#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/63/2226313.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226313_Fobs loop_ _publ_author_name 'Wang, Zhiguo' 'Liu, Siman' 'Bian, Qinquan' _publ_section_title ; Bis[1-(3,5-di-tert-butyl-2-hydroxybenzyl)-3-isopropylimidazolium] pentachlorido(tetrahydrofuran)samarate(III)--tetrahydrofuran--toluene (1/1/1) ; _journal_coeditor_code VM2015 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m683 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.954 _cell_angle_beta 86.077 _cell_angle_gamma 82.789 _cell_length_a 10.2252 _cell_length_b 17.6968 _cell_length_c 18.3806 _exptl_crystal_F_000 1098.00 _reflns_d_resolution_high 0.8300 _[local]_cod_data_source_file vm2015Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelxl in space group P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 261.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 691.38 543.07 20.94 o 3 0 0 7694.37 8736.12 87.05 o 4 0 0 473.51 626.27 16.22 o 5 0 0 1582.99 1732.44 40.21 o 6 0 0 4427.31 4485.83 77.60 o 7 0 0 23.49 17.73 21.12 o 8 0 0 3973.99 4096.70 92.46 o 9 0 0 15.63 33.54 14.06 o 10 0 0 549.02 468.56 40.91 o 11 0 0 630.71 613.24 66.98 o 12 0 0 1304.56 1149.97 89.92 o -12 1 0 550.29 441.20 65.51 o -11 1 0 1286.59 1352.86 109.29 o -10 1 0 570.79 526.23 50.49 o -9 1 0 165.94 222.72 26.46 o -8 1 0 1383.72 1511.58 59.44 o -7 1 0 812.52 781.32 43.13 o -6 1 0 2273.60 2306.69 54.57 o -5 1 0 2432.40 1924.80 69.39 o -4 1 0 8108.03 7767.37 84.46 o -3 1 0 10434.31 11584.42 220.45 o -2 1 0 5828.88 5405.85 62.77 o 2 1 0 5551.01 5658.33 71.96 o 3 1 0 4352.39 6213.35 98.85 o 4 1 0 503.63 658.56 16.15 o 5 1 0 2579.86 2625.21 46.26 o 6 1 0 2503.81 2427.04 71.52 o 7 1 0 146.91 167.65 17.90 o 8 1 0 4012.66 4197.04 127.65 o 9 1 0 1204.29 1291.69 48.77 o 10 1 0 23.50 25.88 21.18 o 11 1 0 684.88 576.51 67.25 o 12 1 0 1029.53 953.28 79.29 o -12 2 0 76.71 8.68 31.98 o -11 2 0 1357.49 1482.04 101.40 o -10 2 0 33.02 86.55 20.76 o -9 2 0 336.97 352.40 29.63 o -8 2 0 52.27 38.20 19.99 o -7 2 0 170.56 195.04 28.46 o -6 2 0 5407.06 5229.51 94.58 o -5 2 0 5923.33 5790.00 71.95 o -4 2 0 1078.11 1169.34 51.66 o -3 2 0 35648.87 37161.78 223.76 o -2 2 0 34379.68 34642.63 355.54 o -1 2 0 11852.65 8205.39 58.18 o 2 2 0 5769.53 5160.01 96.54 o 3 2 0 4256.92 5194.04 121.95 o 4 2 0 3326.08 3387.88 62.97 o 5 2 0 1529.26 1205.47 51.52 o 6 2 0 964.43 1186.60 31.52 o 7 2 0 39.86 37.65 18.54 o 8 2 0 1520.30 1527.28 63.07 o 9 2 0 5658.82 5656.93 113.03 o 10 2 0 220.53 211.49 29.08 o 11 2 0 1073.90 1000.92 86.86 o 12 2 0 467.67 594.78 69.36 o -11 3 0 1334.38 1195.35 105.67 o -10 3 0 301.80 256.20 57.93 o -9 3 0 349.28 303.93 84.11 o -8 3 0 41.70 26.22 21.12 o -7 3 0 274.72 287.00 29.75 o -6 3 0 16752.88 17373.41 259.52 o -5 3 0 14159.34 14597.69 138.53 o -4 3 0 140.85 96.33 12.59 o -3 3 0 5527.70 4694.09 63.51 o -2 3 0 14380.62 15147.78 149.02 o -1 3 0 19441.32 20018.10 228.08 o 0 3 0 6029.00 10267.79 159.48 o 1 3 0 9215.13 4336.72 13.98 o 2 3 0 1367.16 1664.27 43.43 o 3 3 0 9689.79 10111.48 97.22 o 4 3 0 5333.32 5263.76 92.96 o 5 3 0 1094.56 1208.39 35.67 o 6 3 0 2625.53 2676.75 58.47 o 7 3 0 359.35 427.21 31.35 o 8 3 0 1383.20 1427.96 56.58 o 9 3 0 7380.37 7516.87 124.31 o 10 3 0 236.65 232.62 28.89 o 11 3 0 1417.43 1474.50 108.42 o 12 3 0 206.27 211.67 93.78 o -11 4 0 547.57 541.91 70.57 o -10 4 0 155.57 124.42 23.65 o -9 4 0 1251.12 1273.27 79.01 o -8 4 0 629.13 536.11 52.11 o -7 4 0 61.01 37.76 20.81 o -6 4 0 15152.51 16068.82 218.07 o -5 4 0 10779.21 10931.06 126.07 o -4 4 0 985.64 1080.91 37.22 o -3 4 0 8882.74 8707.28 136.93 o -2 4 0 5726.88 5829.51 99.73 o -1 4 0 8367.84 9774.14 112.82 o 0 4 0 6049.28 9092.84 159.63 o 1 4 0 714.08 1986.11 94.52 o 2 4 0 2065.88 1619.38 13.45 o 3 4 0 1639.07 1122.56 14.48 o 4 4 0 741.03 720.53 123.35 o 5 4 0 7318.17 7486.43 97.85 o 6 4 0 4745.96 4787.99 106.71 o 7 4 0 15.38 3.98 20.03 o 8 4 0 1737.18 1664.34 54.03 o 9 4 0 10795.08 10903.23 321.49 o 10 4 0 255.62 252.19 38.51 o 11 4 0 1054.07 1071.80 97.01 o 12 4 0 200.44 116.13 48.63 o -11 5 0 391.82 386.19 73.95 o -10 5 0 161.70 100.56 35.84 o -9 5 0 1469.32 1535.32 166.88 o -8 5 0 2801.56 2646.93 81.73 o -7 5 0 105.35 104.93 14.72 o -6 5 0 11329.86 11302.28 235.00 o -5 5 0 6597.37 6724.34 99.17 o -4 5 0 717.63 702.53 35.74 o -3 5 0 5317.76 5492.06 64.94 o -2 5 0 7668.62 7561.11 122.87 o -1 5 0 7978.07 8505.98 95.30 o 0 5 0 41.17 54.60 26.24 o 1 5 0 1067.84 699.23 8.13 o 2 5 0 4455.22 6079.39 137.99 o 3 5 0 8966.52 10249.65 161.42 o 4 5 0 7077.29 7026.70 87.82 o 5 5 0 5381.73 5471.58 78.42 o 6 5 0 4539.66 4486.72 78.49 o 7 5 0 95.93 59.35 27.14 o 8 5 0 488.47 413.19 49.37 o 9 5 0 10058.50 10116.10 163.68 o 10 5 0 357.96 375.71 44.82 o 11 5 0 465.07 582.29 73.60 o 12 5 0 112.02 76.22 29.71 o -11 6 0 823.85 746.18 95.93 o -10 6 0 328.55 227.05 57.71 o -9 6 0 1074.72 1083.84 96.86 o -8 6 0 4845.26 4940.17 217.62 o -7 6 0 268.56 317.24 37.43 o -6 6 0 7184.61 7194.57 112.05 o -5 6 0 4074.36 4109.23 77.58 o -4 6 0 1011.00 981.61 41.08 o -3 6 0 587.91 637.99 25.53 o -2 6 0 4386.29 4038.38 111.14 o -1 6 0 8065.08 7463.13 72.72 o 0 6 0 1716.86 1667.54 39.68 o 1 6 0 75.62 183.09 14.99 o 2 6 0 2826.21 2495.44 33.61 o 3 6 0 12297.73 10846.26 133.68 o 4 6 0 6090.65 5432.49 242.30 o 5 6 0 6478.58 6841.69 108.90 o 6 6 0 6577.74 6998.19 155.32 o 7 6 0 859.56 814.98 31.13 o 8 6 0 429.33 540.69 30.37 o 9 6 0 4875.81 5014.11 136.59 o 10 6 0 178.70 148.08 14.89 o 11 6 0 341.79 239.35 47.96 o 12 6 0 116.69 137.90 54.69 o -11 7 0 462.61 433.77 60.53 o -10 7 0 45.66 1.91 68.10 o -9 7 0 586.04 633.44 53.36 o -8 7 0 4973.87 4992.74 270.88 o -7 7 0 16.89 5.12 36.57 o -6 7 0 4980.31 5214.58 139.35 o -5 7 0 1237.32 1175.93 63.91 o -4 7 0 567.60 512.83 27.61 o -3 7 0 2783.90 2870.13 71.06 o -2 7 0 5516.56 5572.05 63.03 o -1 7 0 166.85 134.59 17.02 o 0 7 0 2183.65 2198.33 46.67 o 1 7 0 786.48 1097.14 39.76 o 2 7 0 1610.61 1528.03 48.70 o 3 7 0 18193.86 19126.02 149.59 o 4 7 0 9186.98 8533.39 215.19 o 5 7 0 3807.75 3738.75 119.78 o 6 7 0 3303.77 3388.50 123.66 o 7 7 0 2116.59 2186.69 67.28 o 8 7 0 2148.80 2288.49 62.78 o 9 7 0 2089.80 2117.23 73.65 o 10 7 0 84.56 75.89 28.60 o 11 7 0 140.07 134.98 57.07 o -10 8 0 3.95 2.71 41.69 o -9 8 0 70.81 59.08 39.02 o -8 8 0 3369.53 3173.17 168.64 o -7 8 0 165.55 139.36 58.96 o -6 8 0 4166.14 4047.18 99.24 o -5 8 0 1303.20 1349.23 39.00 o -4 8 0 1294.33 1328.65 64.39 o -3 8 0 527.83 553.42 35.54 o -2 8 0 4794.52 4897.01 69.42 o -1 8 0 2508.44 2643.35 60.41 o 0 8 0 9955.97 9071.52 104.10 o 1 8 0 718.30 644.52 29.74 o 2 8 0 2011.43 2202.77 34.94 o 3 8 0 17124.61 17689.19 203.11 o 4 8 0 5750.18 5671.22 79.84 o 5 8 0 106.90 162.64 17.90 o 6 8 0 1257.41 1154.41 115.08 o 7 8 0 1739.33 1570.92 86.80 o 8 8 0 2068.84 2049.55 90.66 o 9 8 0 969.15 901.80 102.51 o 10 8 0 184.74 157.62 47.55 o 11 8 0 6.40 72.85 40.24 o -10 9 0 59.25 60.70 25.00 o -9 9 0 7.57 47.89 50.37 o -8 9 0 1458.67 1447.48 100.73 o -7 9 0 98.70 20.90 30.70 o -6 9 0 2722.00 2785.95 129.52 o -5 9 0 2793.33 2678.38 87.71 o -4 9 0 1067.40 1129.76 42.94 o -3 9 0 714.96 694.68 40.52 o -2 9 0 2169.39 2138.01 63.16 o -1 9 0 44.60 67.32 9.52 o 0 9 0 23062.17 23819.15 265.04 o 1 9 0 8504.86 8583.12 91.51 o 2 9 0 2569.29 2722.16 72.43 o 3 9 0 14829.47 15031.20 127.30 o 4 9 0 937.42 862.65 46.96 o 5 9 0 3.65 6.11 21.58 o 6 9 0 3195.04 3455.00 110.69 o 7 9 0 1102.53 995.26 61.97 o 8 9 0 2068.28 2028.07 156.98 o 9 9 0 282.25 401.74 111.09 o 10 9 0 210.54 114.77 37.64 o 11 9 0 3.47 64.19 41.27 o -10 10 0 131.91 101.90 59.52 o -9 10 0 231.55 299.28 105.04 o -8 10 0 1043.62 927.95 119.92 o -7 10 0 146.16 155.61 28.88 o -6 10 0 412.76 275.17 63.73 o -5 10 0 2070.18 1982.22 63.60 o -4 10 0 166.47 136.17 26.92 o -3 10 0 1313.34 1349.73 49.16 o -2 10 0 2453.72 2356.70 70.43 o -1 10 0 176.79 263.65 19.75 o 0 10 0 10580.79 11187.55 118.30 o 1 10 0 12173.26 12467.16 135.89 o 2 10 0 1287.62 1161.88 37.65 o 3 10 0 9898.79 10050.93 147.30 o 4 10 0 232.27 226.60 20.14 o 5 10 0 166.31 200.07 58.27 o 6 10 0 767.92 791.69 55.44 o 7 10 0 2197.58 2168.64 180.69 o 8 10 0 1873.19 1926.95 152.39 o 9 10 0 526.28 553.21 84.10 o 10 10 0 12.29 33.41 37.47 o 11 10 0 54.72 50.37 35.98 o -9 11 0 287.37 174.94 49.75 o -8 11 0 721.71 739.16 77.68 o -7 11 0 75.00 123.84 70.50 o -6 11 0 141.90 141.69 34.04 o -5 11 0 1601.56 1829.10 78.93 o -4 11 0 1098.27 1029.41 59.79 o -3 11 0 6707.88 6732.60 113.49 o -2 11 0 3272.08 3205.82 74.84 o -1 11 0 489.30 475.45 26.17 o 0 11 0 2231.31 2322.52 69.08 o 1 11 0 11566.31 12237.04 192.83 o 2 11 0 111.40 95.41 16.57 o 3 11 0 10845.81 10954.24 165.72 o 4 11 0 882.65 749.42 40.44 o 5 11 0 54.24 55.19 28.02 o 6 11 0 209.62 212.84 54.87 o 7 11 0 468.90 456.39 71.24 o 8 11 0 295.66 260.89 60.55 o 9 11 0 2723.85 3271.43 194.71 o 10 11 0 58.45 106.68 46.17 o 11 11 0 41.23 22.54 37.42 o -9 12 0 90.95 56.59 30.63 o -8 12 0 322.35 354.41 60.27 o -7 12 0 92.22 88.30 41.84 o -6 12 0 127.54 112.38 41.38 o -5 12 0 1668.22 1720.90 197.24 o -4 12 0 1444.52 1633.50 77.73 o -3 12 0 5707.37 5819.47 143.44 o -2 12 0 6826.13 6734.73 109.06 o -1 12 0 1385.66 1374.91 47.37 o 0 12 0 48.89 52.16 17.61 o 1 12 0 3495.94 3509.59 74.14 o 2 12 0 74.86 47.24 20.00 o 3 12 0 8074.43 8203.63 114.52 o 4 12 0 5466.75 5626.13 104.80 o 5 12 0 49.10 69.98 20.74 o 6 12 0 1171.51 1186.92 98.31 o 7 12 0 20.41 41.45 40.15 o 8 12 0 11.78 1.63 32.09 o 9 12 0 2486.64 2617.88 173.88 o 10 12 0 154.53 92.45 42.27 o -8 13 0 567.92 653.26 69.86 o -7 13 0 23.57 16.70 31.26 o -6 13 0 682.58 674.02 76.67 o -5 13 0 2378.44 2311.34 86.22 o -4 13 0 368.63 347.74 59.49 o -3 13 0 4224.87 4052.76 199.29 o -2 13 0 5919.83 6094.99 97.63 o -1 13 0 194.74 170.58 31.51 o 0 13 0 207.02 259.50 21.27 o 1 13 0 986.33 956.42 48.70 o 2 13 0 25.05 22.48 14.79 o 3 13 0 2120.67 2019.77 49.60 o 4 13 0 1358.25 1282.63 55.26 o 5 13 0 735.72 676.02 48.06 o 6 13 0 2062.59 2105.10 133.87 o 7 13 0 72.35 143.24 41.10 o 8 13 0 82.32 132.27 55.78 o 9 13 0 1013.42 1054.87 123.16 o 10 13 0 341.82 346.64 90.56 o -8 14 0 717.20 737.19 68.71 o -7 14 0 138.94 106.08 44.85 o -6 14 0 460.63 479.45 61.85 o -5 14 0 2052.09 1990.99 112.71 o -4 14 0 171.62 126.10 26.93 o -3 14 0 2480.21 2501.60 109.05 o -2 14 0 3639.22 3666.19 116.89 o -1 14 0 8.13 45.97 15.36 o 0 14 0 270.09 275.27 34.76 o 1 14 0 834.78 913.50 46.48 o 2 14 0 124.42 84.05 30.44 o 3 14 0 3065.28 3024.94 122.61 o 4 14 0 1595.00 1592.01 67.55 o 5 14 0 187.12 209.96 24.20 o 6 14 0 1125.21 1227.56 1086.36 o 7 14 0 450.29 464.43 100.12 o 8 14 0 531.38 550.89 90.34 o 9 14 0 863.10 828.24 125.37 o -7 15 0 201.55 232.72 42.03 o -6 15 0 837.90 948.21 83.88 o -5 15 0 1237.77 1154.56 100.85 o -4 15 0 26.45 29.84 20.98 o -3 15 0 2592.14 2460.71 111.26 o -2 15 0 3175.83 3325.50 122.88 o -1 15 0 563.91 527.81 39.53 o 0 15 0 226.03 237.19 45.75 o 1 15 0 515.09 565.58 49.59 o 2 15 0 27.51 18.93 21.15 o 3 15 0 409.04 509.52 33.81 o 4 15 0 2461.04 2603.80 90.84 o 5 15 0 19.58 21.53 14.06 o 6 15 0 1823.95 2021.55 160.50 o 7 15 0 1876.55 1926.48 157.82 o 8 15 0 146.74 185.00 68.30 o 9 15 0 571.64 591.49 81.89 o -6 16 0 457.12 415.54 54.76 o -5 16 0 1106.86 1088.33 90.21 o -4 16 0 81.21 119.13 54.77 o -3 16 0 1415.03 1348.13 108.33 o -2 16 0 1358.90 1454.05 69.93 o -1 16 0 1705.52 1730.57 72.45 o 0 16 0 735.96 747.54 65.50 o 1 16 0 1257.56 1325.38 78.07 o 2 16 0 273.38 226.66 41.64 o 3 16 0 250.08 292.24 28.58 o 4 16 0 849.19 974.04 58.90 o 5 16 0 49.14 54.24 29.03 o 6 16 0 1185.48 1244.88 138.67 o 7 16 0 1176.70 946.44 114.59 o 8 16 0 228.00 218.11 57.64 o -5 17 0 1076.75 1083.87 104.84 o -4 17 0 77.73 77.37 30.18 o -3 17 0 436.66 467.48 140.92 o -2 17 0 448.66 488.02 119.12 o -1 17 0 1642.22 1635.35 91.41 o 0 17 0 503.11 533.94 47.94 o 1 17 0 2531.39 2568.12 118.07 o 2 17 0 286.94 284.97 47.18 o 3 17 0 881.83 1010.89 67.99 o 4 17 0 692.77 731.96 47.33 o 5 17 0 205.01 230.04 54.03 o 6 17 0 1302.19 1611.15 157.43 o 7 17 0 1607.58 1634.93 178.07 o 8 17 0 112.17 111.02 57.33 o -4 18 0 72.45 83.57 25.43 o -3 18 0 411.30 370.37 56.99 o -2 18 0 564.60 515.13 93.76 o -1 18 0 1157.73 1117.48 97.38 o 0 18 0 327.65 287.58 115.61 o 1 18 0 2152.87 2229.12 95.25 o 2 18 0 113.86 75.26 40.78 o 3 18 0 788.31 888.03 75.75 o 4 18 0 476.42 605.13 72.45 o 5 18 0 59.54 89.95 53.07 o 6 18 0 1131.94 1206.21 135.38 o 7 18 0 1118.07 1035.58 120.65 o -3 19 0 309.79 210.29 48.88 o -2 19 0 859.69 902.51 80.22 o -1 19 0 652.19 541.03 101.84 o 0 19 0 120.84 122.40 40.03 o 1 19 0 1478.42 1579.65 184.27 o 2 19 0 6.51 28.26 13.10 o 3 19 0 1145.98 1163.66 126.28 o 4 19 0 526.49 562.41 94.45 o 5 19 0 25.45 28.86 46.77 o 6 19 0 962.24 1147.96 132.47 o -1 20 0 97.30 15.57 65.03 o 0 20 0 135.27 85.38 59.41 o 1 20 0 1048.78 1105.10 91.21 o 2 20 0 342.75 324.22 58.34 o 3 20 0 1015.72 903.70 100.80 o 4 20 0 702.61 621.58 96.70 o -4 -20 1 23.63 83.68 34.25 o -3 -20 1 1405.60 1247.90 94.38 o -2 -20 1 334.64 352.05 37.19 o -1 -20 1 46.19 33.48 18.52 o 0 -20 1 230.00 208.74 43.92 o 1 -20 1 346.91 347.47 49.35 o -5 -19 1 1317.96 1255.91 135.47 o -4 -19 1 153.82 166.78 33.57 o -3 -19 1 804.09 768.75 173.51 o -2 -19 1 813.57 914.74 103.39 o -1 -19 1 0.84 23.29 25.40 o 0 -19 1 204.96 184.54 32.28 o 1 -19 1 265.55 217.62 55.39 o 2 -19 1 42.06 75.95 24.58 o 3 -19 1 889.40 922.35 174.22 o -7 -18 1 566.26 534.27 110.70 o -6 -18 1 111.61 129.03 50.24 o -5 -18 1 1146.11 1292.54 154.78 o -4 -18 1 23.43 71.18 19.71 o -3 -18 1 423.03 406.67 63.24 o -2 -18 1 1908.97 2110.93 97.52 o -1 -18 1 22.09 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36.56 o -1 9 21 625.51 713.78 99.99 o 0 9 21 125.22 152.39 65.01 o 1 9 21 51.44 0.26 32.91 o 2 9 21 1063.38 1178.11 128.27 o 3 9 21 2568.27 2428.47 193.45 o -1 10 21 1228.25 1524.58 168.46 o 0 10 21 1131.91 1284.87 139.71 o 1 10 21 1.36 49.71 44.82 o 2 10 21 1217.78 1119.93 129.53 o 3 10 21 2148.63 1973.38 155.29 o 1 11 21 15.79 54.39 47.46 o 2 11 21 2328.35 2266.30 174.48 o 0 3 22 914.85 706.76 98.44 o 1 3 22 659.30 705.64 100.12 o 0 4 22 1159.27 1211.66 136.16 o 1 4 22 1114.71 1136.13 125.20 o 2 4 22 60.65 41.83 30.53 o 0 5 22 823.96 884.28 144.73 o 1 5 22 1093.23 1217.09 137.29 o 2 5 22 102.59 20.96 29.14 o 0 6 22 193.15 112.74 52.18 o 1 6 22 778.67 892.55 144.95 o 2 6 22 86.49 38.21 45.39 o 1 7 22 746.49 667.42 96.75 o