#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/67/2226727.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226727_Fobs loop_ _publ_author_name 'Ali, Yousuf' 'Peng, Yu' 'Hua, Erbing' 'Afza, Nighat' 'Khan, Rashid Ali' _publ_section_title ; 2,2-Bis(hydroxymethyl)-2,3-dihydro-1H-pyrrolizin-1-one ; _journal_coeditor_code XU2763 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1579 _journal_page_last o1580 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.273 _cell_angle_gamma 90.000 _cell_length_a 10.2601 _cell_length_b 39.8630 _cell_length_c 12.4120 _exptl_crystal_F_000 2304.00 _reflns_d_resolution_high 0.8073 _[local]_cod_data_source_file xu2763Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _c100331d' _shelx_refln_list_code 4 _shelx_f_calc_maximum 482.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12.04 13.90 2.96 o 2 0 0 15823.12 16434.92 167.98 o 3 0 0 0.04 10.42 6.75 o 4 0 0 8762.83 8986.91 137.08 o 5 0 0 268.63 268.46 43.61 o 6 0 0 3157.32 3312.36 116.76 o 7 0 0 68.72 69.19 9.06 o 8 0 0 1608.81 1607.29 41.15 o 9 0 0 9.61 12.72 9.05 o 10 0 0 63670.43 68705.66 2380.52 o 11 0 0 24.01 18.45 7.54 o 12 0 0 418.61 362.01 29.39 o 1 1 0 10.30 14.47 1.96 o 2 1 0 137.83 83.29 9.55 o 3 1 0 17.81 26.97 5.07 o 4 1 0 28146.77 29668.37 247.97 o 5 1 0 33.41 40.12 8.25 o 6 1 0 301.72 239.43 27.15 o 7 1 0 0.23 9.50 3.86 o 8 1 0 588.06 585.07 20.27 o 9 1 0 39.94 37.58 8.02 o 10 1 0 680.17 684.27 23.76 o 11 1 0 11.56 23.04 6.67 o 12 1 0 46.51 24.04 7.84 o 0 2 0 2468.10 82.46 29.10 o 1 2 0 216.09 197.09 5.75 o 2 2 0 19279.32 18202.41 97.69 o 3 2 0 83.72 80.90 9.34 o 4 2 0 334.52 536.30 15.05 o 5 2 0 51.55 63.97 11.79 o 6 2 0 220.23 340.41 45.07 o 7 2 0 7.08 13.37 4.00 o 8 2 0 2.28 7.52 4.51 o 9 2 0 89.11 70.29 9.75 o 10 2 0 501.31 493.10 31.51 o 11 2 0 108.58 107.72 16.13 o 12 2 0 802.59 787.33 38.62 o 1 3 0 433.89 391.24 8.52 o 2 3 0 109269.91 103937.98 691.20 o 3 3 0 20.70 21.74 4.89 o 4 3 0 8377.74 9007.14 96.97 o 5 3 0 149.82 171.66 19.30 o 6 3 0 0.06 2.92 10.92 o 7 3 0 61.31 56.19 6.72 o 8 3 0 246.49 215.54 16.74 o 9 3 0 4.84 16.82 4.98 o 10 3 0 2125.21 2109.36 73.97 o 11 3 0 2.04 4.14 5.63 o 12 3 0 2786.78 2819.99 96.20 o 0 4 0 2521.04 2153.79 36.12 o 1 4 0 1.90 9.76 4.15 o 2 4 0 42230.25 41922.27 327.42 o 3 4 0 69.22 76.51 9.62 o 4 4 0 473.06 531.06 17.49 o 5 4 0 0.00 15.87 6.69 o 6 4 0 139.00 278.06 31.80 o 7 4 0 1.17 3.91 5.69 o 8 4 0 3491.63 3517.55 57.00 o 9 4 0 161.04 138.81 17.69 o 10 4 0 1761.48 1766.17 54.10 o 11 4 0 21.62 19.49 6.13 o 12 4 0 53.29 18.58 11.22 o 1 5 0 67.08 72.02 9.18 o 2 5 0 8537.76 7836.65 128.65 o 3 5 0 356.08 375.14 14.38 o 4 5 0 18566.79 20320.25 185.84 o 5 5 0 0.50 6.50 6.40 o 6 5 0 32410.80 35078.96 214.36 o 7 5 0 1.25 13.01 4.52 o 8 5 0 210.25 181.99 13.79 o 9 5 0 345.96 264.16 34.86 o 10 5 0 21.81 40.45 7.31 o 11 5 0 25.70 21.78 5.62 o 12 5 0 56.25 66.43 15.56 o 0 6 0 150978.87 138559.72 365.55 o 1 6 0 221.41 201.58 13.23 o 2 6 0 4325.69 4045.79 76.43 o 3 6 0 1212.43 1195.74 23.54 o 4 6 0 2356.13 2360.45 40.99 o 5 6 0 625.00 584.89 19.87 o 6 6 0 2316.50 2615.87 53.85 o 7 6 0 47.75 43.47 4.79 o 8 6 0 698.02 681.17 21.28 o 9 6 0 106.92 86.69 13.92 o 10 6 0 12622.52 14121.09 397.81 o 11 6 0 22.09 18.19 7.09 o 12 6 0 59.44 48.17 8.10 o 1 7 0 497.74 449.73 13.63 o 2 7 0 8416.23 7966.59 152.76 o 3 7 0 1.74 12.61 6.42 o 4 7 0 1966.92 1816.24 40.15 o 5 7 0 21.25 26.44 6.62 o 6 7 0 328.33 315.91 27.57 o 7 7 0 1.21 9.09 5.15 o 8 7 0 1410.75 1380.67 34.57 o 9 7 0 42.51 35.42 6.12 o 10 7 0 206.50 226.93 28.31 o 11 7 0 40.96 40.85 9.86 o 12 7 0 24.90 31.75 7.53 o 0 8 0 7582.93 6541.75 137.73 o 1 8 0 233.48 220.58 12.23 o 2 8 0 1202.01 1112.08 25.06 o 3 8 0 88.55 112.28 14.81 o 4 8 0 9763.42 9370.05 127.19 o 5 8 0 144.96 164.82 19.40 o 6 8 0 606.64 552.32 24.94 o 7 8 0 2.19 12.82 5.22 o 8 8 0 225.30 241.65 19.88 o 9 8 0 114.49 95.40 16.41 o 10 8 0 1264.51 1250.04 46.12 o 11 8 0 393.63 392.86 26.99 o 12 8 0 44.76 32.00 7.54 o 1 9 0 633.53 594.91 14.72 o 2 9 0 263.74 281.33 40.20 o 3 9 0 378.69 374.72 25.89 o 4 9 0 59.91 74.01 13.31 o 5 9 0 164.10 139.54 22.68 o 6 9 0 1204.78 1183.79 32.22 o 7 9 0 55.65 63.14 8.71 o 8 9 0 126.34 99.12 12.45 o 9 9 0 17.64 19.16 6.59 o 10 9 0 32.83 52.38 9.22 o 11 9 0 103.63 96.85 24.88 o 12 9 0 10.05 6.54 6.26 o 0 10 0 232651.88 207068.33 557.57 o 1 10 0 265.69 219.99 21.54 o 2 10 0 16646.16 16461.40 203.86 o 3 10 0 9834.69 10180.44 170.40 o 4 10 0 624.50 697.94 24.44 o 5 10 0 282.24 362.28 47.12 o 6 10 0 225.30 243.42 20.81 o 7 10 0 2508.01 2419.87 52.40 o 8 10 0 800.89 641.53 43.83 o 9 10 0 1.61 19.90 8.14 o 10 10 0 1330.79 1403.19 32.84 o 11 10 0 80.28 75.84 14.64 o 12 10 0 11.49 6.51 4.38 o 1 11 0 1231.31 1198.31 28.67 o 2 11 0 10557.56 10489.54 186.99 o 3 11 0 2605.08 2613.90 54.85 o 4 11 0 1114.22 1081.64 37.40 o 5 11 0 79.92 109.55 17.63 o 6 11 0 43.69 63.74 5.82 o 7 11 0 836.94 832.31 25.44 o 8 11 0 1664.64 1574.84 67.86 o 9 11 0 13.54 17.65 8.99 o 10 11 0 4.28 4.76 7.54 o 11 11 0 410.87 455.48 26.37 o 12 11 0 268.30 204.27 41.57 o 0 12 0 736.04 659.41 31.21 o 1 12 0 334.89 276.56 20.46 o 2 12 0 1167.59 1301.85 34.66 o 3 12 0 233.78 305.79 46.77 o 4 12 0 20638.20 23516.58 291.17 o 5 12 0 474.37 428.12 63.72 o 6 12 0 5221.51 5417.41 81.07 o 7 12 0 39.19 41.61 5.03 o 8 12 0 67.57 71.44 10.05 o 9 12 0 155.25 209.96 28.93 o 10 12 0 1.82 5.07 7.80 o 11 12 0 90.06 70.57 15.85 o 12 12 0 140.90 48.55 27.26 o 1 13 0 712.36 690.76 19.17 o 2 13 0 268.63 318.77 49.46 o 3 13 0 2440.36 2557.33 66.86 o 4 13 0 3136.00 3426.28 78.88 o 5 13 0 1062.11 1104.66 44.27 o 6 13 0 136.19 125.27 12.03 o 7 13 0 56.10 58.23 6.88 o 8 13 0 46.38 38.20 6.01 o 9 13 0 5.24 17.76 9.54 o 10 13 0 3234.20 3781.70 65.20 o 11 13 0 28.94 25.41 6.46 o 12 13 0 8.29 4.39 4.90 o 0 14 0 2625.54 2271.43 48.54 o 1 14 0 218.74 233.67 16.43 o 2 14 0 2254.35 2411.46 49.71 o 3 14 0 1064.72 977.09 35.09 o 4 14 0 1419.03 1696.30 45.68 o 5 14 0 3238.75 3130.25 66.78 o 6 14 0 4.75 13.77 5.05 o 7 14 0 90.25 94.08 9.74 o 8 14 0 28.73 32.29 7.25 o 9 14 0 29.81 40.33 9.16 o 10 14 0 368.64 464.83 51.93 o 11 14 0 9.55 12.70 5.70 o 12 14 0 245.55 226.12 28.14 o 1 15 0 3292.46 3113.23 53.47 o 2 15 0 1967.81 1968.57 55.20 o 3 15 0 3606.00 3781.21 84.93 o 4 15 0 11567.00 12630.65 186.75 o 5 15 0 386.91 430.83 26.44 o 6 15 0 6054.40 6101.53 76.67 o 7 15 0 57.30 58.42 7.53 o 8 15 0 1694.15 1653.46 94.96 o 9 15 0 1629.74 1742.90 49.48 o 10 15 0 76.39 85.28 10.89 o 11 15 0 94.48 96.00 23.15 o 12 15 0 1.06 8.60 5.76 o 0 16 0 4302.05 4284.94 195.61 o 1 16 0 1858.47 1851.98 36.30 o 2 16 0 13822.70 14736.54 233.60 o 3 16 0 2551.26 2685.48 73.73 o 4 16 0 983.45 1137.09 37.80 o 5 16 0 96.24 106.91 10.45 o 6 16 0 553.19 541.04 24.48 o 7 16 0 1272.35 1260.62 29.96 o 8 16 0 5656.54 5439.90 134.14 o 9 16 0 104.04 106.54 14.04 o 10 16 0 7.56 9.81 6.91 o 11 16 0 2.43 3.15 6.29 o 12 16 0 4.75 1.74 5.04 o 1 17 0 0.22 10.50 5.99 o 2 17 0 11513.29 12003.86 259.48 o 3 17 0 179.29 225.44 33.24 o 4 17 0 9.36 26.73 13.44 o 5 17 0 803.72 782.91 19.91 o 6 17 0 1583.24 1636.63 31.62 o 7 17 0 1195.78 1185.47 27.43 o 8 17 0 747.48 688.44 55.76 o 9 17 0 208.51 204.14 22.10 o 10 17 0 379.08 400.48 28.44 o 11 17 0 6.97 5.38 10.05 o 0 18 0 239.32 196.83 33.91 o 1 18 0 498.63 513.05 17.71 o 2 18 0 5858.37 6570.90 160.16 o 3 18 0 64.80 84.32 15.12 o 4 18 0 972.82 1078.39 36.59 o 5 18 0 2486.02 2324.88 48.95 o 6 18 0 508.05 416.96 27.99 o 7 18 0 6.40 14.97 6.76 o 8 18 0 2222.18 2175.22 85.49 o 9 18 0 1411.50 1296.60 102.34 o 10 18 0 207.65 213.41 27.66 o 11 18 0 184.96 112.42 34.07 o 1 19 0 678.08 687.92 30.04 o 2 19 0 1285.22 1447.79 58.22 o 3 19 0 1054.95 1007.35 39.50 o 4 19 0 101.20 100.37 8.81 o 5 19 0 76.39 64.05 7.88 o 6 19 0 27.25 27.64 5.42 o 7 19 0 1109.56 1091.71 40.98 o 8 19 0 416.57 331.74 50.21 o 9 19 0 15.92 17.94 5.69 o 10 19 0 2094.89 2254.15 62.02 o 11 19 0 515.74 569.74 23.10 o 0 20 0 207.36 468.04 66.45 o 1 20 0 0.03 14.74 7.19 o 2 20 0 888.64 730.39 35.33 o 3 20 0 12925.42 13230.64 192.61 o 4 20 0 351.19 386.44 32.11 o 5 20 0 1067.33 1027.30 25.54 o 6 20 0 540.10 527.57 26.46 o 7 20 0 6569.10 6731.11 116.76 o 8 20 0 1230.61 1323.90 32.60 o 9 20 0 16.89 16.73 4.52 o 10 20 0 33.29 49.94 10.19 o 11 20 0 69.22 30.84 12.62 o 1 21 0 2.28 23.26 13.89 o 2 21 0 1118.23 1075.52 128.77 o 3 21 0 0.49 4.73 7.03 o 4 21 0 3707.59 3707.01 69.90 o 5 21 0 60.06 85.01 7.74 o 6 21 0 7238.61 7058.76 86.65 o 7 21 0 386.12 373.03 40.11 o 8 21 0 4648.51 4997.81 122.96 o 9 21 0 1363.82 1393.85 33.75 o 10 21 0 551.31 512.19 27.93 o 11 21 0 122.10 47.38 25.59 o 0 22 0 903.60 1266.42 83.49 o 1 22 0 1981.14 2344.61 71.05 o 2 22 0 2682.20 2842.87 115.77 o 3 22 0 63.36 53.84 5.90 o 4 22 0 136.42 107.87 9.25 o 5 22 0 218.15 210.44 17.58 o 6 22 0 438.48 465.57 30.88 o 7 22 0 933.91 859.74 76.03 o 8 22 0 2466.12 2605.54 60.96 o 9 22 0 1907.94 1766.95 31.19 o 10 22 0 0.90 5.01 4.52 o 11 22 0 466.56 410.42 17.19 o 1 23 0 3.92 4.39 13.46 o 2 23 0 817.96 821.08 42.84 o 3 23 0 2733.20 2428.75 52.30 o 4 23 0 36.60 47.76 5.47 o 5 23 0 409.25 489.85 30.32 o 6 23 0 88.55 102.03 11.25 o 7 23 0 272.91 196.94 33.94 o 8 23 0 38.81 36.53 10.34 o 9 23 0 120.56 102.93 11.81 o 10 23 0 295.84 333.47 17.95 o 11 23 0 3.10 5.29 5.39 o 0 24 0 259.53 428.86 57.67 o 1 24 0 841.58 866.41 41.47 o 2 24 0 443.52 465.16 36.27 o 3 24 0 2117.84 2190.50 50.57 o 4 24 0 3171.94 2997.79 46.45 o 5 24 0 102.21 117.79 11.44 o 6 24 0 39.82 24.95 7.64 o 7 24 0 3252.42 3317.82 150.71 o 8 24 0 651.78 640.23 24.69 o 9 24 0 266.02 275.40 29.30 o 10 24 0 4.20 13.36 5.42 o 11 24 0 3.92 0.52 4.26 o 1 25 0 1784.22 1854.31 45.55 o 2 25 0 52.56 80.01 30.88 o 3 25 0 4241.92 4435.30 65.01 o 4 25 0 222.31 228.62 22.89 o 5 25 0 202.78 202.92 18.12 o 6 25 0 679.64 590.48 45.72 o 7 25 0 311.52 349.83 31.96 o 8 25 0 76.74 117.74 11.96 o 9 25 0 172.40 152.51 17.89 o 10 25 0 256.96 251.29 26.60 o 0 26 0 13507.09 14431.76 327.47 o 1 26 0 369.02 376.68 29.68 o 2 26 0 73.96 84.18 8.42 o 3 26 0 1246.09 1196.82 28.67 o 4 26 0 63.20 72.88 8.18 o 5 26 0 7454.60 7269.55 157.88 o 6 26 0 23.62 23.23 8.84 o 7 26 0 3936.31 4055.92 113.86 o 8 26 0 74.30 86.19 10.38 o 9 26 0 305.90 350.18 22.67 o 10 26 0 454.54 377.76 38.04 o 1 27 0 814.53 817.50 30.52 o 2 27 0 0.17 6.46 4.38 o 3 27 0 267.00 257.64 23.49 o 4 27 0 90.25 86.11 9.32 o 5 27 0 385.73 323.46 37.13 o 6 27 0 0.55 14.93 8.16 o 7 27 0 50.55 45.02 15.50 o 8 27 0 2.89 11.92 5.70 o 9 27 0 320.77 319.81 19.66 o 10 27 0 16.08 11.26 4.08 o 0 28 0 31.81 34.92 7.84 o 1 28 0 229.83 244.97 20.94 o 2 28 0 776.74 788.82 23.53 o 3 28 0 3654.20 3805.87 54.46 o 4 28 0 7.90 25.44 7.04 o 5 28 0 3197.90 3234.05 87.58 o 6 28 0 797.50 681.34 97.73 o 7 28 0 3323.52 3832.34 75.34 o 8 28 0 35.05 30.21 6.79 o 9 28 0 14.90 12.94 6.02 o 10 28 0 22.18 19.90 6.01 o 1 29 0 925.98 1102.30 24.81 o 2 29 0 1277.35 1371.10 36.68 o 3 29 0 2.62 9.56 6.26 o 4 29 0 666.16 712.08 39.65 o 5 29 0 45.16 39.98 8.96 o 6 29 0 1.51 9.97 10.43 o 7 29 0 4.20 3.81 6.76 o 8 29 0 53.14 51.51 10.57 o 9 29 0 24.90 21.96 5.18 o 10 29 0 0.52 0.53 7.87 o 0 30 0 1186.80 1174.46 53.65 o 1 30 0 455.40 419.30 34.71 o 2 30 0 2737.38 2880.95 48.30 o 3 30 0 1933.36 1892.18 49.95 o 4 30 0 234.40 240.38 24.17 o 5 30 0 13964.15 15244.38 715.05 o 6 30 0 396.01 513.75 52.35 o 7 30 0 433.06 504.42 46.92 o 8 30 0 34.81 40.64 7.16 o 9 30 0 83.17 70.39 14.19 o 10 30 0 49.56 24.90 13.16 o 1 31 0 77.44 86.73 10.39 o 2 31 0 1913.19 1959.09 38.23 o 3 31 0 284.93 336.81 29.70 o 4 31 0 248.06 290.11 33.20 o 5 31 0 6.66 10.39 6.27 o 6 31 0 863.18 909.75 25.10 o 7 31 0 204.20 245.04 26.21 o 8 31 0 8.29 9.25 5.84 o 9 31 0 594.87 607.03 21.25 o 0 32 0 146.41 151.40 35.88 o 1 32 0 586.12 531.26 50.06 o 2 32 0 896.40 867.43 49.69 o 3 32 0 276.22 352.88 41.26 o 4 32 0 4.28 11.49 7.34 o 5 32 0 1001.09 1090.33 29.68 o 6 32 0 411.68 446.04 50.36 o 7 32 0 189.61 175.02 21.21 o 8 32 0 58.37 79.69 14.06 o 9 32 0 88.74 50.70 14.91 o 1 33 0 231.04 251.88 22.83 o 2 33 0 133.63 103.58 16.98 o 3 33 0 0.23 15.00 8.61 o 4 33 0 1118.90 1170.80 108.51 o 5 33 0 326.16 484.19 57.88 o 6 33 0 157.50 206.21 25.33 o 7 33 0 782.32 742.57 27.05 o 8 33 0 223.50 247.01 31.01 o 9 33 0 15.05 8.81 4.74 o 0 34 0 497.74 530.07 118.07 o 1 34 0 4.04 5.76 9.56 o 2 34 0 1115.56 1008.67 85.61 o 3 34 0 6113.68 5812.94 238.00 o 4 34 0 2665.66 2764.38 58.01 o 5 34 0 4028.44 4630.11 80.17 o 6 34 0 2.56 2.89 11.38 o 7 34 0 16.16 13.70 6.23 o 8 34 0 632.02 662.64 29.95 o 9 34 0 172.66 78.89 38.37 o 1 35 0 1971.36 2112.53 97.06 o 2 35 0 0.00 0.00 7.00 o 3 35 0 919.30 955.41 29.27 o 4 35 0 68.56 87.59 9.62 o 5 35 0 2.66 0.00 7.91 o 6 35 0 122.32 164.98 24.96 o 7 35 0 22.09 23.42 8.14 o 8 35 0 13.25 22.43 6.34 o 0 36 0 149.08 66.80 53.85 o 1 36 0 1688.39 1888.23 139.04 o 2 36 0 277.89 343.01 39.81 o 3 36 0 162.82 170.52 16.94 o 4 36 0 174.77 191.31 21.13 o 5 36 0 2852.63 3300.80 60.09 o 6 36 0 0.94 15.39 7.32 o 7 36 0 70.90 77.19 12.08 o 8 36 0 66.91 44.30 13.25 o 1 37 0 16.08 5.04 6.03 o 2 37 0 296.87 344.54 40.08 o 3 37 0 2996.47 3080.76 53.32 o 4 37 0 222.31 281.83 30.63 o 5 37 0 880.31 930.80 24.79 o 6 37 0 241.18 221.65 36.85 o 7 37 0 445.21 583.71 26.59 o 8 37 0 21.44 10.47 6.13 o 0 38 0 89.11 105.88 18.46 o 1 38 0 2025.90 2086.25 71.80 o 2 38 0 86.30 109.09 14.56 o 3 38 0 1002.36 930.01 32.27 o 4 38 0 161.04 301.19 71.71 o 5 38 0 38.94 19.84 7.44 o 6 38 0 165.12 170.73 27.77 o 7 38 0 41.34 30.07 6.99 o 8 38 0 49.14 15.49 10.90 o 1 39 0 7.08 12.57 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7.79 o -6 16 2 303.11 322.21 25.71 o -5 16 2 11265.70 11096.59 215.89 o -4 16 2 119.03 137.92 16.82 o -3 16 2 153.26 168.63 19.95 o -2 16 2 1201.32 1429.03 39.87 o -1 16 2 38.69 49.26 7.03 o 0 16 2 5199.85 5298.66 84.86 o 1 16 2 430.56 477.65 18.99 o 2 16 2 5056.63 5513.07 118.45 o 3 16 2 414.94 574.57 56.70 o 4 16 2 9.80 7.41 16.43 o 5 16 2 8275.54 8358.09 191.13 o 6 16 2 351.94 338.56 25.94 o 7 16 2 166.15 145.65 13.26 o 8 16 2 16.24 12.24 5.09 o 9 16 2 76.39 76.02 10.42 o 10 16 2 3005.23 3266.97 54.16 o 11 16 2 14.06 6.82 5.72 o -11 17 2 156.75 140.30 38.30 o -10 17 2 38.94 36.35 6.80 o -9 17 2 32.15 36.14 8.75 o -8 17 2 5.29 0.00 9.52 o -7 17 2 986.59 1002.07 48.12 o -6 17 2 5.15 20.92 6.30 o -5 17 2 342.25 311.36 20.79 o -4 17 2 727.38 657.12 35.89 o -3 17 2 171.09 181.28 20.59 o -2 17 2 787.36 848.14 37.34 o -1 17 2 552.72 608.22 35.19 o 0 17 2 624.00 729.30 31.33 o 1 17 2 430.15 466.78 26.02 o 2 17 2 119.68 160.54 24.55 o 3 17 2 394.02 342.23 58.21 o 4 17 2 95.26 88.63 9.65 o 5 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194.55 17.43 o 2 28 2 4329.64 4255.57 65.64 o 3 28 2 141.61 143.87 12.68 o 4 28 2 11752.73 11391.18 208.93 o 5 28 2 141.13 126.23 19.54 o 6 28 2 0.48 2.99 7.32 o 7 28 2 295.84 257.79 27.55 o 8 28 2 32.38 40.26 7.02 o 9 28 2 485.76 463.29 23.96 o 10 28 2 6.20 4.79 3.87 o -10 29 2 1612.83 1832.00 69.43 o -9 29 2 0.44 7.12 6.17 o -8 29 2 210.25 231.60 33.23 o -7 29 2 34.57 50.99 9.27 o -6 29 2 403.21 491.88 40.28 o -5 29 2 526.70 433.44 65.43 o -4 29 2 128.37 128.15 14.57 o -3 29 2 15.52 23.09 5.48 o -2 29 2 6084.00 5733.66 77.52 o -1 29 2 915.67 980.53 35.65 o 0 29 2 1627.32 1639.63 29.72 o 1 29 2 108.37 96.58 15.52 o 2 29 2 1486.87 1412.78 28.17 o 3 29 2 1387.56 1249.04 35.60 o 4 29 2 454.54 447.54 45.57 o 5 29 2 3.69 15.91 7.99 o 6 29 2 301.37 365.66 37.82 o 7 29 2 4.84 8.56 4.75 o 8 29 2 96.04 82.69 10.95 o 9 29 2 0.67 7.11 3.14 o 10 29 2 95.06 9.55 20.56 o -9 30 2 2.96 4.53 5.22 o -8 30 2 676.00 762.32 27.42 o -7 30 2 466.13 509.16 48.21 o -6 30 2 564.54 580.28 40.46 o -5 30 2 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6.42 4.38 o