#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:44:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181189 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/68/2226821.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226821_Fobs loop_ _publ_author_name 'Demirta\,s, G\"une\,s' 'Dege, Necmi' 'Ye\,silel, Okan Zafer' 'Erer, Hakan' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; Tris(ethylenediamine)nickel(II) 1H-pyrazole-3,5-dicarboxylate 1.67-hydrate ; _journal_coeditor_code CI5127 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m925 _journal_page_last m926 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.008 _cell_angle_beta 75.446 _cell_angle_gamma 73.480 _cell_length_a 12.8145 _cell_length_b 12.9218 _cell_length_c 18.6311 _exptl_crystal_F_000 1348.00 _reflns_d_resolution_high 0.7965 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77.93 o 10 5 21 8.80 23.71 75.16 o -2 6 21 332.05 217.53 68.08 o -1 6 21 48.71 67.27 63.43 o 0 6 21 39.49 56.33 65.42 o 1 6 21 136.14 87.59 73.84 o 2 6 21 16.28 70.17 77.49 o 3 6 21 9.09 -0.55 74.16 o 4 6 21 223.07 323.17 75.41 o 5 6 21 1.21 86.14 76.30 o 6 6 21 539.52 571.27 79.48 o 7 6 21 3.35 27.28 79.08 o 8 6 21 12.55 143.68 77.33 o 9 6 21 40.46 61.69 94.62 o 10 6 21 2.67 108.42 75.01 o -2 7 21 3.08 12.98 67.73 o -1 7 21 77.38 86.86 66.37 o 0 7 21 41.78 132.05 60.07 o 1 7 21 59.02 70.16 76.63 o 2 7 21 24.88 7.54 73.41 o 3 7 21 274.87 320.10 75.79 o 4 7 21 19.52 43.05 76.99 o 5 7 21 60.94 10.86 109.58 o 6 7 21 46.08 131.23 75.80 o 7 7 21 0.28 10.58 78.07 o 8 7 21 265.86 288.42 74.37 o 9 7 21 74.42 46.67 114.60 o 10 7 21 31.31 6.88 81.64 o -1 8 21 27.42 119.39 66.18 o 0 8 21 0.26 65.20 64.84 o 1 8 21 24.03 51.35 74.48 o 2 8 21 563.81 443.37 77.68 o 3 8 21 83.11 126.14 75.74 o 4 8 21 83.13 112.90 76.43 o 5 8 21 16.58 -26.97 77.95 o 6 8 21 197.69 181.35 76.23 o 7 8 21 123.86 105.71 74.41 o 8 8 21 27.85 177.53 73.94 o 9 8 21 13.15 137.32 90.49 o 10 8 21 7.90 75.93 73.40 o 0 9 21 41.00 109.71 76.11 o 1 9 21 280.26 138.78 77.01 o 2 9 21 268.80 213.06 77.15 o 3 9 21 4.62 24.84 76.81 o 4 9 21 0.33 54.25 77.77 o 5 9 21 3.93 45.77 77.85 o 6 9 21 258.93 247.10 77.02 o 7 9 21 70.03 154.89 75.03 o 8 9 21 9.65 24.03 75.89 o 9 9 21 79.61 7.41 110.75 o 1 10 21 129.16 124.72 77.31 o 2 10 21 25.46 110.57 78.69 o 3 10 21 101.62 80.93 80.04 o 4 10 21 7.61 55.35 78.93 o 5 10 21 119.87 156.84 83.95 o 6 10 21 153.64 61.57 76.42 o 7 10 21 55.36 64.10 75.48 o 8 10 21 0.69 -4.53 90.05 o 4 11 21 11.64 92.16 84.47 o 5 11 21 132.76 124.45 79.68 o 6 11 21 216.58 161.18 83.00 o 7 11 21 0.28 55.65 79.01 o 1 0 22 37.34 99.38 77.59 o 2 0 22 2.32 4.09 81.32 o 3 0 22 114.48 116.98 77.68 o 4 0 22 28.59 51.29 79.52 o 0 1 22 13.58 104.14 76.55 o 1 1 22 13.36 17.56 74.09 o 2 1 22 47.72 89.72 74.29 o 3 1 22 37.64 127.89 81.68 o 4 1 22 3.53 47.40 81.25 o 5 1 22 59.22 104.26 84.50 o 6 1 22 21.05 109.97 83.54 o -1 2 22 28.50 34.85 74.77 o 0 2 22 0.62 -85.60 73.23 o 1 2 22 96.23 153.37 76.36 o 2 2 22 155.75 92.18 87.84 o 3 2 22 43.74 94.86 74.43 o 4 2 22 8.50 48.77 81.72 o 5 2 22 31.20 102.92 79.66 o 6 2 22 5.93 124.10 87.21 o 7 2 22 96.68 227.63 123.83 o -1 3 22 74.74 76.13 82.40 o 0 3 22 65.91 103.24 79.51 o 1 3 22 72.70 35.78 72.75 o 2 3 22 86.64 118.77 73.65 o 3 3 22 9.63 51.33 74.08 o 4 3 22 0.22 -17.50 75.09 o 5 3 22 49.60 143.90 98.00 o 6 3 22 113.15 77.19 112.32 o 7 3 22 296.90 286.48 181.24 o 8 3 22 0.29 115.81 151.52 o -1 4 22 132.23 134.72 75.20 o 0 4 22 213.93 210.43 73.33 o 1 4 22 87.02 88.54 73.23 o 2 4 22 9.78 69.33 83.96 o 3 4 22 4.22 -16.84 74.28 o 4 4 22 14.40 17.28 103.88 o 5 4 22 63.18 91.89 120.59 o 6 4 22 311.16 194.16 184.70 o 7 4 22 0.41 76.11 114.86 o 8 4 22 5.90 -45.81 90.73 o -1 5 22 69.89 14.12 75.89 o 0 5 22 95.47 84.55 74.35 o 1 5 22 0.04 106.81 74.39 o 2 5 22 8.20 110.30 74.64 o 3 5 22 34.51 16.96 94.49 o 4 5 22 41.12 24.49 95.69 o 5 5 22 72.33 15.89 100.57 o 6 5 22 8.23 112.56 81.11 o 7 5 22 2.03 78.08 87.76 o 8 5 22 31.29 19.84 82.02 o 9 5 22 32.08 170.31 96.08 o 0 6 22 3.11 74.06 65.60 o 1 6 22 81.30 121.92 66.77 o 2 6 22 308.64 365.01 85.07 o 3 6 22 24.30 4.86 76.30 o 4 6 22 450.54 346.17 83.46 o 5 6 22 19.44 203.05 91.21 o 6 6 22 31.33 63.48 80.76 o 7 6 22 167.19 185.65 81.07 o 8 6 22 3.73 72.60 82.80 o 9 6 22 8.21 32.53 109.08 o 0 7 22 81.26 55.64 66.37 o 1 7 22 320.53 308.73 66.56 o 2 7 22 68.40 199.70 76.49 o 3 7 22 202.34 205.30 77.96 o 4 7 22 1.51 178.59 78.04 o 5 7 22 15.15 4.60 79.12 o 6 7 22 179.14 82.62 80.81 o 7 7 22 1.81 13.89 79.18 o 8 7 22 19.68 46.88 82.34 o 1 8 22 1.24 18.06 77.62 o 2 8 22 4.34 20.95 67.61 o 3 8 22 15.17 114.02 86.09 o 4 8 22 34.17 60.79 80.22 o 5 8 22 177.82 151.38 81.49 o 6 8 22 80.13 147.86 83.84 o 7 8 22 0.27 4.50 79.52 o 8 8 22 75.07 91.40 79.99 o 2 9 22 70.31 99.90 78.08 o 3 9 22 7.93 43.39 80.69 o 4 9 22 106.39 185.09 82.71 o 5 9 22 280.81 213.07 81.79 o 6 9 22 6.38 12.24 80.56 o 7 9 22 43.07 33.24 80.83 o 2 3 23 0.90 46.82 78.82 o 3 3 23 10.82 24.94 76.65 o 4 3 23 30.78 56.52 77.62 o 5 3 23 136.52 89.66 80.73 o 2 4 23 2.37 28.12 74.97 o 3 4 23 30.58 49.60 77.01 o 4 4 23 130.49 81.85 78.56 o 5 4 23 75.62 178.42 108.58 o 6 4 23 2.55 -67.51 105.80 o 2 5 23 29.15 -31.78 75.68 o 3 5 23 118.83 80.96 77.12 o 4 5 23 24.32 50.64 98.51 o 5 5 23 74.63 54.40 109.08 o 6 5 23 22.09 62.07 83.89 o 2 6 23 200.98 95.64 67.56 o 3 6 23 2.33 79.97 82.20 o 4 6 23 38.36 9.38 78.18 o 5 6 23 2.29 7.01 86.45 o 6 6 23 1.40 23.32 84.34 o 3 7 23 0.20 24.62 79.23 o 4 7 23 22.64 71.87 80.74 o 5 7 23 34.37 14.33 82.65 o 6 7 23 19.20 38.00 82.89 o