#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/62/2226276.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226276_Fobs loop_ _publ_author_name 'Vikneswaran, M. R.' 'Teoh, Siang Guan' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; Ferrocene-1-carbaldehyde 4-ethylthiosemicarbazone ; _journal_coeditor_code RZ2450 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m697 _journal_page_last m698 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 77.975 _cell_angle_beta 83.807 _cell_angle_gamma 78.076 _cell_length_a 7.4432 _cell_length_b 10.6906 _cell_length_c 18.4616 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.7087 _[local]_cod_data_source_file rz2450Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fe1dam in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 161.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 86.63 91.26 2.94 o 2 0 0 4837.85 4977.10 71.87 o 3 0 0 243.28 311.51 7.70 o 4 0 0 1.28 3.99 3.92 o 5 0 0 986.15 1057.00 21.57 o 6 0 0 7.44 14.31 7.50 o 7 0 0 1562.09 1424.29 34.15 o 8 0 0 2.49 38.16 10.10 o 9 0 0 332.43 325.17 30.61 o 10 0 0 3.28 30.53 16.79 o -10 1 0 450.64 469.03 35.12 o -9 1 0 3.42 34.22 13.69 o -8 1 0 650.91 613.26 26.49 o -7 1 0 52.72 102.05 11.76 o -6 1 0 2.07 31.29 12.62 o -5 1 0 443.88 386.89 11.86 o -4 1 0 439.88 363.40 11.62 o -3 1 0 3810.72 3766.17 59.22 o -2 1 0 117.35 114.01 4.56 o -1 1 0 1432.50 1845.92 31.52 o 0 1 0 19.06 -3.71 3.71 o 1 1 0 921.49 1253.62 25.27 o 2 1 0 1093.96 1119.18 19.46 o 3 1 0 6000.19 5867.58 85.54 o 4 1 0 989.37 1064.03 20.38 o 5 1 0 1000.89 1129.17 48.41 o 6 1 0 2.72 8.56 7.10 o 7 1 0 453.70 467.62 21.17 o 8 1 0 1770.50 1710.04 40.67 o 9 1 0 70.44 98.47 14.29 o 10 1 0 573.64 556.40 31.53 o -9 2 0 113.73 147.84 33.32 o -8 2 0 40.19 45.58 13.12 o -7 2 0 972.76 890.13 25.36 o -6 2 0 123.94 137.58 11.02 o -5 2 0 173.20 148.80 12.50 o -4 2 0 129.41 214.44 8.68 o -3 2 0 25.70 62.41 4.92 o -2 2 0 2641.17 2325.27 39.47 o -1 2 0 2289.28 3153.38 80.81 o 0 2 0 26008.59 26174.66 663.99 o 1 2 0 5339.17 6062.40 99.72 o 2 2 0 123.39 188.63 6.76 o 3 2 0 57.05 56.87 4.17 o 4 2 0 1.29 0.67 4.31 o 5 2 0 1174.61 1177.65 23.49 o 6 2 0 6.28 -2.92 6.31 o 7 2 0 401.83 455.71 15.80 o 8 2 0 25.82 14.98 8.63 o 9 2 0 574.01 520.37 23.29 o 10 2 0 122.99 148.81 21.70 o -9 3 0 93.24 88.98 20.16 o -8 3 0 4.92 112.77 20.69 o -7 3 0 263.25 285.11 18.72 o -6 3 0 37.64 52.50 9.04 o -5 3 0 543.81 640.09 18.35 o -4 3 0 54.90 71.43 7.09 o -3 3 0 594.80 500.45 13.38 o -2 3 0 1864.89 1910.92 31.46 o -1 3 0 284.09 294.96 9.96 o 0 3 0 1116.14 904.05 22.48 o 1 3 0 3957.14 4071.81 63.56 o 2 3 0 786.15 727.02 14.15 o 3 3 0 850.02 818.39 15.28 o 4 3 0 3809.27 3869.32 63.28 o 5 3 0 15.03 34.19 8.92 o 6 3 0 256.30 279.62 12.64 o 7 3 0 170.83 181.82 12.55 o 8 3 0 365.29 404.61 18.34 o 9 3 0 368.24 357.93 23.88 o 10 3 0 12.62 36.09 30.89 o -9 4 0 53.34 97.84 24.14 o -8 4 0 224.42 230.80 24.59 o -7 4 0 10.50 9.04 13.83 o -6 4 0 295.08 316.85 19.97 o -5 4 0 291.42 283.66 22.75 o -4 4 0 4.70 9.42 6.01 o -3 4 0 176.20 345.62 11.06 o -2 4 0 1642.08 1531.73 30.79 o -1 4 0 2516.44 2346.14 44.78 o 0 4 0 48.48 25.99 5.23 o 1 4 0 7542.71 7799.38 128.39 o 2 4 0 113.96 163.59 7.35 o 3 4 0 11.81 25.54 3.84 o 4 4 0 65.17 102.69 6.45 o 5 4 0 33.24 18.80 6.41 o 6 4 0 430.90 459.03 14.11 o 7 4 0 223.30 260.69 14.20 o 8 4 0 191.87 281.02 24.03 o 9 4 0 91.01 42.49 15.88 o 10 4 0 323.02 321.75 27.55 o -8 5 0 1.68 43.02 16.41 o -7 5 0 105.91 106.41 17.68 o -6 5 0 6.97 12.06 9.79 o -5 5 0 128.54 116.54 12.41 o -4 5 0 1178.13 944.33 26.81 o -3 5 0 356.37 330.55 10.51 o -2 5 0 2209.91 2281.10 44.39 o -1 5 0 2064.29 2282.70 65.03 o 0 5 0 1314.92 1212.92 45.29 o 1 5 0 36.00 55.73 5.04 o 2 5 0 1468.54 1163.80 23.02 o 3 5 0 2609.02 2819.01 50.45 o 4 5 0 4207.57 4263.79 69.68 o 5 5 0 1723.64 1770.64 35.42 o 6 5 0 235.47 340.54 26.92 o 7 5 0 877.71 813.12 25.76 o 8 5 0 43.74 45.31 12.60 o 9 5 0 608.38 555.16 30.34 o 10 5 0 20.50 45.10 21.99 o -8 6 0 305.20 393.50 45.94 o -7 6 0 65.02 34.77 19.49 o -6 6 0 1169.49 1127.52 43.91 o -5 6 0 64.38 41.65 10.82 o -4 6 0 20.96 48.50 10.04 o -3 6 0 91.82 80.95 6.19 o -2 6 0 306.30 390.64 13.84 o -1 6 0 9135.01 10427.45 315.66 o 0 6 0 502.86 517.58 15.40 o 1 6 0 4253.02 4276.21 68.13 o 2 6 0 1368.61 1619.37 30.67 o 3 6 0 702.76 647.72 16.12 o 4 6 0 234.64 210.82 11.31 o 5 6 0 136.24 198.68 13.00 o 6 6 0 968.29 902.54 24.44 o 7 6 0 193.18 224.19 17.81 o 8 6 0 83.54 153.44 17.94 o 9 6 0 485.18 542.80 30.69 o 10 6 0 183.56 245.46 46.29 o -8 7 0 6.62 30.68 26.90 o -7 7 0 0.02 33.06 18.89 o -6 7 0 11.43 37.32 21.01 o -5 7 0 416.85 381.09 24.81 o -4 7 0 1023.80 951.69 30.11 o -3 7 0 219.04 240.88 8.87 o -2 7 0 366.16 301.95 11.66 o -1 7 0 45.08 29.65 5.92 o 0 7 0 2305.52 2175.40 39.69 o 1 7 0 10.82 29.30 4.32 o 2 7 0 4441.48 3870.34 73.37 o 3 7 0 179.14 215.93 16.20 o 4 7 0 2456.15 2225.42 51.01 o 5 7 0 27.02 51.39 9.02 o 7 7 0 1454.93 1262.27 40.17 o 8 7 0 0.95 15.67 12.49 o 9 7 0 649.14 625.78 29.32 o -7 8 0 60.79 48.10 32.38 o -6 8 0 63.24 76.20 46.21 o -5 8 0 59.55 60.89 20.25 o -4 8 0 9.13 16.78 11.47 o -3 8 0 666.10 743.78 25.67 o -2 8 0 243.98 529.39 30.52 o -1 8 0 2278.64 2135.65 44.67 o 0 8 0 4.04 6.13 4.74 o 1 8 0 125.94 102.00 7.08 o 2 8 0 16.73 30.09 7.26 o 3 8 0 38.21 54.19 8.54 o 4 8 0 3006.34 2555.95 65.64 o 5 8 0 3.08 -1.85 8.41 o 6 8 0 296.45 255.26 18.97 o 7 8 0 56.93 77.12 13.74 o 8 8 0 223.27 210.47 19.22 o 9 8 0 42.93 58.20 14.88 o -6 9 0 76.06 52.78 21.82 o -5 9 0 34.09 44.45 21.83 o -4 9 0 298.27 358.46 47.55 o -3 9 0 60.23 88.34 20.69 o -2 9 0 39.20 20.98 9.92 o -1 9 0 203.69 253.13 13.45 o 0 9 0 3257.20 3246.83 69.73 o 1 9 0 508.98 558.82 24.69 o 2 9 0 2164.83 2087.42 48.59 o 3 9 0 713.56 645.07 21.42 o 4 9 0 96.00 81.65 11.56 o 5 9 0 5.75 14.85 8.96 o 6 9 0 51.35 75.84 13.44 o 7 9 0 868.74 906.71 33.42 o 8 9 0 166.49 163.42 18.34 o 9 9 0 76.90 30.73 21.77 o -6 10 0 46.60 123.05 41.42 o -5 10 0 228.19 237.61 44.73 o -4 10 0 102.42 191.90 38.81 o -3 10 0 56.76 126.58 19.64 o -2 10 0 859.36 899.55 38.25 o -1 10 0 51.37 68.26 13.86 o 0 10 0 954.34 881.02 29.22 o 1 10 0 751.62 718.19 22.64 o 2 10 0 34.03 26.13 8.24 o 3 10 0 14.87 39.45 10.02 o 4 10 0 860.44 851.75 30.56 o 5 10 0 3.38 -1.61 10.21 o 6 10 0 52.23 103.24 16.19 o 7 10 0 106.03 105.43 24.05 o 8 10 0 141.28 178.92 18.42 o -5 11 0 51.90 132.41 28.32 o -4 11 0 79.62 107.45 26.56 o -3 11 0 637.80 659.66 45.70 o -2 11 0 73.02 138.87 25.71 o -1 11 0 56.62 33.88 18.26 o 0 11 0 4.60 10.97 10.76 o 1 11 0 692.95 870.82 37.14 o 2 11 0 142.33 143.27 22.04 o 3 11 0 748.28 617.77 33.85 o 4 11 0 169.60 216.11 27.07 o 5 11 0 496.14 468.54 35.73 o 6 11 0 4.51 23.80 26.65 o 7 11 0 32.05 74.21 19.54 o 8 11 0 311.23 349.82 37.45 o -4 12 0 23.42 30.07 34.25 o -3 12 0 49.07 65.42 25.48 o -2 12 0 531.85 549.93 45.05 o -1 12 0 48.77 162.50 42.12 o 0 12 0 898.36 832.28 47.97 o 1 12 0 221.97 223.15 26.95 o 2 12 0 44.54 50.41 16.75 o 3 12 0 95.16 132.51 23.70 o 4 12 0 301.93 382.90 33.67 o 5 12 0 667.53 745.72 35.92 o 6 12 0 30.52 66.59 16.17 o 7 12 0 10.69 17.64 18.15 o -3 13 0 110.51 150.21 32.23 o -2 13 0 111.05 91.95 27.59 o -1 13 0 149.69 175.85 43.85 o 0 13 0 437.32 442.92 60.45 o 1 13 0 592.46 707.87 67.73 o 2 13 0 478.96 515.26 39.08 o 3 13 0 925.17 898.53 51.59 o 4 13 0 535.66 452.09 37.35 o 5 13 0 77.29 57.33 21.83 o 6 13 0 59.96 125.25 39.89 o -1 14 0 19.70 -9.63 30.56 o 0 14 0 42.07 108.11 41.03 o 1 14 0 12.00 37.25 28.90 o 2 14 0 78.83 57.62 34.96 o 3 14 0 737.22 764.75 48.68 o 4 14 0 120.66 153.56 28.08 o 5 14 0 1144.63 1063.29 87.59 o -4 -14 1 25.94 144.04 27.47 o -3 -14 1 700.40 643.07 44.82 o -2 -14 1 149.59 221.55 51.13 o -1 -14 1 87.46 251.67 50.83 o 0 -14 1 9.84 -16.49 30.38 o 1 -14 1 70.30 60.89 37.77 o -6 -13 1 468.12 426.40 38.09 o -5 -13 1 480.20 550.26 41.08 o -4 -13 1 233.85 270.74 41.38 o -3 -13 1 162.19 298.63 34.30 o -2 -13 1 48.08 92.99 20.33 o -1 -13 1 99.44 81.66 35.10 o 0 -13 1 3.44 82.20 35.07 o 1 -13 1 320.93 366.99 57.76 o 2 -13 1 42.35 99.63 38.58 o -7 -12 1 0.93 4.83 33.41 o -6 -12 1 209.98 228.30 24.17 o -5 -12 1 413.99 368.94 26.42 o -4 -12 1 23.33 27.79 12.85 o -3 -12 1 613.00 540.74 37.51 o -2 -12 1 347.07 376.88 32.17 o -1 -12 1 2.87 -5.47 13.18 o 0 -12 1 102.30 131.87 37.23 o 1 -12 1 37.85 13.87 21.19 o 2 -12 1 77.22 93.04 25.91 o 3 -12 1 215.82 252.42 33.54 o 4 -12 1 1.95 3.06 30.63 o -8 -11 1 196.45 208.98 33.85 o -7 -11 1 90.50 102.40 18.82 o -6 -11 1 1.31 12.71 11.37 o -5 -11 1 494.85 473.69 27.29 o -4 -11 1 135.10 209.19 20.11 o -3 -11 1 204.69 252.99 21.47 o -2 -11 1 538.53 448.65 24.47 o -1 -11 1 0.58 34.17 14.93 o 0 -11 1 1.08 2.16 13.50 o 1 -11 1 238.60 203.40 27.09 o 2 -11 1 235.89 373.25 35.30 o 3 -11 1 66.57 77.98 24.31 o 4 -11 1 20.86 65.21 22.80 o 5 -11 1 17.98 87.99 34.93 o -8 -10 1 1307.56 1135.56 40.68 o -7 -10 1 159.87 160.95 21.45 o -6 -10 1 528.08 559.80 37.85 o -5 -10 1 149.32 181.44 19.46 o -4 -10 1 53.63 79.43 12.48 o -3 -10 1 15.85 13.17 8.46 o -2 -10 1 414.22 373.59 20.98 o -1 -10 1 1537.10 1604.36 39.72 o 0 -10 1 55.88 87.30 9.69 o 1 -10 1 241.43 212.30 19.86 o 2 -10 1 309.63 366.23 32.36 o 3 -10 1 308.72 331.74 31.41 o 4 -10 1 166.57 209.41 40.27 o 5 -10 1 40.35 111.82 37.29 o 6 -10 1 152.35 176.54 45.83 o -9 -9 1 83.95 85.71 25.68 o -8 -9 1 353.55 444.37 47.11 o -7 -9 1 228.51 271.45 25.18 o -6 -9 1 507.80 448.74 23.30 o -5 -9 1 802.93 1020.38 43.01 o -4 -9 1 420.95 364.00 18.65 o -3 -9 1 1201.92 1079.59 33.67 o -2 -9 1 17.46 36.00 11.28 o -1 -9 1 21.80 18.84 7.27 o 0 -9 1 1114.01 1029.36 27.51 o 2 -9 1 558.87 537.66 25.82 o 3 -9 1 158.92 162.48 23.76 o 4 -9 1 35.07 153.66 29.85 o 5 -9 1 0.42 10.43 15.92 o 6 -9 1 713.36 601.37 61.38 o -9 -8 1 2.79 17.54 11.74 o -8 -8 1 792.60 722.68 30.33 o -7 -8 1 21.51 21.95 10.56 o -6 -8 1 14.43 29.93 10.92 o -5 -8 1 612.63 557.92 23.55 o -4 -8 1 3.30 48.17 9.78 o -3 -8 1 2112.58 1984.70 46.28 o -2 -8 1 1257.80 1143.61 29.75 o -1 -8 1 2324.35 2522.15 74.29 o 0 -8 1 92.44 98.27 8.12 o 1 -8 1 134.40 136.29 9.94 o 2 -8 1 2736.77 2507.54 50.94 o 3 -8 1 427.52 457.27 26.34 o 4 -8 1 1385.59 1368.29 49.45 o 5 -8 1 1394.40 1378.73 64.98 o 6 -8 1 5.51 49.12 20.02 o 7 -8 1 85.74 64.43 23.77 o -9 -7 1 21.19 26.01 12.22 o -8 -7 1 439.17 452.09 24.09 o -7 -7 1 816.96 762.08 29.43 o -6 -7 1 860.25 822.53 30.25 o -5 -7 1 435.25 436.81 20.26 o -4 -7 1 3810.65 3579.34 76.80 o -3 -7 1 79.34 141.42 9.53 o -2 -7 1 0.79 -0.24 4.89 o -1 -7 1 213.81 195.75 9.09 o 0 -7 1 2376.12 2090.46 42.81 o 1 -7 1 39.60 41.73 7.06 o 2 -7 1 360.82 354.10 11.98 o 3 -7 1 65.65 110.03 8.44 o 4 -7 1 84.95 62.54 10.22 o 5 -7 1 846.63 810.27 34.69 o 6 -7 1 113.43 131.38 25.48 o 7 -7 1 517.64 515.10 82.35 o 8 -7 1 80.48 107.97 44.92 o -10 -6 1 57.64 149.59 39.80 o -9 -6 1 480.12 460.73 27.69 o -8 -6 1 125.68 157.81 17.48 o -7 -6 1 319.60 365.87 48.95 o -6 -6 1 70.09 83.24 19.46 o -5 -6 1 142.62 172.13 12.23 o -4 -6 1 422.27 531.52 17.81 o -3 -6 1 1858.83 1731.59 34.90 o -2 -6 1 165.84 200.91 9.33 o -1 -6 1 816.46 634.77 13.30 o 0 -6 1 250.38 367.67 13.52 o 1 -6 1 28.89 17.21 4.93 o 2 -6 1 2351.69 2170.68 40.48 o 3 -6 1 383.21 398.88 16.13 o 4 -6 1 635.80 590.53 19.51 o 5 -6 1 0.03 -1.26 8.79 o 6 -6 1 12.75 23.89 13.80 o 7 -6 1 57.51 51.93 16.31 o 8 -6 1 88.48 50.92 38.17 o -10 -5 1 260.78 237.73 48.38 o -9 -5 1 20.95 27.57 12.90 o -8 -5 1 71.87 123.38 15.81 o -7 -5 1 16.86 41.93 10.82 o -6 -5 1 175.58 233.25 12.70 o -5 -5 1 558.68 542.78 16.59 o -4 -5 1 929.69 781.65 17.08 o -3 -5 1 5165.90 5291.49 90.14 o -2 -5 1 66.46 99.64 6.13 o -1 -5 1 33.38 106.49 6.30 o 0 -5 1 11.46 2.30 3.44 o 1 -5 1 1410.99 1142.59 35.98 o 2 -5 1 22.94 80.90 8.43 o 3 -5 1 153.24 131.94 7.28 o 4 -5 1 207.89 276.74 14.02 o 5 -5 1 948.18 998.06 28.16 o 6 -5 1 176.08 186.85 16.58 o 7 -5 1 227.17 225.77 23.11 o 8 -5 1 42.93 78.09 23.93 o -10 -4 1 28.76 15.09 15.98 o -9 -4 1 293.94 322.10 26.61 o -8 -4 1 52.98 60.95 13.11 o -7 -4 1 354.83 383.12 16.36 o -6 -4 1 4.24 10.18 6.22 o -5 -4 1 63.29 89.86 7.86 o -4 -4 1 46.34 55.02 5.48 o -3 -4 1 1323.58 1322.52 24.02 o -2 -4 1 4027.97 3973.08 67.64 o -1 -4 1 1938.26 2309.42 52.96 o 0 -4 1 283.95 250.01 14.80 o 1 -4 1 28.69 17.40 5.16 o 2 -4 1 3044.93 3092.69 63.00 o 3 -4 1 1380.46 1290.98 23.34 o 4 -4 1 250.21 222.38 10.80 o 5 -4 1 1058.31 984.88 27.70 o 6 -4 1 9.25 -6.92 9.34 o 7 -4 1 44.43 64.66 16.02 o 8 -4 1 62.03 54.02 17.11 o 9 -4 1 105.13 132.07 22.87 o -10 -3 1 255.48 257.68 56.21 o -9 -3 1 399.63 409.27 28.91 o -8 -3 1 313.95 370.24 18.04 o -7 -3 1 560.78 855.50 45.13 o -6 -3 1 1469.30 1400.35 29.99 o -5 -3 1 1409.61 1350.49 26.12 o -4 -3 1 1823.03 1847.51 33.61 o -3 -3 1 835.17 791.89 14.93 o -2 -3 1 155.09 207.79 6.83 o -1 -3 1 47.19 54.63 3.23 o 0 -3 1 27.50 44.43 3.79 o 1 -3 1 4009.66 3756.25 83.23 o 2 -3 1 3.95 4.23 3.13 o 3 -3 1 1011.32 826.85 18.98 o 4 -3 1 44.78 65.27 10.53 o 5 -3 1 244.78 271.54 14.44 o 6 -3 1 2864.79 2529.18 58.62 o 7 -3 1 1.01 44.28 10.11 o 8 -3 1 2184.05 2055.29 69.43 o 9 -3 1 51.23 61.44 18.86 o -10 -2 1 12.84 54.24 21.42 o -9 -2 1 970.38 881.63 39.59 o -8 -2 1 45.85 54.60 10.43 o -7 -2 1 281.16 341.37 15.82 o -6 -2 1 398.72 442.31 17.95 o -5 -2 1 459.99 567.40 15.21 o -4 -2 1 6298.11 6435.04 100.12 o -3 -2 1 1.40 2.95 3.15 o -2 -2 1 13100.51 13614.51 196.32 o -1 -2 1 0.18 8.89 2.58 o 0 -2 1 43.33 139.93 6.24 o 1 -2 1 397.40 365.94 11.16 o 2 -2 1 601.29 742.39 14.69 o 3 -2 1 4861.92 4559.62 79.35 o 4 -2 1 1199.92 1193.31 22.29 o 5 -2 1 279.04 230.58 11.71 o 6 -2 1 8.33 12.67 7.29 o 7 -2 1 351.86 320.80 23.96 o 8 -2 1 29.86 37.98 15.22 o 9 -2 1 26.59 24.14 17.17 o -10 -1 1 61.08 71.64 17.35 o -9 -1 1 11.47 32.81 12.85 o -8 -1 1 391.92 525.53 35.65 o -7 -1 1 410.39 430.47 16.47 o -6 -1 1 297.53 277.18 13.79 o -5 -1 1 1154.82 1270.97 33.99 o -4 -1 1 70.47 89.42 5.82 o -3 -1 1 41.81 31.52 3.65 o -2 -1 1 179.54 154.80 5.54 o -1 -1 1 15013.12 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