#------------------------------------------------------------------------------
#$Date: 2010-10-08 09:13:40 +0300 (Fri, 08 Oct 2010) $
#$Revision: 1452 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226364.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2226364_Fobs
loop_
_publ_author_name
'Yapo, Yapi Marcellin'
'Konan, Kouakou Michel'
'Adjou, An\'e'
'Timotou, Ad\'eyol\'e'
'Tenon, Jules A.'
_publ_section_title
;
 Ethyl
 5-cyano-8-nitro-2,3,4,4a,5,6-hexahydro-1<i>H</i>-pyrido[1,2-<i>a</i>]quinoline-5-carboxylate
;
_journal_coeditor_code           BQ2218
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o1735
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             09-12-18
_audit_creation_method           CRYSTALS
_cell_angle_alpha                88.246(4)
_cell_angle_beta                 75.089(2)
_cell_angle_gamma                83.289(3)
_cell_length_a                   8.8257(4)
_cell_length_b                   9.2256(5)
_cell_length_c                   10.5011(6)
_[local]_cod_data_source_file    bq2218Isup2.hkl
_[local]_cod_data_source_block   I
loop_
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1 0 0 5.20 0.00 1.60 x
4 0 0 2513.20 2456.53 67.30 o
5 0 0 50398.80 49199.38 1349.90 o
6 0 0 2014.00 2090.54 65.50 o
7 0 0 1436.20 1444.82 50.30 o
8 0 0 1775.70 1686.25 69.30 o
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10 0 0 263.80 446.98 53.00 o
11 0 0 1863.60 21.81 545.50 o
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-2 1 0 15951.40 16689.59 509.70 o
-1 1 0 41.30 0.00 25.60 <
0 1 0 1.90 0.00 1.30 <
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4 1 0 40302.50 38387.43 1043.60 o
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7 1 0 46.40 45.96 18.20 <
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11 1 0 158.00 238.48 71.40 <
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1 3 0 3461.60 3736.93 86.00 o
2 3 0 2444.80 2488.85 72.80 o
3 3 0 2270.60 2278.01 74.80 o
4 3 0 831.10 773.10 36.60 o
5 3 0 75.80 19.92 20.40 o
6 3 0 -15.20 47.50 22.20 <
7 3 0 1754.90 1828.93 59.10 o
8 3 0 523.10 611.15 42.10 o
9 3 0 44.90 188.21 28.90 <
10 3 0 306.30 246.67 67.00 o
11 3 0 35.70 15.81 72.60 <
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0 4 0 5.20 1.97 3.40 <
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2 4 0 1473.80 1357.83 40.10 o
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4 4 0 685.40 658.08 34.70 o
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6 4 0 544.90 615.77 37.90 o
7 4 0 937.40 948.31 61.30 o
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0 5 0 1987.40 1905.82 39.80 o
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2 5 0 187.00 167.27 11.50 o
3 5 0 0.80 0.11 20.93 <
4 5 0 986.10 989.48 35.70 o
5 5 0 44.60 41.79 19.50 <
6 5 0 144.00 118.77 31.30 o
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8 5 0 40.30 11.06 33.40 <
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2 6 0 27.10 0.04 10.80 <
3 6 0 186.40 205.94 16.40 o
4 6 0 158.10 141.30 20.20 o
5 6 0 41.10 22.83 16.50 <
6 6 0 279.10 241.35 30.10 o
7 6 0 21.00 0.07 33.30 <
8 6 0 -31.40 1.68 36.50 <
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9 7 0 66.90 1.30 52.10 <
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1 8 0 35327.50 33904.75 596.00 o
2 8 0 -5.60 5.22 12.10 <
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5 8 0 3598.00 3347.91 97.00 o
6 8 0 3048.40 3004.37 93.90 o
7 8 0 17.10 9.25 27.20 <
8 8 0 471.30 570.07 58.20 o
9 8 0 -19.30 16.44 61.20 <
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0 9 0 -8.60 7.37 30.30 <
1 9 0 360.20 416.60 17.30 o
2 9 0 12.50 3.95 13.10 <
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5 9 0 9.10 3.79 20.50 <
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8 10 0 -24.10 58.91 86.60 <
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1 11 0 230.50 370.69 47.70 o
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