#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/63/2226326.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226326_Fobs loop_ _publ_author_name 'Bon, Vladimir V.' 'Orysyk, Svitlana I.' 'Pekhnyo, Vasily I.' _publ_section_title ; [1-(2-Oxidobenzylidene)-4-phenylthiosemicarbazidato-\k^3^O,N^1^,S](pyridine-\kN)copper(II) ; _journal_coeditor_code WM2343 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m676 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.602 _cell_angle_gamma 90.000 _cell_length_a 18.2958 _cell_length_b 4.5610 _cell_length_c 20.4733 _exptl_crystal_F_000 844.00 _reflns_d_resolution_high 0.7987 _[local]_cod_data_source_file wm2343Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 965 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 276.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19007.70 18964.22 578.20 o 4 0 0 47046.55 47442.07 896.97 o 6 0 0 204.49 215.60 17.91 o 8 0 0 7777.26 7872.55 164.62 o 10 0 0 3139.10 3031.14 78.63 o 12 0 0 6055.46 5761.77 121.69 o 14 0 0 5617.12 5475.37 180.65 o 16 0 0 148.11 125.26 36.59 o 18 0 0 212.12 211.17 47.41 o 20 0 0 178.64 198.24 134.54 o 22 0 0 2280.16 2467.56 273.10 o 1 1 0 6845.98 6815.02 98.90 o 2 1 0 1547.42 1576.59 27.89 o 3 1 0 6235.77 6223.90 96.83 o 4 1 0 15882.36 16295.58 226.18 o 5 1 0 60.90 92.97 10.08 o 6 1 0 2090.51 2183.49 40.90 o 7 1 0 9568.25 9223.79 135.82 o 8 1 0 1.09 -0.68 8.47 o 9 1 0 547.03 583.43 21.70 o 10 1 0 578.46 554.56 30.06 o 11 1 0 155.30 199.01 15.03 o 12 1 0 466.99 492.26 26.81 o 13 1 0 297.80 305.08 23.73 o 14 1 0 46.53 20.52 16.52 o 15 1 0 3297.86 3218.29 90.98 o 16 1 0 2.72 12.40 20.90 o 17 1 0 47.57 43.22 30.76 o 18 1 0 502.13 514.04 49.83 o 19 1 0 1890.19 1937.65 90.78 o 20 1 0 372.72 377.45 65.86 o 21 1 0 406.48 443.52 54.87 o 22 1 0 0.83 51.39 55.54 o 0 2 0 3682.98 3526.72 82.77 o 1 2 0 33.38 61.10 13.08 o 2 2 0 282.14 243.41 17.09 o 3 2 0 2218.63 2205.65 49.77 o 4 2 0 1283.55 1297.83 33.35 o 5 2 0 2717.35 2644.15 47.10 o 6 2 0 2448.56 2288.48 45.30 o 7 2 0 208.87 215.53 17.39 o 8 2 0 963.15 930.75 29.94 o 9 2 0 832.23 851.50 38.67 o 10 2 0 62.77 73.87 19.65 o 11 2 0 318.69 344.91 31.81 o 12 2 0 41.17 39.95 23.13 o 13 2 0 477.91 458.24 37.95 o 14 2 0 104.93 99.11 25.06 o 15 2 0 291.16 243.66 35.26 o 16 2 0 75.71 65.57 28.12 o 17 2 0 63.00 101.82 31.72 o 18 2 0 32.63 35.59 30.44 o 19 2 0 30.00 35.05 33.45 o 20 2 0 629.59 651.83 63.23 o 21 2 0 4.13 -11.03 43.46 o 1 3 0 5482.90 5482.24 97.25 o 2 3 0 2830.49 2921.97 60.34 o 3 3 0 620.21 605.72 31.74 o 4 3 0 1357.31 1438.22 41.27 o 5 3 0 394.93 405.67 29.70 o 6 3 0 42.03 47.56 19.44 o 7 3 0 978.00 1022.58 44.46 o 8 3 0 85.96 55.07 21.38 o 9 3 0 4035.84 4179.59 98.52 o 10 3 0 7.17 42.47 26.92 o 11 3 0 235.50 321.09 42.93 o 12 3 0 536.70 592.98 51.20 o 13 3 0 2209.29 2385.49 98.29 o 14 3 0 1.47 -32.15 32.15 o 15 3 0 4.17 -2.87 34.19 o 16 3 0 332.37 350.42 43.64 o 17 3 0 1.20 -32.09 32.09 o 18 3 0 95.04 102.43 38.63 o 19 3 0 8.17 -39.20 43.49 o 0 4 0 145.84 131.32 39.84 o 1 4 0 667.81 664.43 32.73 o 2 4 0 732.16 732.17 35.10 o 3 4 0 2596.58 2752.97 75.91 o 4 4 0 777.13 793.68 42.06 o 5 4 0 2149.69 2353.22 86.19 o 6 4 0 1615.36 1710.83 78.38 o 7 4 0 77.60 90.14 34.42 o 8 4 0 591.36 579.47 50.14 o 9 4 0 901.91 928.85 59.78 o 10 4 0 598.12 745.45 60.64 o 11 4 0 446.88 501.87 53.88 o 12 4 0 154.22 157.12 42.67 o 13 4 0 1.82 22.80 38.97 o 14 4 0 201.21 199.36 46.89 o 15 4 0 42.31 59.24 47.15 o 16 4 0 553.81 576.43 68.85 o 1 5 0 2.05 -29.32 29.32 o 2 5 0 740.79 696.93 54.34 o 3 5 0 147.14 200.11 50.22 o 4 5 0 579.62 676.90 58.44 o 5 5 0 13.58 -19.29 40.58 o 6 5 0 83.25 113.67 45.94 o 7 5 0 19.95 -32.83 40.94 o 8 5 0 30.13 11.41 43.35 o 9 5 0 5.33 -30.04 42.14 o 10 5 0 77.20 156.32 57.24 o -21 0 1 22.75 38.12 60.49 o -19 0 1 120.39 150.69 46.86 o -17 0 1 262.50 283.82 48.51 o -15 0 1 539.14 507.33 51.46 o -13 0 1 2860.55 2973.42 75.42 o -11 0 1 12617.25 12343.72 231.91 o -9 0 1 1223.34 1201.85 38.72 o -7 0 1 2352.29 2203.58 77.57 o -5 0 1 4003.86 3695.19 91.14 o -3 0 1 4267.75 4151.15 95.16 o -1 0 1 2669.41 2666.22 90.36 o 3 0 1 16330.04 15805.20 412.16 o 5 0 1 127.56 144.95 17.24 o 7 0 1 2.26 10.09 10.78 o 9 0 1 3819.91 3564.31 86.75 o 11 0 1 6301.22 6126.97 139.24 o 13 0 1 70.08 32.81 16.37 o 15 0 1 2392.68 2583.85 105.98 o 17 0 1 629.81 706.51 75.65 o 19 0 1 277.27 292.24 71.89 o 21 0 1 3.31 52.50 64.15 o -22 1 1 13.39 -14.15 42.56 o -21 1 1 222.97 233.71 43.90 o -20 1 1 87.98 101.16 37.09 o -19 1 1 26.86 44.98 33.75 o -18 1 1 987.08 993.21 64.61 o -17 1 1 45.29 4.09 28.92 o -16 1 1 4.67 -3.73 18.48 o -15 1 1 0.76 -4.77 17.06 o -14 1 1 1701.73 1666.19 50.28 o -13 1 1 335.25 308.70 24.12 o -12 1 1 1385.82 1363.60 43.27 o -11 1 1 192.50 224.75 16.50 o -10 1 1 3244.65 3116.08 58.13 o -9 1 1 3760.95 3787.92 66.25 o -8 1 1 2117.53 2049.01 48.40 o -7 1 1 335.71 354.75 16.12 o -6 1 1 9637.63 9447.39 153.87 o -5 1 1 667.75 797.84 23.75 o -4 1 1 30777.59 30411.50 434.69 o -3 1 1 96.13 121.42 12.52 o -2 1 1 2455.60 2405.38 40.28 o -1 1 1 7739.58 7566.91 109.25 o 0 1 1 7439.90 7328.25 101.74 o 1 1 1 2756.43 2769.69 42.27 o 2 1 1 10669.13 10426.30 147.46 o 3 1 1 12816.99 12975.67 191.71 o 4 1 1 5856.35 5579.55 95.48 o 5 1 1 1379.39 1379.46 37.14 o 6 1 1 188.70 205.40 13.75 o 7 1 1 198.39 201.59 15.91 o 8 1 1 6429.64 6307.09 102.80 o 9 1 1 639.56 652.65 29.52 o 10 1 1 3659.60 3665.68 68.22 o 11 1 1 236.30 230.34 18.81 o 12 1 1 59.64 49.87 14.13 o 13 1 1 452.35 451.00 26.99 o 14 1 1 3.78 23.88 18.80 o 15 1 1 1033.63 917.28 43.98 o 16 1 1 462.62 537.45 36.78 o 17 1 1 156.00 110.11 32.01 o 18 1 1 973.87 1040.16 65.30 o 19 1 1 19.40 78.33 35.12 o 20 1 1 1.61 -31.72 31.72 o 21 1 1 415.63 302.08 59.59 o 22 1 1 392.86 525.29 94.29 o -21 2 1 72.02 67.49 45.22 o -20 2 1 41.21 6.26 37.25 o -19 2 1 489.74 417.39 45.09 o -18 2 1 128.27 138.99 34.32 o -17 2 1 602.74 610.28 47.00 o -16 2 1 1134.92 1083.99 94.75 o -15 2 1 166.73 100.41 26.12 o -14 2 1 313.34 316.62 33.90 o -13 2 1 1089.62 1068.11 49.05 o -12 2 1 319.18 333.03 29.05 o -11 2 1 1885.98 1868.65 58.95 o -10 2 1 15.77 18.95 20.64 o -9 2 1 199.77 193.87 26.56 o -8 2 1 4503.90 4512.55 80.57 o -7 2 1 3683.23 3757.98 69.74 o -6 2 1 4821.39 4784.47 76.13 o -5 2 1 5878.25 5811.75 89.51 o -4 2 1 1429.97 1453.06 48.52 o -3 2 1 5465.59 5423.98 81.28 o -2 2 1 4594.76 4611.74 71.63 o -1 2 1 47.15 47.00 12.59 o 0 2 1 38.01 27.43 13.96 o 1 2 1 3636.88 3672.90 62.32 o 2 2 1 1009.91 1010.33 29.73 o 3 2 1 2519.75 2293.38 44.33 o 4 2 1 14.24 17.14 10.51 o 5 2 1 354.41 365.04 18.53 o 6 2 1 5201.99 5351.80 84.07 o 7 2 1 954.77 916.26 31.64 o 8 2 1 164.52 174.70 23.43 o 9 2 1 2526.96 2522.90 57.99 o 10 2 1 62.06 85.54 19.77 o 11 2 1 1938.55 1959.41 67.29 o 12 2 1 280.11 232.04 34.16 o 13 2 1 19.65 -21.81 21.81 o 14 2 1 1426.07 1568.67 128.36 o 15 2 1 575.37 567.37 43.61 o 16 2 1 489.47 485.65 42.35 o 17 2 1 239.95 330.19 40.67 o 18 2 1 628.44 545.54 47.70 o 19 2 1 119.12 143.26 39.60 o 20 2 1 194.40 290.57 50.17 o 21 2 1 54.64 51.38 47.16 o -19 3 1 52.25 31.28 47.61 o -18 3 1 107.19 107.82 42.87 o -17 3 1 37.83 72.33 39.12 o -16 3 1 168.38 196.28 38.73 o -15 3 1 106.99 155.31 35.31 o -14 3 1 252.63 222.05 40.41 o -13 3 1 310.72 338.45 44.64 o -12 3 1 391.81 468.17 47.58 o -11 3 1 194.43 215.46 37.35 o -10 3 1 2109.29 2214.47 82.07 o -9 3 1 1158.27 1201.02 50.29 o -8 3 1 83.45 104.55 23.78 o -7 3 1 358.73 354.07 33.90 o -6 3 1 364.09 358.31 33.58 o -5 3 1 278.49 344.06 30.50 o -4 3 1 532.61 483.34 26.57 o -3 3 1 675.25 662.16 30.47 o -2 3 1 2638.21 2589.39 68.18 o -1 3 1 6309.69 6392.75 99.81 o 0 3 1 217.22 193.05 20.24 o 1 3 1 1246.66 1282.14 43.00 o 2 3 1 2360.85 2305.38 54.97 o 3 3 1 374.73 367.51 23.18 o 4 3 1 375.66 409.10 26.46 o 5 3 1 475.58 479.29 31.15 o 6 3 1 320.01 327.61 27.92 o 7 3 1 406.64 450.98 35.23 o 8 3 1 488.24 537.06 37.48 o 9 3 1 54.95 94.93 27.78 o 10 3 1 543.36 543.75 43.34 o 11 3 1 388.70 444.50 44.64 o 12 3 1 344.71 364.71 44.17 o 13 3 1 961.80 1019.77 64.99 o 14 3 1 285.81 280.90 42.75 o 15 3 1 178.30 172.82 40.24 o 16 3 1 397.14 484.44 61.79 o 17 3 1 0.34 0.67 32.04 o 18 3 1 121.91 100.97 38.54 o 19 3 1 2.36 0.77 39.29 o -16 4 1 116.42 108.04 51.55 o -15 4 1 49.60 6.10 44.01 o -14 4 1 196.12 186.19 50.26 o -13 4 1 2.25 -3.37 39.65 o -12 4 1 84.16 48.41 40.75 o -11 4 1 197.31 169.93 41.95 o -10 4 1 288.00 289.82 42.86 o -9 4 1 1102.33 1144.58 65.09 o -8 4 1 1354.55 1485.37 88.27 o -7 4 1 24.47 42.85 31.84 o -6 4 1 885.33 918.88 56.73 o -5 4 1 552.66 604.16 44.70 o -4 4 1 89.31 122.59 24.96 o -3 4 1 326.41 322.80 30.28 o -2 4 1 1962.56 2022.32 60.07 o -1 4 1 8.10 -4.88 18.43 o 0 4 1 1199.33 1142.76 43.16 o 1 4 1 5.78 -14.53 18.82 o 2 4 1 109.96 77.60 22.95 o 3 4 1 390.43 332.59 33.06 o 4 4 1 433.61 485.88 36.52 o 5 4 1 1083.89 1054.24 59.26 o 6 4 1 110.06 116.63 44.21 o 7 4 1 136.47 131.37 35.06 o 8 4 1 185.67 215.53 37.52 o 9 4 1 233.80 203.89 42.01 o 10 4 1 5.90 17.18 35.10 o 11 4 1 24.58 9.30 36.00 o 12 4 1 469.23 528.11 55.99 o 13 4 1 109.71 118.70 43.03 o 14 4 1 232.41 298.66 51.28 o 15 4 1 2.37 3.13 39.82 o 16 4 1 2.05 -30.59 41.51 o -10 5 1 55.08 75.72 43.62 o -9 5 1 190.89 143.73 49.40 o -8 5 1 49.80 47.19 40.96 o -7 5 1 1466.09 1518.19 95.70 o -6 5 1 20.31 66.53 39.53 o -5 5 1 512.03 463.17 52.90 o -4 5 1 32.32 56.29 50.68 o -3 5 1 269.88 368.01 91.42 o -2 5 1 104.11 141.76 44.20 o -1 5 1 388.13 392.48 47.98 o 0 5 1 20.21 42.69 38.86 o 1 5 1 399.17 361.67 44.90 o 2 5 1 185.90 168.28 39.10 o 3 5 1 73.12 10.83 34.92 o 4 5 1 0.34 7.80 38.33 o 5 5 1 943.81 991.15 80.53 o 6 5 1 0.01 -34.36 39.77 o 7 5 1 1032.41 1098.37 75.11 o 8 5 1 4.25 -27.99 41.61 o 9 5 1 2.95 -24.72 44.28 o 10 5 1 32.98 -1.72 69.99 o -22 0 2 2490.81 2566.03 187.48 o -20 0 2 1.54 29.45 41.58 o -18 0 2 3402.60 3543.90 140.27 o -16 0 2 611.65 642.49 61.88 o -14 0 2 1420.04 1540.27 80.38 o -12 0 2 334.08 342.63 25.66 o -10 0 2 11389.99 11394.42 213.79 o -8 0 2 6601.73 6650.22 129.33 o -6 0 2 844.08 852.48 31.96 o -4 0 2 6280.09 6284.39 116.31 o -2 0 2 16764.10 16995.79 366.94 o 0 0 2 18241.83 19064.02 408.90 o 2 0 2 5847.95 5922.90 153.64 o 4 0 2 3603.20 3439.15 85.04 o 6 0 2 62.33 105.56 14.19 o 8 0 2 627.33 627.80 28.40 o 10 0 2 888.52 1063.03 39.47 o 12 0 2 4363.64 4179.78 181.48 o 14 0 2 979.53 992.13 66.15 o 16 0 2 115.64 132.52 37.54 o 18 0 2 8.41 6.58 50.54 o 20 0 2 885.26 999.51 112.07 o 22 0 2 945.08 1082.39 129.44 o -22 1 2 245.84 210.84 65.50 o -21 1 2 24.00 49.79 37.87 o -20 1 2 119.84 83.08 37.61 o -19 1 2 168.40 177.00 38.79 o -18 1 2 226.16 208.31 37.79 o -17 1 2 372.51 370.72 37.14 o -16 1 2 1169.31 1179.15 46.93 o -15 1 2 1424.78 1416.11 49.25 o -14 1 2 239.46 235.88 22.89 o -13 1 2 141.55 145.03 19.78 o -12 1 2 2012.15 2009.93 50.81 o -11 1 2 169.19 172.80 14.96 o -10 1 2 204.24 196.34 14.46 o -9 1 2 2459.77 2303.97 43.12 o -8 1 2 1452.57 1458.02 39.66 o -7 1 2 14173.48 14186.08 226.12 o -6 1 2 824.45 851.45 35.44 o -5 1 2 898.69 910.24 37.11 o -4 1 2 10151.07 10301.14 172.85 o -3 1 2 76716.37 76206.97 1017.96 o -2 1 2 11485.17 11780.64 151.84 o -1 1 2 1578.17 1376.03 27.51 o 0 1 2 2397.81 2236.74 36.36 o 1 1 2 3374.29 3396.01 50.19 o 2 1 2 1932.26 1910.26 32.83 o 3 1 2 2694.25 2804.56 59.77 o 4 1 2 0.67 -0.61 9.30 o 5 1 2 7729.77 7545.82 112.20 o 6 1 2 177.10 192.41 11.68 o 7 1 2 5143.13 5196.74 81.28 o 8 1 2 80.28 86.24 11.89 o 9 1 2 1757.86 1815.66 37.94 o 10 1 2 369.06 323.80 17.39 o 11 1 2 2335.31 2307.62 52.94 o 12 1 2 204.75 174.36 17.74 o 13 1 2 778.52 796.46 38.70 o 14 1 2 50.33 55.63 20.76 o 15 1 2 199.69 179.88 26.49 o 16 1 2 54.77 51.47 23.34 o 17 1 2 749.59 806.35 50.73 o 18 1 2 52.85 60.29 35.10 o 19 1 2 2395.49 2313.31 114.46 o 20 1 2 212.24 207.32 53.17 o 21 1 2 262.99 241.84 56.60 o 22 1 2 187.34 183.38 62.87 o -21 2 2 2.16 -28.50 42.93 o -20 2 2 81.58 98.67 42.37 o -19 2 2 122.90 109.99 34.11 o -18 2 2 3.41 38.73 29.17 o -17 2 2 7.27 11.54 28.30 o -16 2 2 907.77 966.55 54.38 o -15 2 2 99.53 81.45 25.72 o -14 2 2 598.37 656.19 40.48 o -13 2 2 85.36 104.11 21.79 o -12 2 2 516.59 521.80 31.63 o -11 2 2 18.48 13.56 18.91 o -10 2 2 1364.87 1293.27 48.12 o -9 2 2 68.95 52.62 18.14 o -8 2 2 1062.07 1097.52 58.86 o -7 2 2 5070.30 5257.20 87.59 o -6 2 2 727.56 685.47 21.47 o -5 2 2 1188.96 1071.56 29.85 o -4 2 2 1623.04 1726.93 38.39 o -3 2 2 2758.94 2912.60 50.59 o -2 2 2 9508.63 9338.76 134.41 o -1 2 2 9.54 20.36 12.22 o 0 2 2 1050.04 1003.91 28.87 o 1 2 2 2.80 12.71 11.33 o 2 2 2 230.82 252.00 15.99 o 3 2 2 2305.51 2127.34 55.98 o 4 2 2 4488.38 4497.28 76.01 o 5 2 2 419.78 432.19 19.87 o 6 2 2 5657.31 5675.15 92.26 o 7 2 2 2139.94 2121.77 44.31 o 8 2 2 11.10 9.70 12.45 o 9 2 2 266.97 250.07 29.72 o 10 2 2 864.54 784.57 45.46 o 11 2 2 222.95 261.86 32.00 o 12 2 2 1271.65 1331.70 59.25 o 13 2 2 5.79 -16.48 22.55 o 14 2 2 416.99 433.59 38.96 o 15 2 2 780.83 745.70 48.44 o 16 2 2 528.73 553.15 44.78 o 17 2 2 1025.41 953.12 57.73 o 18 2 2 1537.58 1605.52 80.12 o 19 2 2 70.39 55.01 34.49 o 20 2 2 1177.45 1235.92 88.89 o 21 2 2 255.65 220.50 72.23 o -19 3 2 378.57 375.42 64.46 o -18 3 2 20.20 -23.83 56.80 o -17 3 2 142.18 162.52 45.08 o -16 3 2 17.44 67.89 36.99 o -15 3 2 670.51 657.13 82.62 o -14 3 2 225.18 185.76 40.73 o -13 3 2 1391.17 1300.57 71.51 o -12 3 2 1253.46 1389.09 72.93 o -11 3 2 861.03 767.57 54.66 o -10 3 2 1.34 10.06 21.94 o -9 3 2 4778.43 4792.83 110.64 o -8 3 2 626.23 586.18 36.06 o -7 3 2 180.25 197.18 27.27 o -6 3 2 417.39 402.85 32.33 o -5 3 2 43.06 57.47 27.22 o -4 3 2 561.27 611.99 39.46 o -3 3 2 79.12 83.49 16.36 o -2 3 2 23.11 -10.32 14.24 o -1 3 2 5323.02 5321.13 83.31 o 0 3 2 3621.49 3756.77 67.52 o 1 3 2 1517.92 1607.98 45.76 o 2 3 2 4011.47 4085.80 78.83 o 3 3 2 1726.93 1772.65 49.18 o 4 3 2 104.70 104.46 17.01 o 5 3 2 1025.65 1078.00 43.53 o 6 3 2 245.33 247.97 28.40 o 7 3 2 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24 0.69 -22.90 41.90 o -1 1 24 757.34 612.54 96.81 o 0 1 24 68.29 -21.94 87.15 o 1 1 24 1158.81 915.66 108.98 o 2 1 24 97.05 87.13 64.27 o 3 1 24 0.54 24.63 60.96 o 4 1 24 60.60 57.06 65.70 o 5 1 24 134.98 85.88 70.99 o -2 2 24 376.76 460.26 127.72 o -1 2 24 208.15 105.22 93.18 o -5 0 25 1960.88 2531.82 262.66 o -3 0 25 371.79 285.95 110.04 o -1 0 25 96.06 67.47 87.55 o 1 0 25 18.71 9.64 84.34 o 3 0 25 123.40 135.75 107.63 o -4 1 25 72.92 22.99 58.62 o -3 1 25 123.08 57.45 50.80 o -2 1 25 366.67 370.53 88.16 o -1 1 25 0.60 2.50 61.61 o 0 1 25 8.47 -57.03 57.03 o 1 1 25 2.26 32.13 83.54 o