#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/67/2226735.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2226735_Fobs
loop_
_publ_author_name
'Mohammadnezhad, Gholamhossein'
'Ghanbarpour, Ali Reza'
'Amini, Mostafa M.'
'Ng, Seik Weng'
_publ_section_title
;
 <i>catena</i>-Poly[[(1,10-phenanthroline-\k^2^<i>N</i>,<i>N</i>')lead(II)]-\m-azido-\k^2^<i>N</i>^1^:<i>N</i>^3^-\m-nitrito-\k^3^<i>O</i>,<i>O</i>':<i>O</i>'-[(1,10-phenanthroline-\k^2^<i>N</i>,<i>N</i>')lead(II)]-di-\m-azido-\k^4^<i>N</i>^1^:<i>N</i>^1^]
;
_journal_coeditor_code           XU2775
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m821
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                90.541
_cell_angle_beta                 109.665
_cell_angle_gamma                104.626
_cell_length_a                   7.6860
_cell_length_b                   9.2056
_cell_length_c                   9.9080
_exptl_crystal_F_000             438.00
_reflns_d_resolution_high        0.7696
_[local]_cod_data_source_file    xu2775Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            284.09
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 26656.11 25625.33 1270.00 o
2 0 0 2119.11 2046.35 74.81 o
3 0 0 1280.07 1362.79 61.16 o
4 0 0 23.73 63.47 13.22 o
5 0 0 2804.56 3028.32 118.83 o
6 0 0 4981.86 5156.83 226.48 o
7 0 0 7056.03 7610.56 398.57 o
8 0 0 3463.05 4067.64 267.16 o
9 0 0 1190.20 1377.04 153.20 o
-8 1 0 211.67 238.08 49.30 o
-7 1 0 1472.40 1416.88 88.12 o
-6 1 0 945.01 912.97 64.12 o
-5 1 0 5619.42 5713.29 175.33 o
-4 1 0 16492.28 16293.00 489.89 o
-3 1 0 11209.03 10734.94 308.29 o
-2 1 0 6656.47 5994.11 173.22 o
-1 1 0 324.21 1072.62 90.23 o
0 1 0 2495.47 2733.59 141.66 o
2 1 0 21134.82 21650.67 608.77 o
3 1 0 8015.85 8573.80 301.92 o
4 1 0 4525.49 4600.63 170.61 o
5 1 0 6204.44 6551.05 239.74 o
6 1 0 1572.77 1739.52 92.93 o
7 1 0 109.78 242.92 68.09 o
8 1 0 971.06 1355.97 141.66 o
-9 2 0 3560.23 3809.59 243.93 o
-8 2 0 3863.12 3939.20 436.22 o
-7 2 0 3707.02 3731.13 171.61 o
-6 2 0 1289.41 1315.48 150.17 o
-5 2 0 2.11 28.99 23.87 o
-4 2 0 717.55 684.66 30.71 o
-3 2 0 11462.71 11212.42 322.72 o
-2 2 0 80707.22 68068.98 2447.28 o
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0 2 0 8804.79 9227.15 265.52 o
1 2 0 7899.48 8269.60 235.87 o
2 2 0 1080.39 1331.28 46.17 o
3 2 0 377.54 381.32 23.31 o
4 2 0 3605.34 3905.74 123.78 o
5 2 0 9191.10 10304.49 305.48 o
6 2 0 5750.84 5980.71 353.13 o
7 2 0 2716.76 3146.73 225.32 o
8 2 0 1098.70 1361.46 154.93 o
-9 3 0 53.21 75.72 56.55 o
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-6 3 0 7900.54 7854.73 315.42 o
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0 3 0 16373.10 15824.25 446.28 o
1 3 0 10267.77 10344.54 367.56 o
2 3 0 8733.71 8802.52 254.62 o
3 3 0 8532.32 8774.95 359.03 o
4 3 0 3548.31 3800.64 125.56 o
5 3 0 245.89 263.91 35.52 o
6 3 0 47.24 145.12 61.45 o
7 3 0 1591.68 2143.31 184.07 o
8 3 0 2929.16 3724.60 278.70 o
-9 4 0 2790.47 2788.25 156.67 o
-8 4 0 2284.58 2347.85 294.28 o
-7 4 0 459.57 546.80 204.84 o
-6 4 0 22.27 73.81 36.10 o
-5 4 0 1981.06 2111.31 107.99 o
-4 4 0 19180.56 19407.41 568.16 o
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-1 4 0 12211.42 11800.20 338.19 o
0 4 0 2584.96 2388.59 76.18 o
1 4 0 928.14 996.06 49.12 o
2 4 0 929.84 941.16 49.90 o
3 4 0 7380.27 7643.71 277.20 o
4 4 0 7313.73 7671.71 281.58 o
5 4 0 5213.43 5432.56 254.32 o
6 4 0 3385.54 2937.56 214.65 o
7 4 0 2011.64 1944.24 180.32 o
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0 5 0 5824.28 5665.98 170.54 o
1 5 0 8388.18 8027.50 287.45 o
2 5 0 7945.07 7503.86 272.36 o
3 5 0 2775.28 2687.11 115.77 o
4 5 0 398.00 401.74 42.47 o
5 5 0 565.53 678.28 95.50 o
6 5 0 2170.74 2230.43 190.13 o
7 5 0 3063.51 2978.82 242.63 o
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0 6 0 17.91 42.33 11.97 o
1 6 0 3183.10 3118.21 128.51 o
2 6 0 5636.36 5326.93 204.27 o
3 6 0 6024.18 6000.68 230.20 o
4 6 0 5144.54 5110.91 206.49 o
5 6 0 3006.52 2743.77 133.66 o
6 6 0 856.81 912.54 133.29 o
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2 7 0 1123.99 1107.76 68.75 o
3 7 0 34.73 24.24 28.63 o
4 7 0 621.53 638.75 64.77 o
5 7 0 2863.77 2722.06 137.53 o
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3 8 0 4009.22 3847.55 168.65 o
4 8 0 2693.15 2464.06 128.47 o
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3 9 0 1648.38 1617.12 112.52 o
4 9 0 2858.47 3093.47 156.41 o
-7 10 0 2920.21 2933.44 162.19 o
-6 10 0 3565.03 4020.04 268.17 o
-5 10 0 3970.62 4289.41 194.53 o
-4 10 0 1250.18 1324.01 98.66 o
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-1 10 0 1723.26 1807.14 106.08 o
0 10 0 3440.87 3692.82 280.28 o
1 10 0 4193.32 3908.69 268.60 o
2 10 0 3729.61 3437.54 163.49 o
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-4 11 0 2728.76 3146.26 157.32 o
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-2 11 0 2886.77 3351.03 443.00 o
-1 11 0 2718.37 2994.06 326.44 o
0 11 0 243.81 279.42 56.50 o
1 11 0 324.48 365.82 83.38 o
-1 -11 1 65.98 86.55 62.61 o
0 -11 1 1099.41 1249.80 132.14 o
1 -11 1 2068.75 2276.02 187.24 o
2 -11 1 3805.29 3916.46 267.16 o
3 -11 1 4654.87 4995.76 322.26 o
4 -11 1 2088.35 2454.31 174.55 o
5 -11 1 338.63 383.56 57.32 o
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2 -10 1 156.50 239.04 47.17 o
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5 -10 1 3512.61 3692.19 173.35 o
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0 -8 1 228.72 234.99 38.76 o
1 -8 1 297.85 375.61 32.05 o
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3 -2 1 2286.83 2224.86 98.04 o
4 -2 1 29.92 71.81 23.53 o
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0 -1 1 3450.75 3732.41 108.01 o
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