#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:39:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181184 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/63/2226342.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226342_Fobs loop_ _publ_author_name 'Khan, F. Nawaz' 'Prabakaran, K.' 'Roopan, S. Mohana' 'Hathwar, Venkatesha R.' 'Akkurt, Mehmet' _publ_section_title ; Methyl 1-methyl-1H-1,2,3-triazole-4-carboxylate ; _journal_coeditor_code XU2764 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1468 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.053 _cell_angle_beta 86.865 _cell_angle_gamma 76.528 _cell_length_a 5.6970 _cell_length_b 7.1314 _cell_length_c 8.6825 _exptl_crystal_F_000 148.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file xu2764Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' F-III in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1488.12 1486.75 8.58 o 2 0 0 265.61 274.10 1.96 o 3 0 0 4.87 6.64 0.68 o 4 0 0 86.03 88.39 1.51 o 5 0 0 50.16 41.38 2.70 o 6 0 0 0.25 0.64 2.16 o -6 1 0 11.75 13.43 2.29 o -5 1 0 0.18 5.14 2.44 o -4 1 0 5.98 15.74 1.72 o -1 1 0 97.94 89.81 1.22 o 0 1 0 2.73 3.01 0.39 o 1 1 0 117.62 106.41 1.09 o 2 1 0 35.53 33.79 0.78 o 3 1 0 7.19 3.87 0.77 o 4 1 0 4.56 2.54 0.50 o 5 1 0 3.04 3.27 2.06 o 6 1 0 12.13 9.14 2.44 o -5 2 0 22.81 50.74 5.06 o -4 2 0 49.00 51.57 2.40 o -3 2 0 3.85 3.74 0.75 o -2 2 0 102.11 94.79 2.58 o -1 2 0 374.49 382.83 2.76 o 0 2 0 8690.18 8039.55 23.54 o 1 2 0 1659.37 1610.05 7.12 o 2 2 0 166.96 152.38 2.43 o 3 2 0 8.86 8.71 0.85 o 4 2 0 64.94 63.01 1.63 o 5 2 0 55.59 50.58 2.81 o 6 2 0 0.85 1.72 2.24 o -5 3 0 0.92 2.60 2.80 o -4 3 0 1.38 3.80 1.49 o -3 3 0 0.08 0.59 1.05 o -2 3 0 3.95 2.58 0.76 o -1 3 0 41.51 28.94 0.95 o 0 3 0 4.22 5.45 0.58 o 1 3 0 40.84 38.00 1.22 o 2 3 0 5.87 6.32 1.09 o 3 3 0 0.41 1.00 1.00 o 4 3 0 0.03 0.79 0.96 o -4 4 0 19.03 26.54 2.97 o -3 4 0 8.18 7.93 2.27 o -2 4 0 12.10 10.78 2.82 o -1 4 0 47.52 44.57 1.83 o 0 4 0 1360.85 1269.64 8.14 o 1 4 0 549.94 547.66 4.47 o 2 4 0 24.29 22.08 1.68 o 4 4 0 28.84 39.83 3.61 o 5 4 0 29.82 30.00 6.56 o 6 4 0 0.64 0.33 2.16 o -4 5 0 0.00 1.79 2.84 o -3 5 0 0.02 0.88 2.35 o -2 5 0 1.31 2.01 2.14 o -1 5 0 6.97 17.53 2.53 o 0 5 0 2.11 4.72 0.90 o 1 5 0 7.94 7.84 1.20 o 2 5 0 1.31 2.47 1.36 o 3 5 0 0.16 1.47 1.71 o 4 5 0 1.19 1.40 1.72 o 5 5 0 0.13 0.44 3.15 o 6 5 0 5.00 5.32 3.29 o -3 6 0 4.07 3.78 2.66 o -2 6 0 0.22 2.86 2.80 o -1 6 0 5.43 3.90 2.33 o 0 6 0 215.38 204.07 3.51 o 1 6 0 127.90 119.91 2.73 o 2 6 0 0.73 1.63 1.33 o 3 6 0 0.01 2.73 1.51 o 4 6 0 11.46 13.41 2.07 o 5 6 0 10.87 8.12 2.36 o -1 7 0 1.28 3.43 2.52 o 1 7 0 2.59 3.91 2.33 o 2 7 0 0.33 0.96 1.44 o 3 7 0 0.22 0.49 1.57 o 4 7 0 1.07 1.09 1.82 o 2 8 0 0.12 0.23 2.70 o -4 -7 1 0.05 0.44 2.04 o -3 -7 1 8.35 8.75 1.99 o -2 -7 1 4.01 4.64 2.42 o -1 -7 1 22.18 19.60 2.86 o 0 -7 1 0.59 2.77 2.39 o 1 -7 1 0.12 0.00 2.53 o -5 -6 1 12.72 13.21 2.64 o -4 -6 1 7.94 7.37 2.08 o -3 -6 1 1.67 0.77 1.70 o -2 -6 1 0.12 0.10 1.30 o -1 -6 1 12.07 10.89 1.33 o 0 -6 1 8.60 9.33 2.29 o 1 -6 1 1.66 3.64 2.49 o 2 -6 1 1.82 6.56 2.98 o -5 -5 1 24.72 29.23 4.01 o -4 -5 1 0.35 0.94 2.04 o -3 -5 1 71.54 74.08 3.04 o -2 -5 1 0.68 1.05 1.53 o -1 -5 1 103.44 123.12 2.58 o 0 -5 1 6.37 15.20 1.13 o 1 -5 1 0.03 1.38 2.57 o 2 -5 1 8.99 7.58 2.09 o 3 -5 1 14.43 11.01 2.67 o -6 -4 1 0.86 0.21 2.46 o -5 -4 1 22.80 25.81 3.50 o -4 -4 1 21.35 31.40 2.49 o -3 -4 1 3.51 5.00 2.05 o -1 -4 1 57.88 59.49 4.45 o 0 -4 1 33.96 36.65 1.13 o 1 -4 1 5.49 7.13 1.25 o 2 -4 1 17.23 19.69 2.20 o 3 -4 1 5.38 5.45 2.14 o 4 -4 1 7.35 6.10 2.48 o -6 -3 1 6.26 2.39 2.27 o -5 -3 1 61.75 74.35 4.12 o -4 -3 1 3.50 4.07 1.81 o -3 -3 1 315.11 301.17 5.86 o -2 -3 1 25.48 27.40 1.71 o -1 -3 1 462.35 441.89 3.51 o 0 -3 1 73.72 66.06 1.25 o 1 -3 1 0.04 0.36 0.73 o 2 -3 1 35.92 30.98 1.40 o 3 -3 1 36.17 35.08 3.16 o 4 -3 1 6.04 6.10 2.06 o 5 -3 1 14.35 17.59 3.76 o -6 -2 1 1.56 1.14 2.40 o -5 -2 1 26.72 25.55 2.47 o -4 -2 1 42.95 37.31 1.62 o -3 -2 1 0.38 2.71 0.86 o -2 -2 1 5.46 5.00 1.02 o -1 -2 1 230.47 193.36 2.04 o 0 -2 1 101.58 104.93 1.25 o 1 -2 1 17.32 18.81 0.73 o 2 -2 1 114.04 102.97 4.00 o 3 -2 1 37.47 37.30 1.35 o 4 -2 1 13.99 11.52 1.38 o 5 -2 1 3.38 4.70 3.28 o -6 -1 1 4.84 4.83 2.28 o -5 -1 1 84.20 81.73 3.02 o -4 -1 1 12.75 12.16 1.02 o -3 -1 1 556.84 573.61 6.12 o -2 -1 1 261.61 264.63 2.10 o -1 -1 1 1902.92 1733.06 7.51 o 0 -1 1 252.29 246.19 2.23 o 1 -1 1 0.74 0.90 0.31 o 2 -1 1 112.46 115.85 2.99 o 3 -1 1 102.61 144.15 3.40 o 5 -1 1 32.49 51.01 5.10 o 6 -1 1 5.11 7.36 2.78 o -6 0 1 2.10 3.10 2.17 o -5 0 1 20.59 24.83 2.08 o -4 0 1 48.55 44.28 1.77 o -3 0 1 0.04 0.58 0.44 o -2 0 1 17.05 18.32 1.40 o -1 0 1 382.36 372.26 2.04 o 1 0 1 7.23 7.08 0.43 o 2 0 1 455.21 460.51 2.90 o 3 0 1 125.72 135.56 2.84 o 4 0 1 24.77 23.64 1.05 o 5 0 1 4.39 5.60 1.74 o 6 0 1 5.41 5.23 1.88 o -6 1 1 1.77 0.06 2.45 o -5 1 1 51.04 49.20 2.57 o -4 1 1 28.25 29.10 2.44 o -3 1 1 349.23 354.87 7.71 o -2 1 1 395.16 371.25 4.46 o -1 1 1 1634.52 1474.48 7.99 o 0 1 1 496.85 475.47 2.47 o 1 1 1 0.02 0.34 0.50 o 2 1 1 168.16 179.08 2.40 o 3 1 1 188.12 183.62 2.79 o 4 1 1 31.99 36.51 1.97 o 5 1 1 47.19 38.98 2.65 o 6 1 1 11.31 8.27 2.13 o -6 2 1 1.64 3.69 3.72 o -5 2 1 10.08 16.06 2.62 o -4 2 1 27.90 28.09 2.62 o -3 2 1 1.86 1.58 0.77 o -2 2 1 2.87 2.62 0.75 o -1 2 1 266.03 230.51 2.30 o 0 2 1 228.36 232.92 1.86 o 1 2 1 0.05 0.00 0.54 o 2 2 1 274.68 274.44 2.12 o 3 2 1 157.77 164.12 4.08 o 4 2 1 31.78 32.38 1.89 o 5 2 1 6.92 5.74 1.13 o 6 2 1 6.76 5.86 2.96 o -5 3 1 15.09 14.43 3.09 o -4 3 1 21.89 21.59 2.09 o -3 3 1 85.77 72.95 2.76 o -2 3 1 136.31 118.57 2.93 o -1 3 1 263.70 269.96 3.60 o 0 3 1 317.39 313.75 2.14 o 1 3 1 0.35 1.27 0.55 o 2 3 1 91.86 79.62 1.60 o 3 3 1 112.09 116.06 2.31 o 4 3 1 36.41 38.71 1.73 o 5 3 1 33.26 32.77 2.23 o 6 3 1 15.37 24.30 3.81 o -5 4 1 3.63 4.78 3.08 o -4 4 1 10.87 9.93 2.28 o -3 4 1 2.04 3.02 1.23 o -2 4 1 0.58 0.00 0.62 o -1 4 1 69.28 57.47 1.77 o 0 4 1 98.73 106.95 2.23 o 1 4 1 0.99 2.09 0.87 o 2 4 1 21.73 45.67 3.50 o 4 4 1 20.37 24.60 2.01 o 5 4 1 11.74 16.75 4.79 o 6 4 1 3.68 4.21 2.99 o -4 5 1 6.78 7.64 2.78 o -3 5 1 10.11 8.62 2.50 o -2 5 1 23.07 27.40 3.55 o -1 5 1 53.57 58.56 3.95 o 0 5 1 77.45 77.36 2.06 o 2 5 1 17.76 13.49 1.58 o 3 5 1 44.15 45.28 2.96 o 4 5 1 23.42 20.04 1.99 o 5 5 1 10.77 10.12 2.19 o 6 5 1 12.25 12.75 2.76 o -3 6 1 0.96 5.32 2.40 o -2 6 1 1.06 6.23 2.64 o -1 6 1 7.35 5.56 2.39 o 0 6 1 32.76 33.23 2.00 o 1 6 1 1.18 0.78 1.27 o 2 6 1 1.29 1.97 1.33 o 3 6 1 10.53 9.22 1.62 o 4 6 1 8.41 9.52 1.75 o 5 6 1 8.78 6.60 2.68 o -2 7 1 2.55 4.31 3.11 o -1 7 1 13.90 13.72 3.29 o 0 7 1 19.36 19.00 2.21 o 1 7 1 0.13 1.24 1.60 o 2 7 1 2.56 1.23 1.43 o 3 7 1 13.82 11.91 1.67 o 4 7 1 11.25 9.35 1.77 o 0 8 1 8.46 7.47 2.63 o 1 8 1 1.10 0.00 2.49 o 2 8 1 0.04 2.69 2.54 o 3 8 1 1.00 1.44 1.72 o -3 -7 2 1.96 0.63 2.44 o -2 -7 2 0.18 3.69 2.89 o -1 -7 2 2.53 0.95 2.53 o 0 -7 2 0.61 3.90 2.46 o -4 -6 2 2.60 1.32 2.00 o -3 -6 2 8.79 8.23 1.77 o -2 -6 2 7.17 4.66 1.70 o -1 -6 2 0.50 2.26 2.03 o 0 -6 2 1.16 1.98 2.27 o 1 -6 2 0.00 2.55 2.35 o 2 -6 2 6.07 9.20 2.50 o -5 -5 2 30.87 25.53 3.69 o -4 -5 2 21.38 20.30 2.38 o -3 -5 2 3.86 4.36 1.83 o -2 -5 2 0.10 2.25 1.51 o 0 -5 2 11.23 18.50 2.37 o 2 -5 2 0.71 0.00 2.07 o 3 -5 2 8.64 8.32 3.02 o -6 -4 2 13.61 11.48 2.79 o -5 -4 2 65.34 62.52 3.64 o -2 -4 2 18.46 21.01 1.97 o -1 -4 2 4.21 6.12 1.15 o 0 -4 2 17.65 16.16 1.91 o 1 -4 2 0.35 0.00 1.12 o 2 -4 2 22.56 24.27 2.21 o 3 -4 2 9.23 7.04 2.26 o 4 -4 2 9.69 9.80 2.32 o -6 -3 2 19.01 33.99 3.57 o -5 -3 2 82.25 78.29 3.50 o -4 -3 2 70.36 75.16 3.11 o -3 -3 2 8.35 7.35 1.68 o -2 -3 2 13.81 9.85 1.65 o -1 -3 2 97.26 76.55 2.20 o 0 -3 2 118.11 117.57 2.37 o 1 -3 2 9.59 6.65 0.91 o 2 -3 2 4.47 5.44 1.06 o 3 -3 2 39.95 39.44 2.94 o 4 -3 2 0.01 0.00 2.09 o 5 -3 2 36.15 32.99 4.25 o -6 -2 2 12.96 12.35 2.33 o -5 -2 2 125.45 120.65 3.55 o -4 -2 2 26.53 25.22 1.89 o -3 -2 2 36.81 40.74 2.41 o -2 -2 2 58.20 62.78 2.09 o -1 -2 2 49.46 53.83 1.56 o 0 -2 2 135.58 131.76 2.40 o 1 -2 2 5.34 4.40 0.88 o 2 -2 2 87.42 94.76 2.53 o 3 -2 2 50.95 42.50 1.83 o 4 -2 2 27.67 31.73 4.29 o 5 -2 2 12.95 18.83 3.32 o -6 -1 2 16.31 12.61 2.65 o -5 -1 2 123.86 121.64 3.81 o -4 -1 2 133.62 142.72 4.42 o -3 -1 2 27.25 30.40 1.50 o -2 -1 2 54.22 56.56 1.39 o -1 -1 2 244.99 227.63 2.24 o 0 -1 2 538.12 523.25 3.35 o 1 -1 2 36.73 37.03 1.08 o 5 -1 2 85.53 83.10 3.72 o 6 -1 2 16.87 16.04 2.83 o -6 0 2 6.09 8.70 2.48 o -5 0 2 129.34 132.23 3.46 o -4 0 2 49.22 37.10 1.65 o -3 0 2 38.08 46.39 1.36 o -2 0 2 150.30 156.90 2.46 o -1 0 2 210.69 204.89 2.41 o 1 0 2 38.51 43.01 2.32 o 2 0 2 302.94 300.41 2.01 o 3 0 2 165.20 165.85 2.85 o 4 0 2 52.54 47.70 1.96 o 5 0 2 39.73 39.59 2.42 o 6 0 2 1.22 0.00 1.98 o -6 1 2 7.68 6.00 2.70 o -5 1 2 92.67 92.38 3.31 o -4 1 2 137.16 145.50 3.45 o -2 1 2 60.50 93.48 4.73 o -1 1 2 119.05 118.04 1.50 o 0 1 2 872.90 815.89 3.40 o 1 1 2 33.98 31.25 0.85 o 2 1 2 4.98 5.77 0.47 o 3 1 2 225.18 235.37 2.87 o 4 1 2 22.98 23.93 1.47 o 5 1 2 110.06 103.25 4.02 o 6 1 2 40.92 37.36 2.89 o -5 2 2 76.13 88.62 3.43 o -4 2 2 32.11 27.21 3.26 o -3 2 2 17.25 18.12 1.09 o -2 2 2 76.54 85.08 2.07 o -1 2 2 48.05 46.22 1.22 o 0 2 2 396.67 398.00 2.23 o 1 2 2 72.50 66.66 0.95 o 2 2 2 235.75 223.06 2.87 o 3 2 2 243.90 239.58 2.96 o 4 2 2 46.30 38.94 1.87 o 5 2 2 60.42 53.85 2.15 o 6 2 2 2.15 1.35 1.98 o -5 3 2 37.08 42.44 3.70 o -4 3 2 67.02 66.90 3.04 o -3 3 2 50.44 46.17 1.59 o -2 3 2 25.75 16.96 1.49 o -1 3 2 5.35 3.90 1.32 o 0 3 2 308.68 301.05 2.46 o 1 3 2 89.19 84.35 1.27 o 2 3 2 2.33 1.28 0.62 o 3 3 2 130.52 131.47 1.91 o 4 3 2 41.57 42.17 2.53 o 5 3 2 80.96 77.29 2.67 o 6 3 2 50.33 54.42 3.70 o -5 4 2 26.02 22.27 3.55 o -4 4 2 13.42 10.87 2.54 o -3 4 2 4.31 3.24 1.63 o -2 4 2 23.38 25.02 1.60 o -1 4 2 0.48 0.42 1.01 o 0 4 2 76.77 86.71 2.33 o 1 4 2 39.17 39.54 1.48 o 2 4 2 41.87 55.96 2.15 o 3 4 2 119.34 151.16 2.75 o 4 4 2 13.15 16.26 2.14 o 5 4 2 44.45 41.07 2.68 o 6 4 2 1.29 0.96 2.54 o -4 5 2 18.19 17.04 2.96 o -3 5 2 23.91 21.89 2.37 o -2 5 2 0.62 2.45 1.87 o -1 5 2 0.23 1.24 1.03 o 0 5 2 38.71 57.45 2.13 o 1 5 2 29.59 36.16 1.70 o 2 5 2 0.87 1.13 1.13 o 3 5 2 32.06 34.07 2.03 o 4 5 2 27.41 23.78 1.92 o 5 5 2 34.31 30.64 2.96 o 6 5 2 34.02 39.94 4.32 o -3 6 2 1.02 2.15 2.84 o -2 6 2 8.49 5.73 1.98 o -1 6 2 0.39 0.44 2.04 o 0 6 2 9.70 11.44 1.63 o 1 6 2 8.81 9.25 1.41 o 2 6 2 5.72 6.83 1.38 o 3 6 2 32.80 29.71 1.94 o 4 6 2 2.53 2.22 1.50 o 5 6 2 19.11 17.49 2.54 o -2 7 2 0.55 0.14 2.19 o -1 7 2 0.38 1.02 2.48 o 0 7 2 3.30 3.65 2.24 o 1 7 2 2.79 2.16 1.59 o 2 7 2 0.50 0.00 1.38 o 3 7 2 5.25 2.79 1.47 o 4 7 2 8.49 8.35 1.80 o 0 8 2 0.99 1.34 3.16 o 1 8 2 1.24 0.40 1.93 o 2 8 2 0.78 0.52 1.81 o 3 8 2 7.55 7.04 1.73 o -4 -6 3 4.14 3.57 2.38 o -3 -6 3 2.53 2.89 2.03 o -2 -6 3 2.78 2.55 2.22 o -1 -6 3 0.47 1.24 2.35 o 0 -6 3 0.61 2.70 2.28 o 1 -6 3 0.43 0.46 2.39 o -5 -5 3 3.64 3.04 2.05 o -4 -5 3 11.36 8.65 1.96 o -3 -5 3 15.37 15.44 1.79 o -2 -5 3 18.13 16.49 1.60 o -1 -5 3 7.19 8.97 1.64 o 0 -5 3 3.40 7.39 2.14 o 2 -5 3 0.50 5.74 1.94 o 3 -5 3 0.15 0.00 2.89 o -5 -4 3 0.63 0.02 2.07 o -4 -4 3 8.80 10.53 1.90 o -3 -4 3 21.17 28.95 2.29 o -2 -4 3 5.01 6.57 1.64 o -1 -4 3 4.23 8.85 1.31 o 0 -4 3 4.51 4.77 1.32 o 1 -4 3 5.49 3.36 1.95 o 2 -4 3 17.97 18.26 2.11 o 3 -4 3 1.05 2.54 2.71 o 4 -4 3 10.17 7.01 2.65 o -6 -3 3 8.20 7.21 2.55 o -5 -3 3 5.19 9.00 2.48 o -4 -3 3 29.07 29.69 2.91 o -3 -3 3 68.15 66.97 2.79 o -2 -3 3 88.22 86.04 3.29 o -1 -3 3 25.06 25.43 1.58 o 0 -3 3 24.68 24.71 1.55 o 1 -3 3 2.28 1.36 0.46 o 2 -3 3 7.12 5.44 1.64 o 3 -3 3 0.02 0.00 2.32 o 4 -3 3 9.83 7.89 1.95 o -6 -2 3 3.24 1.65 2.26 o -5 -2 3 3.71 3.86 1.67 o -4 -2 3 5.86 5.43 1.75 o -3 -2 3 73.85 68.95 2.60 o -2 -2 3 1.12 1.05 1.40 o -1 -2 3 13.31 14.61 1.63 o 0 -2 3 18.69 15.24 1.43 o 1 -2 3 54.01 49.03 1.54 o 2 -2 3 51.49 45.87 2.02 o 3 -2 3 11.75 14.08 1.29 o 4 -2 3 28.16 30.65 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2.68 o -2 -2 8 0.89 1.17 2.68 o -1 -2 8 3.90 5.72 2.61 o 0 -2 8 17.26 11.58 2.75 o 1 -2 8 2.51 0.97 2.25 o -3 -1 8 10.90 9.73 2.90 o -2 -1 8 14.53 10.14 3.38 o -1 -1 8 2.55 2.88 2.41 o 0 -1 8 15.17 15.38 2.70 o 1 -1 8 56.39 56.92 3.40 o 2 -1 8 2.60 3.46 2.14 o -3 0 8 0.02 0.43 2.66 o -2 0 8 2.86 3.22 2.60 o -1 0 8 10.34 11.29 2.89 o 0 0 8 39.77 59.03 3.15 o 1 0 8 5.00 7.60 1.90 o 2 0 8 0.06 2.26 2.90 o 3 0 8 0.10 0.00 2.99 o -3 1 8 10.60 9.53 2.02 o -2 1 8 25.61 21.50 2.32 o -1 1 8 4.33 3.81 1.85 o 0 1 8 16.42 14.84 1.96 o 1 1 8 115.86 104.89 3.25 o 2 1 8 9.01 6.57 1.94 o 3 1 8 6.12 5.58 2.34 o 4 1 8 13.82 14.40 4.53 o -3 2 8 0.54 0.00 1.79 o -2 2 8 3.28 6.69 1.85 o -1 2 8 14.16 13.37 2.13 o 0 2 8 64.05 53.11 2.60 o 1 2 8 8.32 7.84 1.71 o 2 2 8 0.04 2.58 1.95 o 3 2 8 0.00 0.88 1.89 o 4 2 8 1.91 1.39 2.22 o -3 3 8 6.97 8.66 1.99 o -2 3 8 26.88 22.59 2.26 o -1 3 8 3.19 2.13 1.71 o 0 3 8 6.51 4.92 1.71 o 1 3 8 130.14 121.18 3.57 o 2 3 8 18.25 12.90 2.01 o 3 3 8 6.36 6.39 2.04 o 4 3 8 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