#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226580.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226580_Fobs loop_ _publ_author_name 'Stibrany, Robert T.' 'Potenza, Joseph A.' _publ_section_title ; Dibromido[1,1'-dibutyl-2,2'-(pentane-1,1-diyl)di-1H-benzimidazole]copper(II) ; _journal_coeditor_code LH5058 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m767 _journal_page_last m768 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.636 _cell_angle_gamma 90.000 _cell_length_a 13.5209 _cell_length_b 14.6045 _cell_length_c 13.8808 _exptl_crystal_F_000 1300.00 _reflns_d_resolution_high 0.8074 _[local]_cod_data_source_file lh5058Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yelred2m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 291.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1375.15 1361.40 78.87 o 4 0 0 1815.15 2163.74 57.97 o 6 0 0 5096.79 4747.48 119.24 o 8 0 0 15282.30 15270.98 357.00 o 10 0 0 2706.53 2461.39 80.98 o 12 0 0 7989.20 7466.13 194.74 o 14 0 0 6782.08 7047.54 223.21 o 16 0 0 81.90 98.78 104.21 o 1 1 0 35681.54 37601.90 721.74 o 2 1 0 144.70 143.55 9.46 o 3 1 0 2517.76 2482.59 44.82 o 4 1 0 4539.57 4712.18 80.26 o 5 1 0 2100.77 2149.92 62.44 o 6 1 0 13682.83 13374.91 218.90 o 7 1 0 4767.83 4673.46 84.28 o 8 1 0 6787.89 6456.76 113.94 o 9 1 0 805.50 735.45 30.03 o 10 1 0 212.87 202.29 37.12 o 11 1 0 5733.63 5372.80 129.79 o 12 1 0 8597.76 8298.70 246.44 o 13 1 0 5682.97 5393.49 237.40 o 14 1 0 2653.07 2564.44 67.72 o 15 1 0 2662.83 2723.52 101.08 o 16 1 0 815.67 738.24 69.00 o 0 2 0 10967.17 11888.41 731.66 o 1 2 0 27635.36 30195.36 479.34 o 2 2 0 2991.70 2999.79 52.22 o 3 2 0 25502.33 28421.45 415.99 o 4 2 0 1788.89 2202.31 42.12 o 5 2 0 7182.85 7109.03 120.40 o 6 2 0 616.83 641.30 24.52 o 7 2 0 21385.50 21133.77 342.61 o 8 2 0 73.47 57.97 20.89 o 9 2 0 5690.16 5635.41 103.56 o 10 2 0 492.39 418.81 51.02 o 11 2 0 4213.41 4116.48 84.97 o 12 2 0 697.27 611.13 35.79 o 13 2 0 4901.81 4659.25 137.21 o 14 2 0 156.76 220.81 42.19 o 15 2 0 1272.12 1439.53 67.98 o 16 2 0 112.56 130.76 57.26 o 1 3 0 63.21 61.61 10.39 o 2 3 0 50018.08 53993.06 855.45 o 3 3 0 4792.93 5313.76 90.64 o 4 3 0 5902.53 6725.08 103.94 o 5 3 0 16688.85 17642.24 316.19 o 6 3 0 752.66 603.30 23.12 o 7 3 0 5062.59 5450.15 97.60 o 8 3 0 5545.58 5550.62 101.12 o 9 3 0 545.84 526.63 29.81 o 10 3 0 131.00 128.20 31.21 o 11 3 0 1015.75 941.76 52.20 o 12 3 0 1435.48 1375.89 52.37 o 13 3 0 44.81 44.65 36.07 o 14 3 0 536.76 520.78 43.78 o 15 3 0 56.10 -15.75 51.58 o 16 3 0 1066.87 1074.91 73.25 o 0 4 0 466.22 525.93 25.20 o 1 4 0 999.33 1027.54 21.91 o 2 4 0 20461.71 22329.48 358.06 o 3 4 0 10624.81 11296.75 185.76 o 4 4 0 9059.62 8726.37 146.04 o 5 4 0 2271.39 2436.71 52.47 o 6 4 0 425.06 350.92 19.33 o 7 4 0 53.29 38.88 18.15 o 8 4 0 849.35 740.67 29.69 o 9 4 0 24.13 38.21 23.68 o 10 4 0 16838.71 16678.46 279.52 o 11 4 0 78.88 95.07 33.68 o 12 4 0 1527.51 1473.31 70.32 o 13 4 0 897.78 887.15 46.75 o 14 4 0 1032.28 1052.54 67.23 o 15 4 0 506.12 616.05 61.95 o 16 4 0 1.48 23.53 58.25 o 1 5 0 13555.10 13756.70 205.53 o 2 5 0 8171.95 8482.18 141.93 o 3 5 0 18598.50 19331.60 313.53 o 4 5 0 52.01 20.70 15.85 o 5 5 0 3032.88 2690.67 54.60 o 6 5 0 115.15 110.94 16.25 o 7 5 0 557.48 499.10 23.04 o 8 5 0 84.49 111.21 22.00 o 9 5 0 15562.36 15712.65 292.98 o 10 5 0 167.03 183.35 35.56 o 11 5 0 20123.60 19022.08 824.72 o 12 5 0 2678.75 2543.84 99.13 o 13 5 0 2556.53 2658.44 86.28 o 14 5 0 156.28 121.40 50.58 o 15 5 0 71.95 152.76 55.75 o 0 6 0 22635.74 22904.87 516.26 o 1 6 0 5254.08 5235.79 83.86 o 2 6 0 11525.07 11478.61 173.83 o 3 6 0 34268.74 34359.24 550.32 o 4 6 0 1327.84 1092.96 31.52 o 5 6 0 20467.64 21429.95 348.88 o 6 6 0 532.51 520.03 26.24 o 7 6 0 233.85 184.12 24.27 o 8 6 0 9820.84 9625.77 185.66 o 9 6 0 332.19 320.56 34.78 o 10 6 0 12056.21 11855.10 259.29 o 11 6 0 266.03 345.12 39.04 o 12 6 0 3838.15 3832.36 106.71 o 13 6 0 97.26 24.22 47.88 o 14 6 0 266.50 164.42 53.32 o 15 6 0 3056.97 3329.95 123.69 o 1 7 0 1943.34 1667.06 34.72 o 2 7 0 20325.69 19509.77 291.61 o 3 7 0 257.38 307.32 21.59 o 4 7 0 40808.05 40700.95 704.71 o 5 7 0 789.06 732.41 29.31 o 6 7 0 6898.77 6398.74 115.79 o 7 7 0 286.96 238.21 26.04 o 8 7 0 2726.55 2536.99 65.85 o 9 7 0 7.08 25.52 32.31 o 10 7 0 5.88 13.73 33.22 o 11 7 0 89.34 87.96 37.74 o 12 7 0 84.89 141.10 43.10 o 13 7 0 140.58 128.60 49.60 o 14 7 0 3653.42 3981.96 134.76 o 15 7 0 271.54 231.16 108.29 o 0 8 0 2777.31 2677.81 65.07 o 1 8 0 702.31 633.39 22.50 o 2 8 0 358.63 437.78 20.18 o 3 8 0 6279.33 6067.80 99.19 o 4 8 0 2933.36 2827.99 69.43 o 5 8 0 7145.48 6910.54 124.24 o 6 8 0 60.65 41.83 23.89 o 7 8 0 7208.69 6852.11 125.72 o 8 8 0 5443.84 5102.67 100.03 o 9 8 0 331.21 318.46 35.89 o 10 8 0 7403.76 7243.00 151.45 o 11 8 0 159.28 151.93 46.64 o 12 8 0 539.33 587.69 58.79 o 13 8 0 13.51 -21.62 51.49 o 14 8 0 908.09 905.90 113.15 o 1 9 0 892.99 787.42 26.24 o 2 9 0 2111.97 2125.18 44.55 o 3 9 0 32.05 -4.50 15.24 o 4 9 0 0.68 13.86 25.68 o 5 9 0 5132.49 5066.16 100.60 o 6 9 0 974.53 865.42 38.53 o 7 9 0 1723.51 1764.16 50.02 o 8 9 0 1325.09 1187.49 46.19 o 9 9 0 1613.31 1654.44 56.37 o 10 9 0 1.80 31.71 42.14 o 11 9 0 2297.78 2204.94 80.78 o 12 9 0 317.71 421.70 64.88 o 13 9 0 159.25 165.56 55.88 o 14 9 0 4.21 30.14 53.53 o 0 10 0 1868.68 1620.41 50.36 o 1 10 0 2961.11 3067.31 54.16 o 2 10 0 2770.25 2692.35 53.85 o 3 10 0 1193.74 1022.14 36.79 o 4 10 0 575.05 552.87 33.27 o 5 10 0 7.17 16.82 26.06 o 6 10 0 813.91 779.61 35.83 o 7 10 0 2552.81 2538.35 62.10 o 8 10 0 1467.54 1445.21 48.31 o 9 10 0 1097.85 1092.93 49.36 o 10 10 0 521.28 483.72 54.63 o 11 10 0 22.20 -37.24 49.58 o 12 10 0 580.69 650.18 66.21 o 13 10 0 762.43 848.65 69.91 o 1 11 0 1817.20 1650.85 37.42 o 2 11 0 26.55 18.75 25.50 o 3 11 0 2571.72 2325.62 78.13 o 4 11 0 150.53 106.82 29.83 o 5 11 0 762.36 780.39 42.15 o 6 11 0 21656.40 20506.64 343.19 o 7 11 0 1062.52 1030.58 48.42 o 8 11 0 4672.36 4782.90 109.07 o 9 11 0 3933.99 3866.37 94.78 o 10 11 0 135.09 113.29 42.30 o 11 11 0 1699.30 1677.75 113.09 o 12 11 0 984.42 952.94 77.10 o 13 11 0 74.23 51.51 60.22 o 0 12 0 4012.03 3899.83 118.44 o 1 12 0 1350.90 1289.79 38.27 o 2 12 0 12.81 17.52 26.59 o 3 12 0 2803.98 2620.04 65.52 o 4 12 0 967.13 884.57 40.80 o 5 12 0 17184.15 16609.79 387.01 o 6 12 0 5985.29 5796.06 117.52 o 7 12 0 9855.16 9446.08 188.98 o 8 12 0 883.39 832.24 45.11 o 9 12 0 2724.08 2640.16 75.39 o 10 12 0 1585.22 1684.70 82.18 o 11 12 0 653.27 607.19 66.25 o 12 12 0 38.42 121.63 60.78 o 1 13 0 7945.27 7575.16 128.53 o 2 13 0 3969.59 3858.25 75.62 o 3 13 0 1370.75 1232.93 50.72 o 4 13 0 11339.76 11013.51 196.97 o 5 13 0 1562.00 1622.20 58.36 o 6 13 0 4061.59 4052.17 89.63 o 7 13 0 505.48 544.50 40.26 o 8 13 0 1888.25 1859.49 63.27 o 9 13 0 222.25 218.11 41.72 o 10 13 0 89.68 126.29 71.70 o 11 13 0 415.72 397.30 61.11 o 0 14 0 5337.47 5176.13 148.70 o 1 14 0 1050.13 1088.01 42.71 o 2 14 0 6960.61 6614.76 116.52 o 3 14 0 1054.67 962.49 39.28 o 4 14 0 699.08 608.01 44.94 o 5 14 0 176.45 220.72 38.35 o 6 14 0 307.44 323.95 39.88 o 7 14 0 250.39 272.67 38.59 o 8 14 0 1834.39 1836.27 65.37 o 9 14 0 19.86 -8.63 41.64 o 10 14 0 1062.20 1142.74 75.95 o 1 15 0 107.54 172.74 32.74 o 2 15 0 471.86 406.71 34.90 o 3 15 0 540.93 509.92 41.34 o 4 15 0 1122.10 1105.58 50.86 o 5 15 0 48.56 66.30 43.48 o 6 15 0 1050.55 958.90 51.75 o 7 15 0 125.88 151.87 39.68 o 8 15 0 2396.60 2228.43 82.95 o 9 15 0 135.68 127.08 48.24 o 0 16 0 149.75 277.40 68.96 o 1 16 0 150.36 185.06 44.28 o 2 16 0 745.62 700.72 48.97 o 3 16 0 1398.01 1352.37 60.14 o 4 16 0 1299.02 1306.01 58.92 o 5 16 0 187.37 256.21 49.77 o 6 16 0 404.08 477.21 53.67 o 7 16 0 277.82 295.63 44.18 o 1 17 0 416.13 410.89 61.49 o 2 17 0 1030.00 1061.15 65.67 o 3 17 0 67.08 196.22 62.27 o 4 17 0 1693.40 1750.11 92.67 o 5 17 0 1196.39 1142.70 97.30 o 0 18 0 409.05 511.31 80.57 o 1 18 0 40.77 88.37 109.69 o -15 0 1 514.15 483.76 71.60 o -13 0 1 1315.64 1447.66 76.38 o -11 0 1 88.00 89.11 39.81 o -9 0 1 26.23 113.17 33.52 o -7 0 1 11000.29 11716.33 275.06 o -5 0 1 996.94 1083.40 50.22 o -3 0 1 29173.34 31467.05 708.11 o -1 0 1 42039.12 45493.80 1205.13 o 1 0 1 20607.86 19930.97 1280.77 o 3 0 1 1056.62 1348.60 40.12 o 5 0 1 1026.52 1307.93 43.11 o 7 0 1 2652.19 2765.39 95.94 o 9 0 1 13017.42 13397.74 318.35 o 11 0 1 7979.08 7394.43 242.69 o 13 0 1 8882.70 8068.40 296.74 o 15 0 1 485.26 465.10 57.30 o -16 1 1 1934.65 2219.57 96.02 o -15 1 1 581.39 660.79 71.43 o -14 1 1 530.04 551.45 39.43 o -13 1 1 3710.96 3666.55 81.31 o -12 1 1 1007.20 990.22 45.41 o -11 1 1 24.00 9.72 26.93 o -10 1 1 95.65 113.57 25.47 o -9 1 1 764.88 808.60 30.94 o -8 1 1 4522.74 4868.23 89.08 o -7 1 1 3063.23 3192.18 61.43 o -6 1 1 197.96 277.21 17.84 o -5 1 1 774.28 701.47 22.50 o -4 1 1 6766.24 6846.47 125.46 o -3 1 1 646.68 635.30 17.24 o -2 1 1 12646.11 13830.04 239.15 o -1 1 1 12861.08 14188.44 274.39 o 0 1 1 1819.06 1862.20 45.35 o 1 1 1 9136.72 10216.37 181.04 o 2 1 1 3048.53 3147.77 63.67 o 3 1 1 434.30 501.64 15.54 o 4 1 1 812.92 657.55 21.61 o 5 1 1 6067.27 6079.24 130.71 o 6 1 1 35.32 31.02 15.67 o 7 1 1 2789.34 2579.40 99.02 o 8 1 1 1545.73 1503.12 47.26 o 9 1 1 617.83 670.57 30.49 o 10 1 1 1814.98 1597.49 55.20 o 11 1 1 161.51 84.14 28.99 o 12 1 1 3880.96 3680.56 80.00 o 13 1 1 6346.19 5932.95 130.13 o 14 1 1 270.11 277.52 36.72 o 15 1 1 13.08 -15.54 60.52 o 16 1 1 537.16 477.62 66.06 o -16 2 1 1.62 127.03 72.36 o -15 2 1 6596.64 6681.94 163.46 o -14 2 1 5072.58 4931.22 154.06 o -13 2 1 3647.79 3596.94 80.22 o -12 2 1 42.00 91.41 29.51 o -11 2 1 1514.84 1328.50 42.67 o -10 2 1 721.93 616.85 31.18 o -9 2 1 594.90 646.16 29.63 o -8 2 1 2066.56 2286.42 61.80 o -7 2 1 9292.80 9122.59 227.64 o -6 2 1 13399.10 14016.42 262.76 o -5 2 1 27465.34 28391.58 453.63 o -4 2 1 4588.52 4659.97 80.12 o -3 2 1 85150.84 91848.23 1452.02 o -2 2 1 8417.03 9165.17 136.19 o -1 2 1 320.76 315.62 12.05 o 0 2 1 22311.95 24770.53 394.24 o 1 2 1 4862.68 5183.70 94.67 o 2 2 1 3819.41 3880.97 74.73 o 3 2 1 47551.51 50707.74 739.90 o 4 2 1 4743.03 4453.94 93.32 o 5 2 1 23116.97 24328.73 391.82 o 6 2 1 1776.30 1435.40 39.21 o 7 2 1 24789.40 25477.08 412.15 o 8 2 1 2592.32 2818.97 59.08 o 9 2 1 12701.00 12442.50 210.92 o 10 2 1 221.81 260.08 28.29 o 11 2 1 201.37 201.92 35.35 o 12 2 1 1024.98 905.00 39.36 o 13 2 1 627.65 652.42 42.89 o 14 2 1 707.08 646.33 51.30 o 15 2 1 2603.86 2571.17 88.96 o 16 2 1 382.80 415.44 62.03 o -16 3 1 2293.81 2816.73 240.12 o -15 3 1 854.87 907.13 58.81 o -14 3 1 12957.82 12521.04 295.41 o -13 3 1 3.21 -21.14 33.92 o -12 3 1 6219.38 5930.72 123.94 o -11 3 1 2622.45 2625.63 70.38 o -10 3 1 15.46 43.34 28.41 o -9 3 1 10096.50 10058.52 172.44 o -8 3 1 15654.00 15564.15 256.88 o -7 3 1 1176.28 1202.32 33.51 o -6 3 1 21464.03 20999.88 339.64 o -5 3 1 320.75 220.82 20.25 o -4 3 1 54033.02 56942.66 903.71 o -3 3 1 13924.86 14596.86 216.47 o -2 3 1 3302.44 3422.54 54.68 o -1 3 1 2181.86 2415.11 40.10 o 0 3 1 1248.31 1287.62 23.98 o 1 3 1 3981.79 4212.92 72.87 o 2 3 1 14541.74 15923.02 256.21 o 3 3 1 14972.99 15233.13 246.59 o 4 3 1 3837.72 3817.63 62.61 o 5 3 1 569.39 356.52 16.41 o 6 3 1 33085.29 34363.52 551.06 o 7 3 1 1676.42 1767.16 41.89 o 8 3 1 35747.16 36872.05 594.14 o 9 3 1 6428.85 6434.48 117.20 o 10 3 1 2761.48 2671.84 61.98 o 11 3 1 12352.07 11917.49 216.76 o 12 3 1 1087.39 1098.13 54.37 o 13 3 1 1124.16 1107.60 50.23 o 14 3 1 4054.30 4182.92 116.85 o 15 3 1 424.66 383.77 52.13 o 16 3 1 3788.73 3747.53 159.37 o -16 4 1 325.57 404.72 59.66 o -15 4 1 49.32 37.96 52.17 o -14 4 1 105.74 97.58 55.27 o -13 4 1 13476.65 12635.98 650.61 o -12 4 1 2288.04 2192.59 65.04 o -11 4 1 2098.14 2060.83 62.25 o -10 4 1 12881.72 12880.85 219.63 o -9 4 1 233.88 273.92 29.58 o -8 4 1 11157.81 10912.59 184.64 o -7 4 1 10041.61 9676.03 163.95 o -6 4 1 4372.94 4343.33 78.93 o -5 4 1 18020.11 18116.59 293.44 o -4 4 1 1452.18 1432.85 28.76 o -3 4 1 533.40 538.90 17.17 o -2 4 1 2868.80 2684.23 45.97 o -1 4 1 7.78 15.19 11.35 o 0 4 1 48680.13 52661.63 767.04 o 1 4 1 511.79 472.66 22.07 o 2 4 1 4896.45 4594.07 80.07 o 3 4 1 3143.15 3076.60 57.15 o 4 4 1 22709.81 22996.48 371.12 o 5 4 1 3555.02 3527.93 60.29 o 6 4 1 196.55 192.55 17.13 o 7 4 1 14527.58 13495.57 224.18 o 8 4 1 9551.90 9828.06 169.05 o 9 4 1 13159.03 13300.67 225.30 o 10 4 1 9078.22 8970.16 178.28 o 11 4 1 3807.20 3625.25 134.45 o 12 4 1 8647.73 8493.15 265.22 o 13 4 1 852.58 887.15 53.97 o 14 4 1 2038.21 2114.92 79.45 o 15 4 1 373.03 380.26 55.04 o 16 4 1 2.69 -35.09 55.03 o -16 5 1 730.66 822.67 70.56 o -15 5 1 702.97 851.18 103.45 o -14 5 1 0.83 -42.41 42.41 o -13 5 1 1093.93 1020.03 61.76 o -12 5 1 2393.80 2263.99 68.97 o -11 5 1 5841.07 5602.34 121.75 o -10 5 1 572.94 631.97 40.35 o -9 5 1 1567.84 1469.18 42.14 o -8 5 1 1222.03 1225.42 36.92 o -7 5 1 7915.85 8024.66 137.86 o -6 5 1 68.97 46.30 16.41 o -5 5 1 274.12 186.12 13.88 o -4 5 1 4246.06 4474.45 73.12 o -3 5 1 5313.70 6096.32 96.27 o -2 5 1 3684.60 3865.84 63.58 o -1 5 1 24591.38 25626.75 376.78 o 0 5 1 715.50 720.40 18.96 o 1 5 1 50887.98 53297.36 931.48 o 2 5 1 17544.66 18066.23 293.20 o 3 5 1 5309.66 4864.51 86.47 o 4 5 1 1913.86 1732.26 39.40 o 5 5 1 8242.56 8950.38 152.14 o 6 5 1 241.23 212.97 21.30 o 7 5 1 5100.76 5428.76 90.51 o 8 5 1 3264.37 3058.42 63.74 o 9 5 1 189.73 239.52 33.98 o 10 5 1 193.99 225.61 36.35 o 11 5 1 578.04 702.26 46.81 o 12 5 1 1.11 7.85 39.40 o 13 5 1 3046.07 3132.05 150.12 o 14 5 1 162.66 192.30 62.84 o 15 5 1 1295.38 1538.43 99.71 o -15 6 1 4.77 -33.79 55.51 o -14 6 1 1816.38 1706.72 93.10 o -13 6 1 0.80 -40.60 40.60 o -12 6 1 721.29 740.41 74.87 o -11 6 1 17.79 23.03 33.62 o -10 6 1 247.14 316.50 37.68 o -9 6 1 306.59 343.89 34.52 o -8 6 1 661.71 691.24 38.92 o -7 6 1 23.72 0.50 16.91 o -6 6 1 3354.90 3146.13 56.90 o -5 6 1 570.68 543.90 24.27 o -4 6 1 5289.92 4769.30 94.23 o -3 6 1 142.69 167.03 14.95 o -2 6 1 290.45 276.39 18.10 o -1 6 1 619.77 719.67 20.22 o 0 6 1 7864.44 7706.02 119.36 o 1 6 1 36.10 18.68 17.31 o 2 6 1 4073.18 3922.17 65.45 o 3 6 1 5564.82 5366.01 95.87 o 4 6 1 1988.28 2172.79 47.48 o 5 6 1 21.87 24.30 19.71 o 6 6 1 2945.18 3203.15 65.28 o 7 6 1 279.63 282.39 32.42 o 8 6 1 1862.40 1763.77 47.85 o 9 6 1 16.23 36.50 31.96 o 10 6 1 7633.10 7507.59 210.59 o 11 6 1 2477.52 2410.17 96.35 o 12 6 1 234.45 309.95 45.28 o 13 6 1 146.34 181.21 46.36 o 14 6 1 851.39 1060.98 72.46 o 15 6 1 802.34 870.45 113.23 o -15 7 1 456.13 446.80 65.83 o -14 7 1 151.09 296.12 59.53 o -13 7 1 5.78 12.22 50.70 o -12 7 1 20.95 37.97 40.41 o -11 7 1 3274.23 3438.92 91.07 o -10 7 1 476.20 528.56 40.00 o -9 7 1 821.57 866.20 46.98 o -8 7 1 61.29 59.69 29.06 o -7 7 1 2.78 -0.37 25.95 o -6 7 1 1771.74 1730.82 43.71 o -5 7 1 5219.43 4895.12 90.97 o -4 7 1 4194.49 3822.98 74.09 o -3 7 1 5377.95 5344.40 87.70 o -2 7 1 13883.28 13899.98 210.20 o -1 7 1 620.27 598.50 20.38 o 0 7 1 298.60 405.83 18.15 o 1 7 1 2779.41 2560.84 50.99 o 2 7 1 4763.15 4691.99 77.86 o 3 7 1 17.95 34.95 18.63 o 4 7 1 74.48 70.04 19.74 o 5 7 1 1323.91 1473.08 40.25 o 6 7 1 4205.70 4089.68 80.44 o 7 7 1 397.12 370.15 28.30 o 8 7 1 340.91 298.80 29.67 o 9 7 1 4447.33 4089.48 126.41 o 10 7 1 1515.17 1590.07 65.44 o 11 7 1 1570.44 1680.26 67.93 o 12 7 1 1178.30 1123.40 59.50 o 13 7 1 705.50 740.12 54.82 o 14 7 1 10.54 2.25 50.80 o 15 7 1 2572.74 2801.58 241.39 o -15 8 1 3560.51 4001.27 235.49 o -14 8 1 96.89 126.25 55.98 o -13 8 1 112.03 116.79 53.84 o -12 8 1 821.15 858.54 63.27 o -11 8 1 83.66 85.97 51.95 o -10 8 1 820.78 808.89 45.39 o -9 8 1 451.35 374.27 37.56 o -8 8 1 2046.74 2107.27 59.94 o -7 8 1 67.77 46.59 24.68 o -6 8 1 5088.55 5155.96 97.36 o -5 8 1 5927.50 5494.31 101.73 o -4 8 1 284.20 255.07 24.16 o -3 8 1 31318.59 30843.62 457.44 o -2 8 1 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