 25 45.04 53.77 146.66 o 5 3 25 273.80 209.12 156.61 o 0 4 25 777.95 632.00 255.01 o 1 4 25 11.93 375.96 167.46 o 2 4 25 370.26 351.53 157.34 o 3 4 25 0.13 -78.15 143.13 o 4 4 25 469.07 526.86 187.00 o 1 5 25 56.04 118.79 149.64 o 2 5 25 15.45 161.12 160.68 o 3 5 25 7.53 -51.12 128.75 o 0 0 26 10.38 80.70 311.38 o 1 0 26 10.27 176.10 288.99 o 2 0 26 119.72 61.86 183.77 o 3 0 26 148.48 215.59 201.28 o 4 0 26 1.63 168.84 231.10 o 5 0 26 31.67 -53.11 189.47 o 1 1 26 552.60 350.69 160.13 o 2 1 26 10.17 224.41 148.42 o 3 1 26 13.06 -28.37 122.05 o 4 1 26 28.69 127.96 153.44 o 0 2 26 245.96 345.44 224.05 o 1 2 26 80.34 214.81 153.39 o 2 2 26 21.68 103.56 144.22 o 3 2 26 1.29 35.52 133.40 o 4 2 26 84.39 275.08 167.04 o 1 3 26 9.37 274.95 194.53 o 2 3 26 300.43 439.78 170.16 o 3 3 26 38.73 171.19 158.11 o 0 4 26 51.72 375.12 402.41 o 1 4 26 1.17 13.07 139.95 o 2 4 26 103.72 64.29 138.06 o 1 1 27 57.97 78.81 145.83 o 2 1 27 26.41 -151.41 151.41 o 0 2 27 4.20 108.91 212.38 o 1 2 27 98.64 -58.76 127.50 o