#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:39:19 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181183 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/62/2226296.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226296_Fobs loop_ _publ_author_name 'Hemamalini, Madhukar' 'Fun, Hoong-Kun' _publ_section_title ; 2-Amino-5-chloropyridine--fumaric acid (1/2) ; _journal_coeditor_code SJ5003 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1416 _journal_page_last o1417 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.442 _cell_angle_gamma 90.000 _cell_length_a 13.6780 _cell_length_b 5.0586 _cell_length_c 11.5313 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.6614 _cod_data_source_file sj5003Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' h48am in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 239.43 323.90 14.76 o 5 0 0 462.29 420.33 19.36 o 6 0 0 349.44 273.17 13.09 o 7 0 0 61.86 116.74 4.45 o 8 0 0 7.75 7.34 1.27 o 9 0 0 181.43 151.33 4.72 o 10 0 0 3815.21 3770.69 85.31 o 11 0 0 91.48 95.46 3.72 o 12 0 0 352.82 360.87 12.23 o 13 0 0 1276.22 1298.26 50.29 o 14 0 0 283.56 273.02 13.75 o 15 0 0 30.99 23.93 4.03 o 16 0 0 596.31 677.61 29.28 o 17 0 0 12.21 11.09 3.50 o 18 0 0 106.06 112.22 9.14 o 19 0 0 98.28 124.46 10.07 o 20 0 0 11.14 16.30 4.77 o 1 1 0 376.09 155.09 7.60 o 2 1 0 1648.88 1568.00 68.04 o 3 1 0 9658.43 9362.25 400.38 o 4 1 0 204.34 218.03 6.81 o 5 1 0 2275.26 2105.49 49.42 o 6 1 0 96.58 92.27 2.96 o 7 1 0 2262.67 2308.18 46.27 o 8 1 0 649.03 562.94 12.14 o 9 1 0 669.04 711.40 12.10 o 10 1 0 2093.59 2181.16 43.03 o 11 1 0 428.05 378.71 10.20 o 12 1 0 21.40 19.98 2.01 o 13 1 0 129.54 138.54 5.15 o 14 1 0 7.22 9.19 2.08 o 15 1 0 19.36 20.92 3.65 o 16 1 0 34.53 34.60 5.06 o 17 1 0 153.58 163.02 10.48 o 18 1 0 126.92 140.35 9.87 o 19 1 0 144.64 159.71 11.03 o 1 2 0 1919.55 1834.22 79.67 o 2 2 0 658.57 573.54 24.69 o 3 2 0 924.32 912.20 28.34 o 4 2 0 138.90 132.73 5.15 o 5 2 0 542.44 520.40 9.61 o 6 2 0 28.68 26.49 1.27 o 7 2 0 113.69 121.00 3.32 o 8 2 0 15.82 7.76 1.37 o 9 2 0 76.63 72.13 3.11 o 10 2 0 713.49 695.31 18.03 o 11 2 0 1018.48 1006.96 20.86 o 12 2 0 72.84 77.42 3.09 o 13 2 0 386.14 391.11 10.95 o 14 2 0 111.43 114.13 4.80 o 15 2 0 319.51 340.46 11.98 o 16 2 0 136.34 139.31 8.28 o 17 2 0 220.30 233.45 18.16 o 18 2 0 191.98 229.93 13.07 o 19 2 0 2.23 3.64 3.03 o 1 3 0 20.62 26.94 2.38 o 2 3 0 1738.61 1755.77 54.70 o 3 3 0 22.32 17.55 1.35 o 4 3 0 192.96 165.23 4.78 o 6 3 0 647.39 607.71 15.43 o 7 3 0 244.51 229.49 6.49 o 8 3 0 4194.82 4132.73 94.79 o 9 3 0 6.06 6.40 0.90 o 10 3 0 19.10 16.23 1.46 o 11 3 0 158.04 171.38 4.78 o 12 3 0 55.91 50.97 2.55 o 13 3 0 29.19 24.39 2.00 o 14 3 0 8.16 7.72 1.45 o 15 3 0 0.68 0.19 1.31 o 16 3 0 53.77 51.18 4.09 o 17 3 0 3.37 -0.01 1.86 o 18 3 0 321.65 356.39 12.82 o 0 4 0 35.03 47.67 4.71 o 1 4 0 845.96 858.87 28.33 o 2 4 0 360.55 377.42 24.23 o 3 4 0 649.14 629.97 16.25 o 4 4 0 23.68 18.07 1.37 o 5 4 0 114.62 102.64 3.35 o 6 4 0 61.82 65.63 3.71 o 7 4 0 1.87 2.65 0.89 o 8 4 0 0.00 0.55 0.89 o 9 4 0 323.46 318.00 9.08 o 10 4 0 69.84 80.25 4.57 o 11 4 0 364.22 377.55 10.92 o 12 4 0 0.80 -0.05 1.32 o 13 4 0 88.90 91.91 4.64 o 14 4 0 78.36 80.87 4.95 o 15 4 0 203.76 214.72 8.04 o 16 4 0 89.15 100.50 7.24 o 17 4 0 122.05 142.48 11.23 o 1 5 0 6.61 3.34 1.62 o 2 5 0 15.64 18.30 2.76 o 3 5 0 86.91 78.03 3.35 o 4 5 0 256.82 279.68 7.37 o 5 5 0 23.39 20.58 2.41 o 6 5 0 164.54 166.55 7.20 o 7 5 0 183.15 195.03 6.06 o 8 5 0 232.76 233.43 7.19 o 9 5 0 284.67 288.64 8.68 o 10 5 0 3.16 2.78 1.39 o 11 5 0 11.48 7.31 1.83 o 12 5 0 0.03 1.20 1.78 o 13 5 0 50.64 47.56 3.75 o 14 5 0 1.23 -0.61 1.71 o 15 5 0 23.90 20.28 5.07 o 0 6 0 544.08 606.53 31.51 o 1 6 0 47.98 59.48 5.44 o 2 6 0 14.37 14.13 2.82 o 3 6 0 20.74 18.66 5.74 o 4 6 0 12.03 12.81 2.19 o 5 6 0 0.33 -0.02 1.49 o 6 6 0 271.47 308.14 11.87 o 7 6 0 0.02 -1.96 1.59 o 8 6 0 8.98 4.31 1.53 o 9 6 0 43.31 46.91 3.25 o 10 6 0 74.11 62.44 3.97 o 11 6 0 11.02 9.72 2.13 o 12 6 0 25.88 23.40 5.80 o 1 7 0 46.35 41.66 7.32 o 2 7 0 19.28 17.97 3.52 o 3 7 0 14.82 10.59 2.92 o 4 7 0 6.28 4.28 3.04 o 5 7 0 1.51 0.45 1.89 o 6 7 0 4.19 2.72 2.14 o 7 7 0 30.06 27.42 3.71 o 8 7 0 14.43 12.25 3.11 o -20 1 1 48.40 43.83 6.31 o -19 1 1 14.43 11.41 4.01 o -18 1 1 41.32 50.21 6.31 o -17 1 1 9.51 6.50 3.20 o -16 1 1 63.44 58.42 6.39 o -15 1 1 3.32 4.42 1.82 o -14 1 1 4.57 3.99 1.41 o -13 1 1 102.78 88.87 4.68 o -12 1 1 16.52 11.34 1.74 o -11 1 1 26.56 31.16 2.33 o -10 1 1 251.11 248.01 5.52 o -9 1 1 228.58 244.27 5.31 o -8 1 1 0.23 0.48 0.52 o -7 1 1 922.41 913.75 18.84 o -6 1 1 36.77 24.94 1.57 o -5 1 1 14.04 19.70 1.28 o -4 1 1 99.37 102.97 3.16 o -3 1 1 97.05 82.69 3.48 o -2 1 1 670.19 688.20 30.19 o -1 1 1 789.78 861.46 21.74 o 0 1 1 148.38 142.38 7.67 o 2 1 1 623.27 610.68 27.36 o 3 1 1 8408.88 7444.32 772.18 o 4 1 1 291.03 269.12 8.31 o 5 1 1 283.07 322.25 16.77 o 6 1 1 1.47 9.33 0.96 o 7 1 1 25.58 32.46 1.83 o 8 1 1 104.28 101.35 2.92 o 9 1 1 137.34 105.33 3.20 o 10 1 1 44.47 37.58 2.05 o 11 1 1 71.49 66.56 3.13 o 12 1 1 2.69 3.21 1.18 o 13 1 1 71.59 83.69 7.28 o 14 1 1 260.76 275.71 11.14 o 15 1 1 67.93 67.98 4.99 o 16 1 1 57.43 67.36 7.00 o 17 1 1 40.32 44.76 6.00 o 18 1 1 2.80 0.97 2.84 o 19 1 1 71.94 84.34 8.63 o -19 2 1 27.36 26.99 4.90 o -18 2 1 4.35 5.34 2.42 o -17 2 1 70.53 71.57 5.10 o -16 2 1 69.46 64.09 6.40 o -15 2 1 6.91 5.94 1.68 o -14 2 1 92.72 103.27 4.54 o -13 2 1 81.38 80.63 3.81 o -12 2 1 362.12 363.36 8.68 o -11 2 1 34.70 33.29 2.04 o -10 2 1 79.12 75.66 3.23 o -9 2 1 86.08 77.56 2.82 o -7 2 1 659.27 616.46 13.07 o -6 2 1 443.12 473.26 8.95 o -5 2 1 46.07 38.33 1.23 o -4 2 1 216.25 87.72 5.84 o -3 2 1 383.71 408.60 18.57 o -2 2 1 23.09 31.21 2.98 o -1 2 1 70.99 1.10 0.67 o 1 2 1 3776.19 3986.45 167.98 o 3 2 1 218.49 268.00 9.19 o 4 2 1 311.30 309.22 8.51 o 5 2 1 129.43 109.99 2.49 o 6 2 1 634.24 741.83 13.64 o 7 2 1 19.25 25.24 2.26 o 8 2 1 349.36 179.61 8.92 o 9 2 1 65.34 70.11 2.54 o 10 2 1 674.52 679.64 14.45 o 11 2 1 1158.33 1193.51 24.41 o 12 2 1 63.20 72.59 3.02 o 13 2 1 221.50 235.44 7.49 o 14 2 1 74.45 63.58 5.20 o 15 2 1 1.26 1.20 1.70 o 16 2 1 6.17 4.06 2.05 o 17 2 1 6.22 4.90 2.31 o 18 2 1 2.39 1.22 2.72 o 19 2 1 1.76 0.56 2.97 o -18 3 1 19.19 17.29 6.75 o -17 3 1 3.01 3.01 1.95 o -16 3 1 53.05 50.84 3.63 o -15 3 1 14.64 16.49 2.62 o -14 3 1 51.80 52.67 4.07 o -13 3 1 68.06 66.60 4.28 o -12 3 1 113.56 113.47 3.76 o -11 3 1 140.78 144.52 4.20 o -10 3 1 34.49 30.63 1.88 o -9 3 1 81.63 60.54 2.30 o -8 3 1 751.66 745.67 18.39 o -7 3 1 333.08 314.53 7.41 o -6 3 1 5.11 1.02 0.76 o -5 3 1 6.68 8.90 1.77 o -4 3 1 83.05 67.32 3.29 o -3 3 1 209.39 210.02 5.23 o -2 3 1 849.28 865.36 27.88 o -1 3 1 295.90 297.27 10.69 o 0 3 1 501.30 500.07 16.86 o 1 3 1 672.11 729.47 23.77 o 2 3 1 307.55 270.02 7.30 o 3 3 1 1134.33 1142.91 27.97 o 4 3 1 2.92 1.85 0.61 o 6 3 1 0.86 -0.05 0.59 o 7 3 1 339.02 326.92 8.79 o 8 3 1 20.90 16.36 1.47 o 9 3 1 34.75 36.61 1.83 o 10 3 1 29.02 27.01 1.73 o 11 3 1 11.82 15.39 1.82 o 12 3 1 5.24 4.47 1.09 o 13 3 1 53.00 49.74 2.70 o 14 3 1 12.07 10.12 1.77 o 15 3 1 143.50 147.58 5.74 o 16 3 1 129.73 124.64 6.13 o 17 3 1 42.94 46.11 4.13 o 18 3 1 24.72 19.10 3.31 o -17 4 1 5.51 5.72 3.40 o -16 4 1 24.14 24.30 3.98 o -15 4 1 89.59 83.88 5.04 o -14 4 1 37.40 31.20 3.12 o -13 4 1 18.69 16.16 2.38 o -12 4 1 9.47 10.45 2.29 o -11 4 1 1.11 1.46 1.24 o -10 4 1 7.59 8.82 1.56 o -9 4 1 163.44 154.04 5.28 o -8 4 1 247.64 252.21 7.36 o -7 4 1 1.37 0.72 0.80 o -6 4 1 13.63 12.46 1.45 o -5 4 1 1683.15 1636.40 40.14 o -4 4 1 5.37 6.58 0.91 o -3 4 1 747.01 728.08 16.28 o -2 4 1 157.84 165.47 7.21 o -1 4 1 2.72 3.90 1.29 o 0 4 1 132.12 126.47 6.03 o 1 4 1 0.27 -0.74 0.99 o 2 4 1 36.00 38.03 3.38 o 3 4 1 9.62 9.39 2.39 o 4 4 1 35.41 50.21 2.54 o 5 4 1 859.08 839.99 25.87 o 6 4 1 17.78 23.20 1.62 o 7 4 1 82.00 69.90 3.34 o 8 4 1 209.37 214.09 7.09 o 9 4 1 30.38 31.20 2.48 o 10 4 1 365.82 359.22 10.34 o 11 4 1 203.30 207.25 7.01 o 12 4 1 40.28 40.17 3.22 o 13 4 1 104.69 103.71 4.91 o 14 4 1 26.56 25.13 4.25 o 15 4 1 10.36 8.98 2.85 o 16 4 1 6.14 2.30 4.04 o -15 5 1 51.53 46.65 6.17 o -14 5 1 27.85 26.71 3.14 o -13 5 1 35.04 30.88 3.92 o -12 5 1 139.78 147.38 6.02 o -11 5 1 423.70 438.48 16.31 o -10 5 1 8.54 5.55 2.24 o -9 5 1 27.52 24.17 2.21 o -8 5 1 625.42 644.64 16.52 o -7 5 1 3.79 3.11 1.52 o -6 5 1 29.68 28.09 2.87 o -5 5 1 2.01 1.39 0.91 o -4 5 1 2.10 1.00 0.85 o -3 5 1 12.35 10.11 1.28 o -2 5 1 62.88 64.77 4.49 o -1 5 1 74.81 82.09 6.91 o 0 5 1 246.63 266.20 11.05 o 1 5 1 174.90 188.68 14.62 o 2 5 1 986.55 980.73 33.41 o 3 5 1 0.13 1.72 0.92 o 4 5 1 43.01 46.00 3.33 o 5 5 1 308.84 311.11 11.22 o 6 5 1 63.64 65.41 4.60 o 7 5 1 108.96 103.21 3.99 o 8 5 1 50.92 46.40 3.03 o 9 5 1 202.30 225.02 7.33 o 10 5 1 14.91 16.16 3.61 o 11 5 1 9.24 8.34 1.93 o 12 5 1 46.63 35.47 3.17 o 13 5 1 118.15 116.37 5.86 o 14 5 1 132.18 153.18 6.68 o -12 6 1 0.17 -0.79 1.68 o -11 6 1 61.12 62.98 4.13 o -10 6 1 17.95 16.11 2.24 o -9 6 1 91.62 103.30 8.85 o -8 6 1 430.25 440.88 12.23 o -7 6 1 28.63 27.13 3.93 o -6 6 1 65.39 65.41 5.24 o -5 6 1 237.35 233.89 9.33 o -4 6 1 107.08 105.37 5.26 o -3 6 1 260.81 279.11 8.21 o -2 6 1 22.10 29.22 3.12 o -1 6 1 201.69 226.84 10.53 o 0 6 1 270.81 278.31 13.35 o 1 6 1 18.46 20.41 4.86 o 2 6 1 74.64 66.07 3.92 o 3 6 1 0.55 0.10 1.39 o 4 6 1 28.38 25.96 4.40 o 5 6 1 21.69 14.61 3.56 o 6 6 1 82.82 83.59 5.54 o 7 6 1 78.96 85.72 5.99 o 8 6 1 107.91 102.83 7.70 o 9 6 1 18.37 15.96 2.13 o 10 6 1 168.26 169.35 6.46 o 11 6 1 179.36 197.95 7.35 o 12 6 1 15.35 13.49 2.41 o -8 7 1 8.06 5.51 2.54 o -7 7 1 3.79 0.75 2.17 o -6 7 1 28.61 24.33 3.41 o -5 7 1 3.14 4.26 2.14 o -4 7 1 65.48 74.30 5.05 o -3 7 1 92.55 99.57 5.49 o -2 7 1 0.09 -1.50 3.27 o -1 7 1 159.19 176.30 15.43 o 0 7 1 60.82 80.04 5.67 o 1 7 1 33.47 46.41 7.84 o 2 7 1 200.85 245.68 17.14 o 3 7 1 423.25 467.86 27.27 o 4 7 1 1.54 1.60 3.50 o 5 7 1 49.45 51.86 4.58 o 6 7 1 94.38 93.45 6.18 o 7 7 1 2.13 0.62 2.23 o -20 0 2 94.45 114.54 9.67 o -19 0 2 171.40 188.06 12.34 o -18 0 2 46.22 42.24 6.07 o -17 0 2 74.02 77.86 7.86 o -16 0 2 0.42 0.56 2.27 o -15 0 2 187.54 184.58 10.83 o -14 0 2 186.31 184.31 10.47 o -13 0 2 459.68 450.62 15.00 o -12 0 2 550.36 601.74 15.36 o -11 0 2 56.83 47.05 3.48 o -10 0 2 520.13 494.52 12.59 o -9 0 2 916.44 896.95 26.46 o -8 0 2 4934.58 4866.90 135.10 o -7 0 2 2948.28 2817.73 78.33 o -6 0 2 133.15 185.64 9.92 o -5 0 2 1674.57 1718.89 74.97 o -4 0 2 17.79 24.50 2.45 o -3 0 2 885.67 827.33 36.65 o -2 0 2 2457.53 2340.38 101.12 o -1 0 2 6326.32 7170.54 306.71 o 4 0 2 68.18 72.35 3.95 o 5 0 2 4317.09 4546.64 194.77 o 6 0 2 685.83 621.03 18.06 o 7 0 2 357.70 335.45 10.45 o 8 0 2 317.64 298.26 7.88 o 9 0 2 666.83 633.43 15.51 o 10 0 2 370.00 360.27 23.75 o 11 0 2 7.61 4.86 1.55 o 12 0 2 462.96 452.95 19.88 o 13 0 2 12.31 11.09 2.93 o 14 0 2 579.60 596.53 25.93 o 15 0 2 675.03 718.50 30.73 o 16 0 2 203.89 225.33 13.09 o 17 0 2 71.45 67.11 7.48 o 18 0 2 181.49 195.79 12.70 o -20 1 2 31.14 23.36 4.83 o -19 1 2 232.14 266.49 14.96 o -18 1 2 36.10 33.06 5.25 o -17 1 2 200.75 216.82 12.34 o -16 1 2 610.80 623.21 26.98 o -15 1 2 119.28 134.86 6.38 o -14 1 2 594.64 605.05 15.85 o -13 1 2 279.41 278.34 8.37 o -12 1 2 73.86 68.20 3.51 o -11 1 2 499.52 525.59 10.52 o -10 1 2 346.65 341.29 6.46 o -9 1 2 339.08 352.74 7.23 o -8 1 2 344.13 356.50 8.10 o -7 1 2 728.25 720.59 16.05 o -6 1 2 1612.38 1654.50 39.24 o -5 1 2 945.62 980.61 23.46 o -4 1 2 830.98 846.85 20.36 o -2 1 2 816.12 871.22 67.97 o -1 1 2 1313.73 1498.39 43.69 o 0 1 2 3988.70 4236.57 305.85 o 1 1 2 43.21 49.10 3.37 o 2 1 2 20973.09 22175.68 950.38 o 3 1 2 975.14 934.16 26.48 o 4 1 2 2685.15 3058.38 84.68 o 5 1 2 105.65 121.01 4.48 o 6 1 2 59.05 50.02 2.88 o 7 1 2 11.58 10.68 1.12 o 8 1 2 325.31 321.47 8.49 o 9 1 2 86.32 72.14 2.60 o 10 1 2 443.65 462.66 11.98 o 11 1 2 273.44 277.78 8.05 o 12 1 2 1765.39 1721.82 52.88 o 13 1 2 1277.97 1260.71 35.65 o 14 1 2 21.36 16.04 2.60 o 16 1 2 41.31 47.88 5.95 o 17 1 2 7.78 6.48 3.08 o 18 1 2 25.31 17.89 4.54 o 19 1 2 3.78 4.28 3.66 o -19 2 2 203.46 219.36 12.71 o -18 2 2 171.40 191.75 8.68 o -17 2 2 3.82 2.03 1.95 o -16 2 2 37.67 38.40 3.21 o -15 2 2 23.95 20.79 3.17 o -14 2 2 60.40 51.92 3.48 o -13 2 2 302.83 302.31 7.68 o -12 2 2 225.71 229.85 6.07 o -11 2 2 403.97 391.37 9.01 o -10 2 2 59.32 75.86 2.48 o -9 2 2 1342.76 1248.88 26.28 o -8 2 2 1893.84 1849.05 45.03 o -7 2 2 1.92 0.12 0.39 o -6 2 2 1862.02 1966.49 34.97 o -5 2 2 1883.62 1846.35 48.23 o -4 2 2 65.14 55.56 5.11 o -3 2 2 117.19 100.32 7.41 o -2 2 2 93.67 100.11 3.47 o 0 2 2 426.59 432.16 14.26 o 2 2 2 1238.17 1167.72 36.37 o 3 2 2 957.00 1004.19 31.40 o 4 2 2 1703.69 1777.55 39.55 o 5 2 2 3859.08 4021.15 77.26 o 6 2 2 10.69 13.67 1.87 o 8 2 2 463.76 443.57 11.52 o 9 2 2 84.29 91.03 3.03 o 10 2 2 996.58 986.92 20.38 o 11 2 2 1.83 1.27 0.91 o 12 2 2 8.77 7.67 1.51 o 13 2 2 30.31 32.95 7.41 o 14 2 2 65.62 70.54 5.99 o 15 2 2 246.81 258.55 10.12 o 16 2 2 34.44 34.08 5.12 o 17 2 2 46.74 46.29 9.00 o 18 2 2 150.62 177.39 11.27 o -18 3 2 68.54 71.92 5.05 o -17 3 2 0.75 0.27 1.57 o -16 3 2 571.69 644.69 17.11 o -15 3 2 661.03 684.39 17.85 o -14 3 2 97.18 92.15 3.77 o -13 3 2 211.68 224.00 6.11 o -12 3 2 28.04 25.17 1.83 o -11 3 2 47.17 50.68 2.83 o -10 3 2 332.70 349.90 8.03 o -9 3 2 521.81 505.72 13.14 o -8 3 2 72.87 74.23 3.30 o -7 3 2 30.55 33.38 2.23 o -5 3 2 1439.45 1379.42 60.57 o -4 3 2 231.01 231.40 6.59 o -3 3 2 555.43 515.53 11.64 o -2 3 2 890.99 839.83 22.15 o -1 3 2 474.00 449.62 15.36 o 0 3 2 626.18 611.23 20.22 o 1 3 2 1274.14 1354.41 32.91 o 2 3 2 68.56 63.91 2.46 o 3 3 2 102.06 80.22 8.90 o 4 3 2 153.10 68.44 4.36 o 5 3 2 57.53 39.10 2.42 o 6 3 2 119.38 125.91 4.15 o 7 3 2 63.12 57.70 2.74 o 8 3 2 453.49 461.34 12.13 o 9 3 2 52.29 46.78 2.56 o 10 3 2 332.06 310.64 7.44 o 11 3 2 282.90 304.99 7.51 o 12 3 2 161.97 165.34 4.93 o 13 3 2 322.48 313.20 7.99 o 14 3 2 282.28 302.07 9.19 o 15 3 2 34.58 34.08 3.42 o 16 3 2 25.22 27.19 3.21 o 17 3 2 34.79 32.14 3.57 o -17 4 2 0.87 -2.99 2.32 o -16 4 2 51.60 51.86 10.30 o -15 4 2 151.44 160.07 6.77 o -14 4 2 29.55 29.61 3.13 o -13 4 2 195.57 214.38 7.54 o -12 4 2 133.23 126.69 6.62 o -11 4 2 234.14 248.51 8.57 o -10 4 2 25.68 22.94 2.17 o -9 4 2 113.39 114.72 4.36 o -8 4 2 320.00 339.76 9.72 o -7 4 2 13.03 12.29 1.55 o -6 4 2 2071.27 2000.36 41.08 o -5 4 2 245.72 242.85 7.30 o -4 4 2 2.53 0.95 0.68 o -3 4 2 42.96 35.73 3.09 o -2 4 2 6.21 6.67 1.30 o -1 4 2 157.31 167.72 7.30 o 0 4 2 35.53 41.57 3.61 o 1 4 2 39.61 38.34 3.40 o 2 4 2 160.48 174.31 5.44 o 3 4 2 3.35 6.78 1.08 o 4 4 2 1199.01 1178.74 35.31 o 5 4 2 749.43 686.46 21.61 o 6 4 2 153.09 156.13 9.39 o 7 4 2 114.72 123.07 4.41 o 8 4 2 189.49 183.49 5.98 o 9 4 2 39.82 37.85 2.75 o 10 4 2 236.31 236.35 9.84 o 11 4 2 41.85 36.49 3.00 o 12 4 2 160.60 173.96 10.27 o 13 4 2 0.45 0.72 1.58 o 14 4 2 0.16 0.06 1.66 o 15 4 2 2.45 1.49 2.41 o 16 4 2 40.04 41.65 6.56 o -15 5 2 71.04 72.61 7.29 o -14 5 2 62.43 62.12 4.50 o -13 5 2 58.69 63.32 4.59 o -12 5 2 6.20 7.03 1.89 o -11 5 2 21.08 23.95 5.64 o -10 5 2 5.16 0.71 1.23 o -9 5 2 1.68 3.62 1.27 o -8 5 2 33.24 34.93 2.49 o -7 5 2 1.29 -0.36 0.92 o -6 5 2 55.34 60.19 3.41 o -5 5 2 333.84 338.62 9.92 o -4 5 2 311.05 338.49 8.67 o -3 5 2 498.13 511.39 12.20 o -2 5 2 0.90 2.25 1.33 o -1 5 2 415.00 417.18 15.69 o 0 5 2 21.71 33.02 3.59 o 1 5 2 53.92 63.72 4.48 o 2 5 2 97.26 85.11 3.58 o 3 5 2 230.83 224.45 8.45 o 4 5 2 59.32 61.67 4.06 o 5 5 2 13.25 9.42 2.00 o 6 5 2 11.60 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