#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:42:37 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181187 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/66/2226680.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226680_Fobs loop_ _publ_author_name 'Alagha, Ahmed B. M.' 'Gaynor, Declan' 'M\"uller-Bunz, Helge' 'Nolan, Kevin B.' 'Parthasarathi, Laavanya' _publ_section_title ; fac-Tris(4-aminobenzohydroxamato)iron(III) ethanol solvate ; _journal_coeditor_code SJ5023 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m853 _journal_page_last m854 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 107.550 _cell_angle_beta 91.085 _cell_angle_gamma 112.217 _cell_length_a 10.6232 _cell_length_b 10.6455 _cell_length_c 13.2253 _exptl_crystal_F_000 578.00 _reflns_d_resolution_high 0.7799 _cod_data_source_file sj5023Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nol36 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 152.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3818.94 4238.11 39.51 o 2 0 0 58.07 61.30 3.80 o 3 0 0 1753.30 1730.71 20.97 o 4 0 0 8077.53 8115.23 79.02 o 5 0 0 488.92 510.17 12.43 o 6 0 0 67.45 45.07 5.29 o 7 0 0 2520.84 2495.25 34.49 o 8 0 0 1442.45 1334.42 27.57 o 9 0 0 121.63 127.63 10.53 o 10 0 0 443.50 460.06 23.13 o 11 0 0 737.22 758.28 33.61 o 12 0 0 162.38 169.81 20.56 o -12 1 0 351.52 330.06 29.33 o -11 1 0 30.03 37.65 8.72 o -10 1 0 37.95 62.77 9.38 o -9 1 0 196.48 197.00 17.53 o -8 1 0 196.72 198.92 10.69 o -7 1 0 188.32 225.81 10.51 o -6 1 0 1948.80 1825.72 25.82 o -5 1 0 246.27 198.41 7.65 o -4 1 0 85.32 100.31 5.58 o -3 1 0 1623.65 1739.16 20.29 o -2 1 0 624.09 582.19 9.53 o -1 1 0 806.59 829.01 10.68 o 0 1 0 6211.80 6764.98 67.77 o 1 1 0 672.39 631.12 9.83 o 2 1 0 119.25 93.55 4.16 o 3 1 0 1.21 4.27 2.46 o 4 1 0 103.16 71.91 5.16 o 5 1 0 252.56 264.66 9.46 o 6 1 0 88.40 105.35 7.08 o 7 1 0 299.10 298.80 13.76 o 8 1 0 1218.92 1222.40 23.76 o 9 1 0 11.89 1.99 5.59 o 10 1 0 0.18 17.63 6.42 o 11 1 0 556.98 555.16 40.40 o 12 1 0 101.96 165.11 32.64 o -13 2 0 245.49 256.35 24.25 o -12 2 0 83.95 80.49 10.83 o -11 2 0 329.35 294.75 19.32 o -10 2 0 1111.89 1029.42 29.28 o -9 2 0 243.93 206.46 14.50 o -8 2 0 707.03 666.20 23.24 o -7 2 0 1.34 10.82 3.27 o -6 2 0 1998.53 1921.39 26.12 o -5 2 0 265.08 255.90 7.59 o -3 2 0 664.00 567.85 11.11 o -2 2 0 5568.72 6197.34 58.77 o -1 2 0 1252.02 1448.58 16.48 o 0 2 0 3476.22 3920.50 41.76 o 1 2 0 2699.83 2691.52 31.98 o 2 2 0 22.02 6.80 2.39 o 3 2 0 68.46 48.44 3.96 o 4 2 0 4.47 12.54 4.15 o 5 2 0 21.15 19.46 4.92 o 6 2 0 1132.66 1111.60 20.76 o 7 2 0 102.07 111.73 8.15 o 8 2 0 408.91 420.88 21.14 o 9 2 0 50.28 53.04 8.94 o 10 2 0 57.44 40.42 8.56 o 11 2 0 16.85 26.41 10.02 o -13 3 0 30.52 36.44 9.79 o -12 3 0 163.32 159.51 14.81 o -11 3 0 218.09 253.86 18.14 o -10 3 0 1310.87 1366.29 34.50 o -9 3 0 109.07 111.21 12.30 o -8 3 0 1665.84 1649.71 29.81 o -7 3 0 907.86 914.27 23.92 o -6 3 0 93.22 107.84 4.69 o -5 3 0 9.27 23.62 4.34 o -4 3 0 208.43 173.02 7.85 o -3 3 0 358.07 396.62 7.81 o -2 3 0 334.93 339.80 7.42 o -1 3 0 67.35 68.88 3.99 o 0 3 0 300.79 343.53 7.24 o 1 3 0 113.25 108.33 6.61 o 2 3 0 13.08 18.15 2.88 o 3 3 0 362.52 343.56 10.63 o 4 3 0 326.28 355.79 10.33 o 5 3 0 57.04 56.38 5.57 o 6 3 0 2039.95 1966.41 34.63 o 7 3 0 290.59 285.65 15.09 o 8 3 0 1.47 10.32 5.99 o 9 3 0 16.08 15.90 7.49 o 10 3 0 122.25 145.38 17.13 o -13 4 0 0.46 0.14 7.52 o -12 4 0 58.82 75.10 10.93 o -11 4 0 41.07 42.76 8.45 o -10 4 0 1.98 3.96 5.73 o -9 4 0 2343.13 2165.53 37.33 o -8 4 0 50.60 52.98 6.48 o -7 4 0 1122.76 1114.67 22.55 o -6 4 0 239.17 222.24 10.42 o -5 4 0 152.23 157.78 8.48 o -4 4 0 133.98 174.76 9.73 o -3 4 0 601.25 539.31 10.59 o -2 4 0 139.40 126.59 7.13 o -1 4 0 266.10 302.64 7.53 o 0 4 0 4400.54 4470.31 46.56 o 1 4 0 10.97 8.40 3.23 o 2 4 0 703.10 782.85 14.09 o 3 4 0 141.09 130.45 6.53 o 4 4 0 1354.05 1385.91 22.13 o 5 4 0 1640.65 1561.66 29.84 o 6 4 0 1469.41 1446.69 30.71 o 7 4 0 120.10 127.79 19.03 o 8 4 0 15.06 22.00 8.05 o 9 4 0 5.80 -0.48 7.39 o 10 4 0 15.08 15.85 10.29 o -13 5 0 456.38 445.73 30.56 o -12 5 0 22.84 12.21 10.12 o -11 5 0 56.97 67.34 10.70 o -10 5 0 59.84 78.61 10.51 o -9 5 0 2379.43 2327.69 39.63 o -8 5 0 192.12 168.00 13.70 o -7 5 0 118.43 93.47 8.10 o -6 5 0 205.69 187.02 10.27 o -5 5 0 398.08 371.10 12.29 o -4 5 0 1733.90 1842.84 24.90 o -3 5 0 1495.23 1518.15 21.74 o -2 5 0 236.09 206.18 7.74 o -1 5 0 3703.02 3862.47 45.33 o 0 5 0 3478.95 3677.01 41.27 o 1 5 0 1670.33 1756.11 27.94 o 2 5 0 1892.13 1838.37 25.41 o 3 5 0 11.05 27.31 3.47 o 4 5 0 1383.92 1356.57 27.12 o 5 5 0 404.25 349.72 19.42 o 6 5 0 1.15 -1.55 4.82 o 7 5 0 377.59 355.86 21.23 o 8 5 0 468.54 486.98 31.60 o 9 5 0 137.31 135.32 18.43 o -13 6 0 3.32 4.63 10.78 o -12 6 0 176.56 164.00 21.52 o -11 6 0 368.46 360.06 25.49 o -10 6 0 63.23 66.99 10.25 o -9 6 0 1637.60 1555.01 33.23 o -8 6 0 2290.50 2156.85 46.66 o -7 6 0 26.35 23.50 5.07 o -6 6 0 577.38 520.95 15.15 o -5 6 0 3330.13 3299.18 40.00 o -4 6 0 628.59 608.52 13.32 o -3 6 0 1483.63 1507.36 22.91 o -2 6 0 364.35 369.31 10.24 o -1 6 0 2465.75 2408.13 31.01 o 0 6 0 5.12 11.20 2.81 o 1 6 0 492.50 484.93 11.25 o 2 6 0 1913.14 1777.66 36.92 o 3 6 0 826.67 804.39 41.88 o 4 6 0 882.57 855.48 26.24 o 5 6 0 121.55 141.60 16.04 o 6 6 0 432.86 439.56 27.06 o 7 6 0 0.80 -7.28 8.72 o 8 6 0 75.56 107.35 20.89 o -13 7 0 13.83 10.65 10.15 o -12 7 0 127.49 140.46 24.74 o -11 7 0 515.11 504.47 23.97 o -10 7 0 4.37 13.59 6.23 o -9 7 0 32.03 20.83 7.88 o -8 7 0 1570.15 1435.50 29.31 o -7 7 0 712.36 637.27 19.16 o -6 7 0 1.64 1.75 4.02 o -5 7 0 279.84 292.92 11.47 o -4 7 0 1247.32 1252.13 21.72 o -3 7 0 1987.68 2010.39 29.11 o -2 7 0 866.62 918.58 17.43 o -1 7 0 758.91 689.32 17.45 o 0 7 0 150.70 136.55 9.19 o 1 7 0 130.87 107.94 10.30 o 2 7 0 133.91 157.59 13.23 o 3 7 0 490.98 489.36 23.10 o 4 7 0 33.73 50.12 8.70 o 5 7 0 77.44 97.82 11.89 o 6 7 0 249.48 309.57 22.03 o 7 7 0 43.23 32.41 10.84 o -13 8 0 47.35 63.24 26.59 o -12 8 0 12.84 1.80 15.12 o -11 8 0 98.77 95.71 14.81 o -10 8 0 56.81 50.32 7.96 o -9 8 0 52.86 53.33 7.77 o -8 8 0 945.05 871.11 23.19 o -7 8 0 899.72 869.75 22.57 o -6 8 0 67.90 75.37 7.95 o -5 8 0 31.78 30.19 6.11 o -4 8 0 106.31 111.36 7.72 o -3 8 0 184.73 187.07 11.56 o -2 8 0 497.27 504.34 16.56 o -1 8 0 5.32 10.16 5.71 o 0 8 0 265.40 278.46 17.38 o 1 8 0 161.07 177.19 14.40 o 2 8 0 10.89 23.34 6.99 o 3 8 0 70.66 59.26 10.15 o 4 8 0 387.35 423.77 23.93 o 5 8 0 812.09 826.23 30.81 o 6 8 0 103.40 94.28 17.68 o -12 9 0 85.78 105.58 22.82 o -11 9 0 0.14 2.57 8.26 o -10 9 0 101.68 100.07 10.38 o -9 9 0 285.46 295.04 16.60 o -8 9 0 0.94 10.38 5.43 o -7 9 0 130.60 125.35 10.53 o -6 9 0 512.71 518.55 19.03 o -5 9 0 359.06 370.17 19.44 o -4 9 0 3.15 6.21 7.58 o -3 9 0 20.89 17.75 5.29 o -2 9 0 87.62 138.60 13.96 o -1 9 0 4.10 15.65 6.43 o 0 9 0 163.62 169.39 14.83 o 1 9 0 5.83 18.40 6.92 o 2 9 0 218.18 215.92 17.04 o 3 9 0 21.61 26.72 8.36 o 4 9 0 211.62 207.75 17.88 o 5 9 0 3.15 6.76 8.20 o -12 10 0 235.24 244.74 34.74 o -11 10 0 51.35 56.14 12.13 o -10 10 0 235.50 235.20 17.87 o -9 10 0 107.62 106.13 10.38 o -8 10 0 120.28 128.67 13.70 o -7 10 0 0.74 11.47 6.74 o -6 10 0 12.08 12.09 6.42 o -5 10 0 875.59 812.07 26.37 o -4 10 0 262.91 238.05 16.46 o -3 10 0 382.44 346.39 17.20 o -2 10 0 356.16 362.58 21.28 o -1 10 0 1847.78 1798.57 43.32 o 0 10 0 88.58 92.42 11.33 o 1 10 0 136.13 144.95 14.70 o 2 10 0 122.42 96.10 14.15 o 3 10 0 245.20 254.08 20.50 o -11 11 0 36.05 48.23 26.66 o -10 11 0 378.15 360.39 34.44 o -9 11 0 97.83 124.82 16.47 o -8 11 0 503.08 534.31 26.59 o -7 11 0 695.74 737.36 28.27 o -6 11 0 147.04 171.62 15.67 o -5 11 0 2.11 8.56 6.67 o -4 11 0 131.91 137.53 15.92 o -3 11 0 367.15 391.68 23.09 o -2 11 0 10.93 12.14 7.24 o -1 11 0 150.81 148.44 15.18 o 0 11 0 217.63 212.36 17.89 o 1 11 0 273.99 279.29 21.23 o -9 12 0 126.54 139.15 18.47 o -8 12 0 171.80 212.99 20.70 o -7 12 0 327.20 364.85 22.48 o -6 12 0 264.39 290.32 20.27 o -5 12 0 122.76 132.93 16.74 o -4 12 0 72.57 100.65 14.78 o -3 12 0 447.34 456.73 35.07 o -2 12 0 642.66 661.10 40.60 o -1 12 0 59.86 86.18 12.79 o 4 -13 1 111.71 114.30 17.39 o 5 -13 1 10.22 33.46 12.05 o 6 -13 1 1.55 20.17 15.27 o 7 -13 1 1.21 15.28 14.22 o 0 -12 1 162.00 218.38 19.60 o 1 -12 1 344.10 334.72 23.33 o 2 -12 1 321.45 348.49 23.42 o 3 -12 1 3.04 1.03 8.93 o 4 -12 1 1.78 22.57 8.93 o 5 -12 1 262.49 387.95 35.39 o 6 -12 1 283.31 332.71 21.02 o 7 -12 1 91.36 118.51 15.78 o 8 -12 1 209.80 209.13 20.24 o 9 -12 1 238.51 272.90 23.86 o 10 -12 1 32.17 50.07 12.75 o -2 -11 1 172.36 158.96 20.36 o -1 -11 1 256.03 250.41 19.80 o 0 -11 1 0.34 7.78 6.68 o 1 -11 1 38.67 53.97 9.43 o 2 -11 1 1057.47 909.32 37.74 o 3 -11 1 130.26 144.58 15.43 o 4 -11 1 100.06 106.43 14.59 o 5 -11 1 194.87 184.65 15.50 o 6 -11 1 511.64 540.33 24.73 o 7 -11 1 2.03 4.70 8.61 o 8 -11 1 125.52 126.09 16.01 o 9 -11 1 176.36 204.56 31.08 o 10 -11 1 165.92 173.85 16.70 o 11 -11 1 0.14 8.60 10.17 o -4 -10 1 37.01 30.63 9.52 o -3 -10 1 189.71 223.78 18.60 o -2 -10 1 119.31 137.38 15.52 o -1 -10 1 861.98 805.06 28.42 o 0 -10 1 339.10 337.38 21.18 o 1 -10 1 213.98 240.76 20.50 o 2 -10 1 112.34 119.37 15.48 o 3 -10 1 313.24 310.25 18.94 o 4 -10 1 365.16 362.47 17.13 o 5 -10 1 39.29 50.21 8.59 o 6 -10 1 481.11 518.57 22.96 o 7 -10 1 338.73 354.48 17.93 o 8 -10 1 1.20 1.68 5.92 o 9 -10 1 205.04 235.37 17.68 o 10 -10 1 444.42 462.40 24.91 o 11 -10 1 49.18 47.08 11.22 o 12 -10 1 17.35 6.35 10.18 o -5 -9 1 54.45 59.05 11.43 o -4 -9 1 138.46 164.77 16.00 o -3 -9 1 221.21 221.04 17.63 o -2 -9 1 257.26 241.81 17.81 o -1 -9 1 26.09 21.50 6.75 o 0 -9 1 498.43 557.88 25.01 o 1 -9 1 780.77 733.25 24.30 o 2 -9 1 5.95 8.42 4.55 o 3 -9 1 47.37 44.65 7.45 o 4 -9 1 483.19 489.81 17.03 o 5 -9 1 298.36 303.71 14.96 o 6 -9 1 2.05 -2.17 4.44 o 7 -9 1 7.03 0.25 5.07 o 8 -9 1 1424.08 1376.13 30.53 o 9 -9 1 74.89 74.45 8.44 o 10 -9 1 364.06 366.38 21.27 o 11 -9 1 419.57 399.88 27.74 o 12 -9 1 318.31 307.38 25.79 o -6 -8 1 331.26 326.62 31.69 o -5 -8 1 449.63 430.44 28.22 o -4 -8 1 88.94 82.74 10.97 o -3 -8 1 71.73 67.63 9.62 o -2 -8 1 306.10 268.11 17.68 o -1 -8 1 151.35 146.19 12.99 o 0 -8 1 52.20 42.34 7.77 o 1 -8 1 98.70 103.05 8.39 o 2 -8 1 228.25 231.73 12.16 o 3 -8 1 91.35 91.13 8.09 o 4 -8 1 228.36 239.46 10.94 o 5 -8 1 1938.96 1865.60 33.23 o 6 -8 1 639.28 592.77 17.46 o 7 -8 1 1604.73 1451.37 45.04 o 8 -8 1 1.20 5.97 4.61 o 9 -8 1 153.80 137.36 11.20 o 10 -8 1 7.14 -0.63 6.60 o 11 -8 1 11.49 9.77 7.59 o 12 -8 1 15.63 36.65 12.90 o 13 -8 1 345.23 362.51 29.19 o -7 -7 1 92.26 68.49 15.31 o -6 -7 1 214.75 207.31 19.97 o -5 -7 1 99.14 99.79 11.45 o -4 -7 1 74.79 85.25 10.81 o -3 -7 1 18.54 13.61 6.20 o -2 -7 1 505.34 478.53 21.52 o -1 -7 1 208.12 216.00 14.64 o 0 -7 1 7.81 9.04 3.85 o 1 -7 1 0.04 6.16 2.84 o 2 -7 1 799.97 730.61 15.37 o 3 -7 1 487.28 513.42 12.89 o 4 -7 1 28.39 34.27 4.64 o 5 -7 1 188.67 209.21 12.42 o 6 -7 1 2176.36 2126.08 35.59 o 7 -7 1 1838.24 1822.02 49.14 o 8 -7 1 161.08 159.21 17.65 o 9 -7 1 641.52 625.81 27.02 o 10 -7 1 1.68 7.91 6.43 o 11 -7 1 28.46 28.53 9.57 o 12 -7 1 11.09 20.58 9.88 o 13 -7 1 295.02 257.47 29.79 o -8 -6 1 58.38 52.72 11.70 o -7 -6 1 358.49 351.04 27.11 o -6 -6 1 5.07 2.01 5.57 o -5 -6 1 34.64 53.12 8.68 o -4 -6 1 305.64 277.56 17.77 o -3 -6 1 2114.57 2067.40 39.22 o -2 -6 1 53.66 57.59 7.21 o -1 -6 1 10.81 6.52 2.62 o 0 -6 1 382.05 353.08 10.39 o 1 -6 1 204.46 160.51 7.56 o 2 -6 1 2433.11 2554.64 32.56 o 3 -6 1 761.37 726.05 14.33 o 4 -6 1 639.52 569.43 12.62 o 5 -6 1 342.66 361.96 14.35 o 6 -6 1 902.61 966.37 20.99 o 7 -6 1 667.14 627.17 18.20 o 8 -6 1 57.99 53.14 6.98 o 9 -6 1 534.02 574.18 27.77 o 10 -6 1 13.18 10.78 9.99 o 11 -6 1 159.04 165.60 14.92 o 12 -6 1 88.64 87.54 14.57 o 13 -6 1 70.99 51.00 12.25 o -9 -5 1 368.62 363.37 40.28 o -8 -5 1 37.39 67.84 12.65 o -7 -5 1 181.58 172.52 20.48 o -6 -5 1 660.05 666.07 20.58 o -5 -5 1 340.96 349.70 17.20 o -4 -5 1 511.97 495.20 17.34 o -3 -5 1 3621.16 3646.65 50.54 o -2 -5 1 1542.61 1567.98 22.22 o -1 -5 1 1344.22 1384.21 24.57 o 0 -5 1 1.01 -1.60 2.64 o 1 -5 1 7332.77 7991.43 79.15 o 2 -5 1 769.39 831.65 16.00 o 3 -5 1 93.12 105.81 6.06 o 4 -5 1 124.25 130.48 7.12 o 5 -5 1 1131.11 1095.77 20.88 o 6 -5 1 36.59 40.87 6.00 o 7 -5 1 186.21 175.05 10.48 o 8 -5 1 1032.17 954.20 22.12 o 9 -5 1 1.17 2.87 5.70 o 10 -5 1 9.38 15.27 6.28 o 11 -5 1 222.30 231.18 17.20 o 12 -5 1 63.52 63.60 11.51 o 13 -5 1 104.63 91.52 20.42 o -10 -4 1 37.52 41.61 12.77 o -9 -4 1 96.68 136.14 16.81 o -8 -4 1 64.05 80.48 10.50 o -7 -4 1 25.46 30.21 6.02 o -6 -4 1 272.97 265.04 17.72 o -5 -4 1 2305.83 2244.56 37.42 o -4 -4 1 226.55 240.28 11.98 o -3 -4 1 110.64 93.66 7.13 o -2 -4 1 17.14 11.05 3.68 o -1 -4 1 1151.26 1092.97 19.22 o 0 -4 1 397.26 367.31 8.27 o 1 -4 1 391.08 344.46 10.45 o 2 -4 1 483.59 399.80 8.92 o 3 -4 1 11.21 2.50 2.27 o 4 -4 1 42.65 47.14 4.72 o 5 -4 1 1667.57 1646.69 26.27 o 6 -4 1 78.63 132.30 8.32 o 7 -4 1 488.28 515.10 14.92 o 8 -4 1 523.19 462.02 23.95 o 9 -4 1 327.80 315.99 15.20 o 10 -4 1 475.57 476.89 21.79 o 11 -4 1 310.06 294.90 18.99 o 12 -4 1 207.43 191.55 16.22 o 13 -4 1 132.68 144.30 17.80 o -11 -3 1 361.03 376.68 43.40 o -10 -3 1 45.70 58.26 10.23 o -9 -3 1 81.71 81.49 11.79 o -8 -3 1 67.07 68.99 9.75 o -7 -3 1 96.85 94.46 9.07 o -6 -3 1 20.51 13.36 4.75 o -5 -3 1 785.18 773.47 18.94 o -4 -3 1 435.47 404.92 10.04 o -3 -3 1 972.86 958.57 15.21 o -2 -3 1 703.26 748.96 14.92 o -1 -3 1 3.04 17.44 2.07 o 0 -3 1 6818.56 7043.19 73.20 o 1 -3 1 855.95 914.88 12.85 o 2 -3 1 2823.28 2762.25 32.16 o 3 -3 1 1873.60 1929.15 22.67 o 4 -3 1 2340.73 2216.01 30.03 o 5 -3 1 132.06 146.36 7.13 o 6 -3 1 173.76 171.67 6.49 o 7 -3 1 2156.05 2230.53 39.69 o 8 -3 1 539.57 522.74 13.52 o 9 -3 1 82.26 95.69 8.75 o 10 -3 1 229.36 219.53 16.08 o 11 -3 1 162.77 199.76 16.06 o 12 -3 1 186.86 198.06 21.40 o 13 -3 1 113.60 148.43 20.17 o -11 -2 1 289.98 365.22 27.55 o -10 -2 1 362.39 333.23 21.26 o -9 -2 1 7.69 17.38 7.03 o -8 -2 1 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