#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226524.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226524_Fobs loop_ _publ_author_name 'H\"okelek, Tuncer' 'Dal, Hakan' 'Tercan, Bar\?i\,s' '\,Cimen, Efdal' 'Necefo\(glu, Hacali' _publ_section_title ; catena-Poly[[(4-methylbenzoato-\kO)manganese(II)]-\m-aqua-bis(\m-4-methylbenzoato-\k^2^O:O')[(4-methylbenzoato-\kO)manganese(II)]-bis(\m-N,N-diethylnicotinamide)-\k^2^N^3^:O;O:N^3^] ; _journal_coeditor_code IM2201 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m734 _journal_page_last m735 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.537 _cell_angle_beta 78.836 _cell_angle_gamma 88.485 _cell_length_a 10.5228 _cell_length_b 19.1361 _cell_length_c 26.6008 _exptl_crystal_F_000 2143.65 _reflns_d_resolution_high 0.7484 _[local]_cod_data_source_file im2201Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tb19 in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 466.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.01 20.53 6.11 o 2 0 0 24368.11 23325.10 333.74 o 3 0 0 252.74 236.65 13.62 o 4 0 0 5309.97 4773.93 64.68 o 5 0 0 307.70 406.38 39.33 o 6 0 0 7486.19 7221.76 107.42 o 7 0 0 491.07 472.33 47.01 o 8 0 0 570.08 496.91 39.96 o 9 0 0 424.86 401.47 54.42 o 10 0 0 1535.32 1656.78 120.65 o 11 0 0 18.56 -35.05 49.19 o 12 0 0 93.83 187.51 93.04 o 13 0 0 10.50 -26.66 65.15 o -13 1 0 90.60 148.33 71.45 o -12 1 0 14.12 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3 3 0 7204.35 7221.95 106.04 o 4 3 0 41.03 31.65 17.12 o 5 3 0 4423.80 5048.93 88.16 o 6 3 0 45.49 24.76 21.58 o 7 3 0 179.50 154.07 31.97 o 8 3 0 138.44 106.64 33.77 o 9 3 0 1273.59 1230.15 72.16 o 10 3 0 140.17 174.55 58.98 o 11 3 0 388.22 451.49 76.22 o 12 3 0 0.14 48.30 64.32 o 13 3 0 1880.26 1889.04 137.74 o -13 4 0 199.65 298.19 68.83 o -12 4 0 69.99 97.26 65.84 o -11 4 0 29.16 21.85 49.25 o -10 4 0 4.03 4.59 34.34 o -9 4 0 8.34 -52.44 52.44 o -8 4 0 587.04 550.04 42.80 o -7 4 0 54.68 61.25 30.05 o -6 4 0 4986.36 4794.99 88.15 o -5 4 0 3054.10 2979.12 73.07 o -4 4 0 23542.15 24485.30 320.00 o -3 4 0 575.17 536.04 49.60 o -2 4 0 6178.88 5984.69 100.32 o -1 4 0 167.98 175.74 14.39 o 0 4 0 405.94 371.08 12.69 o 1 4 0 180.62 231.17 14.51 o 2 4 0 79.26 75.34 9.75 o 3 4 0 2168.72 2147.35 36.32 o 4 4 0 6646.32 6175.86 88.12 o 5 4 0 77.48 38.21 16.76 o 6 4 0 5147.57 5086.33 95.93 o 7 4 0 1537.10 1661.94 80.25 o 8 4 0 3145.31 2941.99 85.70 o 9 4 0 84.11 153.88 105.22 o 10 4 0 1734.20 1791.73 110.50 o 11 4 0 177.17 197.32 124.05 o 12 4 0 264.30 189.03 72.10 o 13 4 0 106.34 160.40 79.05 o -13 5 0 1.25 -24.98 59.37 o -12 5 0 2647.29 2513.09 120.14 o -11 5 0 1032.94 967.89 93.40 o -10 5 0 188.35 121.38 45.21 o -9 5 0 240.48 187.02 44.05 o -8 5 0 6223.35 5938.96 131.16 o -7 5 0 1613.67 1496.47 62.01 o -6 5 0 2790.88 2593.96 72.80 o -5 5 0 73.05 69.90 25.15 o -4 5 0 12982.62 14238.50 257.24 o -3 5 0 24630.34 24721.70 390.07 o -2 5 0 2631.00 2442.70 55.48 o -1 5 0 5739.51 5924.88 72.52 o 0 5 0 1133.45 1107.54 26.62 o 1 5 0 17.35 14.30 11.87 o 2 5 0 702.44 707.60 22.06 o 3 5 0 2881.78 2789.95 43.59 o 4 5 0 2235.33 2251.90 45.45 o 5 5 0 4006.40 4442.64 80.57 o 6 5 0 30.22 38.82 21.25 o 7 5 0 3062.32 3025.85 80.35 o 8 5 0 710.75 799.87 61.31 o 9 5 0 529.57 405.45 65.15 o 10 5 0 8.76 15.17 53.26 o 11 5 0 2351.75 2490.04 133.59 o 12 5 0 250.30 381.32 80.67 o 13 5 0 1323.04 1766.61 137.32 o -13 6 0 172.20 103.95 87.16 o -12 6 0 41.57 12.73 46.37 o -11 6 0 13.65 -12.87 46.09 o 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26.19 47.19 17.23 o 5 8 0 7933.18 7923.55 186.95 o 6 8 0 114.51 107.87 32.25 o 7 8 0 2221.99 2084.97 86.56 o 8 8 0 113.17 160.32 54.78 o 9 8 0 200.16 232.60 101.90 o 10 8 0 53.06 47.37 73.10 o 11 8 0 1482.46 1542.59 122.87 o 12 8 0 57.83 -32.43 69.58 o -12 9 0 820.10 776.96 85.71 o -11 9 0 66.12 115.28 51.50 o -10 9 0 158.72 127.52 47.81 o -9 9 0 221.82 249.76 54.35 o -8 9 0 9913.83 9322.76 208.99 o -7 9 0 371.40 433.99 53.92 o -6 9 0 381.75 286.02 37.30 o -5 9 0 162.78 151.35 26.98 o -4 9 0 6175.11 6407.43 107.98 o -3 9 0 606.34 681.86 30.56 o -2 9 0 2196.57 2180.70 40.98 o -1 9 0 638.90 610.13 22.80 o 0 9 0 3758.06 4183.56 59.15 o 1 9 0 669.15 722.17 24.24 o 2 9 0 4.90 12.25 13.59 o 3 9 0 60.68 79.78 19.63 o 4 9 0 7175.75 7185.89 95.90 o 5 9 0 1956.36 2008.47 67.31 o 6 9 0 63.41 -19.62 31.12 o 7 9 0 1701.32 1697.54 82.83 o 8 9 0 455.38 533.14 72.22 o 9 9 0 109.50 75.17 66.45 o 10 9 0 265.02 152.51 81.96 o 11 9 0 18.51 103.80 114.08 o 12 9 0 14.85 66.54 77.42 o -12 10 0 458.73 587.54 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6921.01 6965.81 134.98 o 6 12 0 117.05 142.27 45.42 o 7 12 0 269.38 233.64 62.13 o 8 12 0 395.75 256.96 90.82 o 9 12 0 2067.69 2461.04 181.64 o 10 12 0 291.33 334.21 80.89 o 11 12 0 3186.95 3238.42 340.03 o -11 13 0 23.37 -52.22 81.75 o -10 13 0 925.92 889.58 86.33 o -9 13 0 3.87 -11.39 72.13 o -8 13 0 3970.91 3770.36 248.57 o -7 13 0 36.54 19.52 48.91 o -6 13 0 0.49 -26.44 43.44 o -5 13 0 18.04 67.81 50.33 o -4 13 0 1424.55 1365.02 62.93 o -3 13 0 2958.47 2901.27 68.85 o -2 13 0 10314.29 10056.62 141.60 o -1 13 0 2704.19 2795.36 74.82 o 0 13 0 860.65 938.87 35.24 o 1 13 0 1034.63 1063.73 37.08 o 2 13 0 238.60 235.32 24.24 o 3 13 0 322.20 348.13 35.09 o 4 13 0 30.46 -13.91 32.80 o 5 13 0 498.45 553.28 44.59 o 6 13 0 346.59 263.66 62.13 o 7 13 0 1517.69 1696.84 107.29 o 8 13 0 3189.78 3411.34 206.01 o 9 13 0 25.47 26.58 86.39 o 10 13 0 107.15 203.79 101.90 o 11 13 0 52.68 106.33 104.11 o -11 14 0 738.79 665.75 88.83 o -10 14 0 188.95 202.04 68.74 o -9 14 0 2815.00 2568.10 187.61 o -8 14 0 397.80 461.29 135.88 o -7 14 0 653.12 689.15 98.21 o -6 14 0 294.72 294.56 55.89 o -5 14 0 1232.63 1179.61 76.94 o -4 14 0 646.49 643.58 51.14 o -3 14 0 596.62 551.44 48.07 o -2 14 0 1977.41 2104.78 70.87 o -1 14 0 890.62 951.87 56.94 o 0 14 0 25.43 10.07 23.43 o 1 14 0 95.63 47.85 22.39 o 2 14 0 2046.45 2091.44 59.82 o 3 14 0 7686.48 7557.31 139.70 o 4 14 0 1474.68 1492.29 65.95 o 5 14 0 347.48 412.68 47.77 o 6 14 0 230.54 138.28 62.13 o 7 14 0 7.01 38.65 61.72 o 8 14 0 196.41 73.10 84.18 o 9 14 0 2.93 -77.53 77.53 o 10 14 0 88.12 -13.29 93.04 o -11 15 0 1.89 -57.21 82.06 o -10 15 0 232.25 269.19 72.96 o -9 15 0 0.56 55.01 60.82 o -8 15 0 681.35 640.35 133.10 o -7 15 0 718.43 773.71 75.65 o -6 15 0 3.62 -79.87 79.87 o -5 15 0 3587.81 3669.27 125.21 o -4 15 0 879.27 994.39 61.21 o -3 15 0 1188.42 1185.44 70.38 o -2 15 0 2631.61 2519.78 79.10 o -1 15 0 10.40 54.78 40.89 o 0 15 0 1359.37 1365.33 55.77 o 1 15 0 165.88 170.85 32.10 o 2 15 0 530.36 450.35 39.77 o 3 15 0 336.66 339.26 39.11 o 4 15 0 315.57 304.46 42.11 o 5 15 0 1086.36 1016.82 64.40 o 6 15 0 1823.69 1980.51 114.34 o 7 15 0 1194.87 1369.03 104.91 o 8 15 0 246.28 292.73 78.13 o 9 15 0 287.14 228.16 106.33 o 10 15 0 7.29 115.19 99.68 o -10 16 0 1201.46 1297.35 104.27 o -9 16 0 50.01 123.70 73.54 o -8 16 0 1015.54 933.22 85.26 o -7 16 0 245.01 191.80 61.06 o -6 16 0 382.22 434.66 65.04 o -5 16 0 1635.94 1577.01 91.86 o -4 16 0 1557.31 1635.88 75.10 o -3 16 0 5323.03 5217.10 141.71 o -2 16 0 545.98 504.83 45.71 o -1 16 0 3746.25 3916.00 113.73 o 0 16 0 1231.82 1196.77 54.07 o 1 16 0 158.42 114.14 39.60 o 2 16 0 463.95 535.33 57.68 o 3 16 0 963.23 1062.87 67.39 o 4 16 0 15.60 -36.03 36.03 o 5 16 0 1985.19 2008.85 86.71 o 6 16 0 1100.61 1127.45 100.21 o 7 16 0 150.55 135.39 72.22 o 8 16 0 202.70 264.70 84.18 o 9 16 0 401.26 436.39 119.62 o -10 17 0 188.02 181.26 74.56 o -9 17 0 453.68 532.71 98.41 o -8 17 0 110.15 153.57 64.91 o -7 17 0 1664.99 1687.01 105.36 o -6 17 0 34.15 9.09 52.70 o -5 17 0 78.24 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