#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226558.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226558_Fobs loop_ _publ_author_name 'Helliwell, Madeleine' 'Aghazadeh, Masomeh' 'Baradarani, Mehdi M.' 'Joule, John A.' _publ_section_title ; 1-[(E)-4-(5-Bromo-1H-indol-3-yl)-1-methyl-2,5,6,7-tetrahydro-1H-azepin-2-ylidene]propan-2-one ; _journal_coeditor_code JJ2030 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1532 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.267 _cell_angle_gamma 90.000 _cell_length_a 14.4959 _cell_length_b 6.6677 _cell_length_c 16.3724 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.7981 _[local]_cod_data_source_file jj2030Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s3357m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 234.87 262.50 8.96 o 4 0 0 106.38 115.75 4.43 o 6 0 0 2.43 -1.08 2.85 o 8 0 0 3197.87 3227.86 50.42 o 10 0 0 2758.28 2726.44 48.05 o 12 0 0 6701.09 6297.89 526.11 o 14 0 0 410.36 406.16 25.49 o 16 0 0 0.61 24.48 15.04 o 18 0 0 15.69 26.90 14.54 o 1 1 0 894.04 962.19 12.94 o 2 1 0 1876.16 2016.72 22.91 o 3 1 0 46279.71 48474.01 561.02 o 4 1 0 37816.95 39378.04 374.41 o 5 1 0 1.79 2.68 1.46 o 6 1 0 10488.99 10729.37 103.72 o 7 1 0 128.41 113.08 3.98 o 8 1 0 1718.85 1601.27 20.27 o 9 1 0 1441.75 1451.54 19.44 o 10 1 0 83.19 96.10 5.52 o 11 1 0 161.90 161.39 7.31 o 12 1 0 267.52 271.41 9.49 o 13 1 0 112.83 116.09 7.63 o 14 1 0 629.80 644.29 21.79 o 15 1 0 6.08 3.43 6.75 o 16 1 0 3066.30 3064.28 60.07 o 17 1 0 32.50 45.92 10.76 o 18 1 0 604.90 654.58 30.71 o 0 2 0 1728.32 1835.25 28.17 o 1 2 0 2829.16 2934.76 30.15 o 2 2 0 5539.50 5839.25 57.19 o 3 2 0 4906.14 5166.36 51.26 o 4 2 0 899.89 884.88 11.41 o 5 2 0 1651.45 1638.76 29.76 o 6 2 0 3540.10 3808.30 44.93 o 7 2 0 5664.23 5857.67 66.63 o 8 2 0 2755.49 2620.85 34.26 o 9 2 0 820.06 758.48 34.89 o 10 2 0 1959.55 1996.72 32.24 o 11 2 0 232.38 227.87 8.57 o 12 2 0 3975.92 3859.93 57.44 o 13 2 0 1291.64 1307.05 36.10 o 14 2 0 480.53 532.53 17.00 o 15 2 0 401.52 395.59 14.90 o 16 2 0 95.95 103.14 10.18 o 17 2 0 9.06 22.08 12.93 o 1 3 0 5525.22 5611.07 56.42 o 2 3 0 2929.77 2955.05 31.86 o 3 3 0 406.80 379.83 7.11 o 4 3 0 1464.40 1440.51 34.74 o 5 3 0 90.16 114.16 5.59 o 6 3 0 240.14 218.01 6.96 o 7 3 0 1770.73 1809.66 25.95 o 8 3 0 2920.04 2840.05 37.33 o 9 3 0 8073.73 8157.18 92.76 o 10 3 0 233.25 223.62 10.68 o 11 3 0 1931.36 1805.68 33.09 o 12 3 0 556.48 561.22 17.28 o 13 3 0 149.25 137.61 9.85 o 14 3 0 830.45 829.48 27.29 o 15 3 0 84.38 87.91 12.18 o 16 3 0 889.07 932.55 24.99 o 0 4 0 1806.26 1904.21 32.96 o 1 4 0 317.21 335.57 7.54 o 2 4 0 422.58 416.72 8.46 o 3 4 0 3161.39 3061.57 34.43 o 4 4 0 1111.05 1124.07 15.93 o 5 4 0 9274.66 9237.34 102.13 o 6 4 0 1094.60 1074.01 18.47 o 7 4 0 3917.83 3604.43 45.85 o 8 4 0 1306.23 1286.87 25.57 o 9 4 0 12.04 15.83 5.88 o 10 4 0 28.06 27.61 6.88 o 11 4 0 562.85 528.46 16.87 o 12 4 0 618.13 617.11 18.85 o 13 4 0 521.80 513.22 18.07 o 14 4 0 79.47 107.00 11.62 o 15 4 0 1175.32 1324.86 36.24 o 1 5 0 6865.79 6887.41 71.38 o 2 5 0 449.63 465.88 10.33 o 3 5 0 2625.48 2611.33 35.34 o 4 5 0 893.93 890.65 16.86 o 5 5 0 1.96 8.76 4.01 o 6 5 0 91.54 98.73 7.63 o 7 5 0 104.58 97.05 8.22 o 8 5 0 813.59 796.30 20.22 o 9 5 0 1915.07 1879.27 37.97 o 10 5 0 3.62 -0.86 7.93 o 11 5 0 4154.38 3949.23 72.15 o 12 5 0 316.24 317.68 17.17 o 13 5 0 525.70 563.81 22.67 o 14 5 0 341.42 288.02 16.52 o 0 6 0 337.21 318.01 14.01 o 1 6 0 601.33 611.91 18.18 o 2 6 0 498.98 491.93 12.82 o 3 6 0 182.41 177.19 12.84 o 4 6 0 2.25 5.21 5.50 o 5 6 0 6166.17 6097.48 83.43 o 6 6 0 49.98 45.95 8.56 o 7 6 0 3312.85 3303.21 61.42 o 8 6 0 279.68 278.78 16.14 o 9 6 0 511.26 541.11 21.03 o 10 6 0 29.77 26.86 8.22 o 11 6 0 95.05 88.71 14.50 o 12 6 0 45.29 59.86 10.04 o 1 7 0 1604.42 1615.37 37.38 o 2 7 0 1340.96 1352.53 31.90 o 3 7 0 261.07 269.96 13.63 o 4 7 0 629.80 616.71 21.19 o 5 7 0 112.49 124.53 10.69 o 6 7 0 256.10 256.22 14.60 o 7 7 0 96.17 100.97 10.83 o 8 7 0 305.21 280.00 15.95 o 9 7 0 736.23 740.68 25.77 o 2 8 0 1313.37 1404.27 60.06 o 3 8 0 207.64 215.88 22.66 o 4 8 0 6.34 15.19 20.57 o 5 8 0 305.40 351.96 19.66 o -17 0 1 529.14 534.06 38.76 o -15 0 1 2180.40 2206.07 55.33 o -13 0 1 4593.39 4513.80 211.94 o -11 0 1 857.86 834.38 20.29 o -9 0 1 291.09 307.35 10.47 o -7 0 1 1346.57 1555.37 27.10 o -5 0 1 31251.01 32069.86 423.85 o -3 0 1 352.24 381.46 7.85 o -1 0 1 1609.00 967.94 27.81 o 1 0 1 6411.39 5777.01 96.30 o 3 0 1 38.73 32.38 2.48 o 5 0 1 3029.22 2876.61 42.87 o 7 0 1 12272.25 12769.36 174.45 o 9 0 1 1211.16 1127.50 23.05 o 11 0 1 715.53 707.33 33.02 o 13 0 1 57.39 76.27 10.16 o 15 0 1 1208.14 1228.22 57.39 o 17 0 1 2185.33 2419.85 93.43 o -18 1 1 398.78 432.40 24.62 o -17 1 1 108.02 134.62 10.89 o -16 1 1 791.07 739.29 29.65 o -15 1 1 11.13 12.28 6.51 o -14 1 1 138.05 163.31 9.32 o -13 1 1 396.87 369.61 11.37 o -12 1 1 129.17 127.39 6.93 o -11 1 1 2192.89 2123.99 30.74 o -10 1 1 2681.98 2692.96 61.33 o -9 1 1 7765.35 7886.38 79.68 o -8 1 1 2422.98 2646.95 51.45 o -7 1 1 3368.31 3235.46 34.98 o -6 1 1 209.61 262.81 5.51 o -5 1 1 11.29 14.46 1.92 o -4 1 1 9590.08 10684.47 112.32 o -3 1 1 3434.95 3571.37 39.55 o -2 1 1 13231.34 14282.13 147.62 o -1 1 1 491.63 448.68 6.47 o 0 1 1 29.42 27.92 1.58 o 1 1 1 3919.21 4249.26 41.22 o 2 1 1 1250.72 1262.32 13.76 o 3 1 1 5330.02 5611.30 59.65 o 4 1 1 1139.96 1113.03 13.24 o 5 1 1 6504.64 6962.85 77.13 o 6 1 1 398.84 433.73 7.59 o 7 1 1 621.09 623.72 10.09 o 8 1 1 332.83 306.82 7.47 o 9 1 1 1963.18 2029.65 27.17 o 10 1 1 304.58 307.86 9.06 o 11 1 1 3788.59 3691.47 47.26 o 12 1 1 72.04 62.55 5.46 o 13 1 1 2452.30 2415.78 40.43 o 14 1 1 818.47 840.71 25.09 o 15 1 1 1090.79 1106.30 30.06 o 16 1 1 212.13 193.96 17.10 o 17 1 1 160.55 165.18 16.65 o 18 1 1 158.96 184.99 22.31 o -17 2 1 538.38 577.63 22.34 o -16 2 1 193.40 192.69 12.82 o -15 2 1 613.69 638.37 22.43 o -14 2 1 79.16 88.19 8.38 o -13 2 1 200.00 201.62 10.65 o -12 2 1 3102.60 3030.32 41.78 o -11 2 1 1669.34 1655.70 26.33 o -10 2 1 91.47 84.16 5.67 o -9 2 1 1944.37 1943.04 35.46 o -8 2 1 31.80 53.34 6.81 o -7 2 1 12798.36 13694.51 146.06 o -6 2 1 3027.67 3059.81 45.26 o -5 2 1 105.98 77.37 4.02 o -4 2 1 2467.90 2775.38 36.76 o -3 2 1 6362.11 6656.14 65.09 o -2 2 1 1009.68 969.88 11.95 o -1 2 1 6303.24 6698.91 64.99 o 0 2 1 2022.55 2144.38 22.83 o 1 2 1 1117.52 1118.32 20.75 o 2 2 1 418.35 373.30 6.32 o 3 2 1 950.21 845.95 10.91 o 4 2 1 4157.62 4207.34 42.80 o 5 2 1 4794.87 5119.43 51.76 o 6 2 1 141.53 125.64 3.75 o 7 2 1 6449.67 6682.86 67.45 o 8 2 1 200.55 190.89 8.94 o 9 2 1 4218.14 4044.30 96.64 o 10 2 1 1235.71 1110.67 26.48 o 11 2 1 1382.08 1385.84 27.02 o 12 2 1 536.97 534.61 16.14 o 13 2 1 4.06 -3.72 6.18 o 14 2 1 996.64 1006.33 24.14 o 15 2 1 97.04 105.00 8.74 o 16 2 1 710.11 682.43 24.04 o 17 2 1 174.00 208.03 13.40 o -16 3 1 581.26 585.00 22.25 o -15 3 1 21.45 9.80 8.94 o -14 3 1 880.42 899.91 23.20 o -13 3 1 950.11 889.56 22.54 o -12 3 1 17.70 19.84 6.56 o -11 3 1 3567.05 3412.82 52.40 o -10 3 1 164.47 173.03 9.76 o -9 3 1 25.99 29.61 5.84 o -8 3 1 120.20 152.47 7.29 o -7 3 1 1408.98 1373.03 21.31 o -6 3 1 5800.49 5947.40 67.96 o -5 3 1 515.48 475.62 10.09 o -4 3 1 4806.58 5164.37 52.84 o -3 3 1 1605.87 1733.01 20.55 o -2 3 1 3728.65 3895.76 52.33 o -1 3 1 3799.15 3987.60 41.38 o 0 3 1 1872.27 2032.76 23.22 o 1 3 1 909.90 834.26 12.95 o 2 3 1 59.00 67.99 3.30 o 3 3 1 4448.64 4692.48 48.23 o 4 3 1 4210.02 4486.19 46.51 o 5 3 1 3019.48 3128.14 34.19 o 6 3 1 2107.77 1940.91 26.58 o 7 3 1 63.55 61.88 4.24 o 8 3 1 2970.67 3049.25 47.54 o 9 3 1 1278.72 1292.55 25.35 o 10 3 1 2904.87 3010.78 47.02 o 11 3 1 449.63 446.16 15.09 o 12 3 1 1085.32 1058.98 31.83 o 13 3 1 21.15 21.22 7.19 o 14 3 1 316.55 306.95 13.60 o 15 3 1 1286.55 1273.55 30.62 o 16 3 1 1223.16 1290.74 30.41 o -15 4 1 251.02 258.30 15.86 o -14 4 1 524.26 477.75 20.63 o -13 4 1 381.60 383.29 18.46 o -12 4 1 651.78 631.97 22.27 o -11 4 1 0.39 4.11 6.00 o -10 4 1 1517.28 1537.64 30.10 o -9 4 1 680.08 641.79 17.39 o -8 4 1 3558.54 3406.37 48.53 o -7 4 1 833.03 824.58 16.12 o -6 4 1 389.55 352.68 9.72 o -5 4 1 1186.41 1158.55 30.79 o -4 4 1 315.00 349.83 7.59 o -3 4 1 55.46 57.79 3.48 o -2 4 1 2913.37 2901.25 32.83 o -1 4 1 259.71 255.12 6.57 o 0 4 1 7757.00 8142.99 81.34 o 1 4 1 111.44 120.78 4.74 o 2 4 1 7899.86 8257.61 82.58 o 3 4 1 551.39 580.56 10.33 o 4 4 1 994.90 935.78 14.07 o 5 4 1 204.65 201.75 12.48 o 6 4 1 221.35 213.41 12.71 o 7 4 1 7.76 6.50 5.27 o 8 4 1 216.60 212.54 10.25 o 9 4 1 6.68 8.18 6.42 o 10 4 1 548.70 539.37 16.73 o 11 4 1 237.02 234.89 11.76 o 12 4 1 3130.03 3070.35 60.08 o 13 4 1 10.43 9.07 6.67 o 14 4 1 1902.97 1890.14 38.15 o 15 4 1 405.73 419.32 16.67 o -14 5 1 1563.63 1618.38 41.39 o -13 5 1 118.18 115.55 13.02 o -12 5 1 1133.39 1077.01 31.30 o -11 5 1 0.55 3.71 7.79 o -10 5 1 69.68 87.27 12.19 o -9 5 1 65.01 72.00 15.21 o -8 5 1 692.91 687.10 22.00 o -7 5 1 3.62 8.21 5.48 o -6 5 1 420.53 434.76 13.71 o -5 5 1 7.64 10.11 4.16 o -4 5 1 4700.46 4788.32 58.16 o -3 5 1 292.04 284.57 9.01 o -2 5 1 5163.57 4929.52 127.78 o -1 5 1 615.43 611.15 11.60 o 0 5 1 189.91 204.91 6.63 o 1 5 1 33.00 36.25 3.87 o 2 5 1 254.68 262.83 7.50 o 3 5 1 31.23 23.30 4.43 o 4 5 1 763.49 720.66 14.77 o 5 5 1 2002.79 1970.14 33.49 o 6 5 1 2366.82 2415.86 39.67 o 7 5 1 32.08 24.28 6.44 o 8 5 1 1065.27 1034.62 27.90 o 9 5 1 304.12 283.60 12.79 o 10 5 1 1665.91 1639.81 33.01 o 11 5 1 0.20 -5.86 5.86 o 12 5 1 41.69 36.04 9.91 o 13 5 1 6.84 16.48 13.68 o 14 5 1 17.22 34.76 7.81 o -12 6 1 462.25 549.83 22.44 o -11 6 1 216.53 212.72 14.49 o -10 6 1 1827.79 1874.38 43.83 o -9 6 1 121.75 128.85 11.83 o -8 6 1 1169.70 1150.95 31.25 o -7 6 1 84.52 88.47 15.71 o -6 6 1 2424.87 2357.72 47.56 o -5 6 1 223.26 210.75 12.41 o -4 6 1 171.99 174.21 9.39 o -3 6 1 182.16 186.40 10.75 o -2 6 1 318.90 316.21 10.28 o -1 6 1 119.96 131.90 7.10 o 0 6 1 2112.88 2085.51 27.96 o 1 6 1 1255.57 1211.33 19.19 o 2 6 1 1314.81 1277.12 25.19 o 3 6 1 262.23 253.46 10.75 o 4 6 1 708.72 720.33 18.53 o 5 6 1 64.05 63.78 7.75 o 6 6 1 927.77 895.82 21.79 o 7 6 1 286.02 277.01 12.43 o 8 6 1 1027.02 972.61 28.20 o 9 6 1 4.44 7.26 8.02 o 10 6 1 698.33 665.33 23.99 o 11 6 1 35.85 38.36 10.60 o 12 6 1 810.70 859.70 28.15 o -9 7 1 553.53 575.92 27.17 o -8 7 1 568.70 598.32 22.90 o -7 7 1 381.97 411.80 18.55 o -6 7 1 1404.23 1390.22 35.19 o -5 7 1 294.36 276.28 15.06 o -4 7 1 1069.62 1100.78 29.42 o -3 7 1 0.24 5.14 6.53 o -2 7 1 300.42 329.49 14.81 o -1 7 1 420.44 425.40 15.95 o 0 7 1 1306.42 1300.68 54.79 o 1 7 1 13.52 17.49 8.76 o 2 7 1 111.35 110.58 8.19 o 3 7 1 574.53 578.67 22.27 o 4 7 1 1462.73 1419.52 34.22 o 5 7 1 14.26 14.17 7.20 o 6 7 1 799.60 785.14 25.33 o 7 7 1 47.64 38.42 8.74 o 8 7 1 754.85 808.89 26.52 o 9 7 1 329.69 346.28 17.26 o -5 8 1 642.70 669.73 39.92 o -4 8 1 80.71 104.59 14.43 o -3 8 1 794.51 890.51 26.19 o 1 8 1 48.47 60.16 12.42 o 2 8 1 422.97 435.28 31.70 o 3 8 1 53.55 79.45 15.85 o 4 8 1 544.84 565.42 25.84 o -18 0 2 1646.29 1683.85 73.14 o -16 0 2 1099.75 1100.60 44.52 o -14 0 2 179.00 196.14 14.18 o -12 0 2 680.85 658.42 24.03 o -10 0 2 6466.86 6426.29 94.57 o -8 0 2 10633.85 11108.14 186.02 o -6 0 2 3699.37 3720.70 66.56 o -4 0 2 3745.93 4054.62 57.39 o -2 0 2 14097.42 15684.90 255.55 o 0 0 2 3882.05 4268.17 57.85 o 2 0 2 32001.62 31117.52 417.31 o 4 0 2 25317.22 26958.08 356.83 o 6 0 2 3418.45 3519.88 52.67 o 8 0 2 264.70 248.38 10.43 o 10 0 2 15.33 12.72 4.33 o 12 0 2 1917.80 1899.40 45.84 o 14 0 2 5420.85 5016.16 150.26 o 16 0 2 2483.28 2499.95 93.33 o 18 0 2 128.94 102.16 20.90 o -17 1 2 11.69 25.75 7.75 o -16 1 2 233.81 257.38 20.83 o -15 1 2 417.81 412.38 21.29 o -14 1 2 3513.27 3499.91 54.16 o -13 1 2 239.14 235.70 9.34 o -12 1 2 2834.54 2776.04 61.51 o -11 1 2 374.02 375.66 14.04 o -10 1 2 913.67 844.14 27.21 o -9 1 2 54.38 64.08 4.71 o -8 1 2 521.66 546.05 9.59 o -7 1 2 2245.59 2287.98 26.20 o -6 1 2 163.83 143.42 4.54 o -5 1 2 63.38 82.13 3.38 o -4 1 2 22173.47 23261.16 218.31 o -3 1 2 12.75 9.29 1.40 o -2 1 2 31039.68 32719.46 309.70 o -1 1 2 6422.14 7047.97 88.99 o 0 1 2 9879.03 10558.58 99.69 o 1 1 2 3226.99 3620.48 35.56 o 2 1 2 3416.99 3753.71 40.98 o 3 1 2 6654.21 6960.97 74.27 o 4 1 2 173.98 143.36 5.29 o 5 1 2 862.62 855.49 11.44 o 6 1 2 321.64 238.14 6.11 o 7 1 2 728.60 750.42 11.48 o 8 1 2 10685.61 11161.54 109.47 o 9 1 2 2.42 4.53 2.56 o 10 1 2 5756.74 5793.80 61.38 o 11 1 2 465.36 471.63 11.69 o 12 1 2 1400.08 1400.71 30.79 o 13 1 2 74.79 67.04 7.44 o 14 1 2 144.44 162.53 11.53 o 15 1 2 5.22 16.74 6.40 o 16 1 2 253.32 261.11 27.66 o 17 1 2 603.49 556.79 28.78 o -17 2 2 0.94 14.31 15.85 o -16 2 2 1861.10 1815.57 42.24 o -15 2 2 301.28 324.38 26.30 o -14 2 2 40.91 34.03 7.00 o -13 2 2 875.23 834.02 18.08 o -12 2 2 287.86 291.89 10.17 o -11 2 2 2330.41 2133.53 60.00 o -10 2 2 333.19 311.60 9.53 o -9 2 2 190.31 164.75 6.73 o -8 2 2 6578.51 6731.64 85.43 o -7 2 2 1112.29 1185.17 18.51 o -6 2 2 6572.27 6812.53 75.69 o -5 2 2 5436.02 5609.61 62.75 o -4 2 2 11626.14 12538.49 196.35 o -3 2 2 26.97 27.61 2.48 o -2 2 2 480.85 479.50 7.19 o -1 2 2 9713.05 10412.28 104.82 o 0 2 2 161.71 156.29 3.67 o 1 2 2 2078.10 2255.80 24.07 o 2 2 2 7882.37 8385.17 80.94 o 3 2 2 953.13 951.36 12.03 o 4 2 2 8951.39 9073.48 87.99 o 5 2 2 6295.55 6780.55 67.23 o 6 2 2 116.26 85.32 4.37 o 7 2 2 3827.23 3967.81 42.40 o 8 2 2 388.73 428.13 9.84 o 9 2 2 303.14 291.83 8.43 o 10 2 2 959.48 969.53 21.01 o 11 2 2 336.37 320.26 12.30 o 12 2 2 1475.67 1380.42 28.89 o 13 2 2 410.96 441.33 15.43 o 14 2 2 1343.60 1389.76 29.71 o 15 2 2 3.52 5.35 5.67 o 16 2 2 869.66 950.53 29.13 o 17 2 2 104.76 145.75 15.34 o -16 3 2 719.56 692.96 24.15 o -15 3 2 411.79 374.23 18.08 o -14 3 2 390.45 415.42 18.74 o -13 3 2 1533.10 1395.42 29.15 o -12 3 2 1214.34 1234.08 26.41 o -11 3 2 2078.18 2010.68 30.99 o -10 3 2 336.37 349.84 10.68 o -9 3 2 4130.47 4134.06 51.75 o -8 3 2 1317.84 1360.27 21.88 o -7 3 2 5863.99 5988.44 69.17 o -6 3 2 1343.66 1340.88 20.49 o -5 3 2 1956.56 1855.87 25.37 o -4 3 2 740.47 680.83 10.33 o -3 3 2 406.79 435.57 7.74 o -2 3 2 1661.24 1715.24 20.36 o -1 3 2 44.48 41.90 3.04 o 0 3 2 12110.31 13206.08 126.60 o 1 3 2 1920.33 1759.12 26.07 o 2 3 2 146.59 121.10 4.03 o 3 3 2 1883.13 1777.66 21.12 o 4 3 2 1.79 5.08 2.30 o 5 3 2 3349.77 3523.04 38.55 o 6 3 2 4182.56 4265.63 45.37 o 7 3 2 633.95 619.28 15.13 o 8 3 2 1413.71 1412.42 26.14 o 9 3 2 243.60 250.69 10.72 o 10 3 2 453.56 475.24 15.65 o 11 3 2 1525.69 1503.55 29.69 o 12 3 2 897.60 882.33 22.45 o 13 3 2 1137.20 1177.09 33.68 o 14 3 2 32.20 35.32 7.35 o 15 3 2 422.73 439.76 16.68 o 16 3 2 287.37 301.07 14.19 o -15 4 2 319.54 359.52 18.02 o -14 4 2 15.81 18.08 8.16 o -13 4 2 4598.23 4514.55 80.14 o -12 4 2 28.20 21.85 8.40 o -11 4 2 3329.29 3369.27 62.08 o -10 4 2 961.61 944.65 26.38 o -9 4 2 727.10 704.13 19.67 o -8 4 2 10.52 20.93 4.74 o -7 4 2 226.33 218.97 8.14 o -6 4 2 224.23 237.83 8.10 o -5 4 2 820.50 775.50 25.80 o -4 4 2 835.95 785.42 14.52 o -3 4 2 7339.96 7367.95 74.57 o -2 4 2 313.41 290.31 7.77 o -1 4 2 3806.50 3662.54 39.96 o 0 4 2 1348.31 1417.16 18.75 o 1 4 2 1286.03 1334.12 17.94 o 2 4 2 741.81 659.72 11.19 o 3 4 2 191.92 210.83 6.80 o 4 4 2 1775.36 1877.69 23.42 o 5 4 2 683.77 633.91 15.23 o 6 4 2 870.58 836.53 22.81 o 7 4 2 3591.76 3343.68 66.53 o 8 4 2 1791.32 1718.02 31.17 o 9 4 2 4615.51 4522.87 95.86 o 10 4 2 915.78 842.55 21.27 o 11 4 2 643.94 660.35 19.33 o 12 4 2 633.94 672.16 20.01 o 13 4 2 13.64 14.39 6.64 o 14 4 2 67.25 91.07 9.36 o 15 4 2 149.69 152.41 10.96 o -14 5 2 1.89 6.02 7.35 o -13 5 2 48.80 50.50 9.79 o -12 5 2 56.27 65.43 10.31 o -11 5 2 32.60 42.46 9.22 o -10 5 2 279.32 259.60 16.18 o -9 5 2 2907.22 2909.37 69.03 o -8 5 2 1.15 11.35 7.27 o -7 5 2 5792.05 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658.46 16.97 o 3 6 2 376.15 371.97 15.61 o 4 6 2 89.21 88.85 8.06 o 5 6 2 421.82 391.00 13.80 o 6 6 2 68.72 70.53 7.89 o 7 6 2 1779.65 1779.30 34.23 o 8 6 2 42.52 41.95 7.68 o 9 6 2 4994.19 4942.10 73.96 o 10 6 2 240.54 225.03 24.38 o 11 6 2 1055.10 975.76 44.67 o 12 6 2 87.80 92.34 10.14 o -9 7 2 1139.82 1100.96 32.04 o -8 7 2 20.25 16.08 7.80 o -7 7 2 480.31 510.22 20.89 o -6 7 2 132.60 133.90 16.85 o -5 7 2 1451.20 1521.83 36.70 o -4 7 2 541.94 550.51 20.32 o -3 7 2 604.35 606.69 20.73 o -2 7 2 1593.21 1658.08 31.70 o -1 7 2 27.98 39.73 7.27 o 0 7 2 24.77 26.57 14.21 o 1 7 2 1356.44 1352.36 39.51 o 2 7 2 346.28 387.93 16.14 o 3 7 2 3031.48 3090.25 57.74 o 4 7 2 58.20 77.41 8.59 o 5 7 2 1080.24 1077.16 42.30 o 6 7 2 1128.87 1089.04 30.20 o 7 7 2 369.43 407.81 18.35 o 8 7 2 284.18 290.72 15.92 o 9 7 2 81.65 93.17 10.21 o -4 8 2 14.68 17.80 6.26 o -3 8 2 1172.00 1210.81 52.39 o -2 8 2 113.72 156.01 19.33 o -1 8 2 417.35 438.82 30.94 o 0 8 2 628.55 648.16 44.27 o 1 8 2 262.18 274.93 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