#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:42:01 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181186 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226531.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226531_Fobs loop_ _publ_author_name 'Gelbrich, Thomas' 'Haddow, Mairi F.' 'Griesser, Ulrich J.' _publ_section_title ; Polymorphic form II of 4,4'-methylenebis(benzenesulfonamide) ; _journal_coeditor_code IM2209 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1619 _journal_volume 66 _journal_year 2010 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.931 _cell_angle_gamma 90.000 _cell_length_a 10.8251 _cell_length_b 5.0791 _cell_length_c 12.6912 _exptl_crystal_F_000 340.00 _reflns_d_resolution_high 0.8111 _cod_data_source_file im2209Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 -5 0 33.84 30.41 14.09 o 7 -5 0 55.30 54.15 13.58 o 3 -4 0 158.47 169.11 15.97 o 4 -4 0 42.80 46.38 11.53 o 5 -4 0 337.15 371.15 19.54 o 6 -4 0 52.91 49.26 9.81 o 7 -4 0 23.02 9.69 9.91 o 8 -4 0 44.67 43.32 9.42 o 9 -4 0 122.35 136.83 15.10 o 10 -4 0 255.51 267.50 32.80 o 2 -3 0 93.17 85.24 9.65 o 3 -3 0 588.44 566.97 26.41 o 4 -3 0 480.30 513.18 22.75 o 5 -3 0 116.01 126.69 9.73 o 6 -3 0 687.18 679.74 39.34 o 7 -3 0 219.33 224.94 10.51 o 8 -3 0 68.61 62.55 14.61 o 9 -3 0 138.42 160.32 14.43 o 10 -3 0 58.60 64.29 19.56 o 11 -3 0 29.94 43.39 11.19 o 1 -2 0 506.38 549.44 45.18 o 2 -2 0 422.96 422.31 19.15 o 3 -2 0 3.72 8.29 3.32 o 4 -2 0 325.73 341.09 13.75 o 5 -2 0 13.49 11.23 4.08 o 6 -2 0 39.37 50.19 8.04 o 7 -2 0 142.08 161.63 12.64 o 8 -2 0 281.28 269.32 36.17 o 9 -2 0 209.54 234.68 23.36 o 10 -2 0 372.00 325.38 37.92 o 11 -2 0 35.92 13.40 9.74 o 12 -2 0 182.98 150.75 41.08 o 1 -1 0 1571.68 1442.80 50.33 o 2 -1 0 48.51 60.18 4.03 o 3 -1 0 3849.48 3614.50 147.85 o 4 -1 0 1501.45 1416.11 53.76 o 5 -1 0 563.71 627.62 22.45 o 6 -1 0 541.09 536.51 21.64 o 7 -1 0 932.96 989.43 33.03 o 8 -1 0 328.06 353.99 17.14 o 9 -1 0 383.86 374.81 21.63 o 10 -1 0 26.55 27.27 7.29 o 11 -1 0 12.50 13.61 5.95 o 12 -1 0 66.72 56.34 9.29 o 2 0 0 1065.05 978.99 27.11 o 3 0 0 175.85 157.81 8.01 o 4 0 0 1071.39 1028.11 24.13 o 5 0 0 1339.47 1389.51 37.45 o 6 0 0 2.34 4.39 2.42 o 7 0 0 266.41 300.82 10.79 o 8 0 0 25.13 22.10 4.03 o 9 0 0 836.49 914.21 38.93 o 10 0 0 682.84 774.69 37.00 o 11 0 0 50.31 76.26 12.94 o 12 0 0 90.91 54.81 38.26 o 13 0 0 213.48 215.15 35.62 o 1 1 0 1584.65 1484.93 57.46 o 2 1 0 50.68 66.56 4.35 o 3 1 0 3882.28 3662.59 89.86 o 4 1 0 1506.03 1448.79 34.09 o 5 1 0 569.76 619.35 14.91 o 6 1 0 560.85 519.63 22.81 o 7 1 0 940.21 969.00 36.72 o 8 1 0 329.56 329.25 20.41 o 9 1 0 383.02 378.63 18.89 o 10 1 0 24.81 20.36 6.52 o 11 1 0 12.52 2.89 5.97 o 12 1 0 65.65 61.68 10.48 o 13 1 0 121.10 145.11 22.63 o 0 2 0 1888.16 1716.31 94.89 o 1 2 0 518.97 556.90 24.70 o 2 2 0 414.91 401.33 16.27 o 3 2 0 1.99 0.00 2.74 o 4 2 0 332.07 346.23 10.17 o 5 2 0 14.33 14.40 2.44 o 6 2 0 40.51 51.27 7.03 o 7 2 0 143.98 171.79 12.98 o 8 2 0 277.99 239.78 14.22 o 9 2 0 213.37 246.80 19.86 o 10 2 0 378.01 327.60 17.78 o 11 2 0 36.78 33.85 47.15 o 12 2 0 177.10 167.70 23.94 o 1 3 0 93.76 107.35 5.29 o 2 3 0 98.37 96.47 6.68 o 3 3 0 592.70 618.26 23.02 o 4 3 0 493.07 527.38 16.81 o 5 3 0 116.68 123.55 5.11 o 6 3 0 671.83 658.85 30.26 o 7 3 0 224.12 196.78 17.74 o 8 3 0 66.32 62.81 12.19 o 9 3 0 135.92 165.33 18.15 o 10 3 0 59.65 55.90 11.43 o 11 3 0 30.47 29.86 12.56 o 0 4 0 864.66 836.59 29.91 o 1 4 0 118.10 113.75 5.49 o 2 4 0 81.02 85.51 5.44 o 3 4 0 159.73 156.22 6.91 o 4 4 0 46.20 47.81 4.35 o 5 4 0 337.86 345.00 14.24 o 6 4 0 51.21 39.52 6.58 o 7 4 0 23.68 31.62 6.95 o 8 4 0 45.78 59.05 7.98 o 9 4 0 125.46 139.01 23.81 o 10 4 0 251.57 275.15 67.64 o 1 5 0 95.40 88.37 5.99 o 2 5 0 169.76 182.60 6.91 o 3 5 0 292.02 296.34 12.66 o 4 5 0 25.48 31.38 4.99 o 5 5 0 34.23 37.74 4.01 o 6 5 0 34.19 51.55 8.17 o 7 5 0 54.63 74.61 17.77 o 8 5 0 65.38 62.25 9.39 o 0 6 0 536.98 547.51 26.05 o 1 6 0 27.27 18.57 4.67 o 2 6 0 306.93 274.54 13.45 o 3 6 0 1.06 0.00 5.56 o -7 -5 1 46.78 55.94 11.79 o -6 -5 1 91.83 68.84 19.82 o -5 -5 1 64.81 93.35 17.25 o 6 -5 1 0.94 7.60 15.72 o 7 -5 1 13.28 16.23 12.47 o -10 -4 1 191.37 223.26 22.04 o -9 -4 1 4.91 13.84 7.43 o -8 -4 1 399.66 401.25 32.50 o -7 -4 1 21.55 37.72 7.93 o -6 -4 1 275.28 297.30 20.06 o -5 -4 1 5.36 5.67 4.91 o -4 -4 1 94.85 95.32 12.47 o -3 -4 1 174.76 207.89 24.09 o 4 -4 1 28.99 34.85 13.24 o 5 -4 1 327.02 346.60 19.10 o 6 -4 1 19.98 22.97 5.29 o 7 -4 1 73.60 65.76 9.18 o 8 -4 1 48.68 48.88 7.78 o 9 -4 1 33.51 24.58 11.41 o 10 -4 1 37.17 59.36 12.30 o -11 -3 1 152.46 139.90 17.59 o -10 -3 1 21.23 0.00 28.95 o -9 -3 1 11.86 2.77 6.70 o -8 -3 1 11.15 5.51 7.99 o -7 -3 1 55.01 42.19 6.01 o -6 -3 1 280.19 279.61 16.67 o -5 -3 1 241.01 276.63 17.77 o -4 -3 1 79.87 87.22 7.73 o -3 -3 1 206.24 205.07 12.51 o -2 -3 1 567.63 555.59 36.47 o 3 -3 1 48.73 59.83 4.88 o 4 -3 1 84.31 104.27 12.68 o 5 -3 1 34.05 34.02 5.68 o 6 -3 1 36.15 46.13 5.35 o 7 -3 1 219.36 214.17 15.99 o 8 -3 1 597.83 574.65 33.40 o 9 -3 1 613.34 632.65 49.92 o 10 -3 1 139.43 123.67 15.01 o 11 -3 1 217.36 241.64 45.78 o -12 -2 1 10.84 0.00 11.79 o -11 -2 1 19.06 3.57 6.92 o -10 -2 1 235.33 258.95 40.70 o -9 -2 1 249.30 241.04 20.20 o -8 -2 1 1258.64 1338.26 60.65 o -7 -2 1 178.07 193.61 11.88 o -6 -2 1 94.70 99.84 7.99 o -5 -2 1 665.35 646.07 39.76 o -4 -2 1 1082.09 1122.23 46.72 o -3 -2 1 61.39 72.42 7.17 o -2 -2 1 90.14 97.46 12.00 o -1 -2 1 130.31 148.19 10.33 o 2 -2 1 940.18 927.65 24.63 o 3 -2 1 863.22 905.62 33.59 o 4 -2 1 1914.13 1926.64 57.74 o 5 -2 1 982.80 931.89 30.71 o 6 -2 1 653.73 629.91 36.04 o 7 -2 1 132.88 140.84 8.36 o 8 -2 1 67.10 60.06 11.15 o 9 -2 1 142.53 122.78 7.48 o 10 -2 1 124.68 114.95 10.02 o 11 -2 1 68.31 57.16 6.43 o 12 -2 1 132.54 93.69 21.69 o -12 -1 1 152.98 129.12 14.45 o -11 -1 1 673.38 696.73 39.20 o -10 -1 1 60.75 63.65 6.33 o -9 -1 1 31.43 38.67 5.31 o -8 -1 1 462.03 461.13 18.14 o -7 -1 1 188.02 202.00 11.37 o -6 -1 1 284.94 301.20 14.83 o -5 -1 1 868.84 863.61 31.81 o -4 -1 1 200.38 174.12 10.96 o -3 -1 1 1255.28 1206.71 50.95 o -2 -1 1 5856.03 5339.03 206.38 o -1 -1 1 7620.06 7013.96 189.04 o 0 -1 1 147.63 141.29 17.77 o 1 -1 1 606.96 573.78 16.08 o 2 -1 1 1634.12 1477.87 40.66 o 3 -1 1 833.68 790.94 27.56 o 4 -1 1 489.71 468.30 15.89 o 5 -1 1 424.40 424.92 17.03 o 6 -1 1 466.11 491.64 23.89 o 7 -1 1 17.31 16.63 3.49 o 8 -1 1 1454.80 1484.50 44.36 o 9 -1 1 317.98 342.41 15.22 o 10 -1 1 102.34 92.02 8.63 o 11 -1 1 51.11 52.26 8.53 o 12 -1 1 67.16 55.21 8.67 o 13 -1 1 55.07 53.81 33.14 o -13 0 1 11.77 40.65 20.33 o -12 0 1 27.18 31.43 10.42 o -11 0 1 102.81 94.03 9.19 o -10 0 1 118.12 96.39 7.28 o -9 0 1 63.93 66.50 5.91 o -8 0 1 288.29 256.86 9.44 o -7 0 1 525.58 538.95 20.52 o -6 0 1 238.72 257.36 10.51 o -5 0 1 1992.55 2026.23 63.94 o -4 0 1 840.71 809.67 28.51 o -3 0 1 331.68 350.96 13.37 o -2 0 1 98.26 104.39 4.91 o 2 0 1 9713.91 8379.98 209.70 o 3 0 1 3622.52 3347.45 82.22 o 4 0 1 1116.60 1126.83 30.02 o 5 0 1 451.89 441.44 13.46 o 6 0 1 1673.78 1681.64 36.29 o 7 0 1 8.76 10.80 2.85 o 8 0 1 1.01 1.11 5.05 o 9 0 1 0.88 0.00 4.05 o 10 0 1 16.01 23.64 4.96 o 11 0 1 230.36 246.08 19.05 o 12 0 1 452.16 383.68 44.20 o 13 0 1 2.48 7.43 14.78 o -13 1 1 146.78 91.75 14.74 o -12 1 1 155.19 144.07 19.95 o -11 1 1 671.38 710.87 32.27 o -10 1 1 56.56 58.12 6.55 o -9 1 1 30.56 32.95 5.25 o -8 1 1 464.73 514.56 16.54 o -7 1 1 185.43 201.40 9.82 o -6 1 1 287.40 298.40 8.49 o -5 1 1 862.61 854.39 37.44 o -4 1 1 214.85 202.93 10.41 o -3 1 1 1255.39 1249.73 38.48 o -2 1 1 5817.35 5346.78 220.91 o -1 1 1 7664.82 7117.43 183.48 o 0 1 1 142.55 134.25 6.13 o 1 1 1 602.78 557.48 16.09 o 2 1 1 1654.18 1533.11 43.04 o 3 1 1 840.41 803.11 27.61 o 4 1 1 494.48 478.25 12.39 o 5 1 1 419.17 424.86 14.58 o 6 1 1 477.05 515.67 14.84 o 7 1 1 16.61 21.07 3.37 o 8 1 1 1466.76 1503.78 53.29 o 9 1 1 321.73 355.52 19.42 o 10 1 1 100.63 100.18 17.39 o 11 1 1 47.22 42.22 7.98 o 12 1 1 69.21 69.10 16.48 o 13 1 1 55.82 56.71 18.11 o -12 2 1 10.15 0.00 8.26 o -11 2 1 21.39 17.52 8.93 o -10 2 1 240.09 253.56 15.14 o -9 2 1 254.29 249.20 18.50 o -8 2 1 1260.70 1307.55 48.61 o -7 2 1 180.38 191.66 10.00 o -6 2 1 93.11 79.41 6.71 o -5 2 1 670.22 623.24 23.99 o -4 2 1 1106.18 1126.01 50.00 o -3 2 1 62.97 61.81 4.90 o -2 2 1 88.36 85.73 4.56 o -1 2 1 134.83 137.36 6.46 o 0 2 1 271.21 283.50 10.18 o 1 2 1 1685.41 1697.84 43.40 o 2 2 1 967.58 968.00 31.04 o 3 2 1 883.00 944.05 25.09 o 4 2 1 1917.47 2015.58 50.62 o 5 2 1 990.55 918.80 22.89 o 6 2 1 651.04 661.77 21.54 o 7 2 1 129.26 137.57 8.22 o 8 2 1 64.16 62.10 4.54 o 9 2 1 144.45 148.90 20.20 o 10 2 1 121.72 118.94 11.94 o 11 2 1 68.55 77.05 10.97 o 12 2 1 131.20 137.49 18.19 o -11 3 1 152.04 157.41 45.10 o -10 3 1 23.44 31.81 7.52 o -9 3 1 12.04 26.29 8.34 o -8 3 1 11.75 12.33 10.08 o -7 3 1 53.44 41.11 6.06 o -6 3 1 276.47 271.17 14.89 o -5 3 1 250.78 253.91 19.91 o -4 3 1 79.26 85.26 7.80 o -3 3 1 202.68 217.84 7.66 o -2 3 1 587.90 612.49 20.20 o -1 3 1 509.47 485.65 15.67 o 0 3 1 23.06 25.68 3.41 o 1 3 1 189.16 178.91 9.34 o 2 3 1 134.76 147.72 7.54 o 3 3 1 47.62 43.35 5.13 o 4 3 1 88.70 99.70 10.55 o 5 3 1 30.96 23.44 3.07 o 6 3 1 38.68 45.19 4.17 o 7 3 1 214.07 172.11 9.11 o 8 3 1 599.54 675.86 32.73 o 9 3 1 612.02 635.95 39.74 o 10 3 1 137.82 107.05 14.37 o 11 3 1 218.90 192.52 29.25 o -10 4 1 188.76 217.77 16.59 o -9 4 1 4.30 3.18 8.23 o -8 4 1 391.94 455.07 57.56 o -7 4 1 19.20 19.93 6.77 o -6 4 1 275.37 289.10 15.26 o -5 4 1 4.26 4.71 3.49 o -4 4 1 91.67 83.44 6.78 o -3 4 1 175.45 193.90 14.50 o -2 4 1 184.63 178.35 7.77 o -1 4 1 55.60 56.93 4.90 o 0 4 1 299.60 305.34 13.20 o 1 4 1 103.43 101.03 6.10 o 2 4 1 675.92 685.18 24.99 o 3 4 1 75.08 76.36 5.27 o 4 4 1 30.88 32.37 3.97 o 5 4 1 330.00 347.02 16.17 o 6 4 1 21.77 19.74 2.87 o 7 4 1 73.80 69.50 15.94 o 8 4 1 49.78 58.56 7.57 o 9 4 1 34.92 36.00 9.43 o 10 4 1 37.32 42.24 11.01 o -8 5 1 19.26 16.53 14.01 o -7 5 1 47.00 40.58 8.80 o -6 5 1 95.93 92.10 9.57 o -5 5 1 63.34 60.76 6.08 o -4 5 1 380.86 419.66 18.55 o -3 5 1 22.73 25.23 4.42 o -2 5 1 321.82 285.91 12.94 o -1 5 1 542.18 547.68 15.11 o 0 5 1 137.57 131.49 7.97 o 1 5 1 271.27 267.85 9.64 o 2 5 1 185.45 176.87 7.80 o 3 5 1 448.23 466.51 18.40 o 4 5 1 18.62 23.50 3.57 o 5 5 1 11.28 9.72 2.81 o 6 5 1 1.57 1.93 5.43 o 7 5 1 14.41 16.06 13.17 o -3 6 1 83.02 81.25 8.55 o -2 6 1 111.18 92.88 8.41 o -1 6 1 56.80 50.54 5.89 o 0 6 1 156.36 155.61 8.40 o 1 6 1 29.62 30.24 6.96 o 2 6 1 131.01 134.85 9.05 o 3 6 1 39.48 31.57 4.91 o -7 -5 2 65.13 40.57 12.90 o -6 -5 2 64.85 73.11 15.37 o -5 -5 2 18.57 28.95 9.05 o -4 -5 2 430.69 456.43 43.05 o -10 -4 2 37.04 31.17 12.81 o -9 -4 2 125.68 98.82 15.89 o -8 -4 2 19.20 19.15 8.58 o -7 -4 2 62.51 61.24 24.68 o -6 -4 2 7.26 0.00 6.23 o -5 -4 2 322.99 343.39 19.76 o -4 -4 2 125.80 142.21 16.91 o -3 -4 2 1278.50 1318.98 87.46 o 5 -4 2 23.94 17.00 8.63 o 6 -4 2 13.88 10.01 5.76 o 7 -4 2 272.05 314.95 24.34 o 8 -4 2 41.69 22.86 8.87 o 9 -4 2 103.77 89.70 12.11 o 10 -4 2 140.05 120.09 33.40 o -11 -3 2 80.62 70.63 17.51 o -10 -3 2 173.43 187.02 33.30 o -9 -3 2 210.38 217.05 27.76 o -8 -3 2 49.61 41.41 9.55 o -7 -3 2 321.05 310.29 16.54 o -6 -3 2 44.61 48.60 8.05 o -5 -3 2 241.19 235.31 14.17 o -4 -3 2 431.26 401.72 25.03 o -3 -3 2 12.98 14.89 4.97 o -2 -3 2 3.52 5.30 5.81 o -1 -3 2 38.01 37.67 11.44 o 3 -3 2 147.95 163.90 10.08 o 4 -3 2 225.01 218.34 13.90 o 5 -3 2 98.51 103.88 8.53 o 6 -3 2 700.90 770.98 36.55 o 7 -3 2 133.79 126.31 23.87 o 8 -3 2 33.17 38.03 7.87 o 9 -3 2 25.41 31.41 7.34 o 10 -3 2 207.27 200.54 27.59 o 11 -3 2 19.97 22.27 10.12 o -11 -2 2 1.72 0.00 7.09 o -10 -2 2 134.29 154.73 14.34 o -9 -2 2 168.11 129.82 12.49 o -8 -2 2 149.90 143.08 19.52 o -7 -2 2 189.91 165.20 17.04 o -6 -2 2 341.79 350.69 17.10 o -5 -2 2 962.36 979.52 33.41 o -4 -2 2 683.88 740.70 35.96 o -3 -2 2 3396.03 3322.79 97.77 o -2 -2 2 693.67 685.44 24.42 o -1 -2 2 203.04 205.84 14.43 o 0 -2 2 31.77 25.31 4.40 o 1 -2 2 194.67 239.83 24.51 o 2 -2 2 39.75 45.14 3.54 o 3 -2 2 812.11 838.90 27.22 o 4 -2 2 584.78 644.61 20.65 o 5 -2 2 280.01 268.32 8.86 o 6 -2 2 697.97 745.12 26.75 o 7 -2 2 1638.04 1685.04 94.08 o 8 -2 2 659.03 689.75 30.12 o 9 -2 2 136.93 128.76 11.10 o 10 -2 2 273.75 290.13 15.83 o 11 -2 2 111.06 114.85 13.29 o 12 -2 2 32.03 17.00 17.85 o -12 -1 2 181.45 157.15 24.09 o -11 -1 2 79.55 70.88 8.27 o -10 -1 2 235.70 264.16 22.71 o -9 -1 2 387.66 395.86 21.68 o -8 -1 2 475.77 526.93 24.71 o -7 -1 2 213.89 224.53 10.30 o -6 -1 2 384.11 352.81 16.90 o -5 -1 2 384.55 373.93 13.01 o -4 -1 2 1115.97 1103.63 40.01 o -3 -1 2 281.46 289.76 13.83 o -2 -1 2 922.12 925.16 26.91 o -1 -1 2 1619.84 1570.43 45.61 o 0 -1 2 5995.15 5467.35 208.40 o 1 -1 2 5465.21 5031.82 187.27 o 2 -1 2 513.68 528.24 16.98 o 3 -1 2 421.81 389.85 12.06 o 4 -1 2 1026.88 1002.92 29.93 o 5 -1 2 502.52 486.65 13.70 o 6 -1 2 159.04 156.70 11.07 o 7 -1 2 67.69 62.69 4.62 o 8 -1 2 140.50 138.46 9.60 o 9 -1 2 18.92 20.14 4.64 o 10 -1 2 547.20 580.76 38.55 o 11 -1 2 213.54 205.12 17.65 o 12 -1 2 103.41 61.03 12.23 o 13 -1 2 117.54 110.35 18.28 o -13 0 2 152.82 128.63 44.41 o -12 0 2 272.01 326.61 37.07 o -11 0 2 0.96 0.00 5.72 o -10 0 2 0.21 0.00 5.34 o -9 0 2 94.63 94.88 7.78 o -8 0 2 103.82 100.32 7.22 o -7 0 2 581.17 582.48 18.12 o -6 0 2 9.01 0.34 2.42 o -5 0 2 14.46 10.22 3.16 o -4 0 2 151.70 144.30 6.98 o -3 0 2 2722.35 2458.10 95.08 o -2 0 2 786.60 741.47 26.18 o -1 0 2 164.64 148.98 4.09 o 1 0 2 3070.29 2829.61 115.20 o 2 0 2 256.71 236.70 13.49 o 3 0 2 193.17 163.46 8.49 o 4 0 2 3.60 0.00 1.88 o 5 0 2 595.55 618.12 27.18 o 6 0 2 323.76 324.10 11.33 o 7 0 2 333.74 323.21 14.88 o 8 0 2 0.52 0.00 3.10 o 9 0 2 127.19 124.95 7.14 o 10 0 2 38.56 41.53 6.43 o 11 0 2 0.01 5.91 5.10 o 12 0 2 30.94 16.61 10.12 o 13 0 2 18.91 10.08 12.38 o -13 1 2 14.72 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3400.82 3445.82 98.46 o -2 2 2 714.20 719.62 26.86 o -1 2 2 198.85 215.59 9.65 o 0 2 2 34.54 40.50 4.25 o 1 2 2 196.19 214.63 9.86 o 2 2 2 42.15 50.82 4.12 o 3 2 2 815.32 794.55 29.91 o 4 2 2 597.78 623.28 20.50 o 5 2 2 281.43 274.52 12.47 o 6 2 2 706.55 720.60 28.33 o 7 2 2 1629.48 1637.33 60.61 o 8 2 2 657.81 726.74 30.32 o 9 2 2 132.12 119.78 8.35 o 10 2 2 279.60 320.53 20.16 o 11 2 2 110.68 98.46 22.51 o 12 2 2 32.03 42.00 11.55 o -11 3 2 80.35 74.15 16.37 o -10 3 2 170.84 197.64 23.94 o -9 3 2 204.91 211.35 14.44 o -8 3 2 46.78 41.29 6.38 o -7 3 2 318.13 323.30 16.79 o -6 3 2 44.74 63.09 8.91 o -5 3 2 235.27 210.91 18.74 o -4 3 2 429.88 437.44 17.65 o -3 3 2 11.44 10.89 4.46 o -2 3 2 2.35 6.78 4.21 o -1 3 2 35.87 36.04 3.76 o 0 3 2 1745.02 1810.24 44.68 o 1 3 2 251.49 227.63 9.02 o 2 3 2 480.30 517.88 18.12 o 3 3 2 151.81 145.79 14.92 o 4 3 2 222.11 228.29 11.22 o 5 3 2 102.17 94.39 5.87 o 6 3 2 697.06 753.62 23.17 o 7 3 2 133.65 112.73 7.62 o 8 3 2 30.83 30.47 6.42 o 9 3 2 24.54 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