#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:42:01 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181186 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/65/2226584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226584_Fobs loop_ _publ_author_name 'Gulab, Shivali A.' 'Cheng, Janice M. H.' 'Timmer, Mattie S. M.' 'Stocker, Bridget L.' 'Gainsford, Graeme J.' _publ_section_title ; Methyl 6-deoxy-6-iodo-\a-D-galactoside ; _journal_coeditor_code LH5062 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1724 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.7745 _cell_length_b 7.9055 _cell_length_c 22.1835 _exptl_crystal_F_000 591.97 _reflns_d_resolution_high 0.6192 _cod_data_source_file lh5062Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SH38 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 203.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7685.25 8086.79 99.39 o 4 0 0 3804.60 3769.69 54.72 o 6 0 0 1114.60 1175.56 30.54 o 8 0 0 0.92 0.75 5.16 o 1 1 0 914.16 1014.50 11.32 o 2 1 0 104.74 139.58 2.22 o 3 1 0 18073.52 18870.03 211.34 o 4 1 0 875.58 889.79 11.14 o 5 1 0 1741.69 1734.55 24.21 o 6 1 0 116.20 109.06 4.56 o 7 1 0 237.61 239.01 8.53 o 8 1 0 9.07 10.39 3.41 o 0 2 0 41178.07 42614.01 552.84 o 1 2 0 162.26 157.52 2.05 o 2 2 0 7993.47 8496.90 102.64 o 3 2 0 2.12 5.46 1.40 o 4 2 0 3967.67 4028.50 46.54 o 5 2 0 115.76 98.31 2.98 o 6 2 0 2309.65 2331.07 37.21 o 7 2 0 6.04 2.66 2.79 o 8 2 0 15.04 16.78 3.55 o 1 3 0 5094.24 5226.96 59.74 o 2 3 0 3394.42 3533.63 43.11 o 3 3 0 6713.48 6678.84 93.08 o 4 3 0 209.70 216.44 5.50 o 5 3 0 555.63 563.12 12.02 o 6 3 0 146.07 147.36 4.62 o 7 3 0 524.63 535.52 13.10 o 8 3 0 46.77 59.06 6.14 o 0 4 0 10211.89 10749.54 154.38 o 1 4 0 1658.32 1603.88 19.43 o 2 4 0 1324.38 1292.11 17.97 o 3 4 0 245.54 246.41 4.08 o 4 4 0 1073.67 1083.32 17.85 o 5 4 0 593.99 589.25 11.98 o 6 4 0 434.98 412.34 10.48 o 7 4 0 43.04 57.33 6.03 o 8 4 0 19.74 4.57 9.84 o 1 5 0 1675.59 1704.02 20.09 o 2 5 0 3907.17 3905.43 52.24 o 3 5 0 3993.97 3992.61 53.46 o 4 5 0 984.28 998.61 14.67 o 5 5 0 1.76 -0.82 3.64 o 6 5 0 182.53 176.21 7.48 o 7 5 0 158.22 176.31 9.62 o 8 5 0 190.47 222.69 24.80 o 0 6 0 3292.66 3506.91 51.40 o 1 6 0 3029.26 3030.04 35.13 o 2 6 0 29.49 17.58 2.42 o 3 6 0 252.79 274.99 5.57 o 4 6 0 754.00 763.67 13.36 o 5 6 0 1358.82 1343.01 28.80 o 6 6 0 646.88 624.82 17.98 o 7 6 0 100.98 117.82 9.23 o 1 7 0 406.37 400.66 6.48 o 2 7 0 1132.87 1110.62 18.13 o 3 7 0 1244.73 1221.39 19.95 o 4 7 0 1234.90 1175.57 19.55 o 5 7 0 211.90 191.67 6.86 o 6 7 0 164.49 178.29 10.38 o 7 7 0 207.19 220.31 26.23 o 0 8 0 285.38 286.30 10.41 o 1 8 0 1350.29 1293.29 20.93 o 2 8 0 605.31 547.73 10.58 o 3 8 0 1816.34 1822.72 28.86 o 4 8 0 353.11 362.27 8.37 o 5 8 0 937.91 978.82 22.63 o 6 8 0 286.54 276.83 13.11 o 1 9 0 721.92 734.56 13.34 o 2 9 0 729.79 737.45 13.53 o 3 9 0 79.28 86.88 5.01 o 4 9 0 213.85 202.79 8.21 o 5 9 0 13.41 5.83 3.60 o 6 9 0 12.43 26.70 15.26 o 0 10 0 51.91 52.14 6.40 o 1 10 0 513.18 502.97 12.09 o 2 10 0 41.82 31.56 5.03 o 3 10 0 1.00 3.98 4.18 o 4 10 0 0.22 2.14 4.37 o 5 10 0 337.01 336.66 30.04 o 1 11 0 40.19 41.46 5.47 o 2 11 0 416.77 444.91 13.73 o 3 11 0 4.32 2.99 6.13 o 4 11 0 233.40 204.10 23.84 o 1 0 1 2193.24 2252.89 24.50 o 2 0 1 21984.37 22791.64 201.79 o 3 0 1 149.93 141.11 2.36 o 4 0 1 6138.90 6361.92 67.94 o 5 0 1 138.87 138.64 3.59 o 6 0 1 152.51 138.49 5.10 o 7 0 1 51.64 49.85 3.74 o 8 0 1 383.30 388.23 10.11 o 9 0 1 52.24 47.65 11.97 o -9 1 1 51.15 68.67 18.12 o -8 1 1 27.14 28.72 3.84 o -7 1 1 299.90 315.00 8.44 o -6 1 1 136.78 127.68 4.73 o -5 1 1 3130.20 3177.47 42.42 o -4 1 1 67.69 73.25 2.06 o -3 1 1 509.21 553.04 7.05 o -2 1 1 1255.16 1350.83 14.45 o -1 1 1 23232.73 24236.57 234.52 o 0 1 1 2033.77 1991.22 31.66 o 1 1 1 22711.87 23921.46 246.89 o 2 1 1 1233.19 1310.39 15.75 o 3 1 1 559.17 601.65 7.61 o 4 1 1 62.40 68.84 2.12 o 5 1 1 2844.61 2884.14 40.81 o 6 1 1 122.36 120.61 4.40 o 7 1 1 309.11 327.15 8.49 o 8 1 1 27.74 29.07 3.84 o -8 2 1 343.92 356.75 9.64 o -7 2 1 206.71 200.57 6.53 o -6 2 1 449.28 422.53 11.00 o -5 2 1 51.43 53.73 2.24 o -4 2 1 6303.94 6432.98 71.41 o -3 2 1 1364.74 1392.72 17.63 o -2 2 1 17946.29 18471.59 218.26 o -1 2 1 3115.99 3266.71 32.55 o 0 2 1 53.91 53.79 1.27 o 1 2 1 2975.11 3138.25 31.70 o 2 2 1 17162.51 17685.79 217.91 o 3 2 1 1386.13 1419.64 17.49 o 4 2 1 6221.23 6406.68 73.49 o 5 2 1 47.04 46.29 2.18 o 6 2 1 491.28 442.71 8.95 o 7 2 1 238.55 239.61 6.78 o 8 2 1 382.51 386.06 9.82 o -8 3 1 77.76 77.49 6.62 o -7 3 1 874.30 883.15 16.96 o -6 3 1 743.05 751.72 13.32 o -5 3 1 2813.14 2809.67 44.53 o -4 3 1 503.53 492.22 9.10 o -3 3 1 375.39 391.25 7.07 o -2 3 1 1205.02 1223.31 16.63 o -1 3 1 12019.13 12252.10 144.13 o 0 3 1 7173.93 7348.82 74.20 o 1 3 1 12073.28 12235.05 145.29 o 2 3 1 1273.34 1291.66 17.32 o 3 3 1 360.20 380.03 6.48 o 4 3 1 460.96 459.04 9.49 o 5 3 1 2795.52 2793.24 43.67 o 6 3 1 675.43 678.37 13.55 o 7 3 1 798.41 796.93 18.23 o 8 3 1 75.73 77.67 6.65 o -8 4 1 270.25 311.39 23.84 o -7 4 1 81.16 101.11 7.04 o -6 4 1 152.48 150.82 6.76 o -5 4 1 35.36 34.91 3.32 o -4 4 1 2991.51 2983.97 43.43 o -3 4 1 2855.05 2848.94 34.56 o -2 4 1 9771.95 10037.93 132.80 o -1 4 1 1399.99 1427.23 16.70 o 0 4 1 1195.14 1270.25 13.56 o 1 4 1 1293.43 1307.67 16.63 o 2 4 1 9886.99 10157.13 132.82 o 3 4 1 2773.74 2739.79 37.69 o 4 4 1 2804.69 2755.34 48.15 o 5 4 1 42.31 42.47 3.87 o 6 4 1 146.69 140.95 6.12 o 7 4 1 88.85 95.22 6.12 o 8 4 1 245.73 264.22 20.56 o -8 5 1 2.01 5.25 9.84 o -7 5 1 260.76 265.53 11.56 o -6 5 1 447.12 462.86 13.22 o -5 5 1 1744.49 1640.13 33.84 o -4 5 1 953.06 928.44 13.52 o -3 5 1 738.06 737.69 11.06 o -2 5 1 433.15 411.92 6.92 o -1 5 1 4631.85 4752.24 54.98 o 0 5 1 5140.12 5009.49 51.38 o 1 5 1 4737.62 4881.21 56.64 o 2 5 1 432.46 408.73 6.87 o 3 5 1 694.90 709.51 11.03 o 4 5 1 801.27 794.02 12.70 o 5 5 1 1740.04 1637.52 36.74 o 6 5 1 465.14 471.52 13.40 o 7 5 1 252.24 249.24 11.29 o 8 5 1 1.72 2.86 11.92 o -7 6 1 260.18 303.28 13.86 o -6 6 1 22.35 20.84 5.01 o -5 6 1 124.66 117.59 6.27 o -4 6 1 789.77 750.89 12.46 o -3 6 1 1960.08 1897.24 26.11 o -2 6 1 3476.73 3486.58 47.90 o -1 6 1 1205.00 1212.59 14.04 o 0 6 1 42.27 36.22 1.74 o 1 6 1 1124.35 1128.87 14.75 o 2 6 1 3243.17 3265.08 47.77 o 3 6 1 1910.02 1836.02 27.38 o 4 6 1 674.79 636.97 12.14 o 5 6 1 108.82 103.06 6.10 o 6 6 1 20.70 21.69 5.10 o 7 6 1 255.42 297.97 12.22 o -7 7 1 178.80 182.64 23.84 o -6 7 1 406.81 440.50 15.19 o -5 7 1 659.04 633.01 16.34 o -4 7 1 844.14 875.27 15.62 o -3 7 1 62.06 56.22 3.40 o -2 7 1 270.34 232.89 5.96 o -1 7 1 722.62 741.41 10.97 o 0 7 1 2632.07 2570.34 30.28 o 1 7 1 835.40 849.66 12.90 o 2 7 1 258.90 226.06 5.85 o 3 7 1 59.47 52.98 3.35 o 4 7 1 914.09 937.33 15.73 o 5 7 1 613.79 611.18 14.09 o 6 7 1 397.67 411.16 15.85 o 7 7 1 202.10 205.53 25.27 o -6 8 1 34.53 40.57 8.66 o -5 8 1 6.79 1.38 3.06 o -4 8 1 100.87 91.15 4.40 o -3 8 1 1488.45 1455.31 24.35 o -2 8 1 689.89 699.98 12.48 o -1 8 1 790.88 797.36 13.89 o 0 8 1 28.14 24.43 2.43 o 1 8 1 795.02 799.85 13.91 o 2 8 1 754.21 768.49 13.22 o 3 8 1 1601.37 1569.86 24.48 o 4 8 1 124.93 106.49 4.64 o 5 8 1 10.69 5.25 3.04 o 6 8 1 34.29 40.58 8.11 o -6 9 1 372.71 342.86 31.47 o -5 9 1 45.59 47.94 5.14 o -4 9 1 485.60 521.21 14.87 o -3 9 1 82.00 72.69 4.75 o -2 9 1 671.66 657.65 11.90 o -1 9 1 254.15 258.59 6.97 o 0 9 1 2427.31 2351.37 41.39 o 1 9 1 247.43 251.20 6.59 o 2 9 1 572.37 564.56 11.66 o 3 9 1 85.29 76.42 4.75 o 4 9 1 496.12 537.54 13.94 o 5 9 1 57.20 59.63 4.71 o -5 10 1 53.58 60.56 17.17 o -4 10 1 138.84 140.98 8.53 o -3 10 1 1038.77 1070.41 25.48 o -2 10 1 95.20 103.51 6.45 o -1 10 1 299.40 303.98 10.81 o 0 10 1 16.19 10.81 3.78 o 1 10 1 311.33 346.50 9.91 o 2 10 1 91.63 89.74 5.66 o 3 10 1 1136.90 1144.19 21.78 o 4 10 1 115.64 115.01 7.09 o 5 10 1 63.51 73.02 11.26 o -4 11 1 151.32 196.94 23.37 o -3 11 1 44.36 36.81 7.59 o -2 11 1 182.13 160.58 8.32 o -1 11 1 48.07 47.45 5.70 o 0 11 1 939.98 953.04 25.17 o 1 11 1 47.04 57.75 9.70 o 2 11 1 176.33 165.01 8.34 o 3 11 1 43.36 41.76 7.53 o 4 11 1 159.36 208.87 23.37 o -3 12 1 255.13 259.41 27.18 o 1 0 2 5265.30 5461.55 47.21 o 2 0 2 2436.98 2542.39 23.75 o 3 0 2 6.10 6.77 0.93 o 4 0 2 4349.39 4394.51 49.07 o 5 0 2 28.30 24.32 2.01 o 6 0 2 3046.95 3007.14 47.07 o 7 0 2 90.95 95.15 4.72 o 8 0 2 36.31 51.83 4.44 o 9 0 2 14.06 18.60 14.31 o -9 1 2 172.24 213.16 25.75 o -8 1 2 64.03 66.39 4.59 o -7 1 2 1257.75 1208.42 22.73 o -6 1 2 393.01 369.88 8.64 o -5 1 2 154.64 161.46 6.37 o -4 1 2 116.26 124.51 2.74 o -3 1 2 12566.29 12965.58 132.70 o -2 1 2 3587.46 3914.66 39.00 o -1 1 2 11121.98 11675.45 102.10 o 0 1 2 2644.26 2705.30 33.67 o 1 1 2 10486.42 11033.71 107.35 o 2 1 2 3555.54 3854.49 44.22 o 3 1 2 12237.83 12557.59 160.28 o 4 1 2 134.28 141.75 2.91 o 5 1 2 115.78 115.93 3.64 o 6 1 2 376.47 354.81 7.64 o 7 1 2 1241.40 1210.94 22.77 o 8 1 2 55.95 63.99 4.56 o 9 1 2 195.23 209.82 25.27 o -8 2 2 25.73 27.74 3.78 o -7 2 2 101.19 111.93 4.88 o -6 2 2 1184.29 1195.59 22.05 o -5 2 2 828.71 841.61 13.50 o -4 2 2 4037.08 4104.74 43.57 o -3 2 2 25.18 23.06 1.36 o -2 2 2 722.30 709.32 9.61 o -1 2 2 2822.12 2861.63 27.36 o 0 2 2 41442.21 42806.04 401.88 o 1 2 2 2887.74 2922.06 28.68 o 2 2 2 844.23 834.35 10.29 o 3 2 2 18.04 17.24 1.32 o 4 2 2 3761.82 3831.27 45.93 o 5 2 2 902.85 910.82 13.14 o 6 2 2 1222.73 1214.33 19.73 o 7 2 2 96.15 108.46 4.65 o 8 2 2 23.71 25.42 3.79 o -8 3 2 10.08 17.19 5.19 o -7 3 2 479.21 490.81 10.81 o -6 3 2 29.67 33.79 3.97 o -5 3 2 156.13 151.81 4.45 o -4 3 2 1471.14 1482.35 19.42 o -3 3 2 9655.33 9773.78 124.86 o -2 3 2 2382.14 2336.81 30.58 o -1 3 2 5001.91 5044.53 57.66 o 0 3 2 664.98 674.94 7.35 o 1 3 2 4583.53 4678.76 57.61 o 2 3 2 2425.59 2405.68 31.86 o 3 3 2 9594.06 9714.09 117.40 o 4 3 2 1394.57 1437.60 21.42 o 5 3 2 144.95 147.06 4.38 o 6 3 2 27.57 24.99 3.06 o 7 3 2 447.68 442.40 11.07 o 8 3 2 14.12 21.22 5.22 o -8 4 2 15.08 23.27 8.44 o -7 4 2 100.98 109.51 6.97 o -6 4 2 1850.27 1809.44 37.55 o -5 4 2 542.93 542.27 11.24 o -4 4 2 2484.78 2436.28 35.54 o -3 4 2 18.59 15.86 1.60 o -2 4 2 1495.82 1453.67 20.09 o -1 4 2 4581.82 4561.96 53.03 o 0 4 2 12453.17 13003.05 135.55 o 1 4 2 4443.33 4410.90 59.57 o 2 4 2 1489.03 1451.40 20.10 o 3 4 2 25.92 21.96 1.62 o 4 4 2 2513.13 2487.87 36.75 o 5 4 2 560.45 558.08 12.17 o 6 4 2 1827.19 1752.86 31.98 o 7 4 2 88.74 96.11 6.30 o 8 4 2 12.26 16.71 10.28 o -8 5 2 46.26 64.02 25.04 o -7 5 2 246.48 250.09 15.86 o -6 5 2 47.41 55.04 5.58 o -5 5 2 308.39 293.57 9.35 o -4 5 2 1158.76 1115.89 16.15 o -3 5 2 3631.40 3630.77 48.40 o -2 5 2 3827.39 3760.47 45.49 o -1 5 2 2374.50 2437.97 27.80 o 0 5 2 72.14 97.98 2.20 o 1 5 2 2294.12 2318.17 30.95 o 2 5 2 3692.22 3621.58 49.56 o 3 5 2 3578.77 3566.44 48.39 o 4 5 2 1137.19 1101.34 16.12 o 5 5 2 294.70 272.81 10.04 o 6 5 2 51.05 56.40 5.52 o 7 5 2 258.80 269.36 11.06 o 8 5 2 45.92 54.84 16.69 o -8 6 2 34.56 49.12 16.21 o -7 6 2 72.46 93.63 8.72 o -6 6 2 576.95 566.23 17.24 o -5 6 2 486.63 491.90 14.17 o -4 6 2 374.52 391.42 8.11 o -3 6 2 112.24 119.31 3.85 o -2 6 2 2334.25 2309.36 29.35 o -1 6 2 2955.70 2925.58 32.54 o 0 6 2 2883.90 3044.56 31.72 o 1 6 2 3057.88 3018.02 38.44 o 2 6 2 2197.03 2146.07 32.25 o 3 6 2 110.89 115.89 3.80 o 4 6 2 387.68 402.51 11.25 o 5 6 2 442.54 449.83 19.04 o 6 6 2 593.08 557.76 15.48 o 7 6 2 68.62 80.60 7.12 o -7 7 2 7.70 10.49 13.35 o -6 7 2 59.94 76.74 6.86 o -5 7 2 2.84 0.13 3.21 o -4 7 2 707.83 669.47 12.22 o -3 7 2 1448.72 1433.47 23.70 o -2 7 2 4109.41 4027.01 59.44 o -1 7 2 1393.04 1418.62 18.53 o 0 7 2 505.76 481.15 6.99 o 1 7 2 1382.61 1405.90 21.21 o 2 7 2 4052.59 3992.67 59.38 o 3 7 2 1587.80 1545.34 23.85 o 4 7 2 658.88 639.14 12.07 o 5 7 2 0.52 -3.03 3.03 o 6 7 2 73.61 82.92 7.97 o 7 7 2 3.07 -3.77 8.48 o -7 8 2 83.60 59.13 17.64 o -6 8 2 77.07 63.84 8.43 o -5 8 2 486.36 522.81 13.37 o -4 8 2 9.17 6.85 3.06 o -3 8 2 457.18 417.09 8.79 o -2 8 2 318.58 313.40 6.52 o -1 8 2 1978.72 1918.33 29.36 o 0 8 2 843.98 890.91 15.06 o 1 8 2 1934.39 1850.44 29.32 o 2 8 2 276.57 272.34 6.94 o 3 8 2 414.82 369.20 8.52 o 4 8 2 18.32 21.53 3.11 o 5 8 2 485.97 512.97 12.24 o 6 8 2 81.07 76.92 8.15 o -6 9 2 64.56 54.84 17.17 o -5 9 2 131.18 117.93 7.35 o -4 9 2 738.69 683.96 20.38 o -3 9 2 457.64 451.92 11.68 o -2 9 2 1496.46 1499.91 29.81 o -1 9 2 18.65 20.71 3.56 o 0 9 2 0.08 1.54 3.34 o 1 9 2 10.30 13.99 2.97 o 2 9 2 1634.33 1624.65 26.80 o 3 9 2 492.42 484.30 11.27 o 4 9 2 740.63 678.16 16.64 o 5 9 2 146.34 135.29 6.41 o 6 9 2 56.47 82.97 15.26 o -5 10 2 322.39 330.94 30.52 o -4 10 2 3.79 8.52 4.92 o -3 10 2 219.45 260.07 10.01 o -2 10 2 93.23 86.86 6.26 o -1 10 2 1356.50 1346.18 29.39 o 0 10 2 38.45 41.32 4.35 o 1 10 2 1335.94 1301.27 25.22 o 2 10 2 94.85 89.00 4.97 o 3 10 2 215.05 252.36 8.31 o 4 10 2 3.46 7.25 4.04 o 5 10 2 322.27 343.37 19.82 o -4 11 2 186.35 177.87 22.89 o -3 11 2 16.41 18.90 6.95 o -2 11 2 425.24 437.96 13.86 o -1 11 2 86.42 84.79 6.58 o 0 11 2 70.36 75.08 6.53 o 1 11 2 81.86 80.11 7.86 o 2 11 2 454.59 470.92 15.07 o 3 11 2 14.60 8.71 6.54 o 4 11 2 184.81 178.03 14.26 o -3 12 2 11.17 21.46 14.78 o -2 12 2 47.86 50.07 15.26 o 1 0 3 2231.04 2375.08 22.42 o 2 0 3 11802.83 11916.75 109.88 o 3 0 3 578.94 569.51 7.27 o 4 0 3 6425.99 6785.71 77.74 o 5 0 3 9.61 16.40 2.05 o 6 0 3 316.69 306.71 8.01 o 7 0 3 28.09 33.57 3.56 o 8 0 3 688.61 694.36 15.09 o 9 0 3 55.96 44.83 16.21 o -9 1 3 62.12 44.35 16.21 o -8 1 3 152.78 160.26 6.24 o -7 1 3 625.02 644.51 13.43 o -6 1 3 81.04 79.83 4.02 o -5 1 3 7183.49 7172.13 95.58 o -4 1 3 72.52 79.57 2.41 o -3 1 3 1649.06 1821.18 20.40 o -2 1 3 2619.23 2824.93 28.91 o -1 1 3 30424.24 31268.05 276.07 o 0 1 3 149.08 159.92 2.42 o 1 1 3 31190.35 32271.84 317.55 o 2 1 3 2726.46 2919.05 32.33 o 3 1 3 1606.89 1747.31 22.68 o 4 1 3 96.20 108.47 2.59 o 5 1 3 7407.86 7351.41 99.93 o 6 1 3 89.81 91.18 3.74 o 7 1 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