#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226559.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226559_Fobs loop_ _publ_author_name 'Lin, Jin Rui' _publ_section_title ; 4-(Cyanomethyl)anilinium 4-methylbenzenesulfonate monohydrate ; _journal_coeditor_code JJ2033 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1557 _journal_volume 66 _journal_year 2010 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.9310 _cell_length_b 22.9310 _cell_length_c 5.9460 _exptl_crystal_F_000 1359.78 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file jj2033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 291.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'y, -x, -z' '-x, -y, z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-x+1/2, -y+1/2, z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 3 0 4833.51 4834.72 27.76 o -2 4 0 10997.01 8635.76 48.00 o 0 4 0 3417.07 2752.84 30.63 o 2 4 0 589.46 375.32 13.26 o 4 4 0 14479.14 15932.23 100.76 o -3 5 0 51112.45 51737.58 168.06 o -1 5 0 14137.38 14473.60 55.11 o 1 5 0 2317.92 1980.99 19.53 o 3 5 0 1567.93 2341.02 20.41 o 5 5 0 2197.35 2480.28 17.10 o -4 6 0 13391.46 14969.08 86.58 o -2 6 0 58757.27 53952.33 414.51 o 0 6 0 11784.68 13533.04 78.37 o 2 6 0 2312.22 2088.11 19.13 o 4 6 0 153.34 165.36 13.24 o 6 6 0 661.37 651.19 16.00 o -5 7 0 221.94 164.43 11.22 o -3 7 0 575.25 543.30 20.96 o -1 7 0 57471.16 60779.36 238.11 o 1 7 0 425.98 642.27 19.62 o 3 7 0 7057.59 4465.31 39.56 o 5 7 0 30240.44 25937.01 112.60 o 7 7 0 2087.40 1920.88 24.73 o -6 8 0 2185.23 2627.67 38.59 o -4 8 0 3779.27 3741.80 25.45 o -2 8 0 3190.69 2614.37 26.14 o 0 8 0 6835.13 7081.62 62.37 o 2 8 0 1.97 19.49 7.54 o 4 8 0 2676.68 2383.06 35.09 o 6 8 0 3951.89 3859.39 56.45 o 8 8 0 1746.02 1587.18 23.98 o -7 9 0 14167.54 14557.46 102.85 o -5 9 0 7.86 39.63 12.07 o -3 9 0 40.70 79.16 14.89 o -1 9 0 4860.87 6006.51 49.71 o 1 9 0 485.73 734.33 19.13 o 3 9 0 5989.36 4705.71 76.41 o 5 9 0 6199.30 4283.29 56.60 o 7 9 0 3264.11 3135.76 49.71 o 9 9 0 3841.64 3666.62 96.19 o -8 10 0 30.43 31.52 17.68 o -6 10 0 5246.95 6205.36 93.67 o -4 10 0 114.59 131.20 13.91 o -2 10 0 3669.70 3595.97 40.60 o 0 10 0 247.78 234.72 21.09 o 2 10 0 8.11 3.71 11.58 o 4 10 0 1575.47 1469.19 50.35 o 6 10 0 1120.90 1292.65 25.52 o 8 10 0 574.32 440.66 18.30 o 10 10 0 2089.92 1992.75 63.15 o -9 11 0 112.75 152.03 35.61 o -7 11 0 6153.95 6510.01 140.43 o -5 11 0 1.78 31.71 10.38 o -3 11 0 1197.40 1557.64 24.71 o -1 11 0 13380.09 14037.37 124.04 o 1 11 0 6605.93 5752.57 61.29 o 3 11 0 75.02 46.13 13.48 o 5 11 0 667.74 786.94 33.73 o 7 11 0 1006.97 894.93 24.60 o 9 11 0 2869.11 2523.11 63.56 o 11 11 0 124.20 83.33 16.26 o -10 12 0 1296.54 1713.10 63.08 o -8 12 0 5550.07 5132.59 106.61 o -6 12 0 100.71 82.06 18.43 o -4 12 0 15531.25 16628.06 95.54 o -2 12 0 33.16 48.31 9.81 o 0 12 0 9845.57 9737.54 90.22 o 2 12 0 208.60 161.57 20.17 o 4 12 0 1994.38 1792.19 49.65 o 6 12 0 1234.28 1360.94 30.65 o 8 12 0 7629.46 7721.88 132.46 o 10 12 0 41.75 13.42 14.61 o 12 12 0 419.89 402.64 37.00 o -11 13 0 3856.51 4411.13 89.02 o -9 13 0 857.02 892.63 62.85 o -7 13 0 320.59 345.64 32.11 o -5 13 0 3053.67 2946.30 53.55 o -3 13 0 1718.35 1366.32 24.82 o -1 13 0 86.57 79.20 13.19 o 1 13 0 148.91 229.57 26.49 o 3 13 0 474.36 596.77 56.62 o 5 13 0 896.18 943.43 38.19 o 7 13 0 3157.65 3032.39 57.83 o 9 13 0 954.90 1133.43 32.16 o 11 13 0 150.86 76.55 26.02 o 13 13 0 488.62 518.17 55.01 o -12 14 0 281.40 248.09 32.85 o -10 14 0 0.59 62.69 24.29 o -8 14 0 547.74 521.03 53.42 o -6 14 0 656.26 783.46 36.59 o -4 14 0 5408.34 5803.09 101.60 o -2 14 0 729.63 730.53 26.58 o 0 14 0 126.67 176.24 23.05 o 2 14 0 61.59 64.98 23.02 o 4 14 0 2257.94 2412.50 57.95 o 6 14 0 840.61 713.42 40.61 o 8 14 0 1513.34 1822.60 34.57 o 10 14 0 1.73 11.19 18.93 o 12 14 0 227.55 258.13 36.52 o 14 14 0 32.86 79.51 28.39 o -13 15 0 58.97 99.71 26.72 o -11 15 0 1005.45 924.37 48.96 o -9 15 0 33.03 28.27 20.82 o -7 15 0 1131.30 1118.58 48.84 o -5 15 0 0.02 10.04 8.97 o -3 15 0 365.86 468.64 25.94 o -1 15 0 699.45 757.20 42.24 o 1 15 0 4117.33 4292.97 86.01 o 3 15 0 76.81 66.51 28.57 o 5 15 0 3284.42 3159.06 75.95 o 7 15 0 34.88 38.81 17.07 o 9 15 0 2867.59 2718.35 73.78 o 11 15 0 581.19 588.19 47.62 o 13 15 0 1615.54 1740.84 94.60 o 15 15 0 45.30 53.42 25.69 o -14 16 0 418.99 374.78 51.63 o -12 16 0 1012.82 1092.99 64.99 o -10 16 0 95.05 84.62 24.89 o -8 16 0 510.93 449.60 47.39 o -6 16 0 2694.00 2708.25 59.43 o -4 16 0 1222.95 1018.00 46.19 o -2 16 0 1907.04 1540.72 41.46 o 0 16 0 3456.74 3326.21 74.89 o 2 16 0 399.49 361.69 30.45 o 4 16 0 3994.49 4243.59 59.73 o 6 16 0 1422.29 1321.78 36.43 o 8 16 0 4280.96 5257.95 95.19 o 10 16 0 737.06 864.42 52.44 o 12 16 0 2899.33 2744.59 75.43 o 14 16 0 616.13 583.00 70.70 o 16 16 0 1897.28 1741.83 70.89 o -15 17 0 595.13 778.64 80.39 o -13 17 0 7.81 8.39 18.14 o -11 17 0 2699.37 2873.10 69.24 o -9 17 0 1456.03 1623.85 70.80 o -7 17 0 1006.52 1138.93 57.49 o -5 17 0 46.53 36.27 15.80 o -3 17 0 3132.23 3092.42 63.65 o -1 17 0 1173.00 1067.86 37.93 o 1 17 0 3490.18 3633.85 64.35 o 3 17 0 28.30 34.66 25.86 o 5 17 0 3569.52 3535.92 63.53 o 7 17 0 2.91 38.05 17.01 o 9 17 0 183.65 196.94 23.73 o 11 17 0 246.05 174.40 27.68 o 13 17 0 1177.36 1228.71 64.53 o 15 17 0 150.34 197.75 33.31 o 17 17 0 275.74 255.18 54.27 o -16 18 0 9.02 58.61 41.54 o -14 18 0 0.02 26.18 39.49 o -12 18 0 1321.33 1800.42 172.20 o -10 18 0 377.02 240.52 31.84 o -8 18 0 9.85 48.28 23.51 o -6 18 0 277.89 236.04 28.18 o -4 18 0 685.58 708.73 54.30 o -2 18 0 939.69 801.41 44.97 o 0 18 0 1883.06 1972.90 70.15 o 2 18 0 1151.78 1119.95 48.56 o 4 18 0 488.11 480.51 59.42 o 6 18 0 0.13 60.48 18.11 o 8 18 0 21.26 81.21 19.64 o 10 18 0 202.40 326.36 37.22 o 12 18 0 12.80 40.30 24.95 o 14 18 0 31.49 59.03 22.18 o 16 18 0 75.68 100.40 28.52 o 18 18 0 12.08 0.00 37.23 o -17 19 0 17.50 120.52 33.58 o -15 19 0 46.66 98.54 29.11 o -13 19 0 426.54 413.97 44.27 o -11 19 0 146.58 158.29 38.58 o -9 19 0 34.28 126.40 38.95 o -7 19 0 209.13 175.38 21.07 o -5 19 0 437.64 383.45 44.57 o -3 19 0 990.19 866.59 43.22 o -1 19 0 2.35 40.42 20.75 o 1 19 0 1041.48 951.31 49.35 o 3 19 0 276.98 295.21 31.72 o 5 19 0 8604.71 9147.07 164.87 o 7 19 0 140.27 95.35 23.27 o 9 19 0 58.81 52.33 18.67 o 11 19 0 1409.62 1567.61 67.20 o 13 19 0 1268.52 1387.66 156.90 o 15 19 0 0.00 57.05 35.22 o 17 19 0 65.57 99.20 29.58 o 19 19 0 27.96 64.66 31.89 o -18 20 0 7.57 62.84 31.04 o -16 20 0 153.66 134.26 36.27 o -14 20 0 26.40 64.81 37.03 o -12 20 0 197.17 132.76 28.22 o -10 20 0 1267.31 1111.97 78.86 o -8 20 0 195.14 300.39 37.49 o -6 20 0 495.72 485.32 53.85 o -4 20 0 642.85 553.56 39.53 o -2 20 0 1057.66 830.97 47.63 o 0 20 0 69.67 104.12 21.94 o 2 20 0 2220.25 2152.08 50.79 o 4 20 0 73.47 65.37 22.55 o 6 20 0 1419.99 1488.76 45.16 o 8 20 0 931.50 857.64 48.11 o 10 20 0 286.39 338.79 43.23 o 12 20 0 727.58 640.41 68.27 o 14 20 0 53.09 90.88 30.19 o 16 20 0 53.75 89.66 31.56 o 18 20 0 555.94 629.99 77.93 o 20 20 0 105.51 72.63 72.35 o -17 21 0 30.86 69.35 23.27 o -15 21 0 420.09 316.69 41.21 o -13 21 0 20.94 93.49 30.47 o -11 21 0 436.37 499.67 62.36 o -9 21 0 19.10 28.25 24.91 o -7 21 0 446.19 442.21 64.26 o -5 21 0 85.55 90.50 28.85 o -3 21 0 2540.25 2213.87 95.34 o -1 21 0 86.77 98.17 16.60 o 1 21 0 767.75 849.38 35.28 o 3 21 0 387.95 366.91 32.16 o 5 21 0 19.27 50.68 21.71 o 7 21 0 85.71 58.91 24.54 o 9 21 0 1564.16 1678.18 126.45 o 11 21 0 339.10 289.67 42.42 o 13 21 0 21.84 52.33 19.93 o 15 21 0 128.27 143.10 26.37 o 17 21 0 274.79 210.63 45.94 o -16 22 0 85.70 75.97 29.07 o -14 22 0 143.15 152.45 62.69 o -12 22 0 5.48 136.48 61.17 o -10 22 0 115.95 101.81 43.75 o -8 22 0 160.67 151.34 44.82 o -6 22 0 204.81 215.73 43.10 o -4 22 0 30.95 90.08 26.80 o -2 22 0 393.83 382.94 49.82 o 0 22 0 136.77 144.19 42.42 o 2 22 0 225.12 192.18 28.85 o 4 22 0 119.80 119.35 23.08 o 6 22 0 48.38 76.17 30.96 o 8 22 0 33.59 62.34 16.62 o 10 22 0 338.92 353.65 46.43 o 12 22 0 30.13 71.71 26.93 o 14 22 0 0.08 29.49 28.34 o 16 22 0 123.58 123.08 30.09 o -15 23 0 1.01 52.39 67.30 o -13 23 0 7.71 39.51 24.82 o -11 23 0 94.22 30.88 29.29 o -9 23 0 0.02 89.65 36.90 o -7 23 0 79.42 137.12 27.63 o -5 23 0 0.90 8.51 38.52 o -3 23 0 199.41 224.20 42.42 o -1 23 0 16.65 26.69 31.77 o 1 23 0 3.90 37.44 22.70 o 3 23 0 49.16 89.57 22.43 o 5 23 0 2.96 58.07 22.01 o 7 23 0 12.18 58.83 28.11 o 9 23 0 130.44 150.94 29.32 o 11 23 0 380.15 341.19 42.88 o 13 23 0 166.87 136.20 43.45 o 15 23 0 147.81 109.98 33.23 o -14 24 0 285.12 236.84 41.16 o -12 24 0 289.56 256.21 75.41 o -10 24 0 42.52 126.67 42.65 o -8 24 0 210.16 109.51 63.66 o -6 24 0 560.97 707.58 98.87 o -4 24 0 1290.75 1250.54 181.30 o -2 24 0 65.13 105.65 32.81 o 0 24 0 194.70 186.91 36.26 o 2 24 0 491.18 458.80 48.53 o 4 24 0 336.53 304.52 39.80 o 6 24 0 200.53 204.49 47.87 o 8 24 0 52.56 39.64 24.02 o 10 24 0 27.71 41.61 24.34 o 12 24 0 98.97 101.71 29.81 o 14 24 0 61.49 51.44 26.53 o -13 25 0 42.58 19.01 43.38 o -11 25 0 354.60 572.53 176.36 o -9 25 0 9.82 0.00 35.36 o -7 25 0 289.49 373.15 58.20 o -5 25 0 82.85 123.06 27.15 o -3 25 0 108.75 138.27 31.14 o -1 25 0 297.89 247.39 41.22 o 1 25 0 711.25 751.17 72.55 o 3 25 0 5.24 51.06 22.37 o 5 25 0 259.94 251.96 75.69 o 7 25 0 72.03 127.82 33.51 o 9 25 0 33.39 63.03 34.72 o 11 25 0 15.90 43.86 22.36 o 13 25 0 33.11 76.29 17.50 o -10 26 0 28.70 44.24 40.98 o -8 26 0 8.60 20.45 48.39 o -6 26 0 12.68 36.39 47.62 o -4 26 0 30.80 98.37 49.85 o -2 26 0 119.24 184.17 37.00 o 0 26 0 9.05 65.52 21.63 o 2 26 0 67.65 108.66 37.18 o 4 26 0 20.24 68.70 41.25 o 6 26 0 2.06 51.55 30.59 o 8 26 0 147.90 147.01 46.14 o 10 26 0 61.46 65.03 24.93 o -7 27 0 144.21 150.11 47.00 o -5 27 0 35.31 10.21 46.44 o -3 27 0 267.62 343.41 51.18 o -1 27 0 62.64 120.22 43.00 o 1 27 0 74.34 50.45 32.05 o 3 27 0 0.00 35.71 33.44 o 5 27 0 44.27 22.51 35.13 o 7 27 0 64.65 70.48 48.43 o -4 28 0 357.21 356.63 58.34 o -2 28 0 268.10 326.58 61.13 o 0 28 0 140.53 162.25 47.59 o 2 28 0 94.66 81.92 31.00 o 4 28 0 123.87 138.13 66.13 o 1 0 1 2019.16 1732.00 19.22 o 3 0 1 50632.25 49523.83 158.01 o 5 0 1 11083.82 11311.99 60.55 o 7 0 1 525.24 448.44 18.03 o 9 0 1 996.40 1510.74 22.80 o 11 0 1 835.16 822.19 28.04 o 13 0 1 503.44 551.62 30.06 o 15 0 1 325.57 355.32 24.40 o 17 0 1 1638.64 1616.37 70.17 o 19 0 1 718.38 834.89 48.77 o 21 0 1 179.81 193.27 25.80 o 23 0 1 357.17 343.29 72.60 o 25 0 1 93.53 155.68 33.29 o 27 0 1 76.63 88.33 33.12 o -28 1 1 316.15 304.42 63.82 o -26 1 1 55.99 17.69 45.49 o -24 1 1 219.81 186.21 35.23 o -22 1 1 340.52 313.06 53.62 o -20 1 1 321.97 332.33 44.10 o -18 1 1 477.93 492.88 52.40 o -16 1 1 1115.94 899.82 34.38 o -14 1 1 1246.76 1331.81 44.41 o -12 1 1 1518.31 1616.03 35.39 o -10 1 1 455.12 392.24 15.00 o -8 1 1 1366.30 1330.57 23.61 o -6 1 1 19088.75 20163.15 120.81 o -4 1 1 206.19 150.59 13.12 o -2 1 1 1311.18 1528.71 13.25 o 0 1 1 2096.70 1798.55 15.31 o 2 1 1 19708.70 19795.92 93.15 o 4 1 1 15119.67 13311.03 73.15 o 6 1 1 85044.52 81029.49 183.26 o 8 1 1 11344.07 11038.92 70.01 o 10 1 1 4091.27 4174.46 53.10 o 12 1 1 8969.71 9745.93 98.19 o 14 1 1 1370.78 1369.31 50.42 o 16 1 1 869.47 886.43 48.53 o 18 1 1 2241.98 2477.10 49.80 o 20 1 1 278.88 276.86 32.03 o 22 1 1 354.50 388.87 30.01 o 24 1 1 52.17 70.38 22.37 o 26 1 1 170.33 192.03 34.58 o 28 1 1 13.20 45.86 28.26 o -27 2 1 20.74 73.15 33.72 o -25 2 1 215.82 203.07 30.12 o -23 2 1 21.03 53.93 17.73 o -21 2 1 757.61 799.35 59.61 o -19 2 1 2044.21 2067.64 64.96 o -17 2 1 2276.47 2402.76 65.88 o -15 2 1 1858.81 1938.37 41.16 o -13 2 1 3670.63 3460.15 57.75 o -11 2 1 768.78 784.77 28.08 o -9 2 1 7706.05 7513.32 72.34 o -7 2 1 395.67 345.14 16.34 o -5 2 1 5742.05 5471.46 40.00 o -3 2 1 12668.67 13104.16 83.83 o -1 2 1 19884.30 19760.42 59.77 o 1 2 1 1346.04 1536.07 18.58 o 3 2 1 13917.50 13292.82 89.43 o 5 2 1 3469.64 2832.59 26.30 o 7 2 1 22391.91 21874.26 104.22 o 9 2 1 8910.42 8640.16 106.32 o 11 2 1 2007.13 2002.58 43.11 o 13 2 1 7230.83 7062.78 89.97 o 15 2 1 2137.00 2270.19 76.83 o 17 2 1 1543.87 1528.24 48.39 o 19 2 1 482.91 423.66 41.86 o 21 2 1 31.55 42.24 21.11 o 23 2 1 314.95 234.51 43.54 o 25 2 1 254.93 215.75 40.08 o 27 2 1 145.90 155.21 32.25 o -26 3 1 335.95 288.34 45.32 o -24 3 1 53.68 33.28 19.99 o -22 3 1 783.72 605.19 44.48 o -20 3 1 523.55 538.22 37.36 o -18 3 1 447.49 389.51 26.28 o -16 3 1 184.58 137.82 22.15 o -14 3 1 2405.97 2688.07 64.74 o -12 3 1 1807.04 1952.01 31.75 o -10 3 1 1579.66 1528.87 46.27 o -8 3 1 1719.89 1770.99 24.21 o -6 3 1 2786.54 2578.67 30.38 o -4 3 1 2277.66 2520.22 27.86 o -2 3 1 14154.36 13341.85 50.89 o 0 3 1 50714.21 49414.71 256.31 o 2 3 1 12626.86 13011.12 50.20 o 4 3 1 8396.19 8778.21 59.13 o 6 3 1 8349.75 8111.63 36.80 o 8 3 1 1701.07 1904.38 32.59 o 10 3 1 2289.94 2401.55 53.96 o 12 3 1 6333.98 6706.01 77.36 o 14 3 1 67.38 77.23 32.95 o 16 3 1 459.82 453.62 30.74 o 18 3 1 1799.25 2011.00 44.78 o 20 3 1 124.47 94.28 25.15 o 22 3 1 81.47 118.93 31.02 o 24 3 1 279.73 213.89 49.53 o 26 3 1 18.77 47.63 25.87 o -27 4 1 77.58 20.94 29.26 o -25 4 1 219.09 241.16 38.55 o -23 4 1 165.22 148.80 21.64 o -21 4 1 221.96 151.86 21.06 o -19 4 1 380.96 307.68 31.36 o -17 4 1 82.33 68.09 15.54 o -15 4 1 1487.92 1300.28 30.58 o -13 4 1 1038.33 934.62 30.70 o -11 4 1 988.12 1011.54 45.86 o -9 4 1 3921.07 3643.17 39.04 o -7 4 1 911.80 893.66 20.93 o -5 4 1 6886.56 6742.73 29.57 o -3 4 1 8439.61 8670.76 53.66 o -1 4 1 15089.92 13066.11 124.59 o 1 4 1 212.08 129.17 17.54 o 3 4 1 2262.90 2525.39 23.39 o 5 4 1 1780.28 1799.70 15.44 o 7 4 1 466.31 463.06 24.32 o 9 4 1 10339.19 10960.83 105.21 o 11 4 1 1611.28 1458.59 34.82 o 13 4 1 232.72 296.53 32.69 o 15 4 1 1334.07 1248.04 55.96 o 17 4 1 223.78 263.58 37.01 o 19 4 1 296.84 285.52 35.29 o 21 4 1 533.75 574.07 81.63 o 23 4 1 110.88 132.27 27.56 o 25 4 1 91.41 119.48 35.49 o 27 4 1 192.71 187.03 36.50 o -26 5 1 6.03 55.05 22.12 o -24 5 1 172.83 211.70 36.59 o -22 5 1 136.83 87.13 26.20 o -20 5 1 946.45 994.71 40.35 o -18 5 1 166.36 211.75 36.42 o -16 5 1 1374.56 1455.31 44.63 o -14 5 1 1174.86 1087.03 49.78 o -12 5 1 703.66 664.34 26.49 o -10 5 1 3508.49 3062.64 43.81 o -8 5 1 3563.68 3326.33 40.46 o -6 5 1 2452.49 3026.40 30.05 o -4 5 1 1861.74 1879.95 21.97 o -2 5 1 3385.72 2852.56 33.90 o 0 5 1 11079.04 11452.22 65.47 o 2 5 1 5769.41 5588.83 30.75 o 4 5 1 6828.45 6680.84 40.46 o 6 5 1 342.47 254.50 19.19 o 8 5 1 1524.01 1143.76 24.44 o 10 5 1 4339.20 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