#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:42:01 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181186 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226527.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226527_Fobs loop_ _publ_author_name 'Luo, Zhong-Hua' 'Chang, Jin' 'Feng, Mei-Li' 'Zhang, Qin' 'Zhu, Hong-Jun' _publ_section_title ; 1,4-Dibromo-2,5-dimethoxybenzene ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1806 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.140 _cell_angle_gamma 90.000 _cell_length_a 6.5730 _cell_length_b 8.4380 _cell_length_c 8.7560 _exptl_crystal_F_000 284.00 _reflns_d_resolution_high 0.8318 _cod_data_source_file im2205Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Q in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 145.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12806.30 12402.92 1055.91 o 4 0 0 1558.36 1575.06 25.53 o 6 0 0 585.12 706.55 26.50 o 1 1 0 2755.77 3153.90 516.87 o 2 1 0 167.08 198.69 118.78 o 3 1 0 49.41 63.47 7.29 o 4 1 0 217.71 169.66 111.00 o 5 1 0 160.47 157.71 13.28 o 6 1 0 130.11 162.11 16.81 o 7 1 0 1.58 2.95 17.36 o 0 2 0 1766.57 1840.65 20.10 o 1 2 0 1834.33 1960.02 171.31 o 2 2 0 7342.32 7097.52 4194.89 o 3 2 0 377.32 354.57 66.34 o 4 2 0 2586.50 2387.58 1404.34 o 5 2 0 2.24 10.57 11.28 o 6 2 0 196.14 196.61 16.33 o 7 2 0 0.36 9.99 15.02 o 1 3 0 401.20 395.14 31.05 o 2 3 0 135.38 145.18 22.84 o 3 3 0 98.87 99.74 9.08 o 4 3 0 392.43 377.78 48.28 o 5 3 0 51.15 38.39 20.06 o 6 3 0 48.64 31.04 16.56 o 7 3 0 33.77 74.80 15.13 o 0 4 0 6457.12 6556.42 60.69 o 1 4 0 480.11 466.52 11.48 o 2 4 0 3620.53 3635.18 303.11 o 3 4 0 31.36 14.23 8.84 o 4 4 0 1717.87 1684.40 134.51 o 5 4 0 74.75 63.74 18.19 o 6 4 0 297.22 287.52 27.38 o 7 4 0 3.03 16.94 16.94 o 1 5 0 164.77 160.13 14.89 o 2 5 0 172.94 143.43 10.95 o 3 5 0 548.60 497.85 40.73 o 4 5 0 2.91 0.57 11.77 o 5 5 0 94.84 90.77 15.28 o 6 5 0 14.42 19.72 20.43 o 0 6 0 2963.69 3162.33 51.85 o 1 6 0 587.71 592.30 18.75 o 2 6 0 1604.79 1629.90 112.45 o 3 6 0 834.83 830.36 64.87 o 4 6 0 279.34 290.20 46.02 o 5 6 0 35.82 48.38 24.86 o 6 6 0 85.63 96.61 19.13 o 1 7 0 0.40 2.56 12.46 o 2 7 0 91.48 106.00 15.14 o 3 7 0 19.52 14.82 15.01 o 4 7 0 25.98 52.95 19.77 o 5 7 0 93.38 72.83 20.17 o 0 8 0 288.56 322.95 30.16 o 1 8 0 578.40 555.16 25.34 o 2 8 0 292.92 324.20 21.65 o 3 8 0 39.89 14.56 26.73 o 4 8 0 225.28 275.50 22.98 o 1 9 0 12.10 56.06 22.66 o 2 9 0 16.26 36.02 20.38 o 3 9 0 66.55 43.10 34.83 o 0 10 0 67.59 58.28 31.13 o 1 10 0 103.54 144.71 25.68 o -7 0 1 136.82 186.37 23.43 o -5 0 1 1012.88 1035.19 25.84 o -3 0 1 5771.63 5523.30 199.93 o -1 0 1 2992.64 3361.84 121.48 o 1 0 1 10284.89 10813.04 1194.20 o 3 0 1 6774.09 6766.25 322.71 o 5 0 1 531.55 566.83 23.85 o 7 0 1 71.38 79.47 22.38 o -7 1 1 21.25 62.20 30.34 o -6 1 1 26.40 26.37 13.16 o -5 1 1 237.20 221.38 13.83 o -4 1 1 22.63 18.12 8.05 o -3 1 1 70.15 87.71 7.43 o -2 1 1 1115.51 1144.38 121.80 o -1 1 1 1379.57 1541.81 247.15 o 0 1 1 385.92 454.09 27.29 o 1 1 1 938.83 1050.52 210.46 o 2 1 1 252.37 254.90 26.57 o 3 1 1 523.31 496.79 25.13 o 4 1 1 79.97 81.89 9.24 o 5 1 1 372.12 356.07 15.98 o 6 1 1 0.29 33.58 12.76 o 7 1 1 65.80 50.44 18.52 o -7 2 1 171.07 208.06 22.90 o -6 2 1 64.61 38.21 20.33 o -5 2 1 1481.16 1377.81 167.40 o -4 2 1 8.70 19.12 10.97 o -3 2 1 4204.08 3991.55 583.28 o -2 2 1 215.93 212.00 29.41 o -1 2 1 21310.92 21840.79 3046.08 o 0 2 1 1373.76 1545.04 76.66 o 1 2 1 13145.26 13566.84 800.34 o 2 2 1 393.87 376.27 56.14 o 3 2 1 2112.15 1913.38 239.49 o 4 2 1 4.07 0.38 8.06 o 5 2 1 737.47 653.50 46.37 o 6 2 1 0.23 11.76 14.73 o 7 2 1 55.47 60.21 16.69 o -7 3 1 21.09 23.49 17.77 o -6 3 1 29.71 22.21 14.60 o -5 3 1 59.83 51.30 12.61 o -4 3 1 263.03 236.67 13.54 o -3 3 1 7.80 1.75 8.64 o -2 3 1 152.53 127.76 23.60 o -1 3 1 599.71 581.15 32.94 o 0 3 1 129.64 123.56 5.73 o 1 3 1 858.34 870.72 82.40 o 2 3 1 85.08 71.89 11.93 o 3 3 1 1169.69 1187.76 167.94 o 4 3 1 353.60 346.95 69.72 o 5 3 1 199.17 226.26 42.27 o 6 3 1 59.17 41.32 13.44 o 7 3 1 47.57 59.92 16.37 o -7 4 1 56.99 64.31 20.27 o -6 4 1 0.41 33.17 15.10 o -5 4 1 423.11 462.88 67.95 o -4 4 1 662.26 599.98 85.90 o -3 4 1 3661.42 3690.95 295.06 o -2 4 1 2326.58 2341.13 171.67 o -1 4 1 4291.61 4211.93 58.77 o 0 4 1 232.54 219.45 8.26 o 1 4 1 3413.07 3387.16 170.23 o 2 4 1 331.45 315.02 25.39 o 3 4 1 2133.84 2192.04 314.96 o 4 4 1 129.60 112.15 16.49 o 5 4 1 366.86 273.48 207.39 o 6 4 1 0.33 17.76 21.86 o 7 4 1 50.59 65.73 16.29 o -6 5 1 57.49 61.53 19.07 o -5 5 1 83.59 101.48 16.03 o -4 5 1 13.43 35.43 12.59 o -3 5 1 1.28 10.01 9.60 o -2 5 1 201.11 206.76 11.74 o -1 5 1 455.49 413.90 15.51 o 0 5 1 31.60 33.46 9.74 o 1 5 1 16.64 16.00 7.68 o 2 5 1 148.01 140.09 23.87 o 3 5 1 106.59 59.06 37.81 o 4 5 1 168.35 142.20 14.87 o 5 5 1 64.51 3.44 41.61 o 6 5 1 78.27 86.13 18.00 o -6 6 1 32.81 9.73 33.64 o -5 6 1 396.43 435.99 48.75 o -4 6 1 69.21 66.78 15.28 o -3 6 1 626.40 644.34 47.81 o -2 6 1 391.32 383.28 19.29 o -1 6 1 1443.70 1454.33 65.73 o 0 6 1 1065.16 1092.15 23.37 o 1 6 1 1775.86 1851.00 41.01 o 2 6 1 177.11 168.02 14.36 o 3 6 1 1037.39 930.50 568.26 o 4 6 1 83.23 86.77 28.02 o 5 6 1 293.84 294.98 21.12 o 6 6 1 8.17 12.40 64.16 o -5 7 1 7.19 6.39 19.09 o -4 7 1 146.76 154.57 27.33 o -3 7 1 6.37 16.48 21.45 o -2 7 1 29.27 23.75 14.64 o -1 7 1 52.19 74.32 13.57 o 0 7 1 61.92 65.35 13.94 o 1 7 1 219.20 253.19 27.58 o 2 7 1 323.42 325.42 56.67 o 3 7 1 2.49 8.36 14.57 o 4 7 1 149.78 164.83 28.27 o 5 7 1 14.59 9.48 17.35 o -4 8 1 138.36 141.01 22.04 o -3 8 1 274.89 252.46 38.21 o -2 8 1 248.06 252.79 35.49 o -1 8 1 514.58 539.09 37.02 o 0 8 1 373.47 375.98 26.21 o 1 8 1 569.26 613.84 26.25 o 2 8 1 518.56 583.38 79.33 o 3 8 1 145.14 137.85 20.53 o 4 8 1 35.88 56.03 18.95 o -3 9 1 26.21 23.96 37.23 o -2 9 1 1.09 19.89 19.89 o -1 9 1 0.85 22.11 25.64 o 0 9 1 25.99 4.54 18.55 o 1 9 1 18.93 13.70 19.11 o 2 9 1 11.42 9.13 19.30 o 3 9 1 9.15 12.57 19.11 o -1 10 1 68.77 77.03 22.49 o 0 10 1 180.44 180.78 23.41 o 1 10 1 19.31 20.61 31.46 o -6 0 2 1159.49 1244.14 32.79 o -4 0 2 2912.87 2881.93 34.45 o -2 0 2 5753.01 5710.01 51.03 o 0 0 2 13612.83 10804.54 654.43 o 2 0 2 4746.81 4431.26 210.52 o 4 0 2 782.16 760.15 29.38 o 6 0 2 64.54 114.38 29.01 o -7 1 2 27.89 19.16 16.47 o -6 1 2 0.47 10.31 12.65 o -5 1 2 70.68 74.49 17.60 o -4 1 2 6.20 1.40 7.97 o -3 1 2 25.21 31.26 7.29 o -2 1 2 36.71 22.87 5.62 o -1 1 2 831.43 895.16 106.11 o 0 1 2 2425.23 3035.57 388.23 o 1 1 2 254.97 273.81 58.86 o 2 1 2 3124.35 3431.89 263.42 o 3 1 2 124.07 137.87 16.79 o 4 1 2 918.38 843.47 20.36 o 5 1 2 61.30 53.81 11.24 o 6 1 2 215.68 242.59 17.61 o 7 1 2 37.76 34.02 22.94 o -7 2 2 0.39 16.37 16.37 o -6 2 2 197.08 192.72 16.94 o -5 2 2 160.22 162.21 13.94 o -4 2 2 2724.40 2496.02 291.90 o -3 2 2 663.31 608.42 70.62 o -2 2 2 7887.71 8105.37 471.62 o -1 2 2 17.75 20.86 5.01 o 0 2 2 7299.89 8771.55 1012.53 o 1 2 2 1.73 4.14 4.54 o 2 2 2 5808.46 5648.05 654.99 o 3 2 2 113.57 110.11 14.23 o 4 2 2 1202.73 1058.01 146.02 o 5 2 2 0.70 1.35 14.15 o 6 2 2 153.36 172.24 15.43 o 7 2 2 0.11 6.05 14.90 o -7 3 2 40.74 44.94 18.68 o -6 3 2 51.41 31.10 15.46 o -5 3 2 12.39 2.50 20.33 o -4 3 2 3.72 8.48 11.08 o -3 3 2 201.79 178.16 47.64 o -2 3 2 1598.40 1569.75 173.86 o -1 3 2 95.37 98.30 6.37 o 0 3 2 743.82 743.79 13.61 o 1 3 2 255.76 235.09 151.71 o 2 3 2 257.14 223.58 33.27 o 3 3 2 35.49 36.46 8.65 o 4 3 2 402.85 376.05 70.09 o 5 3 2 41.62 42.33 11.68 o 6 3 2 84.44 98.15 14.53 o 7 3 2 5.50 4.28 14.97 o -7 4 2 16.50 3.50 18.95 o -6 4 2 339.96 376.00 22.82 o -5 4 2 31.01 28.73 14.54 o -4 4 2 943.87 919.88 101.42 o -3 4 2 54.03 37.84 9.45 o -2 4 2 4317.45 4315.89 158.39 o -1 4 2 1703.36 1798.38 22.45 o 0 4 2 5480.03 5819.61 396.02 o 1 4 2 1339.52 1413.74 124.70 o 2 4 2 1431.37 1279.76 179.36 o 3 4 2 68.77 73.10 24.76 o 4 4 2 708.85 677.98 104.23 o 5 4 2 1.18 9.94 13.01 o 6 4 2 91.50 114.17 16.33 o 7 4 2 1.26 6.37 19.29 o -6 5 2 13.14 13.05 17.83 o -5 5 2 94.50 85.82 16.52 o -4 5 2 117.61 154.63 32.44 o -3 5 2 25.99 10.92 10.79 o -2 5 2 16.08 23.46 8.69 o -1 5 2 41.46 49.86 8.77 o 0 5 2 472.01 427.70 13.92 o 1 5 2 99.67 98.52 9.82 o 2 5 2 974.28 984.57 103.58 o 3 5 2 554.23 582.70 116.69 o 4 5 2 355.24 417.14 80.65 o 5 5 2 94.52 65.01 16.05 o 6 5 2 73.79 66.81 18.70 o -6 6 2 199.98 243.33 30.85 o -5 6 2 89.31 83.88 17.87 o -4 6 2 823.70 791.15 44.79 o -3 6 2 786.13 736.82 70.17 o -2 6 2 787.59 762.64 21.39 o -1 6 2 616.14 612.33 18.72 o 0 6 2 1152.10 1100.07 64.49 o 1 6 2 246.01 252.76 14.82 o 2 6 2 1144.24 1181.12 67.86 o 3 6 2 68.73 54.33 14.14 o 4 6 2 179.70 207.96 51.56 o 5 6 2 7.89 35.37 15.58 o 6 6 2 52.01 97.09 19.04 o -5 7 2 56.99 25.87 19.87 o -4 7 2 1.38 3.59 17.07 o -3 7 2 106.29 85.67 22.22 o -2 7 2 94.21 125.29 15.30 o -1 7 2 15.49 7.58 13.76 o 0 7 2 106.66 111.35 14.66 o 1 7 2 162.81 174.10 24.57 o 2 7 2 60.93 61.79 15.10 o 3 7 2 127.74 106.80 17.34 o 4 7 2 14.57 27.66 15.82 o 5 7 2 140.83 166.15 54.20 o -4 8 2 138.44 134.84 22.64 o -3 8 2 198.40 197.58 27.82 o -2 8 2 351.27 318.42 23.07 o -1 8 2 318.83 366.91 26.93 o 0 8 2 319.46 311.15 21.38 o 1 8 2 179.81 200.32 25.03 o 2 8 2 294.51 333.50 22.21 o 3 8 2 79.32 80.74 19.10 o 4 8 2 179.80 219.54 21.80 o -3 9 2 11.34 9.70 19.58 o -2 9 2 75.81 89.33 24.35 o -1 9 2 2.07 3.39 18.73 o 0 9 2 77.27 66.52 20.41 o 1 9 2 102.21 83.42 21.50 o 2 9 2 2.72 8.29 19.13 o 3 9 2 76.45 89.84 26.26 o -7 0 3 44.18 51.90 20.50 o -5 0 3 1372.71 1340.05 29.43 o -3 0 3 8853.38 8181.01 246.36 o -1 0 3 9186.36 9588.49 405.89 o 1 0 3 6411.43 6710.63 331.23 o 3 0 3 2116.01 2049.37 38.02 o 5 0 3 316.29 355.45 18.65 o 7 0 3 3.51 10.78 21.68 o -7 1 3 0.17 30.68 21.12 o -6 1 3 9.80 15.68 26.97 o -5 1 3 42.70 20.31 14.91 o -4 1 3 37.40 40.58 12.68 o -3 1 3 386.07 352.52 44.05 o -2 1 3 485.56 481.04 83.59 o -1 1 3 1839.55 2179.52 176.38 o 0 1 3 162.45 163.13 31.79 o 1 1 3 2963.07 2987.94 355.66 o 2 1 3 2.37 12.44 6.26 o 3 1 3 1230.59 1129.77 80.47 o 4 1 3 6.52 13.66 8.41 o 5 1 3 337.98 296.74 16.54 o 6 1 3 2.62 7.73 13.00 o 7 1 3 83.90 117.14 19.42 o -7 2 3 285.70 286.81 21.69 o -6 2 3 16.08 33.87 13.79 o -5 2 3 970.99 945.44 107.66 o -4 2 3 205.51 198.18 56.77 o -3 2 3 1983.64 1934.34 288.90 o -2 2 3 447.89 442.22 68.59 o -1 2 3 5411.94 6501.84 73.14 o 0 2 3 598.53 660.34 33.21 o 1 2 3 3348.92 3105.06 608.81 o 2 2 3 416.27 431.36 94.12 o 3 2 3 1022.29 904.03 153.60 o 4 2 3 1.08 1.17 9.27 o 5 2 3 87.38 84.66 12.70 o 6 2 3 25.87 4.13 18.34 o 7 2 3 9.45 22.16 15.16 o -7 3 3 0.78 18.74 18.74 o -6 3 3 29.45 35.21 15.52 o -5 3 3 24.89 25.71 12.91 o -4 3 3 24.87 30.16 11.28 o -3 3 3 425.86 393.08 40.23 o -2 3 3 49.74 38.80 7.77 o -1 3 3 1403.15 1480.94 19.63 o 0 3 3 218.78 214.24 15.43 o 1 3 3 2161.52 2247.00 267.06 o 2 3 3 528.82 476.00 79.19 o 3 3 3 1879.31 1970.73 329.69 o 4 3 3 91.27 92.50 12.16 o 5 3 3 476.46 453.11 31.38 o 6 3 3 31.45 36.83 13.50 o 7 3 3 15.00 29.42 16.00 o -6 4 3 36.88 65.80 26.10 o -5 4 3 643.45 662.48 44.35 o -4 4 3 238.33 232.30 31.10 o -3 4 3 1595.15 1503.86 198.76 o -2 4 3 443.87 451.33 53.92 o -1 4 3 2767.11 2761.37 30.24 o 0 4 3 132.41 126.90 15.92 o 1 4 3 2975.30 3170.03 276.59 o 2 4 3 2.89 0.29 14.08 o 3 4 3 579.05 582.66 133.82 o 4 4 3 7.37 0.27 12.38 o 5 4 3 174.69 190.40 34.14 o 6 4 3 5.90 8.87 15.12 o -6 5 3 67.47 79.39 19.98 o -5 5 3 18.24 17.06 16.78 o -4 5 3 121.32 92.79 15.20 o -3 5 3 302.88 253.15 36.19 o -2 5 3 20.52 18.95 17.48 o -1 5 3 737.97 720.71 18.06 o 0 5 3 340.60 325.24 26.23 o 1 5 3 436.92 411.94 45.98 o 2 5 3 113.19 107.31 12.70 o 3 5 3 173.70 178.84 16.91 o 4 5 3 223.56 261.89 37.19 o 5 5 3 78.85 114.19 25.13 o 6 5 3 53.65 65.81 18.47 o -5 6 3 215.85 197.12 33.94 o -4 6 3 160.04 154.83 17.31 o -3 6 3 1061.96 971.00 69.42 o -2 6 3 581.54 539.61 60.24 o -1 6 3 1230.97 1176.36 25.76 o 0 6 3 803.81 847.50 46.58 o 1 6 3 459.13 421.39 43.33 o 2 6 3 179.93 201.53 21.37 o 3 6 3 419.45 443.44 55.29 o 4 6 3 3.76 26.90 14.74 o 5 6 3 67.17 69.60 18.41 o -5 7 3 139.84 150.51 49.18 o -4 7 3 1.93 24.64 16.35 o -3 7 3 99.99 117.30 23.23 o -2 7 3 3.62 6.45 14.06 o -1 7 3 197.31 225.93 16.44 o 0 7 3 23.67 26.29 13.17 o 1 7 3 355.88 361.94 19.17 o 2 7 3 252.76 206.76 29.23 o 3 7 3 133.42 129.62 25.14 o 4 7 3 99.88 106.14 49.88 o 5 7 3 34.65 24.60 19.77 o -4 8 3 273.06 290.45 53.19 o -3 8 3 95.74 110.25 29.74 o -2 8 3 271.64 272.49 20.12 o -1 8 3 108.99 107.48 17.41 o 0 8 3 173.49 150.93 19.26 o 1 8 3 268.26 286.97 20.92 o 2 8 3 87.12 100.13 18.64 o 3 8 3 124.87 136.93 20.11 o 4 8 3 0.90 18.95 18.95 o -2 9 3 0.49 19.52 19.52 o -1 9 3 43.06 40.13 34.04 o 0 9 3 111.96 143.54 19.61 o 1 9 3 29.70 39.94 63.07 o 2 9 3 115.93 80.88 20.11 o -6 0 4 324.42 295.16 21.59 o -4 0 4 1127.75 1118.10 25.38 o -2 0 4 2846.56 2931.62 63.56 o 0 0 4 1632.54 1428.73 19.02 o 2 0 4 1773.02 1650.34 61.71 o 4 0 4 236.71 240.84 14.99 o 6 0 4 4.81 3.07 52.32 o -7 1 4 10.64 29.71 18.24 o -6 1 4 23.85 34.71 14.82 o -5 1 4 10.73 9.80 18.62 o -4 1 4 542.23 454.84 18.52 o -3 1 4 21.68 32.21 8.90 o -2 1 4 1719.85 1693.96 298.36 o -1 1 4 69.81 82.68 7.23 o 0 1 4 2963.24 2925.98 782.21 o 1 1 4 595.76 628.76 109.58 o 2 1 4 3138.52 3332.38 228.89 o 3 1 4 1.24 5.51 8.17 o 4 1 4 969.60 922.91 36.57 o 5 1 4 17.66 22.95 11.23 o 6 1 4 77.75 104.87 16.25 o 7 1 4 1.52 6.46 19.06 o -7 2 4 0.21 7.02 24.07 o -6 2 4 416.01 402.61 60.54 o -5 2 4 3.04 4.89 15.41 o -4 2 4 2099.29 1920.53 254.03 o -3 2 4 206.90 197.76 25.60 o -2 2 4 3805.11 3901.29 425.49 o -1 2 4 126.90 143.50 8.44 o 0 2 4 4366.61 5056.81 544.95 o 1 2 4 61.46 66.88 15.56 o 2 2 4 864.70 746.56 169.48 o 3 2 4 0.82 13.24 8.63 o 4 2 4 213.90 197.48 21.16 o 5 2 4 18.29 7.23 12.68 o 6 2 4 63.31 55.52 26.98 o 7 2 4 9.28 10.22 16.42 o -6 3 4 44.02 68.42 21.52 o -5 3 4 1.86 2.76 14.19 o -4 3 4 125.25 102.96 14.78 o -3 3 4 1.24 9.78 9.78 o -2 3 4 1167.74 1110.61 102.33 o -1 3 4 62.63 63.21 8.23 o 0 3 4 2564.95 2780.12 206.09 o 1 3 4 72.60 80.41 9.72 o 2 3 4 966.52 936.78 153.25 o 3 3 4 256.23 256.75 29.39 o 4 3 4 366.88 368.66 80.75 o 5 3 4 64.30 73.03 13.79 o 6 3 4 247.60 229.34 34.33 o -6 4 4 267.16 277.57 54.60 o -5 4 4 261.94 287.94 20.21 o -4 4 4 682.84 637.64 72.00 o -3 4 4 377.79 335.29 49.78 o -2 4 4 1541.32 1478.70 116.98 o -1 4 4 444.47 458.42 14.55 o 0 4 4 1263.02 1150.93 89.98 o 1 4 4 458.15 455.44 35.01 o 2 4 4 649.80 639.36 81.07 o 3 4 4 19.96 4.23 11.78 o 4 4 4 65.48 95.52 18.24 o 5 4 4 43.57 53.73 22.89 o 6 4 4 2.37 15.15 16.46 o -6 5 4 41.20 46.74 21.00 o -5 5 4 19.33 7.96 18.37 o -4 5 4 268.56 242.08 42.25 o -3 5 4 5.36 3.23 12.30 o -2 5 4 752.32 576.55 353.38 o -1 5 4 58.38 69.37 23.14 o 0 5 4 885.41 829.61 25.94 o 1 5 4 224.20 215.39 13.99 o 2 5 4 702.82 662.96 109.62 o 3 5 4 156.09 167.42 36.00 o 4 5 4 358.75 353.75 44.05 o 5 5 4 79.01 74.20 36.20 o 6 5 4 16.14 60.79 21.27 o -5 6 4 136.30 154.31 20.95 o -4 6 4 269.22 267.92 53.31 o -3 6 4 222.89 239.85 17.98 o -2 6 4 357.82 252.84 165.01 o -1 6 4 304.00 296.59 16.46 o 0 6 4 623.44 632.94 20.77 o 1 6 4 121.21 161.15 15.22 o 2 6 4 431.36 452.17 46.54 o 3 6 4 3.43 11.47 14.53 o 4 6 4 134.04 182.57 18.49 o 5 6 4 0.07 11.42 17.93 o -4 7 4 191.17 180.06 35.95 o -3 7 4 0.12 15.85 15.85 o -2 7 4 201.44 213.75 56.42 o -1 7 4 231.52 223.98 17.82 o 0 7 4 219.27 245.20 17.28 o 1 7 4 276.11 226.11 33.87 o 2 7 4 314.67 300.76 19.65 o 3 7 4 105.95 90.75 17.65 o 4 7 4 41.82 16.38 19.02 o -3 8 4 291.95 297.72 38.81 o -2 8 4 260.95 236.39 20.73 o -1 8 4 243.04 235.35 23.75 o 0 8 4 80.88 87.25 17.49 o 1 8 4 43.33 69.16 30.02 o 2 8 4 32.78 47.29 17.00 o 3 8 4 53.15 37.74 24.97 o -2 9 4 84.89 64.98 20.21 o -1 9 4 4.07 3.02 17.51 o 0 9 4 81.52 88.90 18.75 o 1 9 4 67.76 58.74 18.94 o 2 9 4 4.10 18.12 18.12 o -5 0 5 721.90 701.44 30.20 o -3 0 5 1913.98 1963.85 38.63 o -1 0 5 3925.98 3731.45 103.66 o 1 0 5 424.67 364.42 36.46 o 3 0 5 19.34 12.65 9.16 o 5 0 5 225.28 238.58 22.05 o -6 1 5 1.49 16.76 15.75 o -5 1 5 199.62 172.91 17.40 o -4 1 5 0.52 11.11 12.49 o -3 1 5 1137.80 994.66 154.31 o -2 1 5 66.21 44.12 9.93 o -1 1 5 2545.07 3131.38 31.93 o 0 1 5 112.77 135.16 43.75 o 1 1 5 3009.51 3156.91 439.21 o 2 1 5 86.04 99.07 10.84 o 3 1 5 1392.93 1269.07 43.59 o 4 1 5 395.37 334.49 17.13 o 5 1 5 316.24 335.51 19.18 o 6 1 5 0.02 16.22 16.22 o -6 2 5 35.49 10.12 18.34 o -5 2 5 423.36 408.10 28.80 o -4 2 5 91.41 101.88 14.42 o -3 2 5 1314.08 1220.89 144.76 o -2 2 5 137.75 140.42 11.62 o -1 2 5 826.18 827.25 17.41 o 0 2 5 15.39 28.30 13.83 o 1 2 5 1003.44 965.78 231.72 o 2 2 5 9.53 16.77 9.29 o 3 2 5 323.93 337.97 47.69 o 4 2 5 0.03 1.07 11.31 o 5 2 5 21.50 27.38 12.43 o 6 2 5 0.19 25.61 29.91 o -6 3 5 14.03 26.53 18.55 o -5 3 5 233.90 207.71 19.84 o -4 3 5 10.24 13.42 39.47 o -3 3 5 992.24 901.62 179.35 o -2 3 5 6.47 1.74 14.63 o -1 3 5 2075.47 2271.81 29.24 o 0 3 5 175.50 191.55 12.06 o 1 3 5 1276.41 1251.97 230.83 o 2 3 5 137.00 133.93 18.00 o 3 3 5 662.50 680.82 154.94 o 4 3 5 1.15 9.83 17.22 o 5 3 5 122.61 121.76 15.77 o 6 3 5 8.40 1.65 21.09 o -6 4 5 31.66 43.54 26.12 o -5 4 5 460.00 432.74 47.41 o -4 4 5 134.36 135.99 28.50 o -3 4 5 546.57 515.42 55.08 o -2 4 5 297.19 281.87 15.26 o -1 4 5 918.11 921.09 20.66 o 0 4 5 271.94 302.80 34.76 o 1 4 5 789.90 769.23 109.25 o 2 4 5 2.37 6.95 11.71 o 3 4 5 112.78 101.41 20.49 o 4 4 5 4.36 6.68 13.61 o 5 4 5 15.15 4.28 15.25 o 6 4 5 7.37 6.64 25.55 o -5 5 5 134.84 146.98 40.07 o -4 5 5 8.62 14.60 16.03 o -3 5 5 364.92 348.75 36.38 o -2 5 5 141.24 145.85 14.38 o -1 5 5 861.56 844.49 36.23 o 0 5 5 479.66 506.86 18.63 o 1 5 5 1385.86 1416.90 213.43 o 2 5 5 125.50 122.45 27.55 o 3 5 5 352.31 437.72 91.90 o 4 5 5 37.69 13.38 16.27 o 5 5 5 121.35 178.86 30.27 o -5 6 5 61.95 77.68 21.62 o -4 6 5 293.08 292.57 21.64 o -3 6 5 341.06 301.31 25.89 o -2 6 5 230.92 222.36 17.34 o -1 6 5 280.37 252.77 17.18 o 0 6 5 68.08 78.53 14.02 o 1 6 5 23.56 36.40 13.03 o 2 6 5 111.60 122.48 15.42 o 3 6 5 30.25 28.48 15.31 o 4 6 5 4.38 45.98 45.98 o 5 6 5 28.24 68.27 18.16 o -4 7 5 9.27 34.11 20.26 o -3 7 5 271.62 235.45 22.47 o -2 7 5 24.16 34.07 16.23 o -1 7 5 284.45 274.15 19.21 o 0 7 5 72.85 88.94 15.31 o 1 7 5 76.27 87.48 15.56 o 2 7 5 230.28 225.03 45.63 o 3 7 5 185.03 177.65 20.13 o 4 7 5 117.17 114.91 27.16 o -3 8 5 22.91 30.65 18.60 o -2 8 5 134.87 137.39 19.65 o -1 8 5 67.01 70.21 22.63 o 0 8 5 85.61 57.98 17.73 o 1 8 5 106.42 96.80 35.99 o 2 8 5 10.91 3.15 16.98 o 3 8 5 35.03 28.71 17.55 o -6 0 6 151.27 140.57 22.34 o -4 0 6 722.94 727.81 25.36 o -2 0 6 899.70 894.85 23.19 o 0 0 6 464.48 451.10 14.91 o 2 0 6 312.35 298.95 14.35 o 4 0 6 31.12 8.32 14.55 o 6 0 6 6.41 23.87 30.33 o -6 1 6 86.55 67.84 20.40 o -5 1 6 2.77 15.67 15.67 o -4 1 6 693.67 686.99 108.49 o -3 1 6 4.53 28.27 18.76 o -2 1 6 2180.37 2063.00 283.11 o -1 1 6 1.58 9.16 9.16 o 0 1 6 1690.70 1444.06 394.67 o 1 1 6 10.13 25.88 10.35 o 2 1 6 1058.76 1033.72 63.06 o 3 1 6 119.80 126.67 35.70 o 4 1 6 517.22 487.89 19.96 o 5 1 6 0.05 14.38 13.23 o 6 1 6 63.09 59.85 18.65 o -6 2 6 220.77 197.55 25.73 o -5 2 6 14.37 3.08 16.86 o -4 2 6 363.24 357.12 21.38 o -3 2 6 64.32 40.39 36.54 o -2 2 6 722.20 764.14 98.25 o -1 2 6 457.46 506.05 33.60 o 0 2 6 617.79 583.10 104.80 o 1 2 6 1.19 8.78 10.24 o 2 2 6 3.42 9.78 16.22 o 3 2 6 100.25 108.42 20.83 o 4 2 6 33.60 33.01 17.84 o 5 2 6 0.44 13.94 13.94 o 6 2 6 1.17 12.60 16.39 o -6 3 6 120.47 152.34 23.44 o -5 3 6 5.83 2.67 17.39 o -4 3 6 420.21 424.67 46.09 o -3 3 6 91.81 93.97 16.19 o -2 3 6 865.15 875.90 51.92 o -1 3 6 239.18 264.73 23.58 o 0 3 6 3129.15 3507.04 428.80 o 1 3 6 46.65 42.86 16.01 o 2 3 6 1734.57 1833.03 397.81 o 3 3 6 232.03 231.00 59.48 o 4 3 6 167.20 174.98 17.05 o 5 3 6 31.28 18.14 15.67 o 6 3 6 43.67 42.44 17.66 o -5 4 6 127.65 136.24 21.59 o -4 4 6 355.57 392.05 26.17 o -3 4 6 184.21 213.73 17.20 o -2 4 6 260.25 245.96 15.91 o -1 4 6 7.10 8.38 13.73 o 0 4 6 37.02 28.72 11.98 o 1 4 6 34.70 33.60 12.39 o 2 4 6 164.40 197.86 15.17 o 3 4 6 39.42 25.63 14.66 o 4 4 6 7.54 29.27 26.96 o 5 4 6 16.29 5.88 16.98 o -5 5 6 7.41 68.00 19.76 o -4 5 6 311.99 390.52 94.44 o -3 5 6 6.73 1.61 15.75 o -2 5 6 823.11 819.55 45.87 o -1 5 6 72.95 61.74 14.35 o 0 5 6 302.62 263.73 31.99 o 1 5 6 391.58 408.67 67.44 o 2 5 6 239.44 189.06 32.16 o 3 5 6 64.91 94.47 17.02 o 4 5 6 180.08 232.28 70.13 o 5 5 6 3.78 27.12 17.19 o -4 6 6 54.35 94.55 19.91 o -3 6 6 144.42 144.13 19.70 o -2 6 6 131.22 114.44 18.73 o -1 6 6 194.24 182.72 17.46 o 0 6 6 204.80 203.03 17.40 o 1 6 6 1.59 17.37 18.22 o 2 6 6 13.15 9.27 15.05 o 3 6 6 9.45 26.75 15.63 o 4 6 6 0.22 1.95 17.44 o -3 7 6 41.28 29.45 18.19 o -2 7 6 256.26 246.00 20.81 o -1 7 6 130.49 133.10 19.27 o 0 7 6 334.95 309.86 27.29 o 1 7 6 77.08 81.71 16.88 o 2 7 6 136.97 101.12 17.67 o 3 7 6 38.17 33.91 39.57 o -1 8 6 73.72 60.01 17.77 o 0 8 6 11.83 22.03 16.27 o 1 8 6 16.87 26.07 15.87 o -5 0 7 100.88 143.36 29.59 o -3 0 7 38.70 34.62 15.92 o -1 0 7 580.97 582.77 27.05 o 1 0 7 28.03 16.63 14.93 o 3 0 7 43.10 40.15 20.11 o 5 0 7 5.83 7.48 17.17 o -5 1 7 263.18 279.35 39.87 o -4 1 7 1.45 16.28 16.28 o -3 1 7 991.19 886.63 132.29 o -2 1 7 382.71 359.55 51.35 o -1 1 7 2223.37 2431.58 276.92 o 0 1 7 10.41 1.82 17.70 o 1 1 7 1655.03 1822.95 294.64 o 2 1 7 7.91 4.66 28.80 o 3 1 7 385.17 379.20 26.40 o 4 1 7 26.72 44.74 12.99 o 5 1 7 85.36 98.08 16.93 o -5 2 7 203.15 273.79 31.75 o -4 2 7 18.51 33.40 28.01 o -3 2 7 472.69 481.84 80.45 o -2 2 7 3.83 5.77 12.93 o -1 2 7 17.92 15.00 11.73 o 0 2 7 11.79 14.29 12.04 o 1 2 7 55.25 69.47 30.90 o 2 2 7 37.57 69.36 21.29 o 3 2 7 10.10 43.92 13.12 o 4 2 7 17.91 4.07 14.33 o 5 2 7 5.06 0.59 15.59 o -5 3 7 249.04 285.59 24.88 o -4 3 7 5.29 18.22 18.22 o -3 3 7 818.47 799.88 76.99 o -2 3 7 2.66 13.81 13.81 o -1 3 7 640.42 661.81 21.66 o 0 3 7 176.63 215.31 48.98 o 1 3 7 502.03 497.57 110.56 o 2 3 7 15.83 20.52 15.45 o 3 3 7 581.63 573.03 114.44 o 4 3 7 0.33 6.42 15.31 o 5 3 7 82.93 109.84 18.15 o -5 4 7 63.34 72.11 22.90 o -4 4 7 92.66 104.55 26.67 o -3 4 7 114.30 90.52 18.04 o -2 4 7 234.20 219.62 19.99 o -1 4 7 124.57 159.11 20.73 o 0 4 7 25.23 57.32 21.38 o 1 4 7 6.95 20.38 26.76 o 2 4 7 75.09 73.76 15.93 o 3 4 7 0.09 4.24 15.49 o 4 4 7 0.51 24.99 26.65 o 5 4 7 0.65 27.29 27.29 o -4 5 7 30.17 42.41 19.88 o -3 5 7 347.51 318.08 32.77 o -2 5 7 65.92 97.58 16.20 o -1 5 7 745.68 672.56 24.16 o 0 5 7 60.78 49.12 15.02 o 1 5 7 794.14 803.87 104.32 o 2 5 7 192.24 184.17 21.06 o 3 5 7 108.42 130.44 18.37 o 4 5 7 43.34 41.94 22.98 o -3 6 7 4.82 27.54 17.49 o -2 6 7 49.28 46.04 27.93 o -1 6 7 19.02 31.78 15.95 o 0 6 7 0.73 15.11 40.21 o 1 6 7 57.34 57.89 15.53 o 2 6 7 3.94 16.29 16.29 o 3 6 7 0.43 21.54 23.53 o -2 7 7 121.53 87.98 20.21 o -1 7 7 252.28 230.94 20.01 o 0 7 7 138.09 127.42 17.80 o 1 7 7 53.62 44.75 16.14 o 2 7 7 32.91 20.67 19.44 o -4 0 8 275.25 266.50 25.46 o -2 0 8 4.24 8.01 19.27 o 0 0 8 4.97 22.11 13.17 o 2 0 8 53.20 54.11 14.44 o 4 0 8 1.69 20.85 14.90 o -5 1 8 2.14 7.38 22.04 o -4 1 8 375.58 338.56 51.68 o -3 1 8 84.14 65.30 17.45 o -2 1 8 1005.53 984.19 45.66 o -1 1 8 20.34 0.03 15.97 o 0 1 8 1070.15 1043.04 221.89 o 1 1 8 112.37 130.43 18.86 o 2 1 8 511.95 540.98 25.30 o 3 1 8 1.47 16.62 18.13 o 4 1 8 124.15 87.79 18.07 o 5 1 8 0.26 0.28 16.81 o -4 2 8 4.53 18.43 18.55 o -3 2 8 3.79 0.73 17.55 o -2 2 8 105.29 103.97 16.55 o -1 2 8 4.32 13.70 13.70 o 0 2 8 4.55 10.26 17.85 o 1 2 8 0.33 3.66 25.28 o 2 2 8 93.30 80.43 37.96 o 3 2 8 0.35 0.89 16.20 o 4 2 8 21.23 16.41 22.62 o -4 3 8 514.77 558.07 114.63 o -3 3 8 89.93 56.85 19.80 o -2 3 8 662.32 718.44 26.25 o -1 3 8 64.33 46.60 16.02 o 0 3 8 705.18 719.23 120.53 o 1 3 8 29.27 59.39 13.99 o 2 3 8 311.16 297.58 69.71 o 3 3 8 24.80 41.86 23.69 o 4 3 8 63.86 76.48 17.80 o -4 4 8 40.32 46.93 21.86 o -3 4 8 77.81 50.57 28.99 o -2 4 8 24.96 41.06 16.44 o -1 4 8 1.97 7.12 15.07 o 0 4 8 6.88 4.32 16.22 o 1 4 8 0.11 14.48 17.39 o 2 4 8 0.88 11.10 15.79 o 3 4 8 12.21 20.49 17.55 o 4 4 8 5.22 9.17 18.20 o -3 5 8 81.96 102.34 20.67 o -2 5 8 430.87 429.54 24.32 o -1 5 8 81.27 100.87 36.90 o 0 5 8 224.92 206.25 27.31 o 1 5 8 21.00 20.64 40.56 o 2 5 8 198.55 196.48 38.81 o 3 5 8 12.99 15.87 20.74 o -2 6 8 4.95 23.89 18.07 o -1 6 8 70.86 49.19 18.41 o 0 6 8 15.01 25.40 16.14 o 1 6 8 6.68 16.95 18.13 o 2 6 8 0.23 0.86 15.75 o -3 0 9 17.80 4.20 53.79 o -1 0 9 1.45 9.07 14.51 o 1 0 9 107.16 140.35 23.77 o 3 0 9 51.07 57.88 20.42 o -4 1 9 10.60 35.38 25.58 o -3 1 9 372.50 377.51 63.12 o -2 1 9 0.77 3.68 16.92 o -1 1 9 533.81 466.76 161.55 o 0 1 9 10.25 0.06 16.06 o 1 1 9 444.25 498.53 44.17 o 2 1 9 0.23 15.59 18.38 o 3 1 9 112.89 137.72 20.06 o 4 1 9 1.91 23.88 23.88 o -3 2 9 1.36 10.29 58.94 o -2 2 9 1.06 18.03 18.03 o -1 2 9 9.86 1.65 16.02 o 0 2 9 18.78 14.92 15.75 o 1 2 9 0.63 27.44 17.17 o 2 2 9 1.51 19.92 19.92 o 3 2 9 7.67 16.88 18.36 o -3 3 9 546.96 523.69 85.36 o -2 3 9 23.72 41.23 18.40 o -1 3 9 592.78 606.82 57.06 o 0 3 9 87.08 65.51 18.54 o 1 3 9 230.48 185.31 59.14 o 2 3 9 16.46 32.16 18.92 o 3 3 9 104.89 125.13 20.11 o -2 4 9 20.07 10.14 19.23 o -1 4 9 0.65 10.35 16.69 o 0 4 9 10.48 18.49 18.49 o 1 4 9 31.19 44.16 17.18 o 2 4 9 3.14 6.17 17.95 o -1 5 9 170.80 198.01 59.60 o 0 5 9 43.00 54.23 17.23 o 1 5 9 115.16 99.14 29.48 o -2 0 10 7.53 1.99 19.65 o 0 0 10 31.04 17.06 20.53 o 2 0 10 33.70 34.72 20.71 o -2 1 10 340.04 383.14 24.70 o -1 1 10 14.60 0.45 15.20 o 0 1 10 257.56 260.89 86.99 o 1 1 10 10.41 30.24 23.33 o 2 1 10 109.10 101.95 27.36 o -1 2 10 2.44 0.22 20.44 o 0 2 10 50.53 39.85 18.49 o 1 2 10 0.82 25.46 19.21 o 0 3 10 165.14 174.98 74.41 o