#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/64/2226421.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226421_Fobs loop_ _publ_author_name 'Kruczy\'nski, Tomasz' 'Pikies, Jerzy' 'Ponikiewski, \/Lukasz' _publ_section_title ; Trichloridobis(ethyldiphenylphosphine)(tetrahydrofuran)molybdenum(III) ; _journal_coeditor_code EZ2211 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m786 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 128.874 _cell_angle_gamma 90.000 _cell_length_a 15.4370 _cell_length_b 13.3562 _cell_length_c 20.2292 _exptl_crystal_F_000 1444.00 _reflns_d_resolution_high 0.7829 _[local]_cod_data_source_file ez2211Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KT2kor in P2(1)/n New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 254.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 158.80 226.62 39.30 o 6 0 0 340.48 59.79 128.72 o 7 0 0 207.29 344.04 158.57 o 8 0 0 119.28 -26.90 170.76 o 9 0 0 300.05 333.86 226.02 o 10 0 0 650.35 414.66 199.02 o 11 0 0 20.01 -28.57 203.34 o 12 0 0 612.23 434.94 213.26 o 13 0 0 222.00 273.61 221.64 o 14 0 0 461.02 411.57 266.75 o 15 0 0 171.05 380.58 251.01 o 1 1 0 6700.19 -11.15 43.76 o 2 1 0 5372.52 6283.10 73.98 o 5 1 0 8065.72 8111.28 157.30 o 6 1 0 402.07 344.22 35.11 o 7 1 0 332.61 230.31 100.21 o 8 1 0 30.00 -41.42 110.60 o 9 1 0 2117.46 2285.85 124.32 o 10 1 0 3602.63 3663.23 153.84 o 11 1 0 117.19 114.46 147.53 o 12 1 0 0.82 -68.29 149.67 o 13 1 0 0.12 -4.17 157.88 o 14 1 0 263.35 220.83 162.96 o 15 1 0 454.13 505.32 172.58 o 2 2 0 664.08 905.92 31.73 o 3 2 0 11645.08 13069.58 88.41 o 4 2 0 8039.52 8134.58 55.96 o 5 2 0 9010.68 9052.88 260.97 o 6 2 0 4781.84 4293.28 70.30 o 7 2 0 941.18 877.13 51.82 o 8 2 0 1137.92 1086.30 87.52 o 9 2 0 29.60 41.82 43.96 o 10 2 0 422.63 308.16 126.53 o 11 2 0 262.03 99.78 133.21 o 12 2 0 67.24 67.38 147.64 o 13 2 0 315.46 266.40 158.21 o 14 2 0 702.61 797.66 167.28 o 15 2 0 136.43 247.19 172.37 o 1 3 0 2267.03 2566.62 55.92 o 3 3 0 8104.57 8150.60 75.35 o 4 3 0 6499.98 6916.30 93.22 o 5 3 0 2925.30 2782.38 55.86 o 6 3 0 106.74 131.51 41.67 o 7 3 0 881.24 705.33 41.19 o 8 3 0 865.78 818.65 78.09 o 9 3 0 4182.15 4817.12 132.17 o 10 3 0 4421.29 4714.28 141.67 o 11 3 0 1376.12 1404.39 134.79 o 12 3 0 269.06 378.37 135.00 o 13 3 0 0.81 -105.88 152.26 o 14 3 0 528.81 367.74 161.27 o 15 3 0 777.16 773.64 237.49 o 1 4 0 13381.04 14742.90 228.61 o 2 4 0 3423.17 3534.13 40.34 o 3 4 0 358.88 382.08 55.83 o 4 4 0 5009.58 5634.32 72.30 o 5 4 0 14425.89 14610.72 139.08 o 6 4 0 6126.66 5569.42 64.67 o 7 4 0 2758.05 2763.04 53.94 o 8 4 0 996.03 1053.34 49.34 o 9 4 0 61.81 70.88 109.72 o 10 4 0 451.84 360.27 113.32 o 11 4 0 545.31 529.15 127.01 o 12 4 0 221.15 181.09 135.51 o 13 4 0 168.79 166.94 137.04 o 14 4 0 379.20 521.83 147.91 o 1 5 0 15469.87 16731.35 231.44 o 2 5 0 29741.74 31870.36 393.97 o 3 5 0 13315.64 13605.85 181.07 o 4 5 0 20027.36 20369.19 267.02 o 5 5 0 2957.71 2901.15 68.54 o 6 5 0 1312.24 1368.84 68.58 o 7 5 0 910.30 881.21 67.89 o 8 5 0 194.81 286.35 63.33 o 9 5 0 657.38 616.28 89.08 o 10 5 0 270.14 141.04 111.43 o 11 5 0 265.46 225.08 114.78 o 12 5 0 32.29 150.18 130.30 o 13 5 0 7.17 15.76 134.55 o 14 5 0 96.88 222.14 163.28 o 1 6 0 31856.59 34467.29 368.21 o 2 6 0 1853.84 1647.53 48.79 o 3 6 0 34.12 -5.09 67.80 o 4 6 0 3708.25 3831.07 56.24 o 5 6 0 12075.94 12535.63 138.33 o 6 6 0 3235.45 3190.79 72.75 o 7 6 0 1485.75 1464.66 73.24 o 8 6 0 1030.45 1098.45 74.43 o 9 6 0 342.88 362.27 89.10 o 10 6 0 20.44 68.88 106.77 o 11 6 0 56.99 60.31 110.93 o 12 6 0 125.61 177.50 118.18 o 13 6 0 111.90 93.20 150.63 o 14 6 0 171.43 87.63 159.49 o 1 7 0 6427.10 6307.43 251.68 o 2 7 0 15512.03 15282.25 177.20 o 3 7 0 21865.31 21221.84 453.36 o 4 7 0 6068.19 5996.65 110.88 o 5 7 0 634.06 571.06 89.95 o 6 7 0 271.07 334.41 66.05 o 7 7 0 651.27 600.64 71.82 o 8 7 0 1993.65 2110.61 79.73 o 9 7 0 21.82 -11.00 87.95 o 10 7 0 657.02 652.37 106.84 o 11 7 0 301.00 273.58 123.72 o 12 7 0 16.11 6.30 131.76 o 13 7 0 0.80 -33.42 194.51 o 14 7 0 8.01 -152.82 312.08 o 0 8 0 706.77 709.52 259.47 o 1 8 0 815.87 772.46 187.37 o 2 8 0 874.22 902.61 98.76 o 3 8 0 2.86 -2.79 47.37 o 4 8 0 717.18 759.94 85.28 o 5 8 0 1809.47 1836.39 96.32 o 6 8 0 2171.38 2116.33 100.76 o 7 8 0 5500.52 5487.69 157.56 o 8 8 0 2010.43 2117.19 105.50 o 9 8 0 136.20 145.20 118.30 o 10 8 0 19.33 -61.19 149.86 o 11 8 0 323.71 287.46 162.56 o 12 8 0 1477.19 1232.89 231.68 o 13 8 0 690.56 709.98 174.46 o 1 9 0 1151.96 796.15 192.36 o 2 9 0 8211.26 8512.44 227.29 o 3 9 0 6894.36 6578.67 168.17 o 4 9 0 1847.72 1722.41 123.68 o 5 9 0 10.18 69.38 103.53 o 6 9 0 46.46 70.03 99.43 o 7 9 0 1510.85 1333.06 104.86 o 8 9 0 1424.13 1428.06 104.87 o 9 9 0 1200.78 1227.10 126.16 o 10 9 0 278.71 236.34 149.41 o 11 9 0 592.33 622.21 160.16 o 12 9 0 69.18 49.94 165.16 o 13 9 0 0.09 8.94 232.43 o 0 10 0 3051.23 3342.55 325.96 o 1 10 0 6133.75 6436.03 236.91 o 2 10 0 2818.97 3022.86 233.51 o 3 10 0 11.85 -84.82 196.88 o 4 10 0 1406.33 1471.91 218.26 o 5 10 0 1965.39 1950.38 106.46 o 6 10 0 2350.37 2278.55 107.25 o 7 10 0 1906.48 1948.68 112.79 o 8 10 0 1515.43 1371.72 109.30 o 9 10 0 28.79 65.88 125.34 o 10 10 0 21.21 81.02 151.73 o 11 10 0 161.01 236.09 158.02 o 12 10 0 766.82 633.73 169.63 o 1 11 0 5109.80 5033.96 252.27 o 2 11 0 10977.21 11554.54 282.72 o 3 11 0 11710.33 12052.26 411.97 o 4 11 0 3666.53 3613.00 229.21 o 5 11 0 706.06 495.30 171.89 o 6 11 0 0.69 -64.06 118.56 o 7 11 0 507.83 476.14 119.70 o 8 11 0 1120.21 1135.86 124.93 o 9 11 0 39.36 65.89 147.73 o 10 11 0 27.44 -97.41 179.20 o 11 11 0 0.97 65.19 187.51 o 0 12 0 5742.50 5628.41 363.55 o 1 12 0 6433.13 6367.05 265.06 o 2 12 0 4616.92 4555.33 258.30 o 3 12 0 34.77 -9.27 226.94 o 4 12 0 718.15 635.21 215.40 o 5 12 0 589.31 516.77 174.05 o 6 12 0 679.52 480.76 152.95 o 7 12 0 837.34 1150.78 176.39 o 8 12 0 269.47 335.49 192.91 o 9 12 0 16.10 -48.69 185.35 o 10 12 0 1.24 110.02 245.64 o 1 13 0 1081.21 895.86 239.17 o 2 13 0 3964.15 4007.26 250.31 o 3 13 0 4090.48 4437.42 456.58 o 4 13 0 801.20 708.54 227.19 o 5 13 0 223.86 139.66 175.86 o 6 13 0 92.71 90.05 159.66 o 7 13 0 300.21 171.18 152.35 o 8 13 0 742.42 594.29 198.05 o 9 13 0 170.24 199.77 198.30 o 0 14 0 39.15 101.98 352.39 o 1 14 0 151.46 28.29 243.78 o 2 14 0 684.58 604.52 249.51 o 3 14 0 79.37 81.15 234.29 o 4 14 0 288.52 212.83 228.05 o 5 14 0 301.54 294.29 178.80 o 6 14 0 592.49 628.86 168.96 o 7 14 0 1579.86 1608.62 167.63 o 8 14 0 530.82 533.83 203.25 o 1 15 0 216.71 249.20 242.78 o 2 15 0 1091.20 1013.52 249.92 o 3 15 0 1318.72 1122.82 240.57 o 4 15 0 287.54 262.06 242.39 o 5 15 0 32.82 338.01 195.38 o 6 15 0 83.01 261.59 173.39 o 7 15 0 144.90 171.77 214.23 o 0 16 0 1879.10 1565.87 373.49 o 1 16 0 1494.20 1256.44 258.54 o 2 16 0 533.98 282.35 248.58 o 3 16 0 8.13 -169.30 258.60 o 4 16 0 726.21 651.71 244.65 o 5 16 0 773.86 698.11 191.76 o 1 17 0 329.77 155.22 354.71 o -15 1 1 0.03 -29.16 166.59 o -14 1 1 13.19 119.89 157.62 o -13 1 1 9.87 -125.64 152.99 o -12 1 1 179.90 251.77 147.50 o -11 1 1 4.26 -110.22 140.27 o -10 1 1 105.97 109.03 124.89 o -9 1 1 234.92 164.89 117.46 o -8 1 1 531.08 486.63 106.16 o -7 1 1 1339.75 1237.90 31.95 o -6 1 1 255.31 279.81 43.14 o -5 1 1 4918.67 5524.80 81.25 o -4 1 1 17747.90 19928.59 276.55 o -2 1 1 7335.88 8059.74 87.78 o -1 1 1 152.75 5.99 61.13 o 0 1 1 22.65 -18.56 55.14 o 1 1 1 21.22 28.07 21.97 o 2 1 1 370.31 268.00 36.19 o 4 1 1 0.20 -29.92 48.57 o 5 1 1 0.38 -10.68 40.70 o 6 1 1 0.85 5.84 30.39 o 7 1 1 448.28 429.58 109.43 o 8 1 1 1414.64 1252.04 118.44 o 9 1 1 405.77 302.82 136.72 o 10 1 1 69.84 75.05 143.03 o 11 1 1 63.14 77.04 147.72 o 12 1 1 8.22 16.04 155.48 o 13 1 1 4.95 -46.07 155.88 o 14 1 1 5.32 79.76 165.14 o -15 2 1 90.76 105.57 194.20 o -14 2 1 35.72 0.69 156.80 o -13 2 1 82.58 60.60 152.30 o -12 2 1 0.40 -48.17 133.80 o -11 2 1 10.46 -26.89 125.15 o -10 2 1 117.04 47.64 124.70 o -9 2 1 336.01 341.51 37.16 o -8 2 1 2618.32 2452.33 75.18 o -7 2 1 132.37 179.65 53.39 o -6 2 1 1753.11 1578.50 65.97 o -5 2 1 557.24 521.14 41.05 o -4 2 1 6027.78 5822.98 89.85 o -3 2 1 8604.72 9480.43 81.09 o -2 2 1 2948.60 3284.35 40.46 o -1 2 1 7624.31 9713.01 334.51 o 0 2 1 6780.70 8983.68 143.95 o 1 2 1 830.38 758.28 32.89 o 2 2 1 5050.33 5376.00 45.64 o 3 2 1 1193.38 1385.36 50.78 o 4 2 1 12184.45 12388.19 126.17 o 5 2 1 463.83 414.26 30.13 o 6 2 1 124.08 127.67 52.53 o 7 2 1 1.28 5.92 46.91 o 8 2 1 318.74 277.36 38.52 o 9 2 1 171.61 51.80 118.32 o 10 2 1 27.20 -68.83 124.77 o 11 2 1 157.31 132.07 144.81 o 12 2 1 24.60 18.67 150.78 o 13 2 1 1.78 93.82 154.98 o 14 2 1 40.31 166.58 166.23 o -15 3 1 0.22 136.05 202.29 o -14 3 1 60.08 -48.05 157.64 o -13 3 1 15.30 14.29 137.45 o -12 3 1 317.31 358.69 135.74 o -11 3 1 483.45 414.97 125.74 o -10 3 1 97.15 72.19 118.43 o -9 3 1 160.63 179.53 76.87 o -8 3 1 0.00 -41.34 74.38 o -7 3 1 29.00 22.00 37.26 o -6 3 1 585.69 562.78 49.17 o -5 3 1 63.21 95.95 54.85 o -4 3 1 1033.57 1148.40 63.00 o -3 3 1 112.97 140.87 51.93 o -2 3 1 353.59 378.11 39.89 o 1 3 1 3269.60 3504.34 40.78 o 2 3 1 1129.34 1076.91 47.19 o 3 3 1 4628.64 5389.87 62.34 o 4 3 1 587.15 636.32 52.71 o 5 3 1 415.65 430.69 48.58 o 6 3 1 3550.16 3527.84 95.40 o 7 3 1 15.67 5.74 75.55 o 8 3 1 235.66 151.29 76.54 o 9 3 1 208.00 108.66 117.11 o 10 3 1 37.61 -21.55 125.62 o 11 3 1 22.70 68.16 133.76 o 12 3 1 0.12 127.86 137.10 o 13 3 1 97.55 162.98 156.19 o 14 3 1 45.09 127.49 159.71 o -15 4 1 1.48 54.31 194.23 o -14 4 1 399.85 332.61 163.10 o -13 4 1 26.83 54.48 136.44 o -12 4 1 66.06 99.73 128.35 o -11 4 1 69.56 31.58 124.83 o -10 4 1 118.44 -34.24 112.31 o -9 4 1 48.33 33.12 83.33 o -8 4 1 774.89 682.85 55.69 o -7 4 1 4595.60 4228.39 61.09 o -6 4 1 2700.23 2706.11 67.19 o -5 4 1 72.64 52.36 63.42 o -4 4 1 23.32 19.32 49.03 o -3 4 1 1706.50 1894.52 49.21 o -2 4 1 3959.88 4092.00 92.44 o -1 4 1 730.71 780.88 77.80 o 0 4 1 30.33 62.43 58.49 o 1 4 1 917.48 963.55 54.24 o 2 4 1 235.96 204.63 46.42 o 3 4 1 1513.43 1646.51 54.62 o 4 4 1 1938.03 1930.93 65.09 o 5 4 1 8456.22 8765.57 126.51 o 6 4 1 4003.50 3959.78 61.31 o 7 4 1 289.71 226.69 54.40 o 8 4 1 90.06 110.71 84.75 o 9 4 1 104.05 163.38 110.71 o 10 4 1 841.29 836.60 128.74 o 11 4 1 597.43 672.59 133.81 o 12 4 1 33.97 78.84 134.10 o 13 4 1 190.40 245.48 142.65 o 14 4 1 2.06 35.57 160.29 o -15 5 1 11.10 92.01 217.87 o -14 5 1 7.26 43.33 174.08 o -13 5 1 15.83 26.00 152.20 o -12 5 1 111.99 35.91 127.88 o -11 5 1 756.12 764.96 114.60 o -10 5 1 132.18 90.89 107.11 o -9 5 1 608.05 609.60 61.82 o -8 5 1 141.25 75.95 67.78 o -7 5 1 209.55 172.78 66.33 o -6 5 1 4777.11 4722.28 73.68 o -5 5 1 113.11 128.63 67.23 o -4 5 1 1367.98 1481.80 50.08 o -3 5 1 2047.67 2177.82 57.65 o -2 5 1 199.97 165.60 41.77 o -1 5 1 495.91 477.65 66.71 o 0 5 1 566.83 535.65 51.96 o 1 5 1 8548.54 9050.00 90.35 o 2 5 1 3954.05 4414.33 75.03 o 3 5 1 2057.46 2099.17 61.75 o 4 5 1 1294.79 1325.55 63.69 o 5 5 1 35.52 -4.79 63.09 o 6 5 1 2622.94 2546.00 70.88 o 7 5 1 795.15 795.37 68.42 o 8 5 1 458.22 458.66 61.95 o 9 5 1 2.61 -74.33 106.78 o 10 5 1 51.78 -102.27 102.27 o 11 5 1 3.52 -49.46 123.48 o 12 5 1 7.61 157.33 131.91 o 13 5 1 181.53 171.64 137.98 o 14 5 1 34.79 133.78 223.12 o -14 6 1 177.80 183.46 158.35 o -13 6 1 53.12 -2.31 145.36 o -12 6 1 32.41 -24.63 131.78 o -11 6 1 0.35 -126.40 126.95 o -10 6 1 5.27 40.69 120.60 o -9 6 1 1388.24 1462.38 74.55 o -8 6 1 458.52 397.47 70.72 o -7 6 1 252.12 220.22 75.83 o -6 6 1 727.49 665.82 73.20 o -5 6 1 386.27 450.87 68.61 o -4 6 1 1549.60 1802.45 65.32 o -3 6 1 89.23 51.40 34.51 o -2 6 1 2543.02 2704.21 65.85 o -1 6 1 2288.92 2478.62 78.92 o 0 6 1 526.59 512.50 59.33 o 1 6 1 97.14 113.18 66.40 o 2 6 1 4.68 -5.61 31.00 o 3 6 1 2753.24 2826.83 62.30 o 4 6 1 2013.49 1815.82 70.71 o 5 6 1 65.20 18.97 70.84 o 6 6 1 786.11 674.91 68.41 o 7 6 1 162.96 122.07 69.70 o 8 6 1 574.43 572.57 72.20 o 9 6 1 109.42 197.24 104.28 o 10 6 1 293.46 254.47 112.84 o 11 6 1 304.56 256.45 116.78 o 12 6 1 26.83 47.85 148.59 o 13 6 1 52.46 -27.00 152.40 o -14 7 1 6.33 8.19 205.73 o -13 7 1 1.47 75.78 163.02 o -12 7 1 21.55 -29.10 131.87 o -11 7 1 269.76 304.29 123.60 o -10 7 1 111.75 101.82 119.61 o -9 7 1 842.92 708.71 102.28 o -8 7 1 24.48 -68.52 80.82 o -7 7 1 33.57 40.52 78.01 o -6 7 1 660.72 665.44 74.65 o -5 7 1 3665.15 3826.45 75.06 o -4 7 1 13668.67 13477.77 311.46 o -3 7 1 2159.68 2142.34 66.11 o -2 7 1 608.53 539.31 29.78 o -1 7 1 321.45 270.31 61.69 o 0 7 1 5.53 -3.28 38.19 o 1 7 1 5502.88 5661.22 142.89 o 2 7 1 299.86 235.87 79.54 o 3 7 1 5967.30 5776.07 98.59 o 4 7 1 893.31 850.06 69.51 o 5 7 1 86.96 70.64 73.33 o 6 7 1 433.85 306.53 77.35 o 7 7 1 1253.61 1279.78 83.90 o 8 7 1 2498.44 2389.53 104.68 o 9 7 1 729.91 724.11 118.23 o 10 7 1 89.29 -63.93 126.29 o 11 7 1 27.14 187.27 161.75 o 12 7 1 52.87 128.36 163.86 o 13 7 1 10.47 -54.60 194.61 o -14 8 1 19.23 27.73 354.17 o -13 8 1 11.25 -113.34 167.47 o -12 8 1 72.31 40.49 158.97 o -11 8 1 131.57 210.92 158.13 o -10 8 1 1.84 -43.22 110.03 o -9 8 1 454.19 451.53 98.83 o -8 8 1 723.19 733.11 82.85 o -7 8 1 73.69 56.97 76.02 o -6 8 1 3.69 53.58 70.69 o -5 8 1 172.67 190.94 93.45 o -4 8 1 302.68 263.24 110.97 o -3 8 1 1387.88 1211.74 108.40 o -2 8 1 1128.54 1133.07 98.75 o -1 8 1 1384.20 1680.37 186.44 o 0 8 1 1591.67 1645.40 189.45 o 1 8 1 260.00 305.99 89.21 o 2 8 1 129.87 142.72 100.02 o 3 8 1 2229.36 2115.63 96.11 o 4 8 1 2313.10 2229.73 102.13 o 5 8 1 62.82 113.45 91.93 o 6 8 1 1.62 42.40 80.93 o 7 8 1 91.33 90.61 83.44 o 8 8 1 16.72 -47.54 117.21 o 9 8 1 1.70 -8.29 148.25 o 10 8 1 290.94 218.85 154.31 o 11 8 1 140.05 160.97 159.38 o 12 8 1 0.51 60.92 166.46 o 13 8 1 25.99 -72.87 233.61 o -13 9 1 74.15 271.19 204.75 o -12 9 1 85.16 188.96 186.11 o -11 9 1 156.32 219.63 150.48 o -10 9 1 45.83 -14.35 143.57 o -9 9 1 92.27 63.24 125.06 o -8 9 1 20.89 18.02 99.68 o -7 9 1 448.53 343.72 105.18 o -6 9 1 405.13 458.53 101.18 o -5 9 1 741.90 785.47 117.48 o -4 9 1 23.00 -60.01 112.49 o -3 9 1 3.46 -75.44 104.65 o -2 9 1 498.33 481.38 86.28 o -1 9 1 38.98 125.86 190.08 o 0 9 1 0.16 16.95 192.28 o 1 9 1 314.63 247.31 190.62 o 2 9 1 122.35 110.20 100.53 o 3 9 1 19.62 19.43 113.29 o 4 9 1 41.08 83.80 92.66 o 5 9 1 0.25 22.59 95.90 o 6 9 1 298.36 279.68 98.41 o 7 9 1 571.22 578.49 101.62 o 8 9 1 425.94 318.84 122.11 o 9 9 1 14.84 35.34 144.40 o 10 9 1 105.14 143.58 154.20 o 11 9 1 17.16 105.84 159.08 o 12 9 1 64.93 235.94 172.72 o -12 10 1 60.37 56.17 186.48 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