#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:39:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181184 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/63/2226347.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226347_Fobs loop_ _publ_author_name 'Assey, Gervas' 'Butcher, Ray J.' 'Gultneh, Yilma' 'Yisgedu, Teshome' _publ_section_title ; [2,2'-(2,6,9,13-Tetraazatetradecane-1,14-diyl)diphenolato]iron(III) iodide ; _journal_coeditor_code ZL2278 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m711 _journal_page_last m712 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.3958 _cell_length_b 13.0509 _cell_length_c 19.4047 _exptl_crystal_F_000 1148.00 _reflns_d_resolution_high 0.6220 _cod_data_source_file zl2278Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ga08-4 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 270.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 10029.80 8708.73 93.92 o 6 0 0 370.78 334.05 26.13 o 8 0 0 13.17 6.58 14.79 o 10 0 0 181.59 138.09 47.25 o 12 0 0 21.29 60.39 73.94 o 14 0 0 121.71 160.81 69.59 o 3 1 0 8624.62 8575.15 40.00 o 4 1 0 1285.43 1285.85 12.97 o 5 1 0 1478.05 1464.87 16.83 o 6 1 0 6314.01 6390.31 34.19 o 7 1 0 40.48 46.83 12.01 o 8 1 0 7157.18 7466.53 49.07 o 9 1 0 212.29 142.28 24.90 o 10 1 0 4728.13 4874.74 68.95 o 11 1 0 49.83 77.66 36.22 o 12 1 0 1006.00 1037.15 55.33 o 13 1 0 30.03 29.91 43.62 o 14 1 0 111.44 114.34 48.22 o 2 2 0 10541.34 10879.43 84.09 o 3 2 0 1700.52 1919.35 18.51 o 4 2 0 5080.42 5381.58 56.20 o 5 2 0 241.89 214.89 9.99 o 6 2 0 309.12 311.17 15.77 o 7 2 0 3679.76 3702.93 29.11 o 8 2 0 553.45 486.95 19.23 o 9 2 0 6027.44 6219.16 61.05 o 10 2 0 19.33 4.13 32.01 o 11 2 0 4163.63 4158.96 70.86 o 12 2 0 0.62 -14.86 45.30 o 13 2 0 348.51 359.54 48.07 o 14 2 0 4.66 -3.69 47.19 o 1 3 0 73242.09 78481.94 756.66 o 2 3 0 265.57 243.80 11.60 o 3 3 0 8771.78 7848.08 55.69 o 4 3 0 33.09 43.12 10.95 o 6 3 0 150.22 151.34 13.48 o 7 3 0 3.11 23.80 15.52 o 8 3 0 69.06 77.86 16.94 o 9 3 0 366.89 325.63 27.70 o 10 3 0 1.31 1.11 31.88 o 11 3 0 448.95 390.70 41.01 o 12 3 0 187.98 131.22 40.99 o 13 3 0 39.82 14.53 42.72 o 14 3 0 2.37 29.26 68.52 o 0 4 0 18275.20 19967.84 281.39 o 2 4 0 18592.87 18611.76 69.76 o 3 4 0 866.65 1018.59 19.59 o 4 4 0 781.73 652.35 16.40 o 5 4 0 2802.36 2843.82 32.50 o 6 4 0 1.59 16.14 13.98 o 7 4 0 4152.53 3951.61 37.92 o 8 4 0 354.84 358.08 20.92 o 9 4 0 2632.88 2712.33 46.64 o 10 4 0 88.59 58.96 29.37 o 11 4 0 1636.05 1667.85 53.08 o 12 4 0 15.73 -15.72 40.45 o 13 4 0 116.99 187.29 46.46 o 14 4 0 135.54 103.92 49.23 o 1 5 0 5520.99 5691.40 27.95 o 2 5 0 1023.26 1116.14 15.75 o 3 5 0 2390.05 2341.97 16.12 o 4 5 0 2.21 28.21 12.00 o 5 5 0 19.65 19.21 12.82 o 6 5 0 867.06 782.22 19.76 o 7 5 0 449.87 435.27 19.42 o 8 5 0 7275.92 7608.94 52.28 o 9 5 0 712.79 639.75 32.74 o 10 5 0 5486.05 5602.41 71.38 o 11 5 0 44.12 59.34 37.45 o 12 5 0 937.53 1018.58 51.86 o 13 5 0 1.96 -0.58 44.46 o 14 5 0 33.95 49.99 48.53 o 0 6 0 27906.04 26613.28 180.75 o 2 6 0 9352.12 8486.74 84.71 o 3 6 0 23.18 26.78 5.98 o 4 6 0 4255.73 3892.13 27.90 o 5 6 0 60.53 86.18 11.33 o 6 6 0 3368.57 3456.03 34.83 o 7 6 0 57.04 70.07 17.23 o 8 6 0 64.30 74.84 19.68 o 9 6 0 1563.33 1500.66 37.25 o 10 6 0 131.79 118.20 31.40 o 11 6 0 665.44 643.56 45.54 o 12 6 0 337.75 351.47 48.52 o 13 6 0 21.73 71.43 45.57 o 14 6 0 202.22 133.67 99.53 o 1 7 0 17669.36 17686.08 120.68 o 2 7 0 30.19 65.47 12.65 o 3 7 0 8209.37 8231.54 45.83 o 4 7 0 2.27 21.94 6.97 o 5 7 0 2424.85 2382.45 28.97 o 6 7 0 221.85 204.76 14.37 o 7 7 0 1365.68 1377.47 46.19 o 8 7 0 2744.03 2804.54 58.07 o 9 7 0 15.42 21.27 26.31 o 10 7 0 849.07 973.23 46.36 o 11 7 0 166.40 207.59 41.85 o 12 7 0 768.82 848.24 59.28 o 13 7 0 129.25 172.53 54.23 o 0 8 0 944.13 914.81 22.82 o 1 8 0 2.66 23.53 9.30 o 2 8 0 909.55 864.71 14.08 o 3 8 0 9.91 19.34 16.19 o 4 8 0 226.05 211.32 16.42 o 5 8 0 2468.01 2339.71 36.59 o 6 8 0 805.51 770.92 18.51 o 7 8 0 4830.72 4870.23 56.10 o 8 8 0 74.58 66.47 27.73 o 9 8 0 3010.86 3169.99 53.92 o 10 8 0 0.08 24.73 35.32 o 11 8 0 2084.97 2069.07 69.64 o 12 8 0 315.72 319.61 52.66 o 13 8 0 246.58 351.03 73.45 o 1 9 0 18902.59 18866.61 124.45 o 2 9 0 507.53 469.13 16.43 o 3 9 0 5937.60 5967.86 74.74 o 4 9 0 412.55 426.16 22.60 o 5 9 0 1152.96 987.43 29.70 o 6 9 0 160.82 126.07 24.33 o 7 9 0 293.38 256.32 28.04 o 8 9 0 1021.09 870.09 45.40 o 9 9 0 1.16 -17.67 31.02 o 10 9 0 1409.30 1361.01 54.31 o 11 9 0 4.10 2.48 48.47 o 12 9 0 326.70 296.21 69.64 o 13 9 0 22.67 -16.50 91.24 o 0 10 0 15353.18 15465.01 100.04 o 1 10 0 282.57 247.47 15.65 o 2 10 0 7537.68 7477.01 49.75 o 3 10 0 33.08 45.64 18.49 o 4 10 0 2868.25 2820.53 41.25 o 5 10 0 670.18 663.91 28.52 o 6 10 0 74.11 74.45 24.53 o 7 10 0 220.85 228.40 28.26 o 8 10 0 97.68 65.75 28.73 o 9 10 0 1477.52 1563.25 50.62 o 10 10 0 79.17 128.73 40.71 o 11 10 0 425.46 487.34 55.50 o 12 10 0 148.19 159.82 68.50 o 1 11 0 24.05 33.53 15.35 o 2 11 0 701.35 678.29 22.35 o 3 11 0 2193.83 2133.06 38.21 o 4 11 0 107.86 94.10 22.07 o 5 11 0 102.70 166.21 25.43 o 6 11 0 525.25 486.11 31.04 o 7 11 0 326.65 310.94 30.20 o 8 11 0 1464.73 1489.13 85.23 o 9 11 0 47.31 -11.55 49.83 o 10 11 0 2614.68 2791.46 68.96 o 11 11 0 9.71 23.34 42.43 o 12 11 0 634.65 739.05 62.73 o 0 12 0 8341.48 8415.93 121.26 o 1 12 0 986.19 939.74 24.43 o 2 12 0 6145.10 6028.15 66.51 o 3 12 0 360.27 337.38 23.59 o 4 12 0 1633.05 1594.36 38.02 o 5 12 0 39.68 36.45 25.99 o 6 12 0 417.50 417.29 30.49 o 7 12 0 287.34 293.31 34.05 o 8 12 0 5.29 64.17 49.53 o 9 12 0 620.86 457.15 61.54 o 10 12 0 93.67 102.56 48.96 o 11 12 0 374.79 355.43 55.20 o 12 12 0 33.86 -30.43 89.93 o 1 13 0 4827.73 4860.75 46.08 o 2 13 0 364.98 351.57 21.43 o 3 13 0 3618.94 3607.81 58.22 o 4 13 0 313.96 358.56 31.35 o 5 13 0 9.18 -16.70 28.58 o 6 13 0 75.42 89.80 32.08 o 7 13 0 44.11 48.22 39.07 o 8 13 0 363.18 361.69 59.91 o 9 13 0 0.10 -1.43 54.30 o 10 13 0 34.45 77.38 50.94 o 11 13 0 188.63 135.76 54.27 o 0 14 0 1112.65 1060.18 38.01 o 1 14 0 0.51 1.22 18.85 o 2 14 0 299.49 262.56 21.60 o 3 14 0 0.05 11.34 21.05 o 4 14 0 177.87 186.31 28.22 o 5 14 0 5.53 11.89 29.48 o 6 14 0 104.71 117.62 40.89 o 7 14 0 443.61 444.80 49.77 o 8 14 0 343.43 384.06 86.76 o 9 14 0 583.62 543.68 69.81 o 10 14 0 0.50 22.65 52.11 o 1 15 0 1124.20 1183.72 30.59 o 2 15 0 38.49 59.73 21.88 o 3 15 0 984.44 1003.90 36.96 o 4 15 0 106.62 90.14 27.94 o 5 15 0 776.67 836.53 44.86 o 6 15 0 223.21 222.83 45.84 o 7 15 0 36.73 80.21 45.09 o 8 15 0 269.05 245.25 65.06 o 9 15 0 0.85 -2.36 57.95 o 0 16 0 2008.16 2046.30 50.05 o 1 16 0 27.82 47.12 25.07 o 2 16 0 1399.05 1442.03 41.72 o 3 16 0 558.33 547.53 34.77 o 4 16 0 296.33 344.25 46.04 o 5 16 0 125.94 133.12 38.04 o 6 16 0 66.20 60.85 37.76 o 7 16 0 63.62 83.93 40.86 o 8 16 0 32.15 1.53 62.57 o 1 17 0 827.34 877.01 38.30 o 2 17 0 128.40 98.70 35.99 o 3 17 0 16.60 57.14 34.69 o 4 17 0 1.68 -14.00 35.86 o 5 17 0 0.45 27.31 37.82 o 6 17 0 261.43 341.49 44.06 o 7 17 0 194.67 227.83 53.76 o 8 17 0 616.88 609.55 98.39 o 0 18 0 256.63 290.78 48.79 o 1 18 0 85.79 92.96 35.38 o 2 18 0 216.86 311.05 49.26 o 3 18 0 115.58 126.17 47.91 o 4 18 0 29.87 54.89 48.60 o 5 18 0 36.88 41.73 49.25 o 6 18 0 95.32 111.66 52.20 o 7 18 0 286.54 278.82 96.04 o 1 19 0 877.18 944.48 54.55 o 2 19 0 368.99 425.91 54.91 o 3 19 0 658.09 757.43 61.91 o 4 19 0 163.64 134.42 52.17 o 5 19 0 16.90 -0.43 86.18 o 6 19 0 4.78 -55.98 90.59 o 0 20 0 210.79 252.88 67.64 o 1 20 0 0.02 6.34 52.57 o 2 20 0 107.60 238.04 73.14 o 3 20 0 0.95 31.51 99.03 o 4 20 0 72.96 -20.39 91.63 o 3 0 1 7396.32 7924.04 98.94 o 4 0 1 3733.39 4065.06 28.26 o 5 0 1 13213.19 13051.07 50.86 o 6 0 1 248.52 248.73 10.92 o 7 0 1 4606.39 4238.07 37.89 o 8 0 1 431.34 378.33 13.06 o 9 0 1 1397.74 1331.64 26.53 o 10 0 1 552.64 514.69 30.01 o 11 0 1 42.89 60.98 36.00 o 12 0 1 477.47 509.55 44.46 o 13 0 1 277.87 267.40 45.95 o 14 0 1 0.18 10.26 53.55 o -14 1 1 345.88 395.55 62.71 o -13 1 1 99.07 83.86 45.15 o -12 1 1 74.70 96.08 39.65 o -11 1 1 644.70 585.95 42.64 o -10 1 1 189.75 216.03 28.18 o -9 1 1 326.07 348.28 20.22 o -8 1 1 759.29 672.46 18.39 o -7 1 1 3240.95 3136.94 39.02 o -6 1 1 4650.02 4820.14 28.86 o -5 1 1 11371.03 11339.15 93.70 o -4 1 1 9382.67 9710.54 43.50 o -3 1 1 17672.49 18194.34 84.79 o -2 1 1 257.10 327.30 31.73 o 2 1 1 128.59 198.35 15.93 o 3 1 1 18333.88 18898.59 61.32 o 4 1 1 9062.94 9499.94 59.22 o 5 1 1 12171.87 12471.86 69.07 o 6 1 1 4742.55 4847.93 31.19 o 7 1 1 3375.52 3371.14 28.92 o 8 1 1 729.45 694.02 14.50 o 9 1 1 269.42 249.96 22.90 o 10 1 1 209.97 217.87 34.18 o 11 1 1 671.41 650.61 41.78 o 12 1 1 87.44 96.11 39.77 o 13 1 1 108.26 72.37 43.57 o 14 1 1 366.48 385.40 52.02 o -14 2 1 372.37 373.91 52.05 o -13 2 1 192.71 261.32 44.91 o -12 2 1 141.08 91.72 40.53 o -11 2 1 327.74 321.11 40.08 o -10 2 1 241.89 207.98 28.46 o -9 2 1 523.84 491.50 29.22 o -8 2 1 4151.88 4107.50 68.10 o -7 2 1 2395.94 2499.07 30.61 o -6 2 1 11807.00 11617.26 100.66 o -5 2 1 2448.77 2422.85 22.93 o -4 2 1 17181.99 16901.71 110.27 o -3 2 1 6253.64 6584.51 63.77 o -2 2 1 23347.44 24345.62 185.28 o 2 2 1 23623.13 24726.09 237.78 o 3 2 1 6377.19 6759.49 48.67 o 4 2 1 17522.63 17278.19 83.81 o 5 2 1 2334.20 2330.39 20.69 o 6 2 1 12081.32 12010.78 47.26 o 7 2 1 2107.36 2270.60 24.98 o 8 2 1 4330.37 4452.98 35.07 o 9 2 1 465.80 457.96 23.67 o 10 2 1 254.84 231.00 34.60 o 11 2 1 306.83 286.74 39.66 o 12 2 1 193.51 150.36 41.47 o 13 2 1 159.74 162.31 45.22 o 14 2 1 354.17 403.60 52.03 o -14 3 1 326.53 422.47 54.09 o -13 3 1 31.79 -0.01 43.02 o -12 3 1 717.26 804.97 48.56 o -11 3 1 334.73 301.01 39.59 o -10 3 1 440.51 426.51 31.81 o -9 3 1 164.01 137.78 26.09 o -8 3 1 3145.75 3090.41 33.74 o -7 3 1 445.79 426.39 18.09 o -6 3 1 7178.36 7029.18 56.37 o -5 3 1 794.63 769.88 15.57 o -4 3 1 15031.65 15332.34 142.89 o -3 3 1 6015.47 6671.44 47.51 o -2 3 1 11017.34 11925.29 38.24 o -1 3 1 1338.33 1493.49 10.77 o 0 3 1 772.23 814.16 14.74 o 1 3 1 1468.92 1647.52 22.69 o 2 3 1 11221.41 12137.88 78.99 o 3 3 1 6246.30 7013.62 30.50 o 4 3 1 14642.75 14818.70 72.21 o 5 3 1 845.90 845.79 13.20 o 6 3 1 7255.85 7016.73 58.46 o 7 3 1 423.43 390.48 15.28 o 8 3 1 3230.50 3286.27 43.56 o 9 3 1 218.52 180.86 21.83 o 10 3 1 507.75 554.54 41.43 o 11 3 1 356.22 297.13 40.39 o 12 3 1 699.31 704.52 48.14 o 13 3 1 29.18 -9.74 43.56 o 14 3 1 344.60 363.44 52.56 o -14 4 1 117.68 71.40 48.78 o -13 4 1 96.15 79.94 44.45 o -12 4 1 223.35 198.41 42.41 o -11 4 1 370.54 352.52 34.36 o -10 4 1 93.46 78.70 29.80 o -9 4 1 219.60 207.53 28.45 o -8 4 1 533.38 484.56 20.89 o -7 4 1 2538.61 2442.44 29.03 o -6 4 1 3790.04 3851.25 32.74 o -5 4 1 7941.81 8128.89 80.80 o -4 4 1 19345.41 20080.56 116.02 o -3 4 1 12000.85 12662.19 45.41 o -2 4 1 12493.63 12968.25 98.03 o -1 4 1 91.80 129.56 11.32 o 0 4 1 16169.35 16583.97 115.06 o 1 4 1 187.03 235.73 7.64 o 2 4 1 12811.12 13303.06 94.98 o 3 4 1 12034.97 12864.45 95.75 o 4 4 1 19697.35 20613.44 94.77 o 5 4 1 8244.59 8484.80 49.66 o 6 4 1 3955.40 3988.43 32.09 o 7 4 1 2421.50 2330.19 29.34 o 8 4 1 432.28 404.82 23.45 o 9 4 1 216.88 193.42 23.78 o 10 4 1 95.30 117.23 34.46 o 11 4 1 359.59 343.99 40.97 o 12 4 1 214.81 220.75 42.53 o 13 4 1 97.94 141.96 45.13 o 14 4 1 134.84 163.42 50.09 o -14 5 1 329.09 289.92 51.55 o -13 5 1 496.25 500.00 49.37 o -12 5 1 194.72 271.88 44.62 o -11 5 1 92.24 119.73 32.92 o -10 5 1 326.69 353.10 33.73 o -9 5 1 693.01 615.09 33.19 o -8 5 1 163.31 180.66 23.43 o -7 5 1 5550.83 5633.00 60.44 o -6 5 1 656.25 606.92 19.68 o -5 5 1 8700.07 8613.52 79.37 o -4 5 1 3540.29 3609.10 30.16 o -3 5 1 13496.06 13346.08 43.30 o -2 5 1 3608.38 4048.06 28.93 o -1 5 1 10694.82 10531.16 49.75 o 0 5 1 2823.95 2768.90 31.30 o 1 5 1 10794.12 10754.20 61.14 o 2 5 1 3609.24 3990.76 39.63 o 3 5 1 13646.07 13577.16 46.46 o 4 5 1 3475.99 3565.47 31.20 o 5 5 1 8944.84 8844.85 61.12 o 6 5 1 685.21 647.67 19.44 o 7 5 1 5721.34 5715.06 47.51 o 8 5 1 151.43 181.24 19.24 o 9 5 1 654.96 606.93 28.59 o 10 5 1 324.50 424.75 39.34 o 11 5 1 92.56 84.72 38.24 o 12 5 1 181.36 231.82 44.87 o 13 5 1 517.83 490.53 49.81 o 14 5 1 353.27 379.36 60.07 o -13 6 1 513.76 647.71 62.42 o -12 6 1 136.59 89.53 43.20 o -11 6 1 332.88 364.89 42.18 o -10 6 1 195.05 186.81 32.25 o -9 6 1 1173.57 1193.25 40.65 o -8 6 1 1857.58 1815.20 39.29 o -7 6 1 2665.25 2722.07 38.43 o -6 6 1 325.42 263.20 22.41 o -5 6 1 6300.47 6306.33 54.53 o -4 6 1 1311.14 1325.15 19.36 o -3 6 1 10366.87 10546.80 73.72 o -2 6 1 403.35 401.40 13.01 o -1 6 1 2267.34 2503.52 61.13 o 0 6 1 1218.13 1420.42 18.84 o 1 6 1 2378.14 2619.24 21.73 o 2 6 1 385.99 408.12 11.38 o 3 6 1 10461.04 10814.27 79.85 o 4 6 1 1338.45 1299.94 26.23 o 5 6 1 6085.90 6119.44 44.47 o 6 6 1 336.84 295.97 18.71 o 7 6 1 2700.88 2628.06 31.50 o 8 6 1 1875.28 1740.79 31.27 o 9 6 1 1235.59 1210.02 32.24 o 10 6 1 189.61 168.71 37.19 o 11 6 1 309.52 331.36 41.52 o 12 6 1 133.15 171.69 44.67 o 13 6 1 493.28 630.83 51.47 o 14 6 1 80.98 151.34 99.82 o -13 7 1 142.82 206.72 70.49 o -12 7 1 50.46 55.34 42.75 o -11 7 1 64.38 37.51 39.38 o -10 7 1 125.18 139.73 33.05 o -9 7 1 326.97 305.97 28.98 o -8 7 1 397.78 385.41 22.29 o -7 7 1 2754.11 2743.32 35.15 o -6 7 1 2637.47 2662.10 39.52 o -5 7 1 3984.33 4030.15 31.95 o -4 7 1 5669.76 5810.77 40.13 o -3 7 1 8432.86 8443.83 36.63 o -2 7 1 2084.53 2115.41 41.15 o -1 7 1 6545.43 6861.90 45.41 o 0 7 1 121.62 185.26 12.06 o 1 7 1 6262.63 6485.39 33.43 o 2 7 1 2413.31 2529.45 22.81 o 3 7 1 8257.39 8259.48 74.15 o 4 7 1 5730.41 5729.75 93.34 o 5 7 1 3639.10 3641.37 37.60 o 6 7 1 2666.01 2688.02 27.59 o 7 7 1 2651.43 2595.04 38.92 o 8 7 1 469.71 476.20 25.93 o 9 7 1 298.04 280.64 27.12 o 10 7 1 119.12 147.99 42.78 o 11 7 1 77.15 42.61 45.49 o 12 7 1 54.16 130.79 50.71 o 13 7 1 139.03 144.12 55.78 o -13 8 1 58.38 84.15 69.21 o -12 8 1 109.77 81.39 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