#------------------------------------------------------------------------------ #$Date: 2010-10-08 09:13:40 +0300 (Fri, 08 Oct 2010) $ #$Revision: 1452 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226489.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226489_Fobs loop_ _publ_author_name 'Toumi Akriche, Samah' 'Al Othman, Zeid Abdellah' 'Rzaigui, Mohamed' 'Mahfouz, Refaat Mohamed' _publ_section_title ; Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate ; _journal_coeditor_code HB5497 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m816 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.580 _cell_angle_beta 71.182 _cell_angle_gamma 78.502 _cell_length_a 10.3501 _cell_length_b 13.1331 _cell_length_c 14.3921 _exptl_crystal_F_000 1066.00 _reflns_d_resolution_high 0.5979 _[local]_cod_data_source_file hb5497Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cad4 in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 379.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 616.45 390.73 12.18 o 3 0 0 24562.40 21738.61 245.09 o 4 0 0 477.60 403.91 15.85 o 5 0 0 26061.91 20887.13 204.36 o 6 0 0 1181.55 1007.55 32.21 o 7 0 0 4.45 31.88 30.75 o 8 0 0 5707.58 4392.66 60.22 o 9 0 0 150.64 151.77 29.03 o 10 0 0 510.78 501.52 36.19 o 11 0 0 0.37 26.47 44.20 o 12 0 0 84.90 41.39 59.50 o 13 0 0 116.83 226.53 61.05 o 14 0 0 1.06 36.74 56.73 o 15 0 0 29.44 25.15 59.17 o 16 0 0 2.97 -26.12 66.37 o -16 1 0 75.66 37.10 61.93 o -15 1 0 7.11 -34.21 79.49 o -14 1 0 62.77 103.82 97.59 o -13 1 0 12.68 6.58 58.76 o -12 1 0 252.66 271.30 39.18 o -11 1 0 1053.32 959.24 47.47 o -10 1 0 1672.69 1152.88 78.34 o -9 1 0 97.03 89.06 28.92 o -8 1 0 1610.22 1288.60 39.49 o -7 1 0 4255.35 3216.42 78.54 o -6 1 0 5360.26 4307.79 47.80 o -5 1 0 8671.70 7563.87 113.05 o -4 1 0 534.99 394.81 17.96 o -3 1 0 33316.01 25273.66 177.35 o -2 1 0 22300.16 19487.88 93.54 o -1 1 0 84.71 203.51 8.36 o 2 1 0 74931.77 76420.43 861.69 o 3 1 0 151.54 161.94 12.45 o 4 1 0 983.76 795.57 25.87 o 5 1 0 31214.44 26448.87 338.15 o 6 1 0 269.22 203.62 19.96 o 7 1 0 5323.72 4160.99 52.58 o 8 1 0 226.65 166.47 46.87 o 9 1 0 15.72 -20.56 36.43 o 10 1 0 4034.70 3080.34 63.13 o 11 1 0 130.06 205.34 34.69 o 12 1 0 135.77 166.76 37.51 o 13 1 0 180.33 80.23 44.43 o 14 1 0 22.90 99.00 59.30 o 15 1 0 89.52 -52.89 66.90 o 16 1 0 0.28 -67.44 67.44 o -16 2 0 9.47 39.54 46.62 o -15 2 0 0.01 29.46 124.87 o -14 2 0 38.09 33.94 61.22 o -13 2 0 21.21 36.48 56.92 o -12 2 0 41.76 7.24 55.44 o -11 2 0 243.68 223.15 39.05 o -10 2 0 431.49 369.84 66.39 o -9 2 0 1705.71 1510.45 82.87 o -8 2 0 1492.60 1144.98 38.25 o -7 2 0 538.54 381.86 27.27 o -6 2 0 12939.60 10324.49 73.78 o -5 2 0 17661.67 14253.83 408.46 o -4 2 0 8549.99 6716.94 47.90 o -3 2 0 1406.27 1302.79 27.08 o -2 2 0 17385.17 11943.92 67.19 o -1 2 0 59401.74 39181.74 109.75 o 0 2 0 48976.18 34710.71 497.06 o 1 2 0 4432.38 4543.23 30.13 o 2 2 0 13247.27 17233.48 75.45 o 3 2 0 22514.89 27933.05 111.36 o 4 2 0 9376.72 9228.94 83.54 o 5 2 0 6493.06 5786.04 48.71 o 6 2 0 101.06 86.16 20.06 o 7 2 0 2115.17 1760.38 37.77 o 8 2 0 5478.83 4542.37 94.08 o 9 2 0 3.67 34.34 32.12 o 10 2 0 43.16 77.18 32.08 o 11 2 0 107.77 79.06 34.90 o 12 2 0 275.43 163.29 46.94 o 13 2 0 44.21 91.95 74.83 o 14 2 0 1.56 -15.04 52.34 o 15 2 0 6.80 13.20 61.97 o 16 2 0 3.50 -26.18 80.10 o -15 3 0 2.40 -40.94 114.81 o -14 3 0 48.77 74.70 47.14 o -13 3 0 58.54 94.15 40.21 o -12 3 0 17.71 -10.74 53.16 o -11 3 0 917.60 813.20 46.77 o -10 3 0 369.70 370.19 34.48 o -9 3 0 49.49 -16.92 64.23 o -8 3 0 5459.89 4432.50 64.21 o -7 3 0 24.53 18.65 27.96 o -6 3 0 1596.64 1470.68 34.38 o -5 3 0 104.79 126.14 26.54 o -4 3 0 5372.15 4383.36 42.36 o -3 3 0 22228.05 16565.96 202.74 o -2 3 0 324.09 272.09 17.76 o -1 3 0 2479.77 1904.51 25.46 o 0 3 0 29097.70 21986.96 347.74 o 1 3 0 11777.22 10230.90 140.27 o 2 3 0 44080.79 50846.20 230.70 o 3 3 0 1014.13 809.14 18.72 o 4 3 0 13285.78 17094.99 104.63 o 5 3 0 12382.88 13272.72 89.64 o 6 3 0 4610.37 4876.27 105.96 o 7 3 0 1882.43 1862.47 39.81 o 8 3 0 1590.83 1352.77 40.09 o 9 3 0 1100.03 902.38 39.34 o 10 3 0 3009.34 2437.23 56.96 o 11 3 0 41.95 -28.09 47.75 o 12 3 0 39.62 18.54 40.75 o 13 3 0 289.18 240.10 42.30 o 14 3 0 35.20 -66.05 66.05 o 15 3 0 35.70 7.52 75.44 o 16 3 0 12.10 -63.39 64.23 o -15 4 0 14.60 -10.27 62.91 o -14 4 0 38.82 28.08 53.15 o -13 4 0 4.51 44.66 55.09 o -12 4 0 4.27 35.92 52.84 o -11 4 0 490.93 414.36 42.97 o -10 4 0 2.56 0.15 46.03 o -9 4 0 1071.15 882.20 47.95 o -8 4 0 1326.62 1178.20 41.58 o -7 4 0 59.39 74.25 25.50 o -6 4 0 16687.89 14042.04 198.15 o -5 4 0 3613.66 2936.78 41.98 o -4 4 0 6005.69 4857.75 46.80 o -3 4 0 11884.76 9583.97 111.50 o -2 4 0 221.93 152.98 13.70 o -1 4 0 33022.80 24139.73 482.07 o 0 4 0 2562.47 2559.46 37.41 o 1 4 0 459.45 454.29 14.80 o 2 4 0 27143.43 27302.98 558.99 o 3 4 0 9057.52 10515.77 155.33 o 4 4 0 13459.77 16977.34 110.17 o 5 4 0 110.85 133.12 19.67 o 6 4 0 42.12 38.69 25.20 o 7 4 0 8062.47 8330.25 74.40 o 8 4 0 548.16 507.65 47.68 o 9 4 0 44.22 19.65 42.14 o 10 4 0 777.27 658.58 38.36 o 11 4 0 25.08 34.63 38.23 o 12 4 0 269.28 234.51 40.26 o 13 4 0 0.87 -43.82 55.87 o 14 4 0 53.06 -42.40 62.13 o 15 4 0 25.19 37.06 60.11 o 16 4 0 3.74 -64.12 64.12 o -15 5 0 2.03 78.92 52.25 o -14 5 0 0.10 -60.26 60.26 o -13 5 0 98.97 25.38 62.07 o -12 5 0 17.64 25.17 43.08 o -11 5 0 85.84 43.02 84.35 o -10 5 0 1.80 28.88 46.35 o -9 5 0 716.78 761.05 40.91 o -8 5 0 1414.58 1098.80 42.21 o -7 5 0 903.72 724.59 35.10 o -6 5 0 1288.46 1010.58 35.29 o -5 5 0 322.41 296.72 24.40 o -4 5 0 9537.12 7382.87 60.12 o -3 5 0 1684.61 1200.79 26.65 o -2 5 0 698.76 551.46 18.62 o -1 5 0 15609.47 11509.03 293.92 o 0 5 0 10724.95 8329.47 60.17 o 1 5 0 12770.95 9721.55 152.63 o 2 5 0 1728.28 1706.59 25.84 o 3 5 0 116.37 116.83 15.18 o 4 5 0 21975.07 25828.38 161.21 o 5 5 0 7194.79 9129.06 67.62 o 6 5 0 2553.90 3047.23 46.89 o 7 5 0 1238.00 1457.31 99.89 o 8 5 0 1060.10 1062.43 50.92 o 9 5 0 4635.34 4643.29 70.20 o 10 5 0 231.59 236.16 36.48 o 11 5 0 47.77 53.47 40.80 o 12 5 0 514.35 426.39 44.17 o 13 5 0 403.45 489.22 45.41 o 14 5 0 96.31 80.27 45.13 o 15 5 0 23.43 79.42 62.12 o 16 5 0 0.91 19.62 64.66 o -15 6 0 30.60 16.82 86.11 o -14 6 0 0.43 1.45 82.60 o -13 6 0 1.92 -79.56 91.17 o -12 6 0 101.11 92.09 49.52 o -11 6 0 523.53 480.92 46.08 o -10 6 0 24.52 -26.82 51.53 o -9 6 0 226.47 220.85 45.52 o -8 6 0 1041.22 1002.39 40.64 o -7 6 0 486.13 439.03 86.72 o -6 6 0 7675.69 6106.48 98.40 o -5 6 0 179.02 136.08 31.81 o -4 6 0 49.07 -19.66 28.63 o -3 6 0 5065.59 4054.03 85.97 o -2 6 0 348.48 311.36 55.45 o -1 6 0 12199.14 9826.03 140.47 o 0 6 0 231.70 150.58 15.64 o 1 6 0 3630.69 2896.70 106.03 o 2 6 0 34314.62 31219.63 277.71 o 3 6 0 823.46 889.81 24.88 o 4 6 0 2.40 3.29 25.19 o 5 6 0 1787.69 2171.58 38.96 o 6 6 0 4232.58 5224.97 83.20 o 7 6 0 3364.47 4128.41 83.47 o 8 6 0 23.25 -31.83 45.08 o 9 6 0 828.26 781.60 42.07 o 10 6 0 410.81 500.44 38.78 o 11 6 0 488.50 499.66 42.64 o 12 6 0 0.50 -11.54 58.30 o 13 6 0 0.59 27.86 45.88 o 14 6 0 434.75 399.00 83.61 o 15 6 0 25.51 -54.39 65.33 o 16 6 0 18.67 3.93 68.56 o -14 7 0 0.74 -38.29 64.50 o -13 7 0 20.90 -45.51 79.08 o -12 7 0 9.55 33.03 56.97 o -11 7 0 7.69 -45.17 56.92 o -10 7 0 73.11 117.17 35.42 o -9 7 0 410.50 440.74 56.46 o -8 7 0 56.73 99.13 30.11 o -7 7 0 251.24 236.15 31.28 o -6 7 0 4307.94 3515.35 57.27 o -5 7 0 234.71 261.24 29.78 o -4 7 0 3528.72 2903.42 150.33 o -3 7 0 90.42 157.47 21.96 o -2 7 0 1720.17 1284.38 30.75 o -1 7 0 28857.14 23365.35 378.13 o 0 7 0 57.87 77.88 16.52 o 1 7 0 7428.76 6429.90 130.41 o 2 7 0 8446.89 7556.41 58.88 o 3 7 0 4102.23 3882.48 45.55 o 4 7 0 26704.23 28345.46 185.86 o 5 7 0 6.67 61.39 24.85 o 6 7 0 59.42 91.77 27.12 o 7 7 0 5517.90 6471.27 73.97 o 8 7 0 94.19 171.37 32.44 o 9 7 0 2681.89 3397.71 65.71 o 10 7 0 0.98 -49.57 49.57 o 11 7 0 5.59 -24.03 97.66 o 12 7 0 890.53 991.26 54.37 o 13 7 0 6.22 -62.55 62.55 o 14 7 0 6.18 -7.44 62.03 o 15 7 0 1.76 -1.09 71.25 o -14 8 0 0.10 23.62 95.43 o -13 8 0 5.82 -6.61 69.49 o -12 8 0 123.35 202.92 63.89 o -11 8 0 60.52 90.64 44.85 o -10 8 0 71.05 99.25 42.66 o -9 8 0 50.20 122.55 108.73 o -8 8 0 237.12 195.07 32.98 o -7 8 0 1858.70 1750.56 49.78 o -6 8 0 2837.30 2354.81 101.44 o -5 8 0 4.96 -33.06 36.93 o -4 8 0 6827.73 5510.89 65.61 o -3 8 0 4135.88 3722.85 51.43 o -2 8 0 3295.31 2891.08 92.52 o -1 8 0 2575.42 2373.81 39.67 o 0 8 0 133.78 80.78 25.12 o 1 8 0 18927.23 16307.12 176.07 o 2 8 0 4088.95 3309.83 73.48 o 3 8 0 1.73 -14.05 29.32 o 4 8 0 3131.62 3280.22 48.33 o 5 8 0 3.07 7.37 44.24 o 6 8 0 5176.96 5759.62 69.44 o 7 8 0 372.31 490.08 47.61 o 8 8 0 237.88 314.27 36.91 o 9 8 0 2041.91 2291.78 60.69 o 10 8 0 39.78 27.28 52.65 o 11 8 0 27.70 64.86 61.46 o 12 8 0 139.36 46.73 77.06 o 13 8 0 23.90 33.23 50.07 o 14 8 0 217.62 167.42 50.62 o 15 8 0 2.26 -11.24 91.44 o -13 9 0 3.41 -65.34 65.34 o -12 9 0 1.55 -51.68 61.21 o -11 9 0 11.16 15.87 57.56 o -10 9 0 38.25 93.01 39.32 o -9 9 0 236.65 285.69 38.87 o -8 9 0 20.17 -5.18 47.65 o -7 9 0 596.55 631.00 52.75 o -6 9 0 264.88 222.98 32.71 o -5 9 0 623.28 575.26 35.43 o -4 9 0 1040.63 1054.53 62.34 o -3 9 0 37.65 43.94 28.65 o -2 9 0 8879.70 7458.00 72.15 o -1 9 0 7929.08 7547.66 103.87 o 0 9 0 2441.77 2114.58 41.30 o 1 9 0 838.58 749.81 29.27 o 2 9 0 2467.28 2254.04 94.82 o 3 9 0 9743.67 8628.04 88.88 o 4 9 0 6026.93 5792.31 159.65 o 5 9 0 461.59 505.65 32.98 o 6 9 0 4145.61 4471.80 65.23 o 7 9 0 3042.45 3105.03 60.31 o 8 9 0 1214.27 1310.73 50.75 o 9 9 0 636.08 704.54 45.63 o 10 9 0 248.45 275.15 43.04 o 11 9 0 300.06 279.97 47.97 o 12 9 0 347.06 417.97 67.27 o 13 9 0 4.68 34.82 64.56 o 14 9 0 3.98 85.41 51.96 o 15 9 0 3.32 13.67 65.99 o -13 10 0 0.50 14.94 104.61 o -12 10 0 89.77 156.29 57.14 o -11 10 0 5.64 90.57 51.12 o -10 10 0 45.82 -60.58 60.58 o -9 10 0 228.63 242.83 43.88 o -8 10 0 8.54 -53.39 53.39 o -7 10 0 1042.60 1101.59 47.57 o -6 10 0 36.42 18.07 69.76 o -5 10 0 159.02 160.61 31.60 o -4 10 0 3682.95 3243.16 59.87 o -3 10 0 338.36 450.46 31.03 o -2 10 0 547.36 478.18 31.55 o -1 10 0 6.93 22.34 71.59 o 0 10 0 2284.92 1831.26 42.59 o 1 10 0 7028.22 6487.11 69.84 o 2 10 0 1632.70 1502.46 39.14 o 3 10 0 1314.59 1165.10 37.15 o 4 10 0 2541.74 2482.91 50.08 o 5 10 0 462.57 567.07 60.44 o 6 10 0 12.35 15.43 42.88 o 7 10 0 3.09 68.12 33.86 o 8 10 0 1187.09 1316.57 52.43 o 9 10 0 1180.00 1263.82 53.44 o 10 10 0 195.58 193.83 44.67 o 11 10 0 21.52 15.92 61.69 o 12 10 0 242.66 256.96 50.04 o 13 10 0 102.04 114.32 64.29 o 14 10 0 109.05 51.13 72.14 o 15 10 0 36.41 -72.71 72.71 o -12 11 0 0.51 -7.81 62.76 o -11 11 0 12.82 -44.86 64.70 o -10 11 0 67.60 120.69 49.37 o -9 11 0 0.33 -15.17 56.51 o -8 11 0 21.98 -37.44 53.35 o -7 11 0 651.39 821.32 56.87 o -6 11 0 1.01 -25.25 46.60 o -5 11 0 182.46 195.54 33.92 o -4 11 0 365.06 400.52 35.67 o -3 11 0 185.90 202.77 35.19 o -2 11 0 8558.25 7916.00 88.67 o -1 11 0 43.83 11.90 38.69 o 0 11 0 403.43 358.17 31.65 o 1 11 0 4986.55 4610.63 67.54 o 2 11 0 71.38 28.13 38.73 o 3 11 0 6064.99 5539.43 135.95 o 4 11 0 199.21 197.87 29.32 o 5 11 0 12.22 35.87 32.53 o 6 11 0 3363.28 3411.46 65.04 o 7 11 0 1350.93 1295.66 57.07 o 8 11 0 472.75 572.61 43.27 o 9 11 0 61.53 29.45 57.73 o 10 11 0 0.32 -29.28 57.91 o 11 11 0 241.59 263.80 48.32 o 12 11 0 4.32 17.28 69.04 o 13 11 0 7.51 -37.01 55.86 o 14 11 0 1.82 -41.58 105.83 o -12 12 0 7.74 94.41 54.05 o -11 12 0 8.87 118.27 51.80 o -10 12 0 6.16 43.94 47.23 o -9 12 0 93.68 150.56 55.58 o -8 12 0 28.48 -23.46 57.06 o -7 12 0 63.48 37.08 55.73 o -6 12 0 5.32 -39.37 86.92 o -5 12 0 299.90 375.49 39.42 o -4 12 0 943.52 890.52 57.61 o -3 12 0 18.91 -39.33 43.22 o -2 12 0 7.63 -43.96 43.96 o -1 12 0 152.25 116.98 31.47 o 0 12 0 1665.04 1510.56 70.51 o 1 12 0 890.06 1022.74 41.01 o 2 12 0 78.15 19.78 33.72 o 3 12 0 2498.84 2189.16 91.65 o 4 12 0 283.86 277.44 34.05 o 5 12 0 674.51 618.00 39.49 o 6 12 0 361.72 374.50 39.98 o 7 12 0 90.85 87.05 90.90 o 8 12 0 1702.93 1787.53 61.60 o 9 12 0 98.27 -23.03 58.31 o 10 12 0 127.86 217.20 99.75 o 11 12 0 227.15 251.46 76.18 o 12 12 0 88.33 53.34 56.10 o 13 12 0 194.97 112.26 61.98 o 14 12 0 9.63 31.94 103.26 o -11 13 0 1.00 -60.93 60.93 o -10 13 0 0.18 -64.94 64.94 o -9 13 0 0.08 -63.88 96.71 o -8 13 0 112.27 231.16 44.02 o -7 13 0 221.21 285.98 43.95 o -6 13 0 33.20 -50.90 53.78 o -5 13 0 0.64 4.76 50.31 o -4 13 0 440.02 579.51 41.66 o -3 13 0 813.50 816.29 75.37 o -2 13 0 685.43 780.47 115.35 o -1 13 0 142.90 182.17 68.21 o 0 13 0 157.56 180.14 32.19 o 1 13 0 2622.64 2678.45 59.35 o 2 13 0 358.12 350.54 35.24 o 3 13 0 974.95 923.63 43.26 o 4 13 0 254.26 282.77 35.39 o 5 13 0 326.74 316.62 72.74 o 6 13 0 1719.29 1755.77 64.09 o 7 13 0 0.94 45.51 74.90 o 8 13 0 15.52 88.05 43.82 o 9 13 0 126.73 90.06 49.84 o 10 13 0 109.37 173.68 47.00 o 11 13 0 141.18 177.31 54.77 o 12 13 0 7.70 -29.40 66.21 o 13 13 0 66.83 85.61 62.63 o -10 14 0 27.88 92.94 46.51 o -9 14 0 13.29 -64.75 64.75 o -8 14 0 12.90 -8.79 68.28 o -7 14 0 1.35 71.16 40.30 o -6 14 0 3.46 -57.20 57.20 o -5 14 0 240.92 283.33 42.91 o -4 14 0 87.11 82.67 43.12 o -3 14 0 117.27 155.03 37.57 o -2 14 0 418.40 500.27 78.41 o -1 14 0 5.39 31.81 46.16 o 0 14 0 452.41 495.04 37.49 o 1 14 0 23.14 100.39 32.13 o 2 14 0 539.39 574.72 49.44 o 3 14 0 1573.48 1652.00 54.63 o 4 14 0 99.42 23.49 62.27 o 5 14 0 0.66 22.31 47.09 o 6 14 0 446.82 433.94 43.64 o 7 14 0 135.69 84.65 46.22 o 8 14 0 1054.66 1080.06 57.97 o 9 14 0 15.10 -21.52 58.07 o 10 14 0 7.35 46.34 82.53 o 11 14 0 260.73 211.17 50.47 o 12 14 0 9.57 -8.24 70.53 o 13 14 0 70.96 80.89 97.86 o -10 15 0 5.12 -30.59 69.56 o -9 15 0 0.02 40.43 52.65 o -8 15 0 92.76 152.77 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