#------------------------------------------------------------------------------ #$Date: 2010-10-08 09:13:40 +0300 (Fri, 08 Oct 2010) $ #$Revision: 1452 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226426.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226426_Fobs loop_ _publ_author_name 'Li, Zhengyi' 'Tang, Qiuzheng' 'Wu, Kang' 'Yu, Shuling' 'Sun, Xiaoqiang' _publ_section_title ; 3,9-Bis(2,4-dichlorophenyl)-2,4,8,10-tetraoxaspiro[5.5]undecane ; _journal_coeditor_code EZ2218 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1864 _journal_volume 66 _journal_year 2010 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.275 _cell_angle_gamma 90.000 _cell_length_a 14.3646 _cell_length_b 5.7397 _cell_length_c 11.7464 _exptl_crystal_F_000 460.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file ez2218Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 091117A in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 73.57 24.50 0.77 o 2 0 0 314.80 337.51 6.55 o 3 0 0 2083.14 2058.88 31.74 o 4 0 0 16725.70 16074.37 299.67 o 5 0 0 5923.23 5836.55 149.86 o 6 0 0 1913.57 1860.11 36.65 o 7 0 0 753.33 888.88 18.95 o 8 0 0 2127.68 2214.39 42.10 o 9 0 0 271.50 224.27 5.47 o 10 0 0 507.04 473.16 10.34 o 11 0 0 169.64 160.57 4.60 o 12 0 0 32.03 34.01 2.09 o 13 0 0 174.69 157.45 7.74 o 14 0 0 413.32 391.65 21.53 o 15 0 0 92.42 95.30 5.07 o 16 0 0 186.32 172.74 5.68 o 17 0 0 1.94 2.39 1.91 o 0 1 0 2776.01 2802.45 42.86 o 1 1 0 4286.14 4132.68 67.86 o 2 1 0 535.07 542.11 5.75 o 4 1 0 1481.40 1522.42 18.78 o 5 1 0 652.25 678.50 7.83 o 6 1 0 269.16 282.33 3.51 o 7 1 0 208.36 203.79 3.04 o 8 1 0 252.94 226.99 3.38 o 9 1 0 13.05 11.75 0.86 o 10 1 0 13.43 15.14 1.14 o 11 1 0 275.18 269.26 13.01 o 12 1 0 177.34 172.66 3.56 o 13 1 0 228.18 229.71 4.45 o 14 1 0 21.34 22.05 1.41 o 15 1 0 55.14 54.72 2.05 o 16 1 0 115.06 114.42 3.11 o 1 2 0 453.98 481.47 6.89 o 2 2 0 78.24 76.38 1.53 o 3 2 0 1.53 2.10 0.37 o 4 2 0 32.50 29.75 0.95 o 5 2 0 210.43 196.87 3.29 o 6 2 0 170.96 158.84 3.35 o 7 2 0 62.89 62.55 1.58 o 8 2 0 40.07 43.04 1.87 o 9 2 0 1.28 1.26 0.47 o 10 2 0 299.39 274.54 4.83 o 11 2 0 8.19 8.86 0.98 o 12 2 0 458.52 450.64 9.25 o 13 2 0 0.01 0.34 0.68 o 14 2 0 74.62 65.76 2.25 o 15 2 0 19.13 16.29 1.33 o 16 2 0 27.83 27.70 2.06 o 0 3 0 1351.52 1479.66 39.43 o 1 3 0 89.31 97.78 1.84 o 2 3 0 70.21 88.76 1.75 o 3 3 0 289.56 326.25 4.69 o 4 3 0 44.36 41.46 1.25 o 5 3 0 44.58 50.51 1.39 o 6 3 0 145.51 146.63 2.79 o 7 3 0 38.79 34.44 1.53 o 8 3 0 336.49 337.01 5.03 o 9 3 0 22.75 23.51 1.03 o 10 3 0 328.31 327.50 4.55 o 11 3 0 114.91 106.78 3.20 o 12 3 0 12.36 10.78 1.52 o 13 3 0 21.92 22.88 1.78 o 14 3 0 0.48 1.08 0.98 o 15 3 0 20.86 23.93 1.98 o 1 4 0 349.27 338.49 6.61 o 2 4 0 3.92 5.67 0.97 o 3 4 0 208.84 212.41 4.13 o 4 4 0 562.72 588.19 8.11 o 5 4 0 170.59 162.72 2.99 o 6 4 0 0.04 0.32 0.56 o 7 4 0 194.15 204.67 3.61 o 8 4 0 20.39 18.91 1.40 o 9 4 0 15.06 18.27 1.15 o 10 4 0 158.24 161.77 3.61 o 11 4 0 8.48 12.09 1.35 o 12 4 0 30.15 30.67 2.27 o 13 4 0 30.73 32.54 2.08 o 0 5 0 0.96 1.21 1.13 o 1 5 0 5.82 5.13 0.97 o 2 5 0 0.03 -0.17 0.81 o 3 5 0 52.94 49.24 2.01 o 4 5 0 11.18 10.85 1.25 o 5 5 0 16.03 18.27 1.45 o 6 5 0 4.94 4.14 0.96 o 7 5 0 21.41 20.07 1.50 o 8 5 0 22.84 24.21 1.60 o 9 5 0 2.88 1.78 0.92 o 10 5 0 24.48 22.08 2.29 o 11 5 0 69.31 67.95 3.58 o 0 6 0 242.39 223.70 6.81 o 1 6 0 13.59 10.97 1.38 o 2 6 0 86.89 84.26 2.77 o 3 6 0 51.67 52.95 2.38 o 4 6 0 245.01 244.80 5.15 o 5 6 0 13.04 12.88 1.45 o 6 6 0 15.84 15.06 2.07 o 7 6 0 0.12 2.24 1.05 o 8 6 0 2.94 4.46 1.12 o -16 1 1 14.22 18.66 1.65 o -15 1 1 53.47 56.13 2.11 o -14 1 1 3.76 5.73 0.90 o -13 1 1 18.05 13.79 1.17 o -12 1 1 34.10 34.39 1.50 o -11 1 1 48.85 50.47 1.92 o -10 1 1 62.82 60.60 2.81 o -9 1 1 49.15 41.52 1.39 o -8 1 1 226.74 263.13 3.84 o -7 1 1 0.44 -0.08 0.41 o -6 1 1 18.01 33.56 1.66 o -5 1 1 10.71 11.86 0.57 o -4 1 1 5.70 5.21 0.40 o -3 1 1 109.69 110.38 1.54 o -2 1 1 387.10 382.89 4.90 o -1 1 1 542.12 525.91 14.49 o 0 1 1 364.24 392.24 5.40 o 1 1 1 1005.26 1032.46 15.70 o 2 1 1 737.05 735.18 7.18 o 3 1 1 8150.02 8061.47 82.26 o 4 1 1 449.78 462.52 5.89 o 5 1 1 271.29 271.86 3.71 o 6 1 1 60.71 60.96 1.43 o 7 1 1 1428.98 1420.58 17.48 o 8 1 1 390.25 429.95 5.84 o 9 1 1 86.31 85.24 1.85 o 10 1 1 102.22 100.89 2.72 o 11 1 1 524.83 524.12 8.76 o 12 1 1 103.96 110.42 2.65 o 13 1 1 0.21 0.24 0.64 o 14 1 1 0.53 0.82 0.71 o 15 1 1 48.28 53.63 2.03 o 16 1 1 0.93 1.02 0.78 o -16 2 1 2.53 2.93 1.11 o -15 2 1 22.15 20.33 1.80 o -14 2 1 92.05 95.14 3.19 o -13 2 1 278.33 269.01 11.12 o -12 2 1 510.72 511.34 9.68 o -11 2 1 137.29 133.67 3.11 o -10 2 1 1439.55 1439.54 23.48 o -9 2 1 753.96 716.32 10.64 o -8 2 1 1458.67 1484.01 31.41 o -7 2 1 54.51 56.11 1.53 o -6 2 1 1200.73 1131.42 15.97 o -5 2 1 4243.88 4469.27 59.63 o -4 2 1 2319.01 2337.45 31.51 o -3 2 1 43.72 47.42 1.56 o -2 2 1 30.62 30.98 1.50 o -1 2 1 3960.79 3801.38 59.67 o 0 2 1 1665.80 1709.55 22.93 o 1 2 1 1039.39 994.41 12.25 o 2 2 1 1845.02 2024.59 24.66 o 3 2 1 2460.20 2627.73 31.92 o 4 2 1 684.59 693.14 9.91 o 5 2 1 1088.78 1107.17 15.55 o 6 2 1 131.90 113.85 2.24 o 7 2 1 37.01 37.87 1.11 o 8 2 1 273.65 254.74 4.28 o 9 2 1 242.63 227.49 4.04 o 10 2 1 78.78 75.06 2.03 o 11 2 1 215.99 217.71 4.14 o 12 2 1 15.12 12.32 1.09 o 13 2 1 9.95 12.45 1.14 o 14 2 1 50.91 49.86 1.98 o 15 2 1 22.01 27.03 1.93 o 16 2 1 17.71 16.72 1.41 o -15 3 1 8.13 8.84 2.11 o -14 3 1 85.03 82.51 3.13 o -13 3 1 15.83 17.31 1.62 o -12 3 1 35.33 38.64 2.44 o -11 3 1 135.02 122.24 3.49 o -10 3 1 150.31 137.35 2.67 o -9 3 1 133.72 127.19 2.53 o -8 3 1 343.15 361.26 5.77 o -7 3 1 2122.32 2168.45 26.89 o -6 3 1 0.16 -0.17 0.44 o -5 3 1 61.13 66.63 1.55 o -4 3 1 0.93 1.26 0.46 o -3 3 1 1785.09 1853.33 25.71 o -2 3 1 133.03 137.67 2.98 o -1 3 1 81.88 73.05 1.95 o 0 3 1 6.83 10.64 1.05 o 1 3 1 325.66 304.92 4.96 o 2 3 1 578.47 562.92 7.54 o 3 3 1 1737.27 1888.17 23.41 o 4 3 1 628.10 604.45 6.71 o 5 3 1 78.28 87.10 1.76 o 6 3 1 341.86 360.83 5.17 o 7 3 1 1519.44 1540.57 19.55 o 8 3 1 1798.00 1769.54 22.34 o 9 3 1 158.39 181.68 3.18 o 10 3 1 78.64 88.49 2.05 o 11 3 1 500.94 518.75 8.25 o 12 3 1 391.13 402.46 6.84 o 13 3 1 13.95 13.55 1.46 o 14 3 1 36.44 40.02 2.20 o 15 3 1 43.72 44.01 2.89 o -13 4 1 5.25 4.90 1.55 o -12 4 1 0.32 0.86 1.22 o -11 4 1 125.82 117.17 8.04 o -10 4 1 100.66 102.25 3.19 o -9 4 1 9.86 11.09 1.12 o -8 4 1 978.82 1013.00 15.02 o -7 4 1 696.88 695.50 10.73 o -6 4 1 123.84 121.29 2.91 o -5 4 1 200.88 196.40 3.91 o -4 4 1 541.93 576.62 9.06 o -3 4 1 5.06 3.92 0.88 o -2 4 1 11.27 11.69 1.08 o -1 4 1 356.09 374.50 7.12 o 1 4 1 2.95 3.07 0.89 o 2 4 1 73.29 69.78 1.75 o 3 4 1 0.90 0.85 0.49 o 4 4 1 66.23 64.45 1.73 o 5 4 1 101.87 97.75 2.44 o 6 4 1 256.81 261.21 4.25 o 7 4 1 10.19 9.14 0.89 o 8 4 1 75.39 76.48 1.99 o 9 4 1 81.38 88.55 2.18 o 10 4 1 270.35 261.36 6.11 o 11 4 1 63.12 60.65 2.50 o 12 4 1 22.86 26.14 2.23 o 13 4 1 25.21 21.58 2.68 o -11 5 1 9.59 10.19 1.82 o -10 5 1 37.33 45.09 2.37 o -9 5 1 161.36 165.57 3.87 o -8 5 1 4.91 3.65 1.01 o -7 5 1 0.38 1.34 0.91 o -6 5 1 13.17 16.09 1.41 o -5 5 1 113.68 124.00 3.16 o -4 5 1 95.52 112.80 3.00 o -3 5 1 19.54 20.12 1.49 o -2 5 1 43.62 44.92 1.88 o -1 5 1 17.89 20.95 1.49 o 0 5 1 0.78 1.58 0.85 o 1 5 1 39.30 33.83 1.70 o 2 5 1 65.70 61.04 2.16 o 3 5 1 15.59 12.50 1.49 o 4 5 1 29.05 35.05 1.69 o 5 5 1 24.83 19.27 1.46 o 6 5 1 9.19 9.92 1.18 o 7 5 1 0.17 -0.27 0.80 o 8 5 1 0.47 -0.08 0.82 o 9 5 1 5.17 5.89 1.08 o 10 5 1 58.51 61.05 4.59 o 11 5 1 10.91 13.59 2.87 o -8 6 1 44.99 53.48 2.27 o -7 6 1 3.48 3.10 1.03 o -6 6 1 4.86 3.62 1.10 o -5 6 1 23.50 25.62 1.78 o -4 6 1 2.74 2.11 1.04 o -3 6 1 21.26 25.61 1.78 o -2 6 1 35.40 37.55 2.01 o -1 6 1 33.14 39.22 2.76 o 0 6 1 33.40 29.17 1.83 o 1 6 1 0.01 -0.06 0.93 o 2 6 1 30.82 38.92 1.99 o 3 6 1 12.05 10.01 1.38 o 4 6 1 232.50 245.36 5.18 o 5 6 1 0.27 0.40 1.02 o 6 6 1 36.26 47.03 2.55 o 7 6 1 19.34 21.91 1.94 o -17 0 2 32.04 33.49 4.02 o -16 0 2 22.69 17.42 2.87 o -15 0 2 704.23 703.18 21.82 o -14 0 2 60.81 70.82 4.59 o -13 0 2 201.35 204.03 8.23 o -12 0 2 67.50 73.11 4.40 o -11 0 2 776.00 828.67 17.37 o -10 0 2 401.36 388.39 27.18 o -9 0 2 2067.24 2126.01 48.81 o -8 0 2 496.41 489.30 10.26 o -7 0 2 841.88 759.56 22.58 o -4 0 2 1871.96 2034.32 52.44 o -3 0 2 148.71 161.34 4.98 o -2 0 2 949.22 901.85 23.54 o -1 0 2 95.80 87.66 2.68 o 0 0 2 90.58 86.71 2.02 o 1 0 2 9312.81 9505.82 176.45 o 2 0 2 12863.19 11293.64 1049.79 o 3 0 2 41.73 51.31 4.40 o 4 0 2 639.99 621.07 16.46 o 5 0 2 871.96 795.63 92.73 o 6 0 2 13.52 18.12 1.24 o 7 0 2 551.50 626.28 19.43 o 8 0 2 58.56 70.11 2.53 o 9 0 2 4.28 5.99 1.06 o 10 0 2 15.76 12.12 2.01 o 11 0 2 218.46 218.47 5.66 o 12 0 2 0.00 -0.59 0.81 o 13 0 2 0.92 0.57 1.24 o 14 0 2 348.09 339.45 8.44 o 15 0 2 153.35 157.70 6.60 o 16 0 2 7.34 6.12 1.49 o -16 1 2 41.26 48.42 2.39 o -15 1 2 260.42 238.61 6.89 o -14 1 2 6.47 7.65 1.42 o -13 1 2 221.98 205.61 8.90 o -12 1 2 108.77 90.41 3.00 o -11 1 2 26.81 22.70 2.00 o -9 1 2 0.97 4.25 1.99 o -8 1 2 214.96 191.77 3.91 o -7 1 2 997.39 992.10 15.93 o -6 1 2 283.87 269.31 4.90 o -5 1 2 1375.71 1547.47 24.17 o -4 1 2 1839.28 0.19 0.38 o -3 1 2 3801.89 3885.67 98.95 o -2 1 2 2688.63 2822.67 71.96 o -1 1 2 5209.32 5279.12 79.17 o 0 1 2 2338.62 2350.75 27.93 o 1 1 2 19234.22 18707.34 202.53 o 2 1 2 7711.80 7707.05 90.91 o 3 1 2 1976.25 2021.46 26.75 o 4 1 2 128.80 107.51 1.90 o 5 1 2 199.22 183.17 2.97 o 6 1 2 1665.61 1704.06 20.73 o 7 1 2 2366.21 2302.13 31.59 o 8 1 2 293.44 262.86 3.85 o 9 1 2 0.70 0.42 0.42 o 10 1 2 31.74 33.21 1.55 o 11 1 2 446.94 430.24 6.95 o 12 1 2 67.57 60.92 1.96 o 13 1 2 292.73 280.86 5.14 o 14 1 2 17.33 16.31 1.24 o 15 1 2 64.76 59.66 2.15 o 16 1 2 31.23 34.84 2.60 o -16 2 2 6.47 8.84 1.76 o -15 2 2 5.54 5.29 1.47 o -14 2 2 36.66 32.44 2.44 o -13 2 2 51.06 45.42 3.16 o -12 2 2 7.49 7.87 1.42 o -11 2 2 8.51 6.69 1.28 o -10 2 2 630.09 601.99 14.56 o -9 2 2 107.58 103.98 3.21 o -8 2 2 19.68 22.37 1.25 o -7 2 2 88.94 114.10 3.20 o -6 2 2 36.11 46.72 1.54 o -5 2 2 3625.68 3885.30 52.41 o -4 2 2 44.99 50.38 2.54 o -3 2 2 227.90 215.71 11.86 o -2 2 2 0.28 0.18 0.23 o -1 2 2 146.45 146.00 3.15 o 0 2 2 4.49 6.00 0.60 o 1 2 2 1763.99 1873.04 26.69 o 2 2 2 486.68 541.64 5.92 o 3 2 2 125.96 153.88 2.19 o 4 2 2 105.98 109.49 2.22 o 5 2 2 155.27 172.37 5.86 o 6 2 2 74.54 67.66 1.65 o 7 2 2 2.58 3.38 0.54 o 8 2 2 12.29 9.71 0.74 o 9 2 2 284.91 285.80 4.33 o 10 2 2 7.36 5.93 0.84 o 11 2 2 384.27 372.19 6.22 o 12 2 2 55.48 47.26 1.76 o 13 2 2 99.16 94.48 2.60 o 14 2 2 11.81 13.83 1.85 o 15 2 2 31.68 33.14 1.76 o -15 3 2 59.17 53.01 4.11 o -14 3 2 1.91 1.90 1.82 o -13 3 2 1.23 -1.42 0.95 o -12 3 2 18.21 16.85 1.88 o -11 3 2 56.75 53.81 2.83 o -10 3 2 38.03 37.73 1.87 o -9 3 2 256.06 244.22 5.19 o -8 3 2 3.71 2.52 0.76 o -7 3 2 170.03 155.51 3.15 o -6 3 2 125.85 126.22 2.72 o -5 3 2 38.33 37.73 1.55 o -4 3 2 607.73 659.90 9.84 o -3 3 2 458.54 452.19 5.59 o -2 3 2 611.78 630.92 8.31 o -1 3 2 4.87 5.43 0.49 o 0 3 2 0.02 0.11 0.19 o 1 3 2 443.55 479.16 6.45 o 2 3 2 50.31 40.41 1.42 o 3 3 2 6.02 12.25 0.74 o 4 3 2 21.33 19.97 0.87 o 5 3 2 77.14 73.65 1.61 o 6 3 2 268.41 279.24 4.80 o 7 3 2 39.02 43.04 1.39 o 8 3 2 62.76 57.75 1.60 o 9 3 2 86.03 91.09 2.06 o 10 3 2 2.38 1.92 0.64 o 11 3 2 27.32 38.75 1.64 o 12 3 2 214.91 221.34 4.37 o 13 3 2 139.15 132.66 4.67 o 14 3 2 108.01 111.99 9.47 o -13 4 2 121.01 126.86 5.00 o -12 4 2 8.26 9.45 1.74 o -11 4 2 6.59 6.79 1.49 o -10 4 2 2.13 1.98 1.20 o -9 4 2 342.81 345.43 6.12 o -8 4 2 346.70 365.70 7.24 o -7 4 2 25.98 23.46 1.48 o -6 4 2 226.32 249.43 4.70 o -5 4 2 288.98 293.47 5.29 o -4 4 2 9.17 8.57 0.98 o -3 4 2 112.80 115.62 2.78 o -2 4 2 215.24 241.01 4.54 o -1 4 2 597.10 606.53 9.09 o 0 4 2 1.54 1.92 0.55 o 1 4 2 3.52 6.23 0.72 o 2 4 2 61.35 63.51 1.66 o 3 4 2 72.71 73.93 1.81 o 4 4 2 0.43 0.18 0.57 o 5 4 2 8.97 8.50 0.85 o 6 4 2 41.74 35.97 1.38 o 7 4 2 143.26 128.70 2.63 o 8 4 2 12.10 14.49 1.16 o 9 4 2 4.50 2.62 0.84 o 10 4 2 8.61 8.72 1.23 o 11 4 2 108.35 104.47 3.99 o 12 4 2 1.02 3.92 1.35 o 13 4 2 35.13 39.83 2.70 o -11 5 2 39.58 35.60 2.94 o -10 5 2 25.01 32.96 2.67 o -9 5 2 2.64 1.50 0.92 o -8 5 2 55.96 54.78 3.24 o -7 5 2 25.97 28.10 1.69 o -6 5 2 18.00 16.09 1.42 o -5 5 2 430.34 453.19 7.75 o -4 5 2 54.05 52.70 2.06 o -3 5 2 197.57 200.18 4.28 o -2 5 2 456.11 455.32 7.74 o -1 5 2 186.50 166.25 3.75 o 0 5 2 17.47 20.18 1.46 o 1 5 2 42.12 41.13 1.83 o 2 5 2 376.74 370.27 6.55 o 3 5 2 442.95 408.79 7.10 o 4 5 2 0.43 1.03 0.86 o 5 5 2 82.13 91.02 2.65 o 6 5 2 32.55 39.83 1.81 o 7 5 2 343.16 335.93 7.21 o 8 5 2 2.47 3.06 1.67 o 9 5 2 11.46 9.65 1.79 o 10 5 2 1.02 1.91 1.91 o 11 5 2 272.27 304.89 11.87 o -7 6 2 7.88 8.50 1.29 o -6 6 2 3.31 3.75 1.06 o -5 6 2 45.44 40.38 2.01 o -4 6 2 9.24 8.52 1.28 o -3 6 2 6.83 6.12 1.16 o -2 6 2 13.16 14.88 1.45 o -1 6 2 1.45 0.85 0.96 o 0 6 2 26.40 27.42 2.54 o 1 6 2 2.86 2.98 1.00 o 2 6 2 15.18 16.67 1.47 o 3 6 2 4.07 2.46 1.02 o 4 6 2 20.30 14.88 1.91 o 5 6 2 7.90 8.05 1.48 o 6 6 2 45.77 44.69 2.46 o 7 6 2 11.57 11.07 1.84 o -16 1 3 98.02 92.55 4.05 o -15 1 3 63.63 60.08 4.02 o -14 1 3 18.69 16.19 1.88 o -13 1 3 41.26 39.18 2.49 o -12 1 3 587.81 524.83 28.61 o -11 1 3 389.75 398.71 16.65 o -10 1 3 361.46 353.84 14.07 o -9 1 3 27.62 28.08 1.42 o -8 1 3 1035.12 1038.00 16.78 o -7 1 3 155.66 115.41 3.31 o -6 1 3 3136.57 3607.01 92.83 o -5 1 3 434.04 474.85 13.59 o -3 1 3 3457.99 3449.36 62.46 o -2 1 3 864.40 861.27 13.53 o -1 1 3 5400.12 5279.20 198.72 o 0 1 3 303.81 288.13 4.25 o 1 1 3 2297.70 2265.06 35.13 o 2 1 3 4580.57 4836.35 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