#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/67/2226736.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226736_Fobs loop_ _publ_author_name 'Jabeen, Nadia' 'Ahmad, Saeed' 'Meer, Ali Farooq' 'Khan, Islam Ullah' 'Ng, Seik Weng' _publ_section_title ; Pentakis(ethylenediammonium) tri-\m-sulfato-bis[trisulfatocerate(IV)] trihydrate ; _journal_coeditor_code XU2776 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m797 _journal_page_last m798 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.882 _cell_angle_beta 88.096 _cell_angle_gamma 73.783 _cell_length_a 11.6716 _cell_length_b 13.3506 _cell_length_c 15.4143 _exptl_crystal_F_000 1516.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file xu2776Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 336.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 45.20 -0.57 0.38 o 2 0 0 14112.71 17986.45 289.08 o 3 0 0 251.00 184.66 7.85 o 4 0 0 5981.23 6713.95 86.31 o 5 0 0 445.16 485.18 13.34 o 6 0 0 55170.91 68267.63 1151.28 o 7 0 0 50.04 36.64 9.46 o 8 0 0 991.94 1205.78 32.81 o 9 0 0 71.76 94.17 13.16 o 10 0 0 2239.45 2487.51 83.72 o 11 0 0 42.43 43.43 16.02 o 12 0 0 4244.77 5011.46 182.20 o 13 0 0 687.75 680.01 63.47 o 14 0 0 22.91 29.91 21.57 o -14 1 0 1161.03 1283.87 94.78 o -13 1 0 40.74 25.10 27.01 o -12 1 0 7281.08 8228.66 276.49 o -11 1 0 177.34 205.98 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