#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:42:01 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181186 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226545.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226545_Fobs loop_ _publ_author_name 'Mitsui, Ryosuke' 'Nagasawa, Atsushi' 'Noguchi, Keiichi' 'Okamoto, Akiko' 'Yonezawa, Noriyuki' _publ_section_title ; 1,8-Bis(4-chlorobenzoyl)-7-methoxynaphthalen-2-ol ethanol monosolvate ; _journal_coeditor_code IS2562 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1790 _journal_volume 66 _journal_year 2010 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 25.2992 _cell_length_b 25.2992 _cell_length_c 7.3068 _exptl_crystal_F_000 2064.00 _reflns_d_resolution_high 0.8301 _cod_data_source_file is2562Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yonezawa_081205_2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 298.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'y, -x, -z' '-x, -y, z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-x+1/2, -y+1/2, z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 3454.17 3375.35 35.05 o 2 2 0 3402.34 2373.10 27.07 o -1 3 0 9030.08 6710.19 81.16 o 1 3 0 9612.87 10086.98 133.94 o 3 3 0 2022.13 1845.20 30.47 o -2 4 0 2565.69 2704.35 41.61 o 0 4 0 2450.49 1501.42 24.76 o 2 4 0 2332.39 1792.99 31.98 o 4 4 0 21628.86 22846.89 359.44 o -3 5 0 3618.57 3712.34 63.63 o -1 5 0 1488.39 977.87 25.18 o 1 5 0 17081.12 13979.72 229.95 o 3 5 0 6889.54 7461.63 113.50 o 5 5 0 35855.21 35231.00 564.75 o -4 6 0 22701.34 24383.01 389.82 o -2 6 0 165.52 115.21 9.44 o 0 6 0 19147.58 16432.45 262.64 o 2 6 0 66242.98 67426.96 1262.03 o 4 6 0 84643.50 99111.76 1911.66 o 6 6 0 143.01 148.18 7.83 o -5 7 0 12966.32 12491.49 180.46 o -3 7 0 9083.52 7419.57 103.56 o -1 7 0 15970.73 13227.08 197.34 o 1 7 0 1780.16 2072.06 37.54 o 3 7 0 9471.22 9481.67 143.00 o 5 7 0 40358.29 41304.37 690.80 o 7 7 0 569.91 803.59 15.90 o -6 8 0 17069.21 19219.81 294.38 o -4 8 0 6418.21 7049.83 95.37 o -2 8 0 2526.61 2260.83 36.00 o 0 8 0 9779.77 9035.33 133.80 o 2 8 0 80680.53 92489.42 1847.69 o 4 8 0 274.25 156.12 9.27 o 6 8 0 23.50 17.51 5.03 o 8 8 0 416.30 564.34 18.08 o -7 9 0 891.21 899.90 22.93 o -5 9 0 7883.83 8175.79 123.12 o -3 9 0 20947.75 21933.11 351.56 o -1 9 0 2317.44 1885.14 30.94 o 1 9 0 725.98 615.26 16.32 o 3 9 0 36166.32 39926.89 715.76 o 5 9 0 12400.12 12093.89 182.57 o 7 9 0 3731.14 3850.15 57.60 o 9 9 0 10800.02 11333.63 176.04 o -8 10 0 17497.43 19295.72 324.77 o -6 10 0 4049.47 3874.02 63.25 o -4 10 0 1119.87 1028.14 25.09 o -2 10 0 10559.97 10119.10 146.30 o 0 10 0 688.38 736.30 15.98 o 2 10 0 14202.18 12479.93 191.50 o 4 10 0 43856.90 43907.89 804.71 o 6 10 0 20.48 34.39 5.90 o 8 10 0 1436.88 1283.74 26.58 o 10 10 0 337.01 374.11 12.40 o -9 11 0 584.52 565.98 15.73 o -7 11 0 8425.63 8070.86 128.02 o -5 11 0 529.48 501.63 18.72 o -3 11 0 1253.14 1441.40 27.18 o -1 11 0 5875.96 5697.86 84.91 o 1 11 0 9864.86 9445.83 144.34 o 3 11 0 6226.50 5793.77 86.45 o 5 11 0 2345.33 2837.00 47.28 o 7 11 0 588.48 537.04 16.86 o 9 11 0 8159.40 8934.87 149.62 o 11 11 0 464.22 475.24 16.55 o -10 12 0 187.12 206.47 11.39 o -8 12 0 1759.93 1532.34 29.67 o -6 12 0 493.09 390.32 12.88 o -4 12 0 3499.87 3401.02 58.31 o -2 12 0 2156.82 2047.67 37.57 o 0 12 0 2.39 10.66 4.33 o 2 12 0 13.80 183.24 31.97 o 4 12 0 1326.01 1350.48 25.87 o 6 12 0 11410.92 12111.37 196.07 o 8 12 0 128.66 148.47 9.51 o 10 12 0 7738.60 7608.09 181.12 o 12 12 0 201.31 198.17 13.38 o -11 13 0 55.47 53.39 8.18 o -9 13 0 1680.70 1956.34 38.01 o -7 13 0 4980.63 4307.34 81.90 o -5 13 0 115.28 135.23 8.50 o -3 13 0 2048.92 2574.66 50.74 o -1 13 0 10665.91 11400.65 184.64 o 1 13 0 13675.58 14160.37 224.80 o 3 13 0 210.01 217.04 10.82 o 5 13 0 1146.02 1199.96 24.18 o 7 13 0 3907.50 4307.34 74.40 o 9 13 0 2231.27 2659.19 49.76 o 11 13 0 297.08 316.32 16.26 o 13 13 0 16.19 13.50 10.06 o -12 14 0 0.75 24.41 12.79 o -10 14 0 1003.49 989.49 29.78 o -8 14 0 1450.69 1438.94 30.47 o -6 14 0 14.42 13.44 4.68 o -4 14 0 1140.23 1167.92 27.30 o -2 14 0 390.30 571.82 17.46 o 0 14 0 1441.84 1517.47 29.68 o 2 14 0 26.47 28.46 4.25 o 4 14 0 1916.08 1988.47 35.47 o 6 14 0 13.02 8.86 4.57 o 8 14 0 172.84 139.90 9.95 o 10 14 0 5222.45 5183.53 131.96 o 12 14 0 978.33 881.31 39.55 o 14 14 0 158.55 140.91 16.81 o -13 15 0 90.46 62.99 15.06 o -11 15 0 3.48 0.53 3.02 o -9 15 0 426.25 451.18 19.12 o -7 15 0 393.23 485.78 17.27 o -5 15 0 903.72 994.90 24.42 o -3 15 0 60.50 64.73 7.22 o -1 15 0 38.87 74.09 7.51 o 1 15 0 4450.81 4371.34 72.05 o 3 15 0 1053.00 1195.21 23.92 o 5 15 0 454.09 459.08 14.72 o 7 15 0 2677.47 2719.62 52.86 o 9 15 0 372.71 372.37 19.73 o 11 15 0 95.53 66.97 13.47 o 13 15 0 94.51 67.36 15.51 o 15 15 0 177.57 200.38 21.49 o -14 16 0 697.05 749.95 41.37 o -12 16 0 6.51 21.22 11.22 o -10 16 0 1298.81 1339.06 47.22 o -8 16 0 372.77 349.22 18.74 o -6 16 0 7.51 12.57 5.44 o -4 16 0 393.23 603.07 18.72 o -2 16 0 51.54 63.20 7.31 o 0 16 0 231.36 226.60 11.29 o 2 16 0 1214.60 1378.94 32.10 o 4 16 0 1331.48 1453.96 43.08 o 6 16 0 17.60 20.97 7.36 o 8 16 0 913.09 991.64 43.19 o 10 16 0 15.39 12.55 8.50 o 12 16 0 893.00 1060.01 49.65 o 14 16 0 617.69 672.39 39.62 o 16 16 0 858.82 888.52 56.45 o -15 17 0 598.00 544.06 43.77 o -13 17 0 1754.20 1501.02 97.39 o -11 17 0 279.56 253.56 29.66 o -9 17 0 912.31 836.08 38.11 o -7 17 0 1128.89 1203.76 43.03 o -5 17 0 1642.88 1723.17 62.83 o -3 17 0 111.81 146.35 10.68 o -1 17 0 617.87 697.92 21.65 o 1 17 0 78.58 50.40 8.97 o 3 17 0 1277.99 1298.26 42.98 o 5 17 0 1475.32 1645.61 76.67 o 7 17 0 2628.14 2709.63 112.52 o 9 17 0 35.57 50.75 11.94 o 11 17 0 112.78 136.92 19.00 o 13 17 0 1672.16 1827.85 78.35 o 15 17 0 1846.52 1917.14 122.38 o 17 17 0 102.41 73.29 15.87 o -16 18 0 67.60 56.74 15.58 o -14 18 0 6.38 7.42 11.40 o -12 18 0 1800.91 2115.56 100.09 o -10 18 0 0.25 4.50 11.75 o -8 18 0 498.17 475.12 29.99 o -6 18 0 268.86 256.21 18.27 o -4 18 0 193.26 208.39 14.55 o -2 18 0 1408.27 1589.21 50.64 o 0 18 0 4223.67 4325.57 175.81 o 2 18 0 52.67 53.61 11.81 o 4 18 0 2584.65 2469.74 175.68 o 6 18 0 400.75 443.91 32.91 o 8 18 0 5513.84 5738.51 323.41 o 10 18 0 108.27 116.90 17.65 o 12 18 0 8098.05 9122.70 423.13 o 14 18 0 985.67 1108.27 52.36 o 16 18 0 575.98 612.66 66.65 o 18 18 0 3.28 11.85 9.97 o -17 19 0 140.21 104.71 18.28 o -15 19 0 0.45 -0.47 5.73 o -13 19 0 2205.52 2359.00 116.79 o -11 19 0 8.82 16.77 11.89 o -9 19 0 149.59 134.40 20.41 o -7 19 0 1056.75 1054.39 57.63 o -5 19 0 2029.02 2158.76 137.04 o -3 19 0 800.29 772.78 43.78 o -1 19 0 1378.09 1532.67 75.97 o 1 19 0 3000.25 3030.89 177.01 o 3 19 0 7117.09 7672.45 425.57 o 5 19 0 820.59 862.22 40.64 o 7 19 0 5680.52 6574.53 235.84 o 9 19 0 180.43 159.67 25.04 o 11 19 0 2654.67 2844.27 193.75 o 13 19 0 4.66 38.92 18.71 o 15 19 0 211.00 189.07 32.64 o 17 19 0 140.66 100.25 15.15 o 19 19 0 19.72 25.37 12.06 o -18 20 0 8.25 4.90 8.59 o -16 20 0 75.75 95.48 17.46 o -14 20 0 68.80 60.91 19.96 o -12 20 0 354.82 353.72 33.65 o -10 20 0 815.35 834.63 58.97 o -8 20 0 633.64 642.02 44.42 o -6 20 0 1169.07 1306.63 76.21 o -4 20 0 82.87 92.44 19.48 o -2 20 0 781.65 922.16 54.90 o 0 20 0 4956.26 5139.82 321.31 o 2 20 0 28.42 21.18 10.10 o 4 20 0 4654.51 5131.14 264.39 o 6 20 0 1364.79 1479.27 81.33 o 8 20 0 69.71 82.26 21.42 o 10 20 0 252.21 232.40 26.63 o 12 20 0 662.26 609.00 53.64 o 14 20 0 236.48 216.58 26.75 o 16 20 0 11.32 3.23 6.96 o 18 20 0 1.01 0.77 6.08 o 20 20 0 44.35 33.47 13.57 o -19 21 0 50.51 24.51 10.25 o -17 21 0 88.13 78.27 14.98 o -15 21 0 160.06 139.34 19.22 o -13 21 0 144.71 127.02 18.94 o -11 21 0 37.32 42.87 18.44 o -9 21 0 32.64 16.09 12.94 o -7 21 0 1090.74 1146.18 94.36 o -5 21 0 2808.96 2854.87 196.83 o -3 21 0 3056.82 3215.81 188.85 o -1 21 0 15.63 10.33 9.70 o 1 21 0 816.21 945.27 67.03 o 3 21 0 2761.48 3030.87 187.47 o 5 21 0 1474.99 1903.91 95.41 o 7 21 0 4.90 12.18 12.74 o 9 21 0 0.34 0.56 5.28 o 11 21 0 315.95 439.83 35.18 o 13 21 0 583.48 630.24 64.02 o 15 21 0 15.75 14.34 11.68 o 17 21 0 6.98 3.74 9.13 o 19 21 0 149.25 69.03 20.50 o 21 21 0 210.43 144.82 24.70 o -20 22 0 166.85 168.43 55.14 o -18 22 0 19.85 27.23 10.92 o -16 22 0 865.18 830.14 93.04 o -14 22 0 272.50 184.81 23.16 o -12 22 0 81.81 94.75 17.00 o -10 22 0 212.40 198.34 25.34 o -8 22 0 189.59 293.15 34.60 o -6 22 0 703.97 728.91 63.09 o -4 22 0 143.72 127.62 22.10 o -2 22 0 1909.77 2125.54 144.07 o 0 22 0 228.21 208.07 30.85 o 2 22 0 722.97 874.59 70.62 o 4 22 0 649.37 836.07 60.40 o 6 22 0 1819.38 2399.32 142.23 o 8 22 0 533.22 686.23 48.82 o 10 22 0 1189.40 1280.38 109.59 o 12 22 0 9.28 27.29 13.37 o 14 22 0 249.16 239.27 30.77 o 16 22 0 7.76 1.99 7.53 o 18 22 0 1.71 1.17 6.48 o 20 22 0 59.19 51.33 25.52 o -19 23 0 27.64 27.54 16.04 o -17 23 0 32.61 18.72 9.04 o -15 23 0 837.48 596.15 56.13 o -13 23 0 213.28 183.90 29.60 o -11 23 0 18.58 12.91 13.78 o -9 23 0 44.13 68.21 22.38 o -7 23 0 225.43 199.44 23.92 o -5 23 0 234.43 230.75 34.59 o -3 23 0 296.00 318.15 34.77 o -1 23 0 135.11 105.02 15.99 o 1 23 0 1098.52 1245.82 111.61 o 3 23 0 125.70 139.23 19.93 o 5 23 0 361.60 441.59 39.95 o 7 23 0 187.46 201.02 24.74 o 9 23 0 648.12 822.24 61.96 o 11 23 0 399.68 379.89 35.07 o 13 23 0 114.28 147.51 23.85 o 15 23 0 32.80 30.62 13.36 o 17 23 0 3.48 -0.41 6.12 o 19 23 0 12.59 12.42 13.09 o -18 24 0 16.02 19.32 14.76 o -16 24 0 219.05 154.61 20.79 o -14 24 0 47.58 29.63 13.66 o -12 24 0 56.28 43.80 16.37 o -10 24 0 86.37 58.99 18.87 o -8 24 0 79.30 83.09 21.86 o -6 24 0 454.58 474.62 59.67 o -4 24 0 905.54 828.95 101.04 o -2 24 0 1164.86 909.97 104.32 o 0 24 0 1933.25 1671.06 205.00 o 2 24 0 79.30 110.28 16.10 o 4 24 0 32.57 44.95 16.11 o 6 24 0 162.51 189.87 24.55 o 8 24 0 885.49 1140.50 91.64 o 10 24 0 60.92 47.42 17.17 o 12 24 0 1.39 7.46 8.80 o 14 24 0 1.62 3.09 6.66 o 16 24 0 3.03 3.73 8.71 o 18 24 0 30.15 43.69 25.05 o -17 25 0 148.21 89.85 43.96 o -15 25 0 115.94 66.56 18.53 o -13 25 0 1.64 2.21 8.51 o -11 25 0 52.27 41.77 17.43 o -9 25 0 210.65 249.38 44.53 o -7 25 0 1078.52 1425.20 145.96 o -5 25 0 266.74 259.72 42.62 o -3 25 0 63.94 41.76 14.18 o -1 25 0 467.48 416.27 63.33 o 1 25 0 135.18 116.19 20.40 o 3 25 0 110.77 79.97 19.82 o 5 25 0 38.32 34.69 17.71 o 7 25 0 135.92 146.41 20.42 o 9 25 0 34.89 51.29 14.12 o 11 25 0 1.79 7.01 8.67 o 13 25 0 133.92 137.90 32.86 o 15 25 0 245.48 304.70 77.08 o 17 25 0 13.50 8.05 12.62 o -14 26 0 1.42 2.61 7.60 o -12 26 0 5.94 5.36 9.18 o -10 26 0 37.90 42.18 16.17 o -8 26 0 858.28 686.23 131.85 o -6 26 0 179.28 178.74 30.60 o -4 26 0 109.93 82.52 17.93 o -2 26 0 93.13 74.62 15.63 o 0 26 0 6.04 12.09 10.66 o 2 26 0 268.91 285.31 52.14 o 4 26 0 243.03 234.92 28.64 o 6 26 0 329.45 370.86 29.59 o 8 26 0 21.93 11.23 9.25 o 10 26 0 68.42 51.05 13.98 o 12 26 0 284.70 271.32 57.08 o 14 26 0 201.57 291.14 63.28 o -13 27 0 30.89 20.33 16.84 o -11 27 0 1.26 1.34 7.37 o -9 27 0 9.83 13.68 11.18 o -7 27 0 123.79 130.46 24.47 o -5 27 0 48.53 35.05 12.94 o -3 27 0 13.69 15.79 8.81 o -1 27 0 1011.10 516.91 138.68 o 1 27 0 124.89 82.69 16.94 o 3 27 0 442.93 415.59 49.11 o 5 27 0 601.43 645.78 68.77 o 7 27 0 299.40 332.43 35.69 o 9 27 0 20.98 9.54 10.86 o 11 27 0 4.81 6.55 10.53 o 13 27 0 215.62 311.49 74.48 o -12 28 0 10.27 5.47 15.62 o -10 28 0 4.59 2.26 8.72 o -8 28 0 249.31 172.26 31.33 o -6 28 0 0.28 -0.08 5.55 o -4 28 0 256.35 170.51 43.20 o -2 28 0 71.67 32.44 11.05 o 0 28 0 63.32 32.17 11.19 o 2 28 0 40.25 31.22 12.21 o 4 28 0 5.46 13.03 11.09 o 6 28 0 170.38 142.07 25.43 o 8 28 0 1.69 2.87 8.64 o 10 28 0 49.61 56.84 17.56 o 12 28 0 187.66 266.41 58.57 o -9 29 0 3.95 -0.13 4.36 o -7 29 0 636.43 420.12 100.24 o -5 29 0 234.67 105.79 43.43 o -3 29 0 159.70 96.20 30.91 o -1 29 0 109.86 54.68 22.60 o 1 29 0 297.09 212.27 61.35 o 3 29 0 24.43 23.95 14.31 o 5 29 0 77.91 83.99 22.47 o 7 29 0 192.97 195.04 42.50 o 9 29 0 136.46 259.42 67.64 o -4 30 0 260.19 313.40 83.29 o -2 30 0 9.32 15.18 23.56 o 0 30 0 2.39 4.97 12.90 o 2 30 0 33.10 30.55 15.72 o 4 30 0 1.15 3.61 14.53 o 1 0 1 9058.92 8397.54 102.59 o 3 0 1 40505.77 39418.96 636.46 o 5 0 1 9954.51 8781.03 128.55 o 7 0 1 1282.97 1018.94 19.54 o 9 0 1 1805.57 1675.08 26.39 o 11 0 1 4820.18 4629.88 66.34 o 13 0 1 7944.25 8522.72 139.32 o 15 0 1 4971.42 5245.28 84.70 o 17 0 1 335.38 346.47 20.53 o 19 0 1 1385.09 1417.69 78.75 o 21 0 1 76.37 80.72 12.91 o 23 0 1 1017.53 1020.38 129.07 o 25 0 1 836.36 791.77 126.54 o 27 0 1 20.22 17.42 9.41 o 29 0 1 29.83 21.32 13.08 o -30 1 1 106.68 85.20 35.25 o -28 1 1 112.82 93.61 19.12 o -26 1 1 15.41 17.72 13.98 o -24 1 1 827.84 1104.14 128.87 o -22 1 1 60.68 39.08 15.02 o -20 1 1 471.61 567.05 34.70 o -18 1 1 259.90 271.24 24.76 o -16 1 1 2343.66 2230.57 46.84 o -14 1 1 57.28 29.46 6.18 o -12 1 1 1908.21 1960.56 35.39 o -10 1 1 8344.55 8271.84 120.01 o -8 1 1 3051.76 2535.34 37.17 o -6 1 1 2874.93 2398.90 38.56 o -4 1 1 611.24 646.23 23.58 o -2 1 1 6163.95 5092.43 61.27 o 0 1 1 9306.81 8571.41 108.54 o 2 1 1 39622.62 39960.93 644.17 o 4 1 1 7767.71 6305.26 97.27 o 6 1 1 7667.46 7908.47 112.91 o 8 1 1 11632.50 11430.64 159.37 o 10 1 1 11587.97 11382.10 173.73 o 12 1 1 884.83 815.86 18.55 o 14 1 1 2936.12 3227.03 53.71 o 16 1 1 3346.21 3611.02 74.70 o 18 1 1 1723.69 1740.77 77.94 o 20 1 1 423.72 432.45 33.72 o 22 1 1 1008.48 947.39 116.37 o 24 1 1 165.75 217.98 32.70 o 26 1 1 119.86 123.20 23.99 o 28 1 1 210.42 115.11 30.31 o 30 1 1 46.33 31.54 26.86 o -29 2 1 21.08 14.40 15.76 o -27 2 1 15.15 6.84 10.75 o -25 2 1 45.36 63.53 19.32 o -23 2 1 338.50 408.75 51.05 o -21 2 1 32.12 28.95 12.58 o -19 2 1 2165.74 2143.82 134.53 o -17 2 1 2148.88 2215.37 78.42 o -15 2 1 1557.46 1585.24 33.18 o -13 2 1 2231.26 2100.89 38.98 o -11 2 1 14273.64 14023.51 219.61 o -9 2 1 17831.46 17894.18 280.80 o -7 2 1 4877.97 4523.67 63.83 o -5 2 1 7194.00 6169.33 92.86 o -3 2 1 16098.20 14002.75 208.12 o -1 2 1 39666.02 40152.12 627.48 o 1 2 1 6115.63 5092.04 66.21 o 3 2 1 19616.86 19016.11 305.44 o 5 2 1 61771.05 62467.57 1082.85 o 7 2 1 12650.95 10755.31 162.35 o 9 2 1 1720.36 1689.89 31.61 o 11 2 1 390.91 328.10 11.42 o 13 2 1 1663.25 1905.34 35.05 o 15 2 1 4050.26 4185.00 74.83 o 17 2 1 5031.88 5192.15 174.80 o 19 2 1 162.65 152.35 15.68 o 21 2 1 101.24 83.00 14.09 o 23 2 1 1589.13 1822.76 200.91 o 25 2 1 1143.83 1072.75 191.55 o 27 2 1 100.82 61.50 15.50 o 29 2 1 191.29 114.29 36.39 o -30 3 1 21.72 24.43 18.37 o -28 3 1 240.47 269.56 44.68 o -26 3 1 134.09 162.18 23.90 o -24 3 1 1491.49 1804.35 152.80 o -22 3 1 895.79 1105.86 66.69 o -20 3 1 445.53 521.77 45.62 o -18 3 1 1381.61 1498.21 75.96 o -16 3 1 51.77 55.70 7.12 o -14 3 1 962.90 1111.46 24.10 o -12 3 1 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