#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:43:21 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/67/2226786.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226786_Fobs loop_ _publ_author_name '\,Serb, Mihaela-Diana' 'Kalf, Irmgard' 'Englert, Ulli' _publ_section_title ; [rac-2-(1-Aminoethyl)phenyl-\k^2^C^1^,N](ethylendiamine-\k^2^N,N')palladium(II) 3,5-dimethylbenzoate ; _journal_coeditor_code BT5293 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m977 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.616 _cell_angle_gamma 90.000 _cell_length_a 7.9624 _cell_length_b 28.615 _cell_length_c 8.5964 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high .7709 _cod_data_source_file bt5293Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 353.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 17078.45 17593.10 197.58 o 2 0 0 18672.59 20727.07 294.83 o 3 0 0 3418.78 3344.18 150.60 o 4 0 0 1524.12 1906.28 154.12 o 5 0 0 1862.43 2305.71 195.44 o 6 0 0 308.22 287.18 100.86 o 7 0 0 2776.13 2984.63 255.93 o 8 0 0 5836.80 5887.58 335.02 o 9 0 0 4033.24 3682.41 328.08 o 10 0 0 1316.94 1219.64 202.57 o 1 1 0 8822.79 9339.72 100.39 o 2 1 0 3131.06 2883.81 81.19 o 3 1 0 17889.20 18612.11 241.42 o 4 1 0 22701.35 24118.49 319.00 o 5 1 0 12571.15 12777.62 266.03 o 6 1 0 2181.35 2087.27 142.68 o 7 1 0 1551.25 1757.12 149.14 o 8 1 0 426.01 448.10 93.00 o 9 1 0 236.77 381.04 85.90 o 10 1 0 648.90 735.56 129.00 o 1 2 0 27672.56 29352.25 335.32 o 2 2 0 7625.31 7940.37 130.37 o 3 2 0 2562.62 2627.51 95.68 o 4 2 0 39.94 141.79 46.81 o 5 2 0 614.34 746.23 92.96 o 6 2 0 1991.60 2024.56 141.64 o 7 2 0 7361.76 7040.30 238.69 o 8 2 0 4878.28 4820.93 215.87 o 9 2 0 5436.37 4868.87 252.63 o 10 2 0 1090.34 1012.89 134.19 o 1 3 0 1.80 6.25 9.91 o 2 3 0 3792.76 3577.84 90.37 o 3 3 0 22178.91 23358.38 271.86 o 4 3 0 16441.58 16990.18 290.18 o 5 3 0 12920.54 13234.51 288.12 o 6 3 0 2853.49 2924.45 148.57 o 7 3 0 5.77 94.27 58.74 o 8 3 0 21.69 109.05 68.74 o 9 3 0 503.51 643.94 109.60 o 10 3 0 134.47 221.39 80.80 o 0 4 0 6916.11 6349.03 192.55 o 1 4 0 17940.10 18367.12 210.09 o 2 4 0 1196.42 1162.36 59.55 o 3 4 0 6031.32 6340.79 144.36 o 4 4 0 195.89 274.94 63.01 o 5 4 0 .74 45.50 53.06 o 6 4 0 3100.27 3046.97 161.43 o 7 4 0 3867.13 3693.45 197.42 o 8 4 0 3295.28 3166.22 197.54 o 9 4 0 3584.37 3198.60 218.71 o 10 4 0 917.99 882.21 127.31 o 1 5 0 933.98 927.78 34.62 o 2 5 0 9246.28 9624.20 206.34 o 3 5 0 12255.27 12489.07 221.27 o 4 5 0 16697.35 18088.43 313.94 o 5 5 0 5849.99 5880.81 184.71 o 6 5 0 3395.31 3544.44 158.64 o 7 5 0 23.51 105.85 56.35 o 8 5 0 644.36 664.98 105.08 o 9 5 0 178.32 253.05 77.52 o 10 5 0 219.13 210.62 82.73 o 0 6 0 5428.23 4754.05 114.15 o 1 6 0 15412.86 15235.67 136.17 o 2 6 0 998.42 968.97 58.01 o 3 6 0 1.41 24.09 28.59 o 4 6 0 .08 8.27 37.36 o 5 6 0 29.71 63.41 49.15 o 6 6 0 2135.53 2251.80 142.89 o 7 6 0 341.17 446.18 87.74 o 8 6 0 2435.20 2548.29 187.38 o 9 6 0 1411.36 1326.13 147.58 o 10 6 0 720.88 810.59 122.05 o 1 7 0 27.93 70.22 18.39 o 2 7 0 284.61 288.68 39.67 o 3 7 0 2124.71 1851.25 86.40 o 4 7 0 5310.68 5274.04 237.61 o 5 7 0 3314.89 3144.83 143.44 o 6 7 0 2341.60 2384.52 145.87 o 7 7 0 2927.09 2873.60 173.45 o 8 7 0 353.56 356.00 82.86 o 9 7 0 142.14 169.77 67.85 o 0 8 0 319.23 476.80 57.29 o 1 8 0 1741.03 1570.81 58.22 o 2 8 0 886.15 852.72 55.81 o 3 8 0 821.17 1156.46 75.53 o 4 8 0 47.66 77.29 51.48 o 5 8 0 27.75 91.93 48.34 o 6 8 0 247.20 290.51 66.35 o 7 8 0 812.44 938.83 112.59 o 8 8 0 1367.23 1337.45 143.38 o 9 8 0 387.92 372.27 86.64 o 1 9 0 3.89 23.21 20.36 o 2 9 0 56.87 67.44 27.36 o 3 9 0 3367.55 3467.76 114.93 o 4 9 0 64.09 76.04 48.21 o 5 9 0 1456.38 1686.38 115.44 o 6 9 0 662.36 799.02 98.34 o 7 9 0 801.86 846.45 108.67 o 8 9 0 14.98 31.32 57.40 o 9 9 0 180.17 240.95 73.49 o 0 10 0 10.73 .77 27.69 o 1 10 0 3828.37 3657.78 91.77 o 2 10 0 2491.71 2355.04 82.52 o 3 10 0 283.35 437.89 59.96 o 4 10 0 2507.44 2942.09 126.29 o 5 10 0 11.02 41.52 40.73 o 6 10 0 4.98 21.13 46.04 o 7 10 0 2.29 93.53 52.92 o 8 10 0 295.46 401.59 83.43 o 9 10 0 53.25 83.63 62.80 o 1 11 0 175.81 175.59 31.26 o 2 11 0 152.20 205.37 36.36 o 3 11 0 487.56 682.57 67.72 o 4 11 0 911.52 1152.41 90.80 o 5 11 0 42.09 94.43 46.38 o 6 11 0 240.02 304.17 67.12 o 7 11 0 309.56 324.51 73.78 o 8 11 0 .01 44.24 53.61 o 9 11 0 56.59 15.08 65.85 o 0 12 0 5376.36 5246.83 226.51 o 1 12 0 1952.33 2053.24 75.76 o 2 12 0 87.87 124.45 27.98 o 3 12 0 4.43 53.23 38.43 o 4 12 0 721.32 790.93 84.00 o 5 12 0 102.34 223.61 57.50 o 6 12 0 420.58 479.21 80.82 o 7 12 0 2.77 71.21 55.84 o 8 12 0 .63 9.92 61.20 o 9 12 0 3.53 2.57 60.35 o 1 13 0 3962.39 4026.19 107.80 o 2 13 0 149.14 117.07 31.01 o 3 13 0 2077.10 1974.19 97.71 o 4 13 0 538.65 633.79 75.38 o 5 13 0 1325.51 1395.56 107.02 o 6 13 0 29.12 21.77 43.01 o 7 13 0 168.87 176.79 58.51 o 8 13 0 190.61 268.72 86.23 o 9 13 0 29.01 123.70 85.95 o 0 14 0 1635.62 1660.13 142.97 o 1 14 0 3469.45 3486.24 104.62 o 2 14 0 728.96 724.72 63.03 o 3 14 0 282.74 333.77 52.00 o 4 14 0 190.50 255.80 49.47 o 5 14 0 249.95 326.11 61.03 o 6 14 0 880.12 953.95 106.34 o 7 14 0 93.53 100.17 67.04 o 8 14 0 239.44 297.92 86.80 o 9 14 0 397.12 420.19 113.83 o 1 15 0 1404.79 1416.96 75.83 o 2 15 0 1147.73 1051.27 93.18 o 3 15 0 2269.36 2328.46 115.81 o 4 15 0 989.27 1087.25 84.11 o 5 15 0 2734.11 2674.87 136.76 o 6 15 0 1539.95 1502.48 153.71 o 7 15 0 1304.30 1115.88 140.48 o 8 15 0 336.42 357.65 111.57 o 9 15 0 16.01 79.38 76.42 o 0 16 0 2056.27 1673.73 151.31 o 1 16 0 4699.12 4484.42 126.53 o 2 16 0 1687.37 1660.84 82.45 o 3 16 0 2285.15 2313.87 102.72 o 4 16 0 151.50 274.03 48.52 o 5 16 0 21.94 77.02 58.38 o 6 16 0 1768.85 1723.87 162.71 o 7 16 0 457.86 321.84 93.38 o 8 16 0 1371.41 1507.57 206.62 o 9 16 0 861.90 728.58 153.53 o 1 17 0 3719.01 3727.72 117.69 o 2 17 0 2465.46 2325.11 94.65 o 3 17 0 2828.42 2735.17 109.23 o 4 17 0 7857.73 7099.33 233.79 o 5 17 0 305.77 414.12 87.85 o 6 17 0 2967.45 2540.12 178.40 o 7 17 0 882.67 781.06 146.24 o 8 17 0 37.32 137.77 84.41 o 9 17 0 52.73 65.57 81.44 o 0 18 0 1381.95 1450.25 160.69 o 1 18 0 4739.64 4261.65 156.08 o 2 18 0 5750.48 5438.20 142.81 o 3 18 0 6138.50 6054.35 205.18 o 4 18 0 2157.54 2185.04 149.95 o 5 18 0 724.33 840.00 117.79 o 6 18 0 1649.26 1663.72 197.67 o 7 18 0 1350.64 1478.61 199.82 o 8 18 0 3003.52 2749.90 266.26 o 1 19 0 2052.62 2173.18 119.65 o 2 19 0 2250.34 2236.18 93.14 o 3 19 0 2533.33 2590.11 149.41 o 4 19 0 6263.56 5874.80 219.67 o 6 19 0 2440.96 2577.83 237.19 o 7 19 0 1647.76 1762.33 214.34 o 8 19 0 9.05 157.83 87.37 o 0 20 0 2726.08 2769.41 216.76 o 1 20 0 6896.65 6898.38 173.92 o 2 20 0 6633.62 6724.34 211.62 o 3 20 0 1973.56 2219.31 139.55 o 4 20 0 1446.46 1319.21 132.05 o 5 20 0 1307.92 1498.44 186.53 o 6 20 0 1043.10 1185.16 176.18 o 7 20 0 3182.69 3185.77 327.58 o 8 20 0 1813.85 1877.92 231.02 o 1 21 0 941.11 1102.66 87.27 o 2 21 0 3330.32 3377.38 156.96 o 3 21 0 4649.78 4601.44 188.88 o 4 21 0 295.51 459.35 108.26 o 5 21 0 3083.09 3328.68 252.89 o 6 21 0 2935.46 3104.88 261.91 o 7 21 0 1926.16 1901.43 225.02 o 8 21 0 74.12 129.19 88.14 o 0 22 0 4666.77 4691.43 212.26 o 1 22 0 6571.84 6324.70 206.68 o 2 22 0 7278.37 7031.94 225.27 o 3 22 0 214.81 225.37 60.07 o 4 22 0 15.31 46.82 68.51 o 5 22 0 1148.52 1205.36 174.10 o 6 22 0 1745.06 1882.75 219.01 o 7 22 0 2260.16 2119.27 241.74 o 8 22 0 1293.59 1189.05 188.22 o 1 23 0 335.98 516.19 79.48 o 2 23 0 7141.33 6932.80 228.61 o 3 23 0 1698.57 1961.52 188.66 o 4 23 0 3166.46 3624.37 245.26 o 5 23 0 2157.45 2140.65 217.18 o 6 23 0 2945.26 2782.75 257.55 o 7 23 0 1737.94 1668.70 217.52 o 0 24 0 3011.92 2918.78 256.28 o 1 24 0 3682.97 3550.50 185.70 o 2 24 0 3390.51 2313.17 808.20 o 3 24 0 2683.29 2817.36 200.64 o 4 24 0 331.76 401.47 104.99 o 5 24 0 405.93 416.36 106.82 o 6 24 0 1086.79 1335.31 190.09 o 7 24 0 2585.54 2677.05 267.60 o 1 25 0 446.95 216.01 181.92 o 2 25 0 4411.25 4645.51 232.54 o 3 25 0 4374.00 4422.55 245.96 o 4 25 0 3769.01 3900.73 242.97 o 5 25 0 3900.82 3859.15 272.28 o 6 25 0 2143.36 2176.47 238.83 o 7 25 0 604.18 632.34 134.52 o 0 26 0 891.35 1254.35 209.28 o 1 26 0 3778.02 4056.13 399.55 o 2 26 0 1675.92 1638.83 253.68 o 3 26 0 1990.45 2078.80 203.37 o 4 26 0 6.69 38.41 70.36 o 5 26 0 83.17 162.87 75.65 o 6 26 0 1192.54 1348.67 190.46 o 7 26 0 2294.50 2358.93 258.55 o 1 27 0 389.97 646.67 192.17 o 2 27 0 3265.91 3433.71 272.30 o 3 27 0 3654.22 3847.77 240.32 o 4 27 0 2469.90 2591.99 236.94 o 5 27 0 2234.91 2212.49 230.14 o 6 27 0 1346.67 1483.14 200.71 o 0 28 0 3040.90 3056.93 524.96 o 1 28 0 2215.13 2292.74 332.00 o 2 28 0 1172.46 1304.10 190.60 o 3 28 0 461.92 671.44 145.25 o 4 28 0 56.27 86.76 73.15 o 5 28 0 297.10 373.41 101.99 o 6 28 0 448.37 459.17 116.36 o 1 29 0 299.78 401.86 167.70 o 2 29 0 1244.51 1443.37 284.35 o 3 29 0 1144.72 1474.55 218.55 o 4 29 0 1229.27 557.57 318.23 o 5 29 0 1858.76 1919.97 215.85 o 6 29 0 433.59 452.44 119.57 o 0 30 0 4107.79 3327.24 559.60 o 1 30 0 780.27 940.65 232.23 o 2 30 0 728.57 806.66 268.08 o 3 30 0 565.50 456.88 115.09 o 4 30 0 41.44 162.92 93.85 o 5 30 0 .27 -45.80 65.97 o 1 31 0 575.81 512.01 179.62 o 2 31 0 61.41 191.30 129.76 o 3 31 0 739.86 777.66 213.94 o 4 31 0 274.44 351.72 118.62 o 5 31 0 105.99 226.83 110.28 o 0 32 0 354.56 221.03 207.32 o 1 32 0 141.24 153.56 123.80 o 2 32 0 88.38 86.07 123.08 o 3 32 0 41.57 48.45 117.00 o 4 32 0 94.05 111.30 142.36 o 5 32 0 78.54 93.21 106.41 o 1 33 0 9.71 104.26 114.50 o 2 33 0 .27 39.75 111.32 o 3 33 0 .23 108.19 122.39 o 4 33 0 2.33 .81 123.81 o 0 34 0 1.37 -48.17 137.10 o 1 34 0 11.57 -12.02 116.43 o 2 34 0 .90 5.54 117.10 o 3 34 0 6.45 -13.23 121.06 o 4 34 0 13.68 152.67 141.04 o 1 35 0 76.86 -14.78 132.87 o 2 35 0 199.53 368.19 177.01 o 3 35 0 9.65 134.21 139.47 o 0 36 0 496.12 424.27 263.82 o 1 36 0 307.41 438.09 183.32 o 2 36 0 .33 25.44 132.16 o -10 1 1 7.36 63.38 67.12 o -9 1 1 4.18 6.98 64.68 o -8 1 1 111.16 184.44 74.00 o -7 1 1 1264.73 1430.84 136.57 o -6 1 1 206.62 192.24 61.37 o -5 1 1 348.29 380.72 76.04 o -4 1 1 .27 18.41 32.97 o -3 1 1 495.86 518.76 57.61 o -2 1 1 606.02 767.55 50.06 o -1 1 1 1873.42 2092.95 47.29 o 0 1 1 536.27 613.05 21.77 o 1 1 1 5778.81 5988.38 96.30 o 2 1 1 701.18 889.92 59.68 o 3 1 1 86.11 88.14 36.22 o 4 1 1 501.90 615.74 74.75 o 5 1 1 1333.52 1672.70 123.14 o 6 1 1 1091.40 1025.54 111.03 o 7 1 1 1501.85 1515.87 143.14 o 8 1 1 3.28 88.20 63.50 o 9 1 1 6.23 47.07 61.45 o -10 2 1 151.40 120.44 71.66 o -9 2 1 79.49 145.44 73.02 o -8 2 1 117.65 225.84 85.79 o -7 2 1 27.09 107.85 61.23 o -6 2 1 9.25 -10.35 44.38 o -5 2 1 299.92 405.34 77.27 o -4 2 1 12.35 42.36 37.54 o -3 2 1 9.67 18.60 27.82 o -2 2 1 444.29 486.90 44.10 o -1 2 1 15270.40 16942.09 144.91 o 0 2 1 1143.09 1208.44 32.55 o 1 2 1 11049.44 12446.84 192.23 o 2 2 1 100.09 84.28 31.14 o 3 2 1 1.17 58.38 32.13 o 4 2 1 140.13 244.54 55.65 o 5 2 1 42.83 96.73 50.36 o 6 2 1 4.38 62.31 50.10 o 7 2 1 218.71 320.84 79.26 o 8 2 1 78.49 158.70 65.59 o 9 2 1 313.69 284.52 76.94 o -10 3 1 222.96 207.12 79.93 o -9 3 1 39.52 104.56 67.17 o -8 3 1 2142.44 1926.82 165.97 o -7 3 1 426.83 468.52 98.55 o -6 3 1 1816.03 1997.90 154.94 o -5 3 1 3726.78 3720.94 165.16 o -4 3 1 3423.41 3628.39 141.12 o -3 3 1 5945.52 6265.34 141.16 o -2 3 1 3846.77 3916.33 94.51 o -1 3 1 33.65 41.36 19.08 o 0 3 1 46.48 33.15 6.04 o 1 3 1 14849.01 15671.57 246.36 o 2 3 1 49.26 62.60 29.69 o 3 3 1 417.77 354.76 51.60 o 4 3 1 2986.54 2809.39 119.18 o 5 3 1 1647.04 2072.54 131.94 o 6 3 1 2091.06 2058.69 145.58 o 7 3 1 3315.51 3425.47 186.02 o 8 3 1 232.81 219.79 69.56 o 9 3 1 1.40 59.86 67.08 o -10 4 1 387.91 346.73 89.68 o -9 4 1 464.99 512.08 100.63 o -8 4 1 4470.51 4306.29 208.36 o -7 4 1 65.89 112.28 60.92 o -6 4 1 2673.00 2644.58 156.46 o -5 4 1 1936.99 2260.49 135.60 o -4 4 1 3913.61 4821.81 137.02 o -3 4 1 2880.95 3083.15 102.64 o -2 4 1 68.96 94.94 30.21 o -1 4 1 767.31 877.40 43.94 o 0 4 1 12002.43 12829.53 206.68 o 1 4 1 1948.64 1966.25 43.60 o 2 4 1 2814.74 2789.68 85.27 o 3 4 1 4593.85 4717.54 159.86 o 4 4 1 407.63 547.90 73.92 o 5 4 1 16.04 17.10 41.58 o 6 4 1 128.30 202.30 61.22 o 7 4 1 251.88 321.83 76.48 o 8 4 1 994.37 1011.24 138.42 o 9 4 1 1121.84 1052.17 128.36 o -10 5 1 545.84 562.24 105.16 o -9 5 1 181.55 286.89 82.49 o -8 5 1 401.31 678.09 105.51 o -7 5 1 1552.02 1567.44 142.98 o -6 5 1 1969.88 2060.90 143.05 o -5 5 1 5433.79 5537.69 179.54 o -4 5 1 10820.32 11061.87 220.07 o -3 5 1 1268.44 1030.19 73.35 o -2 5 1 6326.72 6526.23 126.34 o -1 5 1 5622.46 5664.68 108.22 o 0 5 1 943.66 1138.80 65.05 o 1 5 1 9084.96 9002.45 112.64 o 2 5 1 189.43 204.31 36.12 o 3 5 1 2908.23 2617.60 99.10 o 4 5 1 18748.92 20053.63 328.72 o 5 5 1 1098.47 1174.39 113.44 o 6 5 1 1847.88 2249.55 156.63 o 7 5 1 2735.80 2785.58 185.23 o 8 5 1 271.36 293.65 73.73 o 9 5 1 143.45 212.07 72.56 o -10 6 1 849.75 675.22 111.06 o -9 6 1 1367.68 1348.93 149.88 o -8 6 1 6204.00 5902.73 237.73 o -7 6 1 1539.08 1730.22 147.85 o -6 6 1 2126.79 2090.62 143.93 o -5 6 1 353.14 310.31 71.62 o -4 6 1 7345.94 8377.53 193.89 o -3 6 1 4506.93 4849.74 130.35 o -2 6 1 1618.12 1530.84 67.86 o -1 6 1 3318.42 3169.89 79.89 o 0 6 1 55.06 136.88 28.50 o 1 6 1 15252.38 15411.61 309.81 o 2 6 1 7140.98 7686.64 151.13 o 3 6 1 10471.09 10918.79 194.67 o 4 6 1 461.90 607.33 77.80 o 5 6 1 470.88 552.99 79.56 o 6 6 1 1122.91 1146.32 115.67 o 7 6 1 2562.45 2589.19 168.40 o 8 6 1 806.13 868.62 116.37 o 9 6 1 3253.49 2998.75 214.58 o -10 7 1 866.03 940.44 128.56 o -9 7 1 298.84 382.73 90.77 o -8 7 1 79.11 149.20 66.58 o -7 7 1 997.31 1096.30 124.15 o -6 7 1 2241.44 2368.75 146.25 o -5 7 1 7646.27 8083.30 215.44 o -4 7 1 3463.09 3025.67 123.74 o -3 7 1 12880.06 13396.47 216.19 o -2 7 1 3814.19 3835.58 103.57 o -1 7 1 47.18 127.13 30.30 o 0 7 1 1452.01 1516.10 42.42 o 1 7 1 7795.64 7708.61 210.73 o 2 7 1 2538.98 2380.52 76.71 o 3 7 1 2805.77 2640.11 98.92 o 4 7 1 9240.20 9269.41 209.29 o 5 7 1 5673.02 5099.16 197.50 o 6 7 1 3592.29 3594.28 167.36 o 7 7 1 1403.73 1524.66 140.71 o 8 7 1 122.96 117.43 61.92 o 9 7 1 25.49 152.31 64.41 o -10 8 1 1727.60 1589.69 167.10 o -9 8 1 2787.30 2510.69 193.80 o -8 8 1 2750.63 2762.56 191.52 o -7 8 1 4011.59 4201.43 191.14 o -6 8 1 3006.64 3204.10 155.08 o -5 8 1 1955.85 2007.43 129.91 o -4 8 1 .48 2.95 48.51 o -3 8 1 2630.81 2587.36 100.90 o -2 8 1 8704.30 8791.02 158.14 o -1 8 1 13268.85 12527.40 167.46 o 0 8 1 23476.38 23368.75 599.22 o 1 8 1 14621.73 14234.99 308.38 o 2 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