#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/66/2226665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226665_Fobs loop_ _publ_author_name 'Gayathri, P.' 'Jayabharathi, J.' 'Srinivasan, N.' 'Thiruvalluvar, A.' 'Butcher, R. J.' _publ_section_title ; 2-(4-Fluorophenyl)-4,5-dimethyl-1-(4-methylphenyl)-1H-imidazole ; _journal_coeditor_code SI2269 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1703 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.915 _cell_angle_gamma 90.000 _cell_length_a 9.8888 _cell_length_b 7.6693 _cell_length_c 20.1017 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7895 _[local]_cod_data_source_file si2269Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bi2 in P 21/n Z=4 C18H17FN2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2293.46 2265.89 7.21 o 4 0 0 442.67 527.60 4.86 o 6 0 0 1170.80 1309.60 73.84 o 8 0 0 6.95 5.55 0.77 o 10 0 0 3.06 4.69 0.55 o 12 0 0 3.70 3.23 0.55 o 1 1 0 27.76 30.86 0.87 o 2 1 0 3400.65 3532.53 10.17 o 3 1 0 19.58 23.81 0.86 o 4 1 0 226.43 228.79 7.21 o 5 1 0 0.23 0.68 0.39 o 6 1 0 99.36 105.59 2.08 o 7 1 0 150.38 152.26 8.94 o 8 1 0 450.59 449.13 2.83 o 9 1 0 5.69 6.78 0.55 o 10 1 0 1.40 0.69 0.42 o 11 1 0 6.78 8.26 0.53 o 12 1 0 2.91 3.81 0.33 o 1 2 0 524.24 492.94 4.03 o 2 2 0 1945.44 1880.46 27.40 o 3 2 0 468.46 493.88 39.25 o 4 2 0 576.13 712.33 32.23 o 5 2 0 66.42 53.09 1.41 o 6 2 0 345.90 351.25 8.68 o 7 2 0 8.46 6.45 1.64 o 8 2 0 0.30 -0.17 0.62 o 9 2 0 0.00 0.07 0.65 o 10 2 0 0.21 0.60 0.53 o 11 2 0 2.02 1.59 0.33 o 12 2 0 0.70 0.55 0.26 o 1 3 0 5.79 7.28 0.85 o 2 3 0 518.82 531.03 5.60 o 3 3 0 244.80 253.97 2.64 o 4 3 0 6.50 3.60 0.84 o 5 3 0 52.13 40.08 2.07 o 6 3 0 133.27 141.67 4.02 o 7 3 0 83.82 78.76 1.49 o 8 3 0 83.33 78.96 1.78 o 9 3 0 29.92 32.80 0.97 o 10 3 0 24.05 24.92 0.81 o 11 3 0 0.27 0.17 0.29 o 0 4 0 1512.44 1537.83 9.37 o 1 4 0 7.99 7.97 1.05 o 2 4 0 602.44 611.78 4.62 o 3 4 0 262.48 271.86 12.07 o 4 4 0 109.24 102.79 3.45 o 5 4 0 48.26 46.55 2.47 o 6 4 0 32.59 29.95 0.75 o 7 4 0 4.80 5.11 0.73 o 8 4 0 0.49 -0.34 0.57 o 9 4 0 0.19 0.04 0.50 o 10 4 0 0.87 0.70 0.41 o 11 4 0 0.58 0.51 0.42 o 1 5 0 80.75 70.81 2.43 o 2 5 0 19.82 14.80 0.98 o 3 5 0 26.17 33.26 1.33 o 4 5 0 3.88 5.73 1.68 o 5 5 0 10.16 10.77 0.46 o 6 5 0 36.99 39.37 0.94 o 7 5 0 84.44 81.76 1.85 o 8 5 0 64.47 66.79 1.86 o 9 5 0 2.64 3.66 0.47 o 10 5 0 0.49 0.04 0.28 o 0 6 0 1.60 1.09 1.59 o 1 6 0 448.05 427.90 19.91 o 2 6 0 64.27 59.58 0.92 o 3 6 0 17.61 17.84 0.56 o 4 6 0 1.60 0.86 0.35 o 5 6 0 2.75 4.15 0.41 o 6 6 0 2.02 2.00 0.67 o 7 6 0 26.68 30.40 1.17 o 8 6 0 3.33 3.88 0.64 o 9 6 0 0.24 0.27 0.28 o 1 7 0 18.43 17.34 0.71 o 2 7 0 15.33 14.07 0.55 o 3 7 0 0.01 -0.17 0.35 o 4 7 0 2.36 1.70 0.47 o 5 7 0 0.48 0.61 0.61 o 6 7 0 7.35 7.79 0.75 o 7 7 0 17.82 17.50 0.81 o 8 7 0 0.05 0.10 0.36 o 0 8 0 4.23 3.89 0.64 o 1 8 0 11.62 10.10 0.54 o 2 8 0 0.14 0.41 0.43 o 3 8 0 0.20 0.10 0.43 o 4 8 0 4.66 5.09 0.67 o 5 8 0 0.11 -0.05 0.53 o 6 8 0 0.45 0.71 0.45 o 7 8 0 4.91 5.66 0.36 o 1 9 0 0.00 0.08 0.31 o 2 9 0 7.80 7.89 0.41 o 3 9 0 1.58 1.98 0.24 o 4 9 0 0.30 0.24 0.17 o -11 0 1 0.04 -0.09 0.64 o -9 0 1 104.94 92.34 3.15 o -7 0 1 61.61 71.77 2.80 o -5 0 1 350.39 378.95 22.84 o -3 0 1 46.13 36.98 1.95 o 3 0 1 884.30 773.42 4.96 o 5 0 1 15.37 13.79 0.71 o 7 0 1 625.29 629.29 7.50 o 9 0 1 265.70 265.32 3.24 o 11 0 1 7.41 8.27 0.79 o -12 1 1 4.85 5.23 0.33 o -11 1 1 23.85 27.17 1.26 o -10 1 1 6.63 7.49 0.52 o -9 1 1 723.91 732.90 3.11 o -8 1 1 3.82 4.88 0.80 o -7 1 1 341.90 379.24 14.10 o -6 1 1 43.16 40.86 1.60 o -5 1 1 221.09 237.96 2.81 o -4 1 1 0.32 0.02 0.25 o -3 1 1 4.34 1.07 0.77 o -2 1 1 15.64 16.43 0.55 o -1 1 1 7721.88 6628.19 79.86 o 0 1 1 129.51 117.61 0.85 o 1 1 1 271.39 260.12 2.39 o 2 1 1 0.12 0.72 0.18 o 3 1 1 280.18 297.56 1.36 o 4 1 1 28.55 26.22 0.67 o 5 1 1 129.27 135.78 4.52 o 6 1 1 46.49 44.81 1.38 o 7 1 1 6.08 8.59 3.15 o 8 1 1 53.43 50.49 1.00 o 9 1 1 2.89 4.50 0.55 o 10 1 1 22.56 23.60 0.70 o 11 1 1 13.85 13.99 0.64 o 12 1 1 2.39 1.97 0.25 o -12 2 1 8.14 8.22 0.37 o -11 2 1 1.77 2.20 0.47 o -10 2 1 61.86 68.35 2.88 o -9 2 1 41.37 37.63 1.05 o -8 2 1 96.46 88.93 1.80 o -7 2 1 36.56 36.67 1.51 o -6 2 1 46.56 42.26 1.78 o -5 2 1 157.63 161.74 3.67 o -4 2 1 228.08 242.88 5.23 o -3 2 1 11.11 9.83 0.57 o -2 2 1 162.85 146.59 2.56 o -1 2 1 6551.80 6373.28 62.31 o 0 2 1 5579.28 4916.72 42.47 o 1 2 1 37.77 46.96 1.35 o 2 2 1 1085.94 1075.05 6.97 o 3 2 1 121.51 111.13 1.15 o 4 2 1 375.77 445.85 14.38 o 5 2 1 0.01 1.21 0.55 o 6 2 1 40.64 40.09 1.34 o 7 2 1 57.89 54.02 2.57 o 8 2 1 16.69 18.84 1.06 o 9 2 1 19.22 19.93 1.04 o 10 2 1 41.20 40.78 1.12 o 11 2 1 21.21 25.92 0.70 o 12 2 1 2.04 1.81 0.26 o -11 3 1 5.56 5.59 0.48 o -10 3 1 4.06 4.14 0.82 o -9 3 1 286.13 291.05 5.05 o -8 3 1 89.12 78.42 1.74 o -7 3 1 49.00 50.94 1.84 o -6 3 1 12.29 17.41 1.01 o -5 3 1 22.14 16.79 1.48 o -4 3 1 0.10 3.85 1.40 o -3 3 1 485.45 528.53 3.79 o -2 3 1 920.24 955.96 6.69 o -1 3 1 0.05 0.54 0.55 o 0 3 1 117.34 123.34 1.58 o 1 3 1 1744.31 1659.85 9.29 o 2 3 1 6.54 17.11 1.26 o 3 3 1 25.79 35.69 1.08 o 4 3 1 100.38 111.81 3.18 o 5 3 1 81.66 76.69 2.81 o 6 3 1 14.73 13.47 1.60 o 7 3 1 0.02 0.57 1.67 o 8 3 1 10.21 13.18 0.91 o 9 3 1 10.63 9.48 0.83 o 10 3 1 0.17 0.11 0.49 o 11 3 1 4.78 3.77 0.32 o -11 4 1 7.26 6.43 0.53 o -10 4 1 4.55 3.09 0.44 o -9 4 1 80.08 91.27 1.39 o -8 4 1 41.74 37.42 1.04 o -7 4 1 1.34 0.89 0.69 o -6 4 1 62.10 60.04 1.34 o -5 4 1 1.08 2.39 1.60 o -4 4 1 64.18 58.03 2.60 o -3 4 1 39.46 24.18 1.07 o -2 4 1 152.78 165.41 2.77 o -1 4 1 404.44 430.82 5.01 o 0 4 1 633.46 603.90 4.20 o 1 4 1 576.66 572.44 6.14 o 2 4 1 912.94 957.78 8.61 o 3 4 1 12.93 12.38 0.87 o 4 4 1 523.52 571.92 7.70 o 5 4 1 11.59 9.22 1.56 o 6 4 1 36.31 38.59 1.11 o 7 4 1 2.17 0.94 0.67 o 8 4 1 17.84 19.14 1.04 o 9 4 1 0.34 0.13 0.49 o 10 4 1 35.42 37.29 0.83 o 11 4 1 6.11 6.58 0.50 o -10 5 1 1.15 1.17 0.30 o -9 5 1 1.91 2.61 1.08 o -8 5 1 27.50 23.13 0.82 o -7 5 1 41.99 38.38 1.34 o -6 5 1 7.45 8.99 0.47 o -5 5 1 4.70 5.68 0.39 o -4 5 1 10.45 6.92 1.39 o -3 5 1 13.72 17.28 0.99 o -2 5 1 11.77 11.37 0.88 o -1 5 1 12.04 9.17 0.77 o 0 5 1 98.79 85.37 1.79 o 1 5 1 236.39 216.99 4.33 o 2 5 1 74.02 60.10 6.31 o 3 5 1 57.23 64.85 3.48 o 4 5 1 7.55 7.30 1.72 o 5 5 1 15.50 12.16 0.50 o 6 5 1 0.09 1.05 0.70 o 7 5 1 0.31 1.16 0.73 o 8 5 1 6.53 9.42 0.64 o 9 5 1 58.12 64.59 1.03 o 10 5 1 0.03 0.26 0.29 o -9 6 1 11.63 9.74 0.39 o -8 6 1 14.76 15.32 0.82 o -7 6 1 1.91 1.47 0.66 o -6 6 1 11.40 8.42 0.78 o -5 6 1 9.41 8.95 0.49 o -4 6 1 9.57 10.60 0.48 o -3 6 1 0.57 1.40 0.36 o -2 6 1 20.92 20.49 1.14 o -1 6 1 114.76 111.20 3.50 o 0 6 1 325.16 289.76 5.66 o 1 6 1 34.53 31.61 1.17 o 2 6 1 2.13 1.36 0.47 o 3 6 1 1.16 0.39 0.84 o 4 6 1 17.94 18.13 0.58 o 5 6 1 6.28 5.15 0.58 o 6 6 1 13.57 12.68 0.89 o 7 6 1 7.49 8.75 0.79 o 8 6 1 6.43 4.65 0.64 o 9 6 1 0.16 0.22 0.27 o -8 7 1 0.74 0.66 0.27 o -7 7 1 1.28 1.29 0.52 o -6 7 1 0.42 0.87 0.57 o -5 7 1 10.52 8.68 0.57 o -4 7 1 3.66 3.62 0.43 o -3 7 1 15.30 14.22 0.54 o -2 7 1 2.05 2.44 0.39 o -1 7 1 45.80 44.91 1.25 o 0 7 1 28.41 27.55 0.66 o 1 7 1 19.19 18.00 0.71 o 2 7 1 18.66 15.44 0.55 o 3 7 1 4.50 4.28 0.43 o 4 7 1 0.11 0.20 0.39 o 5 7 1 4.88 3.79 0.70 o 6 7 1 4.18 5.52 0.71 o 7 7 1 4.09 6.21 0.64 o 8 7 1 3.07 3.75 0.46 o -7 8 1 0.76 0.61 0.28 o -6 8 1 0.59 -0.02 0.39 o -5 8 1 2.37 2.30 0.53 o -4 8 1 0.96 1.57 0.44 o -3 8 1 3.45 2.66 0.48 o -2 8 1 9.06 9.78 0.57 o -1 8 1 26.11 27.52 1.02 o 0 8 1 7.88 8.88 0.44 o 1 8 1 0.11 0.16 0.33 o 2 8 1 0.69 0.81 0.44 o 3 8 1 2.23 2.08 0.51 o 4 8 1 7.07 7.38 0.74 o 5 8 1 12.56 12.16 0.75 o 6 8 1 0.03 -0.06 0.46 o 7 8 1 3.39 3.91 0.33 o -4 9 1 0.65 0.84 0.37 o -3 9 1 0.05 0.14 0.23 o -2 9 1 3.62 4.70 0.38 o -1 9 1 0.05 0.28 0.30 o 0 9 1 6.99 9.72 0.35 o 1 9 1 6.23 6.99 0.42 o 2 9 1 0.37 0.61 0.41 o 3 9 1 0.20 0.03 0.22 o 4 9 1 0.41 0.45 0.17 o -12 0 2 4.29 4.40 0.41 o -10 0 2 31.79 32.62 1.48 o -8 0 2 11.65 6.51 1.88 o -6 0 2 52.65 33.87 1.86 o -4 0 2 3115.83 3437.46 13.57 o -2 0 2 256.10 256.35 2.05 o 2 0 2 78.11 62.44 1.19 o 4 0 2 129.79 126.60 2.37 o 6 0 2 44.94 58.59 2.85 o 8 0 2 458.70 403.14 3.90 o 10 0 2 55.84 47.37 2.69 o 12 0 2 6.14 6.11 0.57 o -12 1 2 6.13 7.34 0.35 o -11 1 2 5.68 4.89 0.56 o -10 1 2 0.49 -0.49 0.62 o -9 1 2 74.91 79.08 1.58 o -8 1 2 220.60 244.94 3.21 o -7 1 2 7.64 8.76 1.79 o -6 1 2 983.36 999.70 16.37 o -5 1 2 1.15 1.06 0.57 o -4 1 2 175.18 160.40 2.01 o -3 1 2 134.66 140.42 2.22 o -2 1 2 126.34 116.36 2.01 o -1 1 2 890.52 854.26 5.83 o 0 1 2 626.15 573.47 6.96 o 1 1 2 682.68 675.90 4.07 o 2 1 2 4629.64 4972.59 79.89 o 3 1 2 15.57 17.33 0.63 o 4 1 2 81.49 86.44 2.11 o 5 1 2 13.67 16.97 0.65 o 6 1 2 0.35 0.29 0.81 o 7 1 2 5.07 5.89 1.19 o 8 1 2 886.33 819.46 8.45 o 9 1 2 10.56 9.23 0.62 o 10 1 2 52.98 54.67 4.36 o 11 1 2 19.05 19.67 0.90 o 12 1 2 0.38 0.45 0.22 o -12 2 2 0.49 0.21 0.28 o -11 2 2 13.02 12.53 0.52 o -10 2 2 76.29 80.11 2.26 o -9 2 2 47.22 54.54 5.42 o -8 2 2 0.40 1.54 0.77 o -7 2 2 54.85 63.23 1.84 o -6 2 2 43.70 35.46 1.53 o -5 2 2 27.98 18.60 1.50 o -4 2 2 1140.33 1288.28 19.69 o -3 2 2 1562.16 1530.45 9.84 o -2 2 2 414.34 361.39 6.40 o -1 2 2 3804.63 3493.81 16.42 o 0 2 2 6051.12 5690.46 14.22 o 1 2 2 34.16 29.86 1.15 o 2 2 2 398.74 424.64 4.51 o 3 2 2 504.36 539.59 4.61 o 4 2 2 70.32 84.12 1.61 o 5 2 2 121.61 135.95 3.37 o 6 2 2 2.31 2.11 1.17 o 7 2 2 60.39 56.38 2.60 o 8 2 2 314.57 282.52 4.39 o 9 2 2 28.86 25.47 1.13 o 10 2 2 51.71 49.40 1.08 o 11 2 2 0.01 -0.04 0.40 o 12 2 2 0.15 0.08 0.31 o -11 3 2 6.07 6.28 0.48 o -10 3 2 2.93 3.79 0.97 o -9 3 2 301.59 327.52 10.52 o -8 3 2 269.72 264.14 2.42 o -7 3 2 0.14 -0.10 1.49 o -6 3 2 43.12 43.25 2.39 o -5 3 2 2.55 -0.79 1.12 o -4 3 2 2.19 1.75 0.58 o -3 3 2 61.39 65.81 2.72 o -2 3 2 104.86 110.56 1.75 o -1 3 2 103.54 107.20 1.63 o 0 3 2 137.84 155.28 2.50 o 1 3 2 590.90 538.33 5.40 o 2 3 2 0.37 0.61 0.73 o 3 3 2 213.35 209.13 5.42 o 4 3 2 85.43 83.46 2.81 o 5 3 2 164.51 166.98 4.13 o 6 3 2 22.37 23.71 1.91 o 7 3 2 55.13 51.04 1.27 o 8 3 2 135.61 118.36 2.17 o 9 3 2 10.25 8.09 0.80 o 10 3 2 43.81 47.33 1.72 o 11 3 2 16.18 18.57 0.50 o -11 4 2 0.21 0.09 0.44 o -10 4 2 0.09 0.06 0.71 o -9 4 2 0.57 0.66 0.50 o -8 4 2 134.57 137.68 1.78 o -7 4 2 3.88 3.51 0.57 o -6 4 2 71.62 68.83 3.72 o -5 4 2 1.84 4.37 1.51 o -4 4 2 69.70 73.30 4.23 o -3 4 2 200.82 200.53 7.00 o -2 4 2 115.28 104.40 2.29 o -1 4 2 843.21 822.51 14.07 o 0 4 2 1299.65 1332.66 6.07 o 1 4 2 1.94 4.16 1.05 o 2 4 2 101.50 82.62 2.69 o 3 4 2 90.28 97.26 2.19 o 4 4 2 8.34 7.93 1.26 o 5 4 2 93.85 102.14 3.52 o 6 4 2 0.54 1.41 0.73 o 7 4 2 2.74 2.52 0.70 o 8 4 2 2.62 3.15 0.74 o 9 4 2 7.22 7.35 0.62 o 10 4 2 9.01 11.66 0.58 o 11 4 2 9.38 10.02 0.51 o -10 5 2 0.42 -0.19 0.46 o -9 5 2 61.32 65.60 0.82 o -8 5 2 29.16 29.87 0.88 o -7 5 2 18.30 19.62 1.04 o -6 5 2 7.71 8.99 0.46 o -5 5 2 21.57 19.60 0.56 o -4 5 2 15.60 16.35 1.72 o -3 5 2 3.19 3.49 0.93 o -2 5 2 21.62 28.75 1.38 o -1 5 2 29.16 20.85 1.07 o 0 5 2 28.92 22.64 1.27 o 1 5 2 6.08 8.85 1.11 o 2 5 2 7.19 7.71 0.83 o 3 5 2 0.45 0.88 1.13 o 4 5 2 1.50 1.83 1.83 o 5 5 2 14.25 13.24 0.63 o 6 5 2 11.91 12.27 0.87 o 7 5 2 52.30 40.70 1.38 o 8 5 2 0.00 0.41 0.48 o 9 5 2 6.67 4.68 0.58 o 10 5 2 22.79 22.64 1.19 o -9 6 2 2.51 3.61 0.31 o -8 6 2 32.60 34.08 1.04 o -7 6 2 0.00 0.64 0.65 o -6 6 2 44.10 37.73 0.94 o -5 6 2 0.40 0.20 0.34 o -4 6 2 1.73 1.77 0.39 o -3 6 2 0.09 0.79 0.34 o -2 6 2 0.22 0.06 1.26 o -1 6 2 89.12 79.47 3.12 o 0 6 2 189.60 174.62 4.44 o 1 6 2 26.13 23.76 0.79 o 2 6 2 15.02 13.72 0.45 o 3 6 2 98.86 90.49 1.84 o 4 6 2 4.30 3.77 0.53 o 5 6 2 2.46 1.17 0.62 o 6 6 2 6.02 5.94 0.79 o 7 6 2 8.42 7.18 0.80 o 8 6 2 0.16 0.69 0.54 o 9 6 2 0.72 0.95 0.26 o -8 7 2 0.31 0.17 0.26 o -7 7 2 16.69 15.21 0.74 o -6 7 2 2.53 1.46 0.60 o -5 7 2 23.62 22.78 0.62 o -4 7 2 13.22 11.74 0.53 o -3 7 2 0.12 0.66 0.51 o -2 7 2 10.12 11.03 0.86 o -1 7 2 47.52 50.57 1.48 o 0 7 2 61.73 64.11 2.37 o 1 7 2 19.65 17.64 0.95 o 2 7 2 23.70 22.33 0.77 o 3 7 2 7.71 8.81 0.91 o 4 7 2 1.52 1.20 0.43 o 5 7 2 0.28 0.52 0.61 o 6 7 2 13.93 14.92 0.88 o 7 7 2 25.82 21.77 0.87 o 8 7 2 1.60 0.75 0.25 o -7 8 2 2.27 2.69 0.31 o -6 8 2 3.77 3.26 0.48 o -5 8 2 0.38 -0.16 0.50 o -4 8 2 1.01 0.99 0.43 o -3 8 2 5.42 5.21 0.49 o -2 8 2 14.83 15.32 0.52 o -1 8 2 12.12 11.21 0.48 o 0 8 2 13.21 12.23 0.47 o 1 8 2 0.08 0.18 0.32 o 2 8 2 4.38 3.59 0.54 o 3 8 2 0.18 -0.02 0.58 o 4 8 2 0.31 0.23 0.57 o 5 8 2 2.36 2.16 0.60 o 6 8 2 11.82 13.11 0.64 o -4 9 2 6.66 7.92 0.46 o -3 9 2 0.20 0.12 0.31 o -2 9 2 0.93 1.07 0.32 o -1 9 2 3.54 4.96 0.31 o 0 9 2 0.02 0.27 0.24 o 1 9 2 0.03 -0.17 0.31 o 2 9 2 4.06 3.82 0.35 o 3 9 2 0.04 0.04 0.25 o 4 9 2 0.45 0.60 0.17 o -11 0 3 6.61 6.19 0.57 o -9 0 3 2.33 2.97 1.05 o -7 0 3 80.85 96.83 3.33 o -5 0 3 42.11 64.19 2.18 o -3 0 3 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