#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:44:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181189 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/68/2226854.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226854_Fobs loop_ _publ_author_name 'Gunasekaran, N.' 'Karvembu, R.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 1-Benzoyl-3,3-bis(propan-2-yl)thiourea ; _journal_coeditor_code EZ2225 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2113 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.635 _cell_angle_gamma 90.000 _cell_length_a 14.8072 _cell_length_b 13.5832 _cell_length_c 14.9168 _exptl_crystal_F_000 1136.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file ez2225Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 448.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12670.54 12715.92 266.26 o 4 0 0 6244.27 6693.59 115.14 o 6 0 0 3161.46 3022.86 58.19 o 8 0 0 36.17 14.06 7.09 o 10 0 0 2517.71 2364.66 51.87 o 12 0 0 6.25 12.15 16.53 o 14 0 0 1756.07 1967.12 72.03 o 16 0 0 1803.22 1976.17 76.64 o 18 0 0 404.07 463.24 64.21 o 1 1 0 35.34 28.05 5.76 o 2 1 0 196.00 185.53 7.36 o 3 1 0 578.92 549.30 14.10 o 4 1 0 159.66 181.68 10.29 o 5 1 0 1722.43 1698.45 28.74 o 6 1 0 1949.62 2019.44 33.87 o 7 1 0 206.25 206.16 10.40 o 8 1 0 1813.97 2015.34 37.76 o 9 1 0 472.30 430.27 21.41 o 10 1 0 919.67 849.13 22.87 o 11 1 0 0.71 -2.86 10.05 o 12 1 0 127.16 106.94 15.14 o 13 1 0 1467.86 1404.79 40.80 o 14 1 0 2615.91 2524.50 59.14 o 15 1 0 88.07 70.86 15.92 o 16 1 0 86.37 44.54 18.90 o 17 1 0 46.89 31.15 17.22 o 18 1 0 1.08 7.33 18.20 o 19 1 0 162.28 263.17 38.50 o 0 2 0 49561.21 47718.69 1734.98 o 1 2 0 14174.56 12815.57 284.71 o 2 2 0 19317.52 18779.48 218.99 o 3 2 0 1.41 -4.72 3.15 o 4 2 0 5961.42 6229.42 76.59 o 5 2 0 1632.29 1570.88 27.62 o 6 2 0 13963.96 14269.48 243.75 o 7 2 0 3044.00 2891.17 52.41 o 8 2 0 1892.21 1651.57 36.04 o 9 2 0 2564.18 2548.63 50.10 o 10 2 0 663.54 618.33 20.61 o 11 2 0 1376.78 1426.31 32.43 o 12 2 0 628.90 628.82 39.65 o 13 2 0 231.11 241.69 19.75 o 14 2 0 1538.12 1476.05 43.24 o 15 2 0 53.39 74.89 15.64 o 16 2 0 1150.90 1185.50 48.09 o 17 2 0 18.42 0.36 16.78 o 18 2 0 698.31 707.24 50.59 o 1 3 0 190.25 185.49 8.93 o 2 3 0 120.11 117.82 8.66 o 3 3 0 3048.61 2933.55 43.46 o 4 3 0 174.33 191.86 7.61 o 5 3 0 4.39 3.33 3.37 o 6 3 0 554.55 567.66 16.17 o 7 3 0 661.48 730.04 19.20 o 8 3 0 2044.69 2148.74 43.08 o 9 3 0 138.29 139.11 11.29 o 10 3 0 62.29 49.24 9.68 o 11 3 0 304.26 274.45 15.94 o 12 3 0 1325.65 1223.00 73.81 o 13 3 0 12.90 16.48 11.12 o 14 3 0 1061.85 933.64 49.07 o 15 3 0 358.81 317.30 28.54 o 16 3 0 285.41 256.66 27.40 o 17 3 0 222.12 238.86 49.52 o 18 3 0 21.56 18.73 19.40 o 0 4 0 201471.34 184056.53 6453.37 o 1 4 0 100.02 94.35 8.73 o 2 4 0 3183.29 3352.43 45.15 o 3 4 0 8836.50 8774.30 107.64 o 4 4 0 861.99 843.53 21.18 o 5 4 0 4863.46 4944.66 64.55 o 6 4 0 4540.00 4621.69 61.36 o 7 4 0 595.43 641.71 18.47 o 8 4 0 1072.46 918.48 23.21 o 9 4 0 894.72 896.77 24.15 o 10 4 0 5559.33 5756.68 88.22 o 11 4 0 1633.80 1658.91 36.95 o 12 4 0 289.39 314.71 18.03 o 13 4 0 477.23 455.58 32.64 o 14 4 0 479.61 526.15 48.99 o 15 4 0 350.82 402.60 61.34 o 16 4 0 313.51 345.12 61.06 o 17 4 0 1.31 -7.73 16.37 o 18 4 0 30.18 49.42 21.56 o 1 5 0 267.02 267.95 10.13 o 2 5 0 740.50 707.18 15.70 o 3 5 0 781.38 749.65 18.21 o 4 5 0 241.66 252.75 12.13 o 5 5 0 379.03 455.86 13.42 o 6 5 0 3.57 -5.94 5.81 o 7 5 0 278.74 276.75 11.04 o 8 5 0 384.37 408.85 16.83 o 9 5 0 2038.61 2041.62 41.47 o 10 5 0 1013.05 1047.30 27.80 o 11 5 0 853.69 831.62 30.56 o 12 5 0 461.18 498.77 26.19 o 13 5 0 1914.93 1748.72 68.19 o 14 5 0 568.38 451.39 38.74 o 15 5 0 40.09 46.98 17.91 o 16 5 0 91.17 76.79 21.69 o 17 5 0 453.44 381.62 49.25 o 18 5 0 4.16 -0.28 18.97 o 0 6 0 4729.12 5088.94 95.77 o 1 6 0 360.03 392.65 12.65 o 2 6 0 3233.87 3365.19 48.09 o 3 6 0 5215.96 4955.77 66.63 o 4 6 0 2782.68 3048.41 44.89 o 5 6 0 2262.24 2093.88 34.09 o 6 6 0 2826.95 3002.04 45.16 o 7 6 0 4035.43 3860.49 55.53 o 8 6 0 3.45 3.11 7.09 o 9 6 0 2012.32 1959.12 39.53 o 10 6 0 59.93 53.28 13.19 o 11 6 0 947.85 867.97 31.32 o 12 6 0 444.03 394.30 37.94 o 13 6 0 550.27 550.03 28.82 o 14 6 0 156.63 137.12 22.15 o 15 6 0 918.93 866.31 71.95 o 16 6 0 127.64 151.31 24.18 o 17 6 0 93.58 107.93 23.87 o 1 7 0 88.12 85.10 7.55 o 2 7 0 81.04 93.50 7.94 o 3 7 0 847.87 920.16 25.64 o 4 7 0 183.18 211.69 13.28 o 5 7 0 0.56 0.88 5.49 o 6 7 0 168.94 181.07 10.82 o 7 7 0 188.11 198.30 11.44 o 8 7 0 10.25 24.23 8.46 o 9 7 0 267.78 295.72 17.16 o 10 7 0 7.70 11.69 11.24 o 11 7 0 129.47 179.64 20.14 o 12 7 0 2688.56 2599.76 60.29 o 13 7 0 176.96 156.80 21.24 o 14 7 0 10.53 22.52 16.38 o 15 7 0 37.03 12.43 16.98 o 16 7 0 412.78 368.84 63.80 o 17 7 0 105.31 75.56 22.40 o 0 8 0 2846.85 2932.46 64.64 o 1 8 0 6.88 16.36 6.16 o 2 8 0 3770.00 3970.22 62.45 o 3 8 0 2708.84 2646.36 42.70 o 4 8 0 226.44 198.33 13.29 o 5 8 0 620.55 612.39 21.64 o 6 8 0 1468.68 1578.21 30.85 o 7 8 0 463.99 462.34 17.14 o 8 8 0 1.67 2.41 10.75 o 9 8 0 407.99 463.22 25.59 o 10 8 0 1370.40 1384.31 41.61 o 11 8 0 1094.67 1178.52 38.29 o 12 8 0 164.07 160.23 18.52 o 13 8 0 696.68 750.42 39.65 o 14 8 0 20.07 1.48 15.82 o 15 8 0 662.37 705.24 58.12 o 16 8 0 28.33 13.16 22.44 o 1 9 0 261.82 274.52 13.86 o 2 9 0 189.81 201.20 12.22 o 3 9 0 188.48 198.49 12.47 o 4 9 0 116.94 105.60 10.00 o 5 9 0 1215.14 1256.64 30.90 o 6 9 0 285.55 289.65 15.91 o 7 9 0 529.49 523.79 22.07 o 8 9 0 34.04 39.82 14.28 o 9 9 0 171.98 175.67 18.57 o 10 9 0 421.89 402.00 27.76 o 11 9 0 739.57 778.97 33.79 o 12 9 0 716.09 728.13 50.93 o 13 9 0 263.94 259.16 23.13 o 14 9 0 98.83 119.63 24.84 o 15 9 0 65.74 36.81 19.37 o 16 9 0 387.02 421.11 76.10 o 0 10 0 1073.77 1028.48 36.41 o 1 10 0 595.15 589.42 19.95 o 2 10 0 2051.58 2112.38 39.10 o 3 10 0 2208.75 2140.37 51.80 o 4 10 0 24.54 27.02 8.21 o 5 10 0 24.67 49.74 9.22 o 6 10 0 42.13 39.98 10.60 o 7 10 0 1405.32 1427.47 35.57 o 8 10 0 160.70 159.98 17.54 o 9 10 0 197.58 207.23 20.12 o 10 10 0 0.25 9.06 12.49 o 11 10 0 24.73 25.58 14.26 o 12 10 0 491.05 467.56 29.86 o 13 10 0 30.70 25.35 15.29 o 14 10 0 27.50 34.74 23.60 o 15 10 0 483.35 478.87 74.30 o 1 11 0 525.95 521.16 20.52 o 2 11 0 959.16 925.97 25.48 o 3 11 0 86.49 104.49 11.53 o 4 11 0 414.82 418.04 21.65 o 5 11 0 9.84 5.24 9.58 o 6 11 0 283.98 241.32 17.44 o 7 11 0 6.83 5.66 12.01 o 8 11 0 75.22 63.49 15.02 o 9 11 0 4.55 1.51 12.68 o 10 11 0 62.34 29.84 14.95 o 11 11 0 51.04 51.87 15.81 o 12 11 0 309.87 318.27 26.31 o 13 11 0 88.99 43.52 16.86 o 14 11 0 91.21 75.95 19.16 o 0 12 0 96.62 133.34 19.63 o 1 12 0 46.86 60.30 10.74 o 2 12 0 508.92 481.52 20.57 o 3 12 0 843.30 832.58 28.18 o 4 12 0 176.55 154.34 15.75 o 5 12 0 134.31 127.02 14.53 o 6 12 0 306.28 324.37 24.06 o 7 12 0 8.59 22.25 13.05 o 8 12 0 97.02 115.73 34.57 o 9 12 0 48.16 69.74 16.72 o 10 12 0 3.17 -7.66 13.70 o 11 12 0 0.01 -1.80 14.59 o 12 12 0 0.88 5.08 15.36 o 13 12 0 13.02 14.90 16.42 o 1 13 0 56.74 56.95 11.05 o 2 13 0 14.49 7.41 15.73 o 3 13 0 205.38 176.29 16.66 o 4 13 0 0.96 2.88 10.83 o 5 13 0 55.87 44.52 12.63 o 6 13 0 3.41 2.84 10.89 o 7 13 0 236.91 215.33 21.97 o 8 13 0 21.21 7.78 15.61 o 9 13 0 138.55 113.77 19.40 o 10 13 0 151.38 131.43 27.71 o 11 13 0 75.62 115.34 20.33 o 12 13 0 57.68 34.75 17.64 o 0 14 0 78.53 78.76 17.65 o 1 14 0 41.41 65.36 13.90 o 2 14 0 29.36 23.43 12.37 o 3 14 0 267.51 266.39 22.25 o 4 14 0 26.23 21.23 12.56 o 5 14 0 1185.04 1178.16 43.67 o 6 14 0 3.82 6.34 14.05 o 7 14 0 195.82 156.20 20.83 o 8 14 0 7.30 -12.58 14.20 o 9 14 0 13.84 -3.35 15.01 o 10 14 0 28.95 32.67 17.59 o 11 14 0 161.06 145.03 23.09 o 1 15 0 341.48 294.86 22.44 o 2 15 0 213.62 195.46 19.15 o 3 15 0 4.81 -5.84 11.62 o 4 15 0 109.92 75.00 15.29 o 5 15 0 62.87 48.75 14.71 o 6 15 0 209.91 203.33 22.68 o 7 15 0 215.66 237.15 24.85 o 8 15 0 18.14 -2.25 15.16 o 9 15 0 110.49 137.17 22.50 o 10 15 0 7.39 -1.22 17.08 o 0 16 0 200.84 185.78 32.26 o 1 16 0 223.21 199.54 26.00 o 2 16 0 0.63 -6.62 14.75 o 3 16 0 128.92 95.27 16.87 o 4 16 0 220.26 208.52 21.00 o 5 16 0 295.65 223.43 24.28 o 6 16 0 151.32 145.07 22.36 o 7 16 0 1.95 -13.29 21.18 o 8 16 0 27.14 29.37 18.32 o 1 17 0 32.44 -5.54 15.93 o 2 17 0 0.61 1.24 16.20 o 3 17 0 31.58 11.10 16.76 o 4 17 0 7.29 -5.39 16.08 o 5 17 0 0.09 -5.47 18.62 o -19 0 1 809.15 996.89 93.09 o -17 0 1 131.52 163.30 29.44 o -15 0 1 88.89 132.34 25.08 o -13 0 1 50.67 52.96 18.95 o -11 0 1 321.47 298.49 26.87 o -9 0 1 140.02 137.10 13.42 o -7 0 1 4142.03 4152.98 77.95 o -5 0 1 1841.12 1805.28 36.98 o -3 0 1 115.95 112.18 8.92 o -1 0 1 12483.86 11655.63 295.60 o 1 0 1 2511.36 2351.40 50.70 o 3 0 1 957.32 831.46 19.31 o 5 0 1 4037.54 4138.05 145.88 o 7 0 1 57.13 41.68 12.14 o 9 0 1 1912.27 2091.71 47.11 o 11 0 1 923.80 840.28 41.94 o 13 0 1 738.82 648.43 50.56 o 15 0 1 15.10 8.81 19.86 o 17 0 1 159.99 128.74 36.68 o -19 1 1 65.59 71.50 29.41 o -18 1 1 10.05 21.18 18.88 o -17 1 1 433.53 425.17 33.85 o -16 1 1 75.16 80.01 16.54 o -15 1 1 68.28 30.32 13.48 o -14 1 1 1037.56 980.14 43.19 o -13 1 1 1064.08 1193.10 37.40 o -12 1 1 325.25 311.81 26.09 o -11 1 1 449.97 501.48 23.91 o -10 1 1 0.44 11.20 6.99 o -9 1 1 1469.68 1616.78 38.33 o -8 1 1 716.10 680.71 29.46 o -7 1 1 1706.36 1840.12 36.36 o -6 1 1 18.78 14.35 4.00 o -5 1 1 7706.84 7994.50 111.47 o -4 1 1 269.55 263.70 7.45 o -3 1 1 9255.23 9339.54 110.74 o -2 1 1 9294.63 8714.69 102.68 o -1 1 1 9999.64 9521.81 121.70 o 0 1 1 155.79 147.55 4.23 o 1 1 1 35.18 24.89 4.18 o 2 1 1 10788.85 10302.53 144.02 o 3 1 1 5123.77 5095.93 68.67 o 4 1 1 1707.66 1781.02 27.68 o 5 1 1 845.36 863.88 15.47 o 6 1 1 567.26 606.53 16.10 o 7 1 1 6809.81 7216.78 191.95 o 8 1 1 787.79 819.54 16.88 o 9 1 1 319.07 273.04 13.48 o 10 1 1 310.77 318.96 15.20 o 11 1 1 174.19 186.37 16.92 o 12 1 1 0.26 0.67 11.76 o 13 1 1 13.70 9.36 12.05 o 14 1 1 315.77 332.92 23.40 o 15 1 1 638.25 588.01 43.17 o 16 1 1 26.62 21.33 14.53 o 17 1 1 0.82 19.46 15.28 o 18 1 1 20.06 6.65 18.36 o -19 2 1 724.94 864.14 49.94 o -18 2 1 0.01 -11.95 17.33 o -17 2 1 61.27 28.56 18.24 o -16 2 1 7.67 3.87 16.39 o -15 2 1 201.02 208.93 24.01 o -14 2 1 0.37 3.56 9.21 o -13 2 1 1428.92 1414.45 47.84 o -12 2 1 378.45 396.48 27.34 o -11 2 1 92.27 94.68 10.75 o -10 2 1 551.17 556.45 19.41 o -9 2 1 242.06 240.53 12.77 o -8 2 1 23.79 42.31 8.47 o -7 2 1 475.44 511.97 15.78 o -6 2 1 647.75 653.11 20.48 o -5 2 1 33.71 33.04 5.36 o -4 2 1 347.26 348.49 10.75 o -3 2 1 1525.91 1452.40 21.08 o -2 2 1 608.44 596.32 12.76 o -1 2 1 92.61 80.67 3.67 o 0 2 1 1100.99 1134.28 16.45 o 1 2 1 149.11 153.21 5.47 o 2 2 1 3341.10 3193.71 40.59 o 3 2 1 697.98 766.91 15.33 o 4 2 1 274.25 304.22 11.03 o 5 2 1 25.04 29.70 4.11 o 6 2 1 259.51 264.07 11.20 o 7 2 1 54.04 76.45 8.03 o 8 2 1 334.47 317.39 14.21 o 9 2 1 0.07 2.46 6.79 o 10 2 1 231.33 252.22 15.79 o 11 2 1 391.50 334.88 16.98 o 12 2 1 2.26 -7.05 10.90 o 13 2 1 90.05 95.31 15.49 o 14 2 1 417.60 417.72 42.13 o 15 2 1 10.90 -11.24 12.50 o 16 2 1 111.22 79.88 17.16 o 17 2 1 56.48 46.68 23.87 o 18 2 1 35.04 9.46 18.71 o -18 3 1 0.13 -11.66 16.56 o -17 3 1 281.64 271.48 28.94 o -16 3 1 350.91 343.28 30.27 o -15 3 1 44.24 27.17 16.72 o -14 3 1 184.32 156.22 22.63 o -13 3 1 377.59 393.76 23.64 o -12 3 1 2018.84 2070.24 62.29 o -11 3 1 301.99 335.41 17.14 o -10 3 1 321.78 279.49 15.21 o -9 3 1 865.05 972.76 24.56 o -8 3 1 161.01 201.40 12.59 o -7 3 1 5316.77 5610.24 81.29 o -6 3 1 250.72 236.79 8.22 o -5 3 1 233.16 259.56 12.92 o -4 3 1 3630.86 3737.69 48.78 o -3 3 1 0.18 1.29 3.24 o -2 3 1 193.44 148.89 8.09 o -1 3 1 67.99 66.35 4.65 o 0 3 1 1191.71 1185.66 18.54 o 1 3 1 350.79 355.72 9.65 o 2 3 1 641.43 659.79 14.56 o 3 3 1 2.36 6.72 2.91 o 4 3 1 7046.10 7266.21 98.02 o 5 3 1 1042.22 1255.45 25.58 o 6 3 1 361.30 331.35 14.78 o 7 3 1 1246.71 1328.72 38.08 o 8 3 1 1211.82 1199.09 35.22 o 9 3 1 220.18 199.43 16.93 o 10 3 1 268.81 285.27 18.31 o 11 3 1 729.98 713.98 23.74 o 12 3 1 13.23 29.30 12.42 o 13 3 1 81.89 100.94 15.33 o 14 3 1 81.03 70.43 16.84 o 15 3 1 924.33 862.73 40.42 o 16 3 1 8.44 24.36 17.37 o 17 3 1 30.74 49.83 24.88 o 18 3 1 201.99 228.29 36.01 o -18 4 1 19.47 2.02 25.41 o -17 4 1 110.90 69.68 20.80 o -16 4 1 93.77 57.98 19.30 o -15 4 1 103.49 92.44 20.52 o -14 4 1 435.88 396.16 60.12 o -13 4 1 340.82 324.93 27.33 o -12 4 1 5.33 -6.72 8.77 o -11 4 1 389.58 416.85 19.13 o -10 4 1 11.02 15.97 8.49 o -9 4 1 604.71 629.40 22.17 o -8 4 1 117.26 108.38 9.77 o -7 4 1 2161.35 2261.61 34.24 o -6 4 1 5.89 5.57 4.14 o -5 4 1 1778.13 1793.21 27.82 o -4 4 1 923.82 968.93 19.93 o -3 4 1 0.96 2.70 3.55 o -2 4 1 2403.31 2338.10 33.05 o -1 4 1 10991.48 10839.13 130.47 o 0 4 1 30776.91 30671.96 357.33 o 1 4 1 170.50 187.35 9.48 o 2 4 1 369.67 348.79 10.41 o 3 4 1 4439.45 4415.04 75.66 o 4 4 1 40.29 39.76 5.60 o 5 4 1 587.59 590.17 15.05 o 6 4 1 222.37 215.44 9.34 o 7 4 1 386.47 372.34 11.93 o 8 4 1 1126.45 1179.60 27.19 o 9 4 1 3208.09 3461.99 57.98 o 10 4 1 1215.75 1257.56 34.26 o 11 4 1 69.63 66.19 11.01 o 12 4 1 26.32 15.50 9.84 o 13 4 1 301.67 272.34 34.98 o 14 4 1 496.71 426.59 54.54 o 15 4 1 7.75 -11.94 14.93 o 16 4 1 101.27 126.50 21.98 o 17 4 1 138.26 127.98 23.53 o 18 4 1 1.58 12.87 26.86 o -18 5 1 113.21 141.17 31.74 o -17 5 1 17.52 14.85 18.40 o -16 5 1 472.51 474.10 35.58 o -15 5 1 19.54 -7.13 14.98 o -14 5 1 1878.14 1743.60 70.04 o -13 5 1 13.53 6.77 14.41 o -12 5 1 970.61 996.69 33.08 o -11 5 1 106.15 102.67 15.89 o -10 5 1 96.40 90.68 11.01 o -9 5 1 9.65 8.22 7.99 o -8 5 1 2299.90 2455.39 37.91 o -7 5 1 4461.14 4755.88 64.43 o -6 5 1 4525.25 4767.24 71.17 o -5 5 1 924.39 989.10 19.49 o -4 5 1 2012.95 2111.09 32.46 o -3 5 1 2489.35 2516.37 40.49 o -2 5 1 1570.63 1471.99 24.38 o -1 5 1 2496.94 2514.90 36.40 o 0 5 1 1125.25 1222.92 21.48 o 1 5 1 147.36 130.16 12.79 o 2 5 1 436.22 486.88 13.00 o 3 5 1 450.37 454.15 14.42 o 4 5 1 729.83 751.70 23.07 o 5 5 1 2.25 1.49 4.63 o 6 5 1 120.08 151.19 8.64 o 7 5 1 1674.31 1784.26 30.17 o 8 5 1 420.44 462.30 13.67 o 9 5 1 266.09 282.83 15.71 o 10 5 1 40.27 58.44 10.77 o 11 5 1 27.68 8.06 10.44 o 12 5 1 141.59 143.71 14.47 o 13 5 1 205.88 254.18 25.01 o 14 5 1 270.17 284.11 27.17 o 15 5 1 478.68 428.63 60.28 o 16 5 1 0.08 1.62 16.34 o 17 5 1 52.39 26.08 19.13 o 18 5 1 9.36 24.97 19.93 o -18 6 1 6.56 -16.45 17.88 o -17 6 1 18.84 8.61 22.21 o -16 6 1 0.17 -5.78 16.53 o -15 6 1 7.37 -4.86 15.54 o -14 6 1 0.09 -9.47 14.82 o -13 6 1 423.30 497.25 27.64 o -12 6 1 382.46 400.90 27.63 o -11 6 1 782.56 759.11 29.33 o -10 6 1 910.35 916.53 40.37 o -9 6 1 406.14 393.70 18.34 o -8 6 1 76.42 75.60 9.23 o -7 6 1 38.07 18.68 5.91 o -6 6 1 845.69 904.90 22.56 o -5 6 1 3051.43 2952.32 43.89 o -4 6 1 339.61 351.19 13.82 o -3 6 1 1321.88 1211.28 22.83 o -2 6 1 1633.09 1655.10 27.97 o -1 6 1 203.02 145.91 9.10 o 0 6 1 3251.08 3429.91 53.07 o 1 6 1 635.23 721.15 18.35 o 2 6 1 1156.17 1148.19 24.08 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