#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/68/2226805.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226805_Fobs loop_ _publ_author_name 'Saeed, Aamer' 'Kazmi, Madiha' 'Ameen Samra, Shahid' 'Irfan, Madiha' 'Bolte, Michael' _publ_section_title ; 1,1'-(9-Octyl-9H-carbazole-3,6-diyl)diethanone ; _journal_coeditor_code BV2151 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2118 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.7460 _cell_length_b 10.3842 _cell_length_c 20.9940 _exptl_crystal_F_000 1568.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file bv2151Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sa38 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 303.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8713.59 9652.39 10.38 o 4 0 0 23247.41 26246.29 17.23 o 6 0 0 2267.72 1737.49 101.18 o 8 0 0 4002.37 3898.02 133.59 o 10 0 0 6788.73 7382.83 164.88 o 12 0 0 3181.54 3457.24 111.67 o 14 0 0 190.61 187.93 68.92 o 16 0 0 335.69 384.58 78.53 o 18 0 0 1317.27 1356.44 92.57 o 20 0 0 182.42 214.78 86.77 o 22 0 0 30.48 4.54 91.09 o 2 1 0 26914.22 31524.45 19.19 o 4 1 0 14061.26 12407.63 697.69 o 6 1 0 8447.71 7920.96 644.23 o 8 1 0 1123.51 1065.10 90.45 o 10 1 0 20.75 101.51 47.26 o 12 1 0 622.81 690.90 74.60 o 14 1 0 119.37 147.75 39.67 o 16 1 0 5.29 26.19 52.12 o 18 1 0 112.65 113.33 44.13 o 20 1 0 2321.41 2567.76 83.90 o 22 1 0 1803.76 1945.25 144.00 o 0 2 0 1670.85 1749.40 4.35 o 2 2 0 48375.13 57116.06 26.01 o 4 2 0 28047.88 27102.71 285.76 o 6 2 0 18451.97 18374.28 507.84 o 8 2 0 1290.01 1342.61 63.21 o 10 2 0 1478.09 1512.53 61.19 o 12 2 0 442.10 383.37 52.04 o 14 2 0 96.65 101.06 71.96 o 16 2 0 7.06 -15.48 75.68 o 18 2 0 0.49 -6.47 53.62 o 20 2 0 479.83 551.55 63.03 o 22 2 0 618.61 699.10 70.78 o 2 3 0 749.33 781.03 2.90 o 4 3 0 5817.77 5230.14 167.39 o 6 3 0 542.34 512.14 82.95 o 8 3 0 83.79 97.10 49.79 o 10 3 0 345.47 348.87 50.00 o 12 3 0 59.38 71.61 46.34 o 14 3 0 1269.48 1387.02 96.89 o 16 3 0 31.82 15.03 52.69 o 18 3 0 396.07 418.30 90.28 o 20 3 0 29.80 38.00 49.46 o 0 4 0 1477.17 1588.35 4.14 o 2 4 0 175.96 177.73 1.38 o 4 4 0 202.88 145.30 55.90 o 6 4 0 2313.06 2407.63 114.93 o 8 4 0 512.59 511.99 60.68 o 10 4 0 7.32 5.70 39.54 o 12 4 0 811.37 820.39 59.41 o 14 4 0 250.18 216.79 47.27 o 16 4 0 245.99 233.03 59.10 o 18 4 0 0.96 25.37 79.78 o 20 4 0 227.60 192.01 92.29 o 2 5 0 139.06 145.29 1.24 o 4 5 0 1011.70 1064.28 3.39 o 6 5 0 436.80 414.28 57.47 o 8 5 0 511.47 473.33 80.41 o 10 5 0 249.19 256.78 71.45 o 12 5 0 142.67 166.86 75.17 o 14 5 0 50.37 51.57 56.19 o 16 5 0 268.31 229.31 78.59 o 18 5 0 63.47 64.22 0.83 o 20 5 0 240.08 246.25 1.63 o 0 6 0 1998.61 2075.21 4.73 o 2 6 0 4.14 4.16 0.21 o 4 6 0 3694.61 3857.06 6.46 o 6 6 0 1024.68 1020.73 73.51 o 8 6 0 829.13 799.09 82.28 o 10 6 0 566.91 511.19 66.40 o 12 6 0 565.64 493.84 83.30 o 14 6 0 5.85 -3.64 53.06 o 16 6 0 92.62 143.26 81.71 o 18 6 0 168.84 301.79 90.65 o 2 7 0 652.58 671.73 2.69 o 4 7 0 549.69 571.96 2.48 o 6 7 0 212.79 289.00 76.95 o 8 7 0 10.48 30.14 75.01 o 10 7 0 288.38 253.28 59.70 o 12 7 0 525.71 462.11 80.84 o 14 7 0 23.11 -17.63 77.92 o 16 7 0 239.16 272.99 85.96 o 18 7 0 0.95 -1.48 62.51 o 0 8 0 226.07 225.12 1.56 o 2 8 0 0.08 0.10 0.03 o 4 8 0 0.22 0.21 0.04 o 6 8 0 13.66 4.54 76.72 o 8 8 0 821.04 612.58 67.30 o 10 8 0 12.64 24.71 74.94 o 12 8 0 215.13 124.59 60.14 o 14 8 0 100.82 32.22 80.52 o 16 8 0 3.89 -4.54 84.24 o 2 9 0 149.37 153.43 1.28 o 4 9 0 660.63 672.96 2.69 o 6 9 0 53.14 83.20 78.80 o 8 9 0 332.90 347.89 90.44 o 10 9 0 139.04 114.54 80.75 o 12 9 0 114.03 92.35 84.84 o 14 9 0 56.85 94.29 86.32 o 0 10 0 726.17 738.74 2.82 o 2 10 0 0.06 0.00 0.10 o 4 10 0 387.72 394.33 2.05 o 6 10 0 92.19 121.82 85.81 o 8 10 0 14.43 -10.87 61.17 o 10 10 0 75.01 70.03 95.19 o 12 10 0 147.97 189.48 67.20 o 2 11 0 10.00 9.99 0.32 o 4 11 0 181.06 177.21 1.38 o 6 11 0 14.21 -10.57 100.83 o 8 11 0 108.02 56.71 71.44 o 10 11 0 0.16 19.87 92.13 o 0 12 0 1409.18 1408.78 3.90 o 2 12 0 61.24 58.70 0.80 o 4 12 0 0.06 0.07 0.02 o 1 1 1 370.75 389.72 2.05 o 2 1 1 1402.77 1499.87 4.02 o 3 1 1 2248.51 1996.21 74.32 o 4 1 1 13.95 -14.86 36.06 o 5 1 1 752.78 673.56 43.84 o 6 1 1 510.82 454.22 36.15 o 7 1 1 637.60 554.01 41.73 o 8 1 1 101.50 79.45 39.09 o 9 1 1 3.11 34.30 46.50 o 10 1 1 11.36 4.30 45.16 o 11 1 1 2738.71 2566.11 69.48 o 12 1 1 337.45 377.49 47.79 o 13 1 1 63.64 64.67 32.11 o 14 1 1 223.31 251.68 34.87 o 15 1 1 66.18 70.38 31.62 o 16 1 1 14.67 7.52 33.61 o 17 1 1 484.06 503.75 42.57 o 18 1 1 638.78 626.62 35.69 o 19 1 1 666.48 665.38 41.01 o 20 1 1 133.51 143.16 38.41 o 21 1 1 30.62 22.47 38.94 o 22 1 1 50.87 42.53 45.96 o 0 2 1 5294.70 5726.56 7.90 o 1 2 1 5571.80 6074.69 8.13 o 2 2 1 6542.68 4559.05 176.92 o 3 2 1 92288.31 82828.48 2564.03 o 4 2 1 40686.82 39908.43 281.26 o 5 2 1 2309.28 2088.13 81.19 o 6 2 1 3120.53 3122.45 67.60 o 7 2 1 3754.28 3821.14 95.97 o 8 2 1 719.58 757.07 42.92 o 9 2 1 4579.25 4678.75 68.91 o 10 2 1 56.98 55.70 29.53 o 11 2 1 10.72 14.38 44.21 o 12 2 1 0.71 -17.02 36.25 o 13 2 1 106.53 103.80 38.34 o 14 2 1 210.40 285.29 38.18 o 15 2 1 542.06 533.38 56.99 o 16 2 1 184.81 225.54 54.29 o 17 2 1 650.74 661.98 38.49 o 18 2 1 255.95 244.51 32.98 o 19 2 1 319.83 342.42 42.60 o 20 2 1 104.71 162.81 42.03 o 21 2 1 274.66 306.77 45.70 o 22 2 1 4.25 15.79 46.23 o 1 3 1 1122.24 1214.89 3.62 o 2 3 1 1.61 1.65 0.13 o 3 3 1 7572.28 6576.42 186.86 o 4 3 1 1005.42 842.97 60.91 o 5 3 1 10780.57 9742.03 834.49 o 6 3 1 5692.43 5412.25 337.40 o 7 3 1 1987.88 1841.82 60.94 o 8 3 1 309.37 266.96 29.87 o 9 3 1 25.96 13.45 30.07 o 10 3 1 236.15 223.97 25.94 o 11 3 1 0.00 -6.67 28.88 o 12 3 1 34.71 39.84 29.54 o 13 3 1 128.19 131.39 31.59 o 14 3 1 351.51 327.83 47.57 o 15 3 1 312.52 318.24 59.28 o 16 3 1 216.36 208.01 56.02 o 17 3 1 3.98 17.60 43.00 o 18 3 1 65.33 107.80 54.92 o 19 3 1 46.41 72.40 41.28 o 20 3 1 6.31 44.27 42.12 o 21 3 1 32.88 29.48 38.85 o 0 4 1 139.05 139.81 1.22 o 1 4 1 92.46 90.58 0.99 o 2 4 1 98.54 102.22 1.04 o 3 4 1 4657.82 4929.76 7.31 o 4 4 1 216.48 177.15 70.63 o 5 4 1 3629.11 3089.87 80.79 o 6 4 1 9477.67 9270.67 134.32 o 7 4 1 8466.34 7629.62 118.02 o 8 4 1 635.52 686.78 58.74 o 9 4 1 334.32 357.28 39.71 o 10 4 1 4.75 14.31 38.44 o 11 4 1 47.10 41.74 34.63 o 12 4 1 69.60 77.53 32.00 o 13 4 1 177.46 135.60 32.36 o 14 4 1 10.87 44.65 37.51 o 15 4 1 19.02 31.58 34.68 o 16 4 1 32.66 63.47 59.23 o 17 4 1 9.12 19.22 54.09 o 18 4 1 170.10 231.06 59.12 o 19 4 1 50.95 25.78 59.68 o 20 4 1 18.58 49.78 61.04 o 21 4 1 46.84 15.22 46.48 o 1 5 1 584.82 613.31 2.58 o 2 5 1 1326.01 1409.54 3.90 o 3 5 1 36.23 37.11 0.64 o 4 5 1 4887.40 5197.97 7.50 o 5 5 1 146.97 105.41 40.95 o 6 5 1 1042.19 998.12 53.98 o 7 5 1 0.24 -5.94 47.25 o 8 5 1 1173.41 1244.40 148.74 o 9 5 1 176.68 166.74 38.55 o 10 5 1 351.76 328.79 45.46 o 11 5 1 68.18 98.39 50.46 o 12 5 1 58.74 39.00 45.28 o 13 5 1 29.48 28.08 43.34 o 14 5 1 81.30 45.74 39.17 o 15 5 1 139.84 129.71 55.07 o 16 5 1 25.23 41.46 44.21 o 17 5 1 58.19 85.94 57.64 o 18 5 1 63.18 43.98 86.85 o 19 5 1 13.92 -20.69 85.36 o 20 5 1 10.21 16.07 91.46 o 0 6 1 1057.99 1128.58 3.49 o 1 6 1 11.49 11.63 0.36 o 2 6 1 3652.36 3798.35 6.40 o 3 6 1 262.29 263.57 1.68 o 4 6 1 237.89 247.92 1.64 o 5 6 1 205.81 197.53 56.42 o 6 6 1 102.80 107.92 41.16 o 7 6 1 239.31 242.76 44.60 o 8 6 1 859.77 827.40 52.43 o 9 6 1 164.37 163.64 42.59 o 10 6 1 83.49 107.91 43.04 o 11 6 1 215.26 181.10 45.23 o 12 6 1 0.44 -26.16 38.31 o 13 6 1 13.78 57.33 43.60 o 14 6 1 28.93 10.48 42.84 o 15 6 1 7.31 12.44 53.77 o 16 6 1 75.27 53.15 47.24 o 17 6 1 2.34 25.71 56.78 o 18 6 1 6.19 0.54 56.39 o 19 6 1 2.62 2.65 0.17 o 1 7 1 3.84 3.85 0.20 o 2 7 1 121.65 129.44 1.19 o 3 7 1 600.60 611.19 2.57 o 4 7 1 33.21 34.74 0.62 o 5 7 1 1.29 -28.43 49.34 o 6 7 1 384.45 386.75 46.88 o 7 7 1 104.56 96.04 36.61 o 8 7 1 27.11 -11.94 41.70 o 9 7 1 117.43 151.38 44.03 o 10 7 1 356.28 308.53 42.33 o 11 7 1 205.12 178.72 54.91 o 12 7 1 363.69 325.56 55.97 o 13 7 1 0.49 -2.28 43.37 o 14 7 1 42.16 53.42 45.61 o 15 7 1 43.78 48.60 46.57 o 16 7 1 50.09 76.57 61.69 o 17 7 1 61.14 60.29 51.69 o 18 7 1 89.59 108.21 64.85 o 0 8 1 2944.95 2987.28 5.67 o 1 8 1 2094.91 2143.28 4.81 o 2 8 1 19.40 20.06 0.46 o 3 8 1 924.31 945.16 3.18 o 4 8 1 116.48 118.06 1.13 o 5 8 1 53.33 109.02 78.00 o 6 8 1 117.88 114.10 40.01 o 7 8 1 11.36 58.25 45.77 o 8 8 1 0.52 47.44 44.18 o 9 8 1 112.61 98.53 40.35 o 10 8 1 33.12 44.57 53.40 o 11 8 1 228.57 294.12 56.02 o 12 8 1 108.52 119.16 57.51 o 13 8 1 122.25 133.03 57.96 o 14 8 1 45.65 31.84 49.33 o 15 8 1 34.27 70.63 57.76 o 16 8 1 1.96 40.15 61.06 o 1 9 1 137.70 139.26 1.22 o 2 9 1 492.42 500.41 2.32 o 3 9 1 605.03 617.60 2.58 o 4 9 1 527.46 545.20 2.42 o 5 9 1 2.51 53.43 85.20 o 6 9 1 100.79 150.97 47.16 o 7 9 1 9.78 15.83 47.58 o 8 9 1 0.68 14.96 56.71 o 9 9 1 40.50 24.73 46.57 o 10 9 1 28.89 15.40 58.15 o 11 9 1 24.45 26.24 47.35 o 12 9 1 35.35 32.57 51.05 o 13 9 1 5.45 -13.60 58.61 o 14 9 1 26.11 54.07 61.17 o 15 9 1 59.12 101.76 60.39 o 0 10 1 222.07 227.54 1.56 o 1 10 1 44.51 42.58 0.67 o 2 10 1 1372.59 1377.15 3.86 o 3 10 1 228.63 236.27 1.59 o 4 10 1 314.34 313.35 1.84 o 5 10 1 829.31 722.52 74.00 o 6 10 1 11.25 49.75 49.41 o 7 10 1 305.47 284.46 53.63 o 8 10 1 116.47 75.20 43.55 o 9 10 1 0.13 -41.26 63.63 o 10 10 1 3.74 63.60 64.30 o 11 10 1 9.34 -10.11 51.59 o 12 10 1 8.75 81.45 54.94 o 13 10 1 36.60 62.76 54.57 o 1 11 1 846.82 841.64 3.02 o 2 11 1 357.27 358.66 1.97 o 3 11 1 25.53 25.46 0.53 o 4 11 1 84.14 83.07 0.94 o 5 11 1 21.73 103.15 90.86 o 6 11 1 97.84 81.69 55.69 o 7 11 1 4.15 7.62 56.22 o 8 11 1 0.58 25.78 66.93 o 9 11 1 193.66 176.01 57.23 o 10 11 1 2.38 -11.52 54.59 o 0 12 1 489.84 482.51 2.29 o 1 12 1 62.57 62.96 0.82 o 2 12 1 49.08 49.43 0.73 o 3 12 1 16.91 17.28 0.43 o 4 12 1 13.27 10.27 66.75 o 5 12 1 10.67 -16.83 67.40 o 0 0 2 1897.38 2059.43 4.73 o 1 0 2 21638.91 25378.23 17.26 o 2 0 2 603.91 637.33 2.62 o 3 0 2 2367.86 1898.15 117.55 o 4 0 2 6061.24 5000.26 169.29 o 5 0 2 4509.08 4202.79 150.57 o 6 0 2 1.15 16.23 43.16 o 7 0 2 3630.52 3423.89 123.57 o 8 0 2 25.22 26.33 44.23 o 9 0 2 0.31 8.76 42.92 o 10 0 2 300.65 274.07 39.19 o 11 0 2 2226.09 2321.20 101.65 o 12 0 2 9.43 11.45 43.42 o 13 0 2 2958.25 2943.56 125.50 o 14 0 2 171.27 169.84 48.07 o 15 0 2 85.79 71.92 40.16 o 16 0 2 1713.57 1938.18 181.31 o 17 0 2 20.75 51.39 51.38 o 18 0 2 2626.40 2521.26 65.52 o 19 0 2 358.47 365.04 58.52 o 20 0 2 526.86 451.37 52.22 o 21 0 2 12.46 11.07 48.63 o 22 0 2 55.21 65.10 62.70 o 1 1 2 1126.67 1220.59 3.63 o 2 1 2 2070.88 1655.97 82.96 o 3 1 2 3679.98 2986.93 84.66 o 4 1 2 11573.50 10273.53 164.55 o 5 1 2 2417.93 2237.15 65.19 o 6 1 2 840.26 736.59 41.41 o 7 1 2 612.51 612.11 46.36 o 8 1 2 851.32 867.27 59.63 o 9 1 2 1174.60 1067.90 116.63 o 10 1 2 1082.86 1190.48 60.46 o 11 1 2 1.94 36.00 45.65 o 12 1 2 0.90 12.95 44.40 o 13 1 2 2.78 39.81 37.59 o 14 1 2 366.63 378.35 35.96 o 15 1 2 413.17 426.60 36.17 o 16 1 2 21.83 10.43 29.70 o 17 1 2 68.00 62.57 30.46 o 18 1 2 28.61 34.46 30.06 o 19 1 2 738.87 705.76 54.16 o 20 1 2 33.71 53.50 37.20 o 21 1 2 866.06 771.61 46.12 o 22 1 2 165.56 106.37 36.47 o 0 2 2 1463.28 1572.37 4.12 o 1 2 2 12432.56 13763.60 12.33 o 2 2 2 10021.51 7223.65 207.20 o 3 2 2 36388.55 31220.38 1313.22 o 4 2 2 21842.09 20766.63 516.94 o 5 2 2 5606.35 5001.66 144.86 o 6 2 2 1034.65 957.04 46.03 o 7 2 2 94.86 85.09 31.71 o 8 2 2 142.15 144.49 34.43 o 9 2 2 868.68 860.95 39.75 o 10 2 2 219.75 205.99 26.46 o 11 2 2 780.88 881.17 57.62 o 12 2 2 635.34 675.39 53.72 o 13 2 2 81.11 123.87 37.81 o 14 2 2 13.33 34.85 48.40 o 15 2 2 1754.33 1844.95 70.44 o 16 2 2 86.97 102.22 34.13 o 17 2 2 0.10 19.59 32.58 o 18 2 2 309.86 299.14 32.55 o 19 2 2 490.57 457.59 36.72 o 20 2 2 369.58 345.21 38.40 o 21 2 2 181.71 177.03 37.26 o 1 3 2 4636.62 5028.18 7.38 o 2 3 2 249.41 261.37 1.68 o 3 3 2 13176.62 10756.82 219.23 o 4 3 2 2388.64 1895.81 98.39 o 5 3 2 10429.18 9546.29 183.70 o 6 3 2 2934.85 2801.02 129.13 o 7 3 2 4377.49 4366.06 243.55 o 8 3 2 2141.73 2051.87 70.78 o 9 3 2 1170.75 1120.73 39.80 o 10 3 2 46.90 77.53 33.84 o 11 3 2 488.86 502.56 37.30 o 12 3 2 123.67 120.37 33.94 o 13 3 2 90.61 91.81 39.88 o 14 3 2 137.83 104.65 42.41 o 15 3 2 1979.68 2158.12 72.77 o 16 3 2 863.25 786.46 52.79 o 17 3 2 177.25 192.17 45.01 o 18 3 2 928.93 1033.55 64.46 o 19 3 2 59.48 72.23 41.78 o 20 3 2 52.85 73.91 43.11 o 21 3 2 1.44 -1.80 32.34 o 0 4 2 1200.77 1280.81 3.72 o 1 4 2 1417.19 1522.68 4.06 o 2 4 2 48.44 49.38 0.73 o 3 4 2 897.64 952.13 3.20 o 4 4 2 10887.06 10268.44 194.01 o 5 4 2 4496.62 4353.62 100.39 o 6 4 2 4261.01 4419.45 97.04 o 7 4 2 14575.19 14837.23 443.05 o 8 4 2 211.50 178.61 36.10 o 9 4 2 161.54 148.65 37.31 o 10 4 2 4.56 6.48 28.20 o 11 4 2 132.42 155.62 32.68 o 12 4 2 354.33 340.10 43.22 o 13 4 2 30.89 23.62 29.67 o 14 4 2 201.71 231.10 35.81 o 15 4 2 273.93 306.01 45.63 o 16 4 2 15.05 17.68 54.01 o 17 4 2 311.38 325.77 56.66 o 18 4 2 6.50 15.28 59.86 o 19 4 2 104.48 128.05 61.02 o 20 4 2 0.35 -3.66 47.77 o 21 4 2 4.04 35.03 52.67 o 1 5 2 71.04 76.68 0.91 o 2 5 2 6.27 6.35 0.26 o 3 5 2 1089.14 1163.45 3.54 o 4 5 2 1774.88 1474.41 82.14 o 5 5 2 1037.31 932.76 70.76 o 6 5 2 20.87 11.06 39.26 o 7 5 2 52.84 43.30 39.35 o 8 5 2 1713.55 1648.14 118.21 o 9 5 2 1415.64 1207.38 102.95 o 10 5 2 748.51 713.24 56.38 o 11 5 2 1446.41 1457.35 67.29 o 12 5 2 15.34 16.54 42.07 o 13 5 2 107.71 134.55 56.13 o 14 5 2 26.61 37.97 38.45 o 15 5 2 256.98 247.93 40.05 o 16 5 2 129.57 134.73 38.82 o 17 5 2 0.43 -7.53 57.75 o 18 5 2 77.04 82.90 56.41 o 19 5 2 64.34 41.16 77.70 o 20 5 2 20.56 65.63 91.61 o 0 6 2 5468.36 5733.54 7.87 o 1 6 2 35.79 36.16 0.63 o 2 6 2 7.24 7.30 0.28 o 3 6 2 2780.41 2901.97 5.59 o 4 6 2 322.51 278.39 56.34 o 5 6 2 0.00 23.97 68.83 o 6 6 2 0.05 27.87 50.32 o 7 6 2 753.71 789.53 52.11 o 8 6 2 1094.63 995.79 93.50 o 9 6 2 2814.44 2783.37 136.14 o 10 6 2 1192.55 1135.17 109.36 o 11 6 2 873.06 811.49 55.05 o 12 6 2 58.15 42.56 53.95 o 13 6 2 28.70 34.07 43.60 o 14 6 2 16.54 -20.36 43.79 o 15 6 2 325.07 270.48 42.25 o 16 6 2 55.21 40.29 46.62 o 17 6 2 17.25 3.83 58.74 o 18 6 2 76.62 119.29 63.98 o 19 6 2 22.65 22.63 0.49 o 1 7 2 55.22 55.05 0.77 o 2 7 2 157.92 164.48 1.33 o 3 7 2 148.61 153.61 1.28 o 4 7 2 177.15 183.05 1.40 o 5 7 2 120.28 143.48 70.40 o 6 7 2 346.24 301.35 46.49 o 7 7 2 329.78 385.54 56.30 o 8 7 2 55.98 70.23 53.57 o 9 7 2 715.77 760.66 63.18 o 10 7 2 10.68 -2.64 43.87 o 11 7 2 96.20 153.47 55.75 o 12 7 2 372.65 306.30 51.40 o 13 7 2 110.72 85.97 46.31 o 14 7 2 273.61 220.86 43.44 o 15 7 2 56.09 12.40 56.01 o 16 7 2 23.11 1.48 58.08 o 17 7 2 0.72 65.73 60.09 o 18 7 2 30.81 59.05 62.95 o 0 8 2 3.72 3.62 0.19 o 1 8 2 527.75 531.42 2.39 o 2 8 2 17.04 17.42 0.43 o 3 8 2 117.27 122.43 1.15 o 4 8 2 42.61 42.68 0.67 o 5 8 2 441.68 375.53 64.17 o 6 8 2 270.56 226.26 79.87 o 7 8 2 558.11 497.17 49.81 o 8 8 2 75.27 112.11 55.46 o 9 8 2 195.95 144.61 71.82 o 10 8 2 28.98 49.34 44.94 o 11 8 2 106.39 90.17 39.75 o 12 8 2 1.76 24.13 45.97 o 13 8 2 16.12 27.88 39.67 o 14 8 2 19.73 21.16 57.40 o 15 8 2 7.29 8.56 61.38 o 16 8 2 112.60 92.40 63.82 o 1 9 2 46.19 46.19 0.71 o 2 9 2 108.29 109.25 1.09 o 3 9 2 103.82 105.60 1.07 o 4 9 2 109.68 109.36 1.09 o 5 9 2 111.61 73.90 55.75 o 6 9 2 622.07 494.22 70.80 o 7 9 2 23.41 24.57 57.09 o 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3 976.00 889.89 75.65 o 2 1 3 1350.08 1202.44 75.65 o 3 1 3 628.53 485.80 44.53 o 4 1 3 3177.93 2779.41 74.96 o 5 1 3 241.94 221.25 34.43 o 6 1 3 517.94 482.64 41.45 o 7 1 3 76.56 72.66 38.86 o 8 1 3 1916.27 1701.96 66.05 o 9 1 3 164.18 121.11 47.73 o 10 1 3 106.42 101.63 44.94 o 11 1 3 1762.55 1875.45 70.08 o 12 1 3 8.28 40.69 37.82 o 13 1 3 7.20 31.98 37.17 o 14 1 3 46.79 38.15 29.51 o 15 1 3 47.45 44.32 30.70 o 16 1 3 25.04 37.99 29.04 o 17 1 3 32.57 52.19 29.80 o 18 1 3 91.77 109.08 33.99 o 19 1 3 90.28 105.56 36.24 o 20 1 3 7.43 19.82 34.17 o 21 1 3 427.38 444.15 46.42 o 22 1 3 27.96 37.41 45.12 o 0 2 3 12969.78 14411.99 12.62 o 1 2 3 15281.86 11347.23 257.64 o 2 2 3 2220.39 1762.23 74.33 o 3 2 3 5785.45 5271.71 116.26 o 4 2 3 4605.58 4032.82 145.64 o 5 2 3 59.32 55.09 38.41 o 6 2 3 276.27 280.18 42.93 o 7 2 3 78.73 86.60 29.98 o 8 2 3 1036.33 1054.34 42.45 o 9 2 3 2687.25 2975.42 129.73 o 10 2 3 52.87 35.69 31.56 o 11 2 3 162.13 158.95 32.27 o 12 2 3 259.78 266.41 49.75 o 13 2 3 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4 2343.12 2064.15 75.50 o 3 2 4 7433.72 6751.88 244.17 o 4 2 4 9741.70 8955.33 398.73 o 5 2 4 1030.28 899.48 48.97 o 6 2 4 352.10 317.47 38.75 o 7 2 4 2151.97 2263.32 93.17 o 8 2 4 136.65 126.50 29.70 o 9 2 4 118.61 105.24 26.22 o 10 2 4 1387.46 1295.13 45.56 o 11 2 4 321.47 294.54 37.73 o 12 2 4 513.20 560.43 53.90 o 13 2 4 27.77 32.32 46.94 o 14 2 4 1186.34 1342.44 63.95 o 15 2 4 0.34 13.29 32.34 o 16 2 4 29.34 68.54 42.96 o 17 2 4 223.16 189.39 32.43 o 18 2 4 0.11 -8.20 38.20 o 19 2 4 552.41 602.92 42.20 o 20 2 4 0.95 -9.59 35.11 o 21 2 4 336.71 398.55 43.92 o 1 3 4 1373.93 1456.73 3.97 o 2 3 4 19.98 12.35 43.24 o 3 3 4 1757.82 1500.36 84.73 o 4 3 4 1.16 4.24 38.21 o 5 3 4 1018.28 1071.89 52.18 o 6 3 4 215.34 206.74 35.55 o 7 3 4 275.11 259.57 36.44 o 8 3 4 407.93 443.97 38.62 o 9 3 4 1777.52 1782.20 53.64 o 10 3 4 645.22 708.78 46.61 o 11 3 4 1611.03 1533.39 44.76 o 12 3 4 5.00 13.23 29.59 o 13 3 4 26.68 8.67 39.03 o 14 3 4 375.18 458.40 55.37 o 15 3 4 1904.59 2032.54 72.89 o 16 3 4 368.71 371.61 55.68 o 17 3 4 794.59 763.73 54.03 o 18 3 4 173.97 156.34 42.21 o 19 3 4 41.70 29.50 42.32 o 20 3 4 0.49 3.09 40.03 o 21 3 4 22.06 17.72 33.75 o 0 4 4 192.24 194.31 1.45 o 1 4 4 152.87 155.82 1.29 o 2 4 4 127.93 111.11 66.46 o 3 4 4 0.00 5.50 46.06 o 4 4 4 370.05 390.23 55.24 o 5 4 4 2654.18 2492.52 97.73 o 6 4 4 1489.39 1540.25 74.52 o 7 4 4 2353.87 2236.77 59.90 o 8 4 4 54.78 39.94 30.35 o 9 4 4 2117.93 1884.95 78.58 o 10 4 4 61.49 73.37 39.69 o 11 4 4 12.19 25.92 34.04 o 12 4 4 3036.64 3123.73 113.00 o 13 4 4 28.03 22.13 41.96 o 14 4 4 33.46 43.29 33.14 o 15 4 4 11.84 15.73 56.21 o 16 4 4 636.35 732.50 92.98 o 17 4 4 412.04 328.84 87.68 o 18 4 4 42.87 91.76 87.66 o 19 4 4 11.40 -3.42 57.30 o 20 4 4 35.75 26.35 84.91 o 1 5 4 662.35 681.11 2.70 o 2 5 4 1271.21 1306.44 3.74 o 3 5 4 13.28 21.87 66.01 o 4 5 4 0.01 -9.52 45.40 o 5 5 4 1661.67 1544.43 91.66 o 6 5 4 177.66 206.05 52.28 o 7 5 4 1286.99 1195.01 55.72 o 8 5 4 729.56 716.10 56.30 o 9 5 4 46.66 84.00 47.49 o 10 5 4 741.65 769.76 58.47 o 11 5 4 2683.18 2398.45 83.37 o 12 5 4 992.88 960.73 48.11 o 13 5 4 564.86 614.29 45.57 o 14 5 4 533.57 451.90 47.71 o 15 5 4 571.00 572.97 51.01 o 16 5 4 0.88 39.02 45.18 o 17 5 4 87.54 115.44 59.36 o 18 5 4 12.67 35.87 56.93 o 19 5 4 3.95 83.04 88.86 o 20 5 4 0.54 -6.77 89.60 o 0 6 4 708.43 745.98 2.84 o 1 6 4 0.35 0.38 0.07 o 2 6 4 814.30 835.18 2.99 o 3 6 4 73.07 64.00 71.37 o 4 6 4 850.24 868.04 81.69 o 5 6 4 1454.27 1571.87 92.75 o 6 6 4 283.69 283.29 73.69 o 7 6 4 124.25 102.25 42.03 o 8 6 4 289.49 351.31 44.35 o 9 6 4 15.21 56.86 49.65 o 10 6 4 1413.39 1350.84 66.98 o 11 6 4 3742.98 3692.74 89.84 o 12 6 4 1380.08 1222.94 93.32 o 13 6 4 468.35 415.27 57.90 o 14 6 4 51.80 27.27 56.68 o 15 6 4 281.97 252.55 59.84 o 16 6 4 45.37 53.76 59.63 o 17 6 4 182.49 245.46 66.01 o 18 6 4 39.06 31.18 91.98 o 19 6 4 35.51 35.91 0.63 o 1 7 4 16.25 16.45 0.42 o 2 7 4 332.06 354.74 1.96 o 3 7 4 320.76 325.39 1.87 o 4 7 4 721.49 615.28 62.98 o 5 7 4 405.44 432.25 78.30 o 6 7 4 1.10 -26.57 49.34 o 7 7 4 229.43 215.99 46.96 o 8 7 4 697.15 588.04 76.35 o 9 7 4 2653.46 2687.25 81.00 o 10 7 4 1709.38 1574.88 66.37 o 11 7 4 328.64 316.55 58.09 o 12 7 4 114.75 108.45 53.88 o 13 7 4 425.07 352.20 52.29 o 14 7 4 22.47 -22.72 47.87 o 15 7 4 77.55 84.31 61.51 o 16 7 4 14.43 23.64 63.51 o 17 7 4 65.63 85.84 55.00 o 18 7 4 24.63 51.92 53.64 o 0 8 4 0.10 0.10 0.03 o 1 8 4 30.05 29.95 0.57 o 2 8 4 383.68 385.97 2.03 o 3 8 4 28.96 28.82 0.56 o 4 8 4 1.23 35.57 72.85 o 5 8 4 1206.74 1349.92 95.69 o 6 8 4 57.93 52.31 56.93 o 7 8 4 39.02 56.15 45.73 o 8 8 4 618.78 638.75 63.14 o 9 8 4 20.98 59.72 45.39 o 10 8 4 172.11 193.98 48.60 o 11 8 4 436.57 439.53 75.77 o 12 8 4 120.54 159.14 58.14 o 13 8 4 606.63 527.04 65.13 o 14 8 4 987.98 863.34 73.11 o 15 8 4 45.09 82.54 63.80 o 16 8 4 30.94 20.62 65.97 o 1 9 4 2.19 2.24 0.15 o 2 9 4 17.38 17.88 0.44 o 3 9 4 200.50 201.75 1.48 o 4 9 4 237.02 225.51 61.03 o 5 9 4 35.09 49.19 56.78 o 6 9 4 131.71 102.63 53.81 o 7 9 4 465.12 330.69 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87.92 97.74 55.11 o 2 7 11 4.23 19.06 44.00 o 3 7 11 1037.36 1003.88 70.74 o 4 7 11 62.51 39.22 73.75 o 5 7 11 150.98 223.71 77.32 o 6 7 11 272.03 197.83 58.50 o 7 7 11 88.99 108.88 66.98 o 8 7 11 3.02 -5.13 42.78 o 9 7 11 13.61 31.11 52.18 o 10 7 11 95.47 107.81 47.58 o 11 7 11 96.24 162.97 62.42 o 12 7 11 35.60 18.89 46.81 o 13 7 11 8.04 -29.69 64.55 o 14 7 11 13.47 10.52 47.67 o 15 7 11 17.31 -38.63 70.22 o 0 8 11 353.63 326.46 66.24 o 1 8 11 728.21 779.15 66.98 o 2 8 11 1045.74 1071.81 59.60 o 3 8 11 1.14 66.90 77.02 o 4 8 11 156.57 122.05 55.52 o 5 8 11 82.58 138.87 74.94 o 6 8 11 11.34 40.04 51.65 o 7 8 11 2.35 5.66 72.41 o 8 8 11 93.02 79.37 46.96 o 9 8 11 67.51 95.69 60.50 o 10 8 11 0.01 13.96 45.69 o 11 8 11 121.74 136.05 68.65 o 12 8 11 57.46 43.78 53.78 o 13 8 11 71.13 89.71 61.50 o 1 9 11 156.78 149.02 48.84 o 2 9 11 16.81 29.51 58.15 o 3 9 11 6.51 110.29 82.16 o 4 9 11 487.53 409.68 65.05 o 5 9 11 69.22 86.85 79.48 o 6 9 11 39.35 90.64 77.24 o 7 9 11 92.11 50.68 60.43 o 8 9 11 0.22 18.40 50.35 o 9 9 11 3.45 -12.27 62.48 o 10 9 11 22.04 65.79 49.58 o 11 9 11 50.09 45.87 61.09 o 0 10 11 2057.56 2166.95 122.98 o 1 10 11 99.04 143.88 53.01 o 2 10 11 6.16 44.88 48.73 o 3 10 11 795.51 702.12 54.52 o 4 10 11 76.67 208.59 85.51 o 5 10 11 43.24 -24.03 84.16 o 6 10 11 128.71 120.41 84.47 o 7 10 11 11.98 25.82 60.79 o 8 10 11 122.36 155.02 62.54 o 1 11 11 20.86 71.85 53.60 o 2 11 11 55.24 51.43 51.84 o 0 0 12 1162.20 1348.79 97.51 o 1 0 12 84.99 56.07 39.38 o 2 0 12 3387.07 3812.68 95.21 o 3 0 12 6354.03 6956.52 464.96 o 4 0 12 2535.65 2868.10 107.31 o 5 0 12 1443.32 1443.81 73.60 o 6 0 12 871.62 954.56 80.13 o 7 0 12 151.32 157.11 69.06 o 8 0 12 494.10 540.60 73.02 o 9 0 12 72.85 80.60 67.50 o 10 0 12 515.49 570.96 74.30 o 11 0 12 0.31 -0.44 67.35 o 12 0 12 1.48 -13.47 47.70 o 13 0 12 293.86 261.77 71.60 o 14 0 12 1522.65 1393.77 69.63 o 15 0 12 56.49 73.82 75.24 o 16 0 12 997.71 992.01 71.03 o 17 0 12 5.34 -41.08 54.69 o 18 0 12 149.74 220.58 87.00 o 19 0 12 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2 12 252.04 264.19 38.94 o 16 2 12 154.28 150.96 38.36 o 17 2 12 137.18 111.40 42.77 o 18 2 12 95.47 96.27 43.71 o 19 2 12 33.03 96.54 55.04 o 1 3 12 0.04 22.32 45.31 o 2 3 12 1094.12 1161.18 48.26 o 3 3 12 67.04 94.31 30.71 o 4 3 12 2450.17 2476.46 82.90 o 5 3 12 431.24 405.58 37.78 o 6 3 12 17.81 35.61 36.14 o 7 3 12 1265.50 1261.95 53.69 o 8 3 12 2.91 -30.90 38.66 o 9 3 12 2668.96 2691.49 194.66 o 10 3 12 38.61 54.44 49.16 o 11 3 12 904.24 895.92 55.96 o 12 3 12 111.42 103.90 50.33 o 13 3 12 108.63 71.30 39.68 o 14 3 12 195.01 197.92 44.23 o 15 3 12 9.07 22.40 55.62 o 16 3 12 3.59 48.71 57.72 o 17 3 12 0.39 34.82 40.90 o 18 3 12 18.75 16.26 42.83 o 0 4 12 34.61 116.54 69.80 o 1 4 12 216.39 239.00 42.52 o 2 4 12 482.97 558.98 44.48 o 3 4 12 2.33 20.52 37.25 o 4 4 12 485.71 532.72 53.79 o 5 4 12 4.69 41.05 35.98 o 6 4 12 2150.02 2306.62 75.32 o 7 4 12 476.85 461.23 43.45 o 8 4 12 7.81 24.54 46.68 o 9 4 12 954.67 960.92 69.99 o 10 4 12 2940.39 2960.36 156.32 o 11 4 12 164.12 198.86 41.63 o 12 4 12 22.95 18.49 46.68 o 13 4 12 273.39 241.29 39.01 o 14 4 12 144.22 206.74 48.41 o 15 4 12 307.74 318.90 51.80 o 16 4 12 14.81 34.53 60.15 o 17 4 12 68.30 110.38 59.68 o 18 4 12 2.98 51.96 63.21 o 1 5 12 270.65 225.93 43.63 o 2 5 12 93.51 114.49 41.42 o 3 5 12 1501.50 1474.15 58.97 o 4 5 12 1445.04 1311.64 58.00 o 5 5 12 266.48 269.77 54.01 o 6 5 12 539.72 524.21 63.49 o 7 5 12 1.08 -11.09 67.94 o 8 5 12 12.95 11.85 39.32 o 9 5 12 381.60 465.57 48.82 o 10 5 12 8.45 17.13 37.14 o 11 5 12 46.16 50.66 45.11 o 12 5 12 1.37 48.96 51.64 o 13 5 12 0.90 -8.26 39.15 o 14 5 12 86.70 81.48 51.74 o 15 5 12 298.67 373.57 85.67 o 16 5 12 41.18 63.48 86.18 o 17 5 12 18.44 96.89 87.29 o 0 6 12 280.56 289.83 76.29 o 1 6 12 155.39 169.74 47.48 o 2 6 12 892.75 825.73 54.89 o 3 6 12 78.41 56.79 54.00 o 4 6 12 975.72 960.58 64.54 o 5 6 12 1079.74 1059.02 71.26 o 6 6 12 2459.53 2545.29 106.42 o 7 6 12 328.09 346.55 57.31 o 8 6 12 1807.55 1794.47 163.32 o 9 6 12 7.94 12.66 40.51 o 10 6 12 151.14 227.83 60.48 o 11 6 12 32.82 33.20 47.29 o 12 6 12 79.08 84.10 49.82 o 13 6 12 42.52 42.13 66.47 o 14 6 12 8.39 55.04 45.72 o 15 6 12 161.43 138.93 50.47 o 16 6 12 10.14 -21.88 44.19 o 1 7 12 86.50 105.78 56.95 o 2 7 12 113.35 119.91 46.32 o 3 7 12 1324.56 1215.67 137.93 o 4 7 12 38.90 9.71 45.03 o 5 7 12 131.29 147.43 72.56 o 6 7 12 243.22 282.15 77.33 o 7 7 12 45.88 48.89 71.52 o 8 7 12 632.68 641.18 61.12 o 9 7 12 201.81 192.99 49.64 o 10 7 12 65.82 92.10 56.47 o 11 7 12 0.01 22.89 45.82 o 12 7 12 5.73 17.89 63.41 o 13 7 12 1.12 -2.30 65.12 o 14 7 12 2.67 33.46 53.52 o 0 8 12 925.97 1087.53 98.72 o 1 8 12 884.05 839.52 58.79 o 2 8 12 2.49 5.02 43.70 o 3 8 12 123.06 108.24 50.11 o 4 8 12 482.56 437.52 60.29 o 5 8 12 32.90 22.92 77.46 o 6 8 12 5.05 37.36 76.42 o 7 8 12 270.64 236.01 57.83 o 8 8 12 255.48 211.58 61.29 o 9 8 12 53.67 80.76 49.54 o 10 8 12 515.13 473.16 67.77 o 11 8 12 0.98 44.30 59.86 o 12 8 12 24.69 23.90 49.87 o 13 8 12 61.54 68.90 69.26 o 1 9 12 162.88 137.97 43.75 o 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323.56 314.65 64.71 o 7 1 23 1.65 6.04 49.30 o 8 1 23 78.52 83.88 60.35 o 0 2 23 84.59 66.08 90.27 o 1 2 23 0.39 29.46 67.45 o 2 2 23 43.78 48.74 66.97 o 3 2 23 150.71 175.81 55.79 o 4 2 23 242.39 200.38 63.44 o 5 2 23 0.03 18.63 60.75 o 6 2 23 3.10 -37.02 57.27 o 7 2 23 70.35 116.33 62.41 o 1 3 23 21.88 19.08 60.99 o 2 3 23 31.84 32.07 66.34 o 3 3 23 43.58 32.47 67.24 o 4 3 23 43.53 74.78 56.98 o 5 3 23 1.56 49.18 61.50 o 6 3 23 341.22 300.81 57.01 o 0 4 23 152.31 123.46 64.31 o 1 4 23 17.30 31.13 44.41 o 2 4 23 12.10 34.09 42.23 o 3 4 23 52.35 48.54 48.64 o 4 4 23 169.82 104.07 43.79 o 0 0 24 248.97 202.06 93.85 o 1 0 24 143.03 96.37 90.87 o 2 0 24 158.37 219.76 93.63 o 3 0 24 43.53 75.90 65.04 o 4 0 24 196.12 195.13 69.66 o 5 0 24 98.88 133.29 96.89 o 6 0 24 359.21 398.94 72.12 o 1 1 24 0.88 21.68 64.07 o 2 1 24 106.88 108.64 64.24 o 3 1 24 112.20 103.50 62.95 o 4 1 24 28.40 90.77 65.27 o 5 1 24 104.83 130.42 54.78 o 0 2 24 27.95 9.08 89.75 o 1 2 24 1.36 36.16 71.53 o 2 2 24 36.99 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