#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:42:37 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181187 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/66/2226601.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226601_Fobs loop_ _publ_author_name 'Cai, Ying' _publ_section_title ; 1-Cyanomethyl-1,4-diazoniabicyclo[2.2.2]octane tetrabromidocuprate(II) ; _journal_coeditor_code NC2190 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m830 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.751 _cell_angle_gamma 90.000 _cell_length_a 8.4793 _cell_length_b 13.9115 _cell_length_c 12.5056 _exptl_crystal_F_000 1012.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file nc2190Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 371.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3686.38 3739.54 93.39 o 3 0 0 23723.62 23678.88 532.29 o 4 0 0 32854.32 29469.81 795.70 o 5 0 0 47384.82 38639.19 4657.43 o 6 0 0 893.91 945.52 96.69 o 7 0 0 28.61 81.02 38.92 o 8 0 0 2113.62 2244.16 209.73 o 9 0 0 7125.64 6504.44 465.13 o 10 0 0 281.81 297.02 138.82 o 2 1 0 8023.23 8588.00 88.03 o 3 1 0 18923.18 18635.07 228.33 o 4 1 0 34619.57 35868.98 555.60 o 5 1 0 19118.11 19110.11 390.22 o 6 1 0 387.62 665.34 70.02 o 7 1 0 909.43 1031.49 69.54 o 8 1 0 3180.75 3374.91 128.46 o 9 1 0 1079.60 1164.18 102.60 o 10 1 0 621.80 693.44 114.12 o 1 2 0 3766.44 4351.99 49.60 o 2 2 0 29175.82 27086.31 651.51 o 3 2 0 3143.86 3399.93 96.37 o 4 2 0 28988.07 28537.01 429.21 o 5 2 0 8123.42 8593.29 160.53 o 6 2 0 2808.71 2776.66 87.89 o 7 2 0 3976.55 4043.07 121.20 o 8 2 0 1062.24 1079.95 87.86 o 9 2 0 5411.52 5733.52 253.47 o 10 2 0 1.73 56.67 78.64 o 1 3 0 22582.83 22382.55 238.34 o 2 3 0 2242.09 2370.41 41.49 o 3 3 0 23711.62 22288.28 293.44 o 4 3 0 489.45 630.58 29.84 o 5 3 0 13455.22 14215.23 386.11 o 6 3 0 15173.78 15840.26 318.08 o 7 3 0 16440.74 15492.05 452.03 o 8 3 0 7413.39 7177.52 304.52 o 9 3 0 92.16 42.72 60.24 o 10 3 0 2955.33 2716.57 328.11 o 0 4 0 15943.86 19431.53 280.72 o 1 4 0 393.33 425.82 13.28 o 2 4 0 89948.95 80976.22 1133.64 o 3 4 0 1584.70 1616.68 41.79 o 4 4 0 8322.08 8980.94 130.45 o 5 4 0 84.69 203.38 61.97 o 6 4 0 24994.62 25599.21 659.52 o 7 4 0 21336.69 21714.47 631.57 o 8 4 0 265.84 309.69 67.95 o 9 4 0 664.69 835.85 103.22 o 10 4 0 9.39 126.73 80.45 o 1 5 0 15146.68 14971.36 266.86 o 2 5 0 6953.66 7008.28 103.12 o 3 5 0 42296.31 42277.45 626.92 o 4 5 0 85.40 163.50 36.05 o 5 5 0 692.62 733.24 73.87 o 6 5 0 10501.86 11459.83 317.71 o 7 5 0 8219.23 8783.78 406.68 o 8 5 0 1647.80 1728.63 125.83 o 9 5 0 35.54 129.35 87.47 o 10 5 0 2269.47 2361.94 216.43 o 0 6 0 11842.39 12150.72 299.14 o 1 6 0 699.61 705.75 28.58 o 2 6 0 69145.38 65219.68 1108.95 o 3 6 0 11743.62 11092.69 280.66 o 4 6 0 437.40 520.95 58.27 o 5 6 0 4769.47 4826.18 148.90 o 6 6 0 2998.25 3442.21 209.00 o 7 6 0 6361.97 7176.76 265.22 o 8 6 0 0.12 -52.61 55.56 o 9 6 0 566.70 695.62 113.92 o 10 6 0 221.30 79.06 101.08 o 1 7 0 47154.23 44986.91 764.69 o 2 7 0 15579.13 15440.99 239.44 o 3 7 0 11475.44 10309.10 360.06 o 4 7 0 9936.85 9804.13 252.68 o 5 7 0 405.12 428.59 51.31 o 6 7 0 2216.68 2501.95 112.41 o 7 7 0 100.28 385.94 67.68 o 8 7 0 32.60 107.58 83.22 o 9 7 0 40.34 112.22 85.18 o 10 7 0 959.93 784.26 181.56 o 0 8 0 55566.31 56588.78 1395.06 o 1 8 0 2892.86 2870.07 61.98 o 2 8 0 4212.82 4004.67 117.94 o 3 8 0 4740.03 4639.21 103.58 o 4 8 0 12326.58 12024.00 291.50 o 5 8 0 10509.13 10850.10 302.32 o 6 8 0 22.41 -33.31 50.94 o 7 8 0 125.92 132.73 85.60 o 8 8 0 351.34 330.76 100.09 o 9 8 0 2034.35 2133.11 207.54 o 1 9 0 8771.91 8748.09 198.12 o 2 9 0 2938.60 2864.22 70.57 o 3 9 0 246.92 258.04 41.43 o 4 9 0 2949.28 2625.97 134.52 o 5 9 0 9073.76 9963.36 393.79 o 6 9 0 178.67 72.62 64.79 o 7 9 0 3.10 10.77 80.13 o 8 9 0 3052.43 3654.19 281.36 o 9 9 0 1028.26 1183.38 168.91 o 0 10 0 19139.22 18251.93 498.32 o 1 10 0 27.64 10.14 25.20 o 2 10 0 5327.39 5204.64 129.18 o 3 10 0 1003.57 927.72 43.76 o 4 10 0 27760.47 27945.50 961.39 o 5 10 0 735.26 709.75 109.79 o 6 10 0 2394.78 2395.66 171.13 o 7 10 0 1.64 15.37 100.51 o 8 10 0 1422.81 1564.08 166.08 o 9 10 0 8094.48 9195.17 691.72 o 1 11 0 581.27 532.85 41.32 o 2 11 0 3047.37 2983.19 100.10 o 3 11 0 2333.46 2065.57 96.21 o 4 11 0 151.63 200.21 127.47 o 5 11 0 8980.78 9667.22 535.00 o 6 11 0 266.15 166.60 89.86 o 7 11 0 792.14 770.83 157.81 o 8 11 0 2641.16 2735.35 259.75 o 0 12 0 695.64 560.60 75.52 o 1 12 0 4.56 36.61 30.88 o 2 12 0 3179.09 3125.13 160.36 o 3 12 0 4.40 68.26 52.34 o 4 12 0 672.65 724.53 108.21 o 5 12 0 0.02 -34.67 68.46 o 6 12 0 486.18 802.66 157.13 o 7 12 0 1389.86 1344.67 181.77 o 8 12 0 978.69 1133.35 195.18 o 1 13 0 3003.70 2853.94 107.20 o 2 13 0 5008.33 4550.36 232.06 o 3 13 0 3386.49 3146.23 201.76 o 4 13 0 361.27 586.69 117.92 o 5 13 0 231.43 316.92 102.93 o 6 13 0 487.39 431.55 124.98 o 7 13 0 147.85 266.11 151.67 o 0 14 0 15.52 49.66 81.40 o 1 14 0 8.20 86.89 90.69 o 2 14 0 12449.59 11789.06 486.27 o 3 14 0 3567.59 3462.36 226.06 o 4 14 0 2006.04 2210.20 188.77 o 5 14 0 4.67 128.11 106.67 o 6 14 0 87.67 173.25 117.05 o 1 15 0 1835.41 1774.02 129.80 o 2 15 0 1507.19 1391.98 148.05 o 3 15 0 1606.46 1603.67 168.02 o 4 15 0 57.37 235.41 148.86 o 5 15 0 296.88 444.62 203.40 o 6 15 0 569.01 801.76 169.07 o 0 16 0 981.74 684.44 156.19 o 1 16 0 43.63 111.68 81.16 o 2 16 0 504.19 501.05 145.43 o 3 16 0 291.97 258.13 99.97 o 4 16 0 8.85 -99.51 100.66 o 5 16 0 85.41 430.08 168.90 o 1 17 0 229.48 212.64 115.28 o 2 17 0 874.97 484.78 157.87 o 3 17 0 3.55 83.49 184.35 o 0 18 0 211.98 477.26 311.55 o -10 1 1 237.45 202.63 85.88 o -9 1 1 5529.63 5107.63 225.56 o -8 1 1 6.35 91.11 47.87 o -7 1 1 7.97 100.26 41.47 o -6 1 1 16.97 59.09 33.83 o -5 1 1 387.44 457.00 67.22 o -4 1 1 25142.60 25903.36 675.48 o -3 1 1 8131.44 8287.28 260.21 o -2 1 1 31257.30 31490.65 433.88 o -1 1 1 989.21 886.70 21.45 o 1 1 1 7479.23 7591.10 135.90 o 2 1 1 22882.15 23197.19 529.98 o 3 1 1 7288.45 7353.62 251.60 o 4 1 1 11376.93 11050.48 161.75 o 5 1 1 20.37 28.58 32.75 o 6 1 1 468.12 533.02 41.09 o 7 1 1 1246.44 1081.37 65.36 o 8 1 1 1102.46 966.15 117.28 o 9 1 1 2874.40 2700.78 157.47 o 10 1 1 123.44 17.63 76.87 o -10 2 1 335.66 471.74 109.87 o -9 2 1 2.19 43.54 57.70 o -8 2 1 5078.60 4952.12 184.84 o -7 2 1 1205.17 1048.40 59.44 o -6 2 1 863.70 925.03 49.81 o -5 2 1 15240.01 15260.29 268.52 o -4 2 1 6783.11 7676.74 124.38 o -3 2 1 1587.85 1581.78 41.61 o -2 2 1 49069.55 48798.50 1151.79 o -1 2 1 133.44 184.55 8.61 o 0 2 1 3123.08 3454.69 48.61 o 1 2 1 313.11 368.89 10.87 o 2 2 1 8131.71 9404.19 197.54 o 3 2 1 9751.75 10503.86 235.53 o 4 2 1 1452.06 1334.76 69.66 o 5 2 1 24010.36 24274.12 594.19 o 6 2 1 688.47 621.93 47.55 o 7 2 1 717.08 764.90 72.77 o 8 2 1 4714.94 4659.83 198.07 o 9 2 1 1078.40 1242.21 129.51 o 10 2 1 442.60 527.13 115.78 o -10 3 1 263.50 234.62 98.99 o -9 3 1 6163.41 5912.20 304.71 o -8 3 1 2.31 167.75 82.98 o -7 3 1 2177.28 2233.54 82.33 o -6 3 1 14.83 108.10 34.70 o -5 3 1 4925.30 5190.67 127.47 o -4 3 1 12948.68 12661.81 215.27 o -3 3 1 9407.46 9974.33 138.59 o -2 3 1 25877.74 26675.00 541.24 o -1 3 1 111.20 177.98 12.14 o 0 3 1 27853.68 28525.04 453.88 o 1 3 1 2674.55 2960.63 47.27 o 2 3 1 42420.31 41094.84 546.08 o 3 3 1 503.87 489.95 25.60 o 4 3 1 22227.59 24396.18 646.57 o 5 3 1 1363.38 1430.91 103.45 o 6 3 1 2150.90 2348.50 104.18 o 7 3 1 604.66 604.48 69.14 o 8 3 1 593.08 519.22 79.10 o 9 3 1 3039.31 3008.73 223.90 o 10 3 1 74.38 138.30 111.89 o -10 4 1 2.46 112.29 83.14 o -9 4 1 94.11 209.00 86.25 o -8 4 1 764.20 865.84 99.58 o -7 4 1 1945.34 2008.87 131.24 o -6 4 1 197.70 266.68 55.24 o -5 4 1 320.31 453.32 50.98 o -4 4 1 12947.42 13928.10 229.66 o -3 4 1 207.38 304.14 37.58 o -2 4 1 943.78 955.40 26.22 o -1 4 1 7737.20 8196.63 164.17 o 0 4 1 2321.43 2479.32 68.33 o 1 4 1 8138.84 8826.35 94.92 o 2 4 1 8386.76 8401.45 128.30 o 3 4 1 157.85 350.15 89.49 o 4 4 1 2747.98 2951.88 86.46 o 5 4 1 587.27 902.95 73.54 o 6 4 1 64.41 48.75 34.26 o 7 4 1 1288.04 1494.86 104.72 o 8 4 1 3.44 -35.38 58.08 o 9 4 1 35.45 102.39 66.02 o 10 4 1 35.02 175.14 122.67 o -10 5 1 16.72 -115.34 115.34 o -9 5 1 764.42 634.60 124.33 o -8 5 1 122.73 242.95 79.00 o -7 5 1 310.24 386.43 63.82 o -6 5 1 2677.35 2745.06 118.94 o -5 5 1 1992.72 2200.00 65.63 o -4 5 1 3177.43 3292.08 81.06 o -3 5 1 19614.31 20629.21 394.67 o -2 5 1 9473.60 9917.10 255.87 o -1 5 1 7680.41 7969.81 137.16 o 0 5 1 20566.31 21720.10 262.03 o 1 5 1 13.62 194.78 14.82 o 2 5 1 18828.70 19456.06 224.81 o 3 5 1 8084.53 8528.69 157.18 o 4 5 1 959.32 1078.10 45.62 o 5 5 1 2886.35 3128.51 146.27 o 6 5 1 1811.41 1932.77 96.79 o 7 5 1 466.57 429.96 75.97 o 8 5 1 220.04 373.29 73.94 o 9 5 1 1123.75 1078.23 140.61 o 10 5 1 34.60 43.36 86.87 o -10 6 1 1.96 -26.68 101.06 o -9 6 1 60.98 188.49 119.49 o -8 6 1 525.92 540.28 105.97 o -7 6 1 2.44 22.82 54.06 o -6 6 1 4610.64 4817.79 169.40 o -5 6 1 4214.72 4293.94 125.22 o -4 6 1 91.11 163.38 25.01 o -3 6 1 3633.69 3521.93 78.00 o -2 6 1 25754.21 27991.85 491.82 o -1 6 1 4566.12 4988.23 80.95 o 0 6 1 2824.56 3122.55 57.33 o 1 6 1 5711.44 6134.65 90.04 o 2 6 1 4328.95 4321.97 59.26 o 3 6 1 8301.61 7536.00 212.03 o 4 6 1 2140.86 2451.02 72.32 o 5 6 1 6514.73 6809.22 205.13 o 6 6 1 1088.44 1346.18 83.23 o 7 6 1 40.81 35.12 71.47 o 8 6 1 419.91 343.92 91.18 o 9 6 1 711.43 924.99 129.03 o 10 6 1 129.19 163.26 106.58 o -10 7 1 8.24 88.89 112.76 o -9 7 1 835.39 715.97 126.94 o -8 7 1 99.98 167.67 56.78 o -7 7 1 9703.29 10595.23 355.44 o -6 7 1 731.90 938.30 78.35 o -5 7 1 1346.56 1369.71 74.29 o -4 7 1 1731.32 1780.50 57.54 o -3 7 1 5142.18 5149.32 118.25 o -2 7 1 37061.73 38067.88 748.18 o -1 7 1 468.17 581.66 30.59 o 0 7 1 12579.71 12859.08 198.54 o 1 7 1 3.44 70.04 19.33 o 2 7 1 33034.20 33952.12 496.84 o 3 7 1 1976.65 2078.08 90.82 o 4 7 1 5765.98 5627.30 138.58 o 5 7 1 8.61 -27.45 27.45 o 6 7 1 5983.79 6344.32 196.15 o 7 7 1 4065.07 4689.52 256.66 o 8 7 1 435.58 534.00 115.89 o 9 7 1 421.55 404.30 131.71 o -9 8 1 835.88 907.14 140.15 o -8 8 1 1381.86 1220.67 224.16 o -7 8 1 1853.21 1981.65 122.84 o -6 8 1 10513.88 11427.86 473.84 o -5 8 1 1722.84 1815.88 94.38 o -4 8 1 2379.06 2566.49 82.65 o -3 8 1 4299.43 4088.67 110.38 o -2 8 1 239.20 322.32 33.91 o -1 8 1 669.17 721.38 34.12 o 0 8 1 859.27 858.82 37.07 o 1 8 1 417.41 337.89 26.44 o 2 8 1 3247.18 3195.61 77.92 o 3 8 1 5914.34 6068.03 142.51 o 4 8 1 3427.16 3087.39 161.34 o 5 8 1 619.74 783.98 111.15 o 6 8 1 1697.12 2088.90 169.84 o 7 8 1 5253.55 5989.06 377.67 o 8 8 1 89.32 122.33 93.75 o 9 8 1 310.31 582.68 161.09 o -9 9 1 1388.57 1485.09 211.71 o -8 9 1 4.36 -5.66 76.41 o -7 9 1 2948.76 3558.81 244.61 o -6 9 1 4528.62 4583.72 305.15 o -5 9 1 611.42 733.65 63.11 o -4 9 1 428.59 389.70 36.79 o -3 9 1 56.36 53.30 31.23 o -2 9 1 3478.95 3344.25 98.35 o -1 9 1 479.95 506.59 41.47 o 0 9 1 4411.98 4307.90 97.83 o 1 9 1 165.72 238.28 44.44 o 2 9 1 1170.63 1071.86 50.19 o 3 9 1 2669.91 2613.33 134.26 o 4 9 1 1383.87 1559.32 112.24 o 5 9 1 434.20 392.10 92.34 o 6 9 1 5141.10 5633.54 291.53 o 7 9 1 1813.59 2457.45 219.03 o 8 9 1 9.29 29.46 81.02 o 9 9 1 1003.33 1067.70 206.44 o -9 10 1 194.19 394.29 184.62 o -8 10 1 1875.83 1720.10 180.39 o -7 10 1 25.40 125.45 129.24 o -6 10 1 1021.24 1185.11 135.95 o -5 10 1 1991.68 2175.84 157.50 o -4 10 1 543.91 554.26 75.56 o -3 10 1 1985.25 1941.54 70.54 o -2 10 1 823.57 845.23 63.11 o -1 10 1 1822.44 1852.65 65.99 o 0 10 1 802.97 968.63 51.04 o 1 10 1 564.24 583.77 39.36 o 2 10 1 36.30 41.97 19.83 o 3 10 1 291.82 233.70 61.40 o 4 10 1 1420.90 1597.66 139.35 o 5 10 1 2746.55 2821.18 202.72 o 6 10 1 91.49 172.43 79.73 o 7 10 1 6.03 107.94 91.68 o 8 10 1 251.43 206.79 110.40 o -8 11 1 16.20 18.02 85.00 o -7 11 1 511.87 623.49 123.12 o -6 11 1 1152.67 1242.32 149.36 o -5 11 1 8333.86 8778.22 582.05 o -4 11 1 1929.11 2047.25 207.34 o -3 11 1 2101.19 2039.97 88.38 o -2 11 1 3384.24 3288.77 116.46 o -1 11 1 2314.50 2193.41 74.06 o 0 11 1 28571.31 27795.15 591.01 o 1 11 1 259.40 228.14 52.21 o 2 11 1 38.81 58.25 36.51 o 3 11 1 146.10 397.35 76.32 o 4 11 1 3983.54 4335.66 236.71 o 5 11 1 3096.60 3062.33 212.88 o 6 11 1 1876.93 1784.65 181.37 o 7 11 1 525.76 670.65 144.87 o 8 11 1 0.68 23.27 92.22 o -8 12 1 626.57 811.49 341.08 o -7 12 1 1399.03 1582.23 194.28 o -6 12 1 223.99 166.39 94.73 o -5 12 1 7.86 -21.37 70.30 o -4 12 1 15364.48 15878.80 640.48 o -3 12 1 67.72 176.92 75.95 o -2 12 1 2017.63 1973.36 78.72 o -1 12 1 10678.08 10160.36 250.38 o 0 12 1 1519.34 1494.70 73.17 o 1 12 1 10314.91 10111.26 278.91 o 2 12 1 2742.75 2859.30 124.61 o 3 12 1 55.02 -5.45 60.14 o 4 12 1 4391.25 4290.15 244.29 o 5 12 1 864.26 997.48 138.13 o 6 12 1 16.47 80.16 139.24 o 7 12 1 3354.92 3856.40 313.79 o 8 12 1 11.36 27.28 98.77 o -7 13 1 64.12 -105.94 105.94 o -6 13 1 1410.66 1629.39 172.00 o -5 13 1 4007.74 4263.22 276.65 o -4 13 1 499.05 639.71 110.65 o -3 13 1 1247.95 1220.54 90.21 o -2 13 1 82.63 134.18 41.15 o -1 13 1 3355.72 3265.55 120.60 o 0 13 1 17021.11 15806.37 387.29 o 1 13 1 5.49 119.97 52.15 o 2 13 1 118.22 363.79 57.29 o 3 13 1 2815.92 3051.82 213.34 o 4 13 1 3382.16 3321.23 236.27 o 5 13 1 1579.97 1695.47 179.22 o 6 13 1 1891.54 1982.17 230.69 o 7 13 1 176.46 297.96 130.04 o -6 14 1 332.06 188.81 106.01 o -5 14 1 440.47 753.67 147.79 o -4 14 1 1066.33 1317.13 204.97 o -3 14 1 418.99 479.34 106.86 o -2 14 1 43.56 59.87 53.91 o -1 14 1 586.18 623.66 80.10 o 0 14 1 4.38 109.61 53.86 o 1 14 1 685.97 842.14 85.71 o 2 14 1 85.11 179.92 85.99 o 3 14 1 431.72 475.26 111.94 o 4 14 1 4.24 125.26 85.29 o 5 14 1 2.89 -26.06 79.81 o 6 14 1 199.28 169.26 127.47 o -6 15 1 919.74 1065.60 184.02 o -5 15 1 53.67 111.43 94.54 o -4 15 1 581.67 781.76 143.64 o -3 15 1 221.52 103.62 89.43 o -2 15 1 1263.66 1063.09 101.56 o -1 15 1 182.64 108.49 74.11 o 0 15 1 2133.83 1852.13 140.06 o 1 15 1 374.93 410.90 79.62 o 2 15 1 1437.51 1399.89 144.79 o 3 15 1 505.35 611.19 119.19 o 4 15 1 158.90 393.81 123.70 o 5 15 1 334.47 352.74 124.70 o -5 16 1 124.11 211.56 113.58 o -4 16 1 954.45 764.69 150.42 o -3 16 1 1321.67 1377.52 218.01 o -2 16 1 90.73 54.00 99.76 o -1 16 1 57.67 56.08 74.73 o 0 16 1 17.17 -25.00 101.81 o 1 16 1 832.76 830.91 151.92 o 2 16 1 993.01 1255.16 166.93 o 3 16 1 688.59 736.46 147.41 o 4 16 1 454.23 463.92 138.00 o -3 17 1 443.84 1446.08 666.55 o -2 17 1 2431.55 2373.98 275.47 o -1 17 1 69.65 29.99 87.79 o 0 17 1 1260.99 1274.31 200.40 o 1 17 1 57.07 21.40 99.64 o 2 17 1 3362.23 3253.42 321.94 o 3 17 1 1.43 60.23 123.82 o 0 18 1 0.36 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