#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:44:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181189 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/68/2226865.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226865_Fobs loop_ _publ_author_name 'de Lill, Daniel T.' 'de Bettencourt-Dias, Ana' _publ_section_title ; 4-Bromo-N^2^,N^2^,N^6^,N^6^-tetraethylpyridine-2,6-dicarboxamide ; _journal_coeditor_code FL2308 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2124 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.7096 _cell_length_b 8.4987 _cell_length_c 21.5013 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.7907 _cod_data_source_file fl2308Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pbca in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 585.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1072.55 1319.96 30.53 o 4 0 0 97769.16 103662.53 1449.34 o 6 0 0 83.83 43.99 18.28 o 8 0 0 114649.02 123509.32 2189.60 o 10 0 0 4689.19 5531.64 119.87 o 12 0 0 16611.14 16493.94 308.57 o 14 0 0 194.03 147.13 41.65 o 16 0 0 9351.03 9514.10 248.81 o 2 1 0 37740.79 40242.45 361.81 o 4 1 0 8747.01 9773.61 126.46 o 6 1 0 41675.83 41501.51 493.37 o 8 1 0 951.57 1100.67 31.44 o 10 1 0 25094.46 24289.02 440.93 o 12 1 0 602.12 673.83 45.22 o 14 1 0 17110.21 17654.04 276.29 o 16 1 0 182.24 391.78 71.94 o 18 1 0 3957.39 4200.54 209.54 o 0 2 0 6103.09 7682.40 106.08 o 2 2 0 2266.57 2716.85 36.67 o 4 2 0 8689.70 8927.87 108.16 o 6 2 0 1284.60 1249.03 28.42 o 8 2 0 5551.17 5418.00 88.28 o 10 2 0 40.82 35.12 19.72 o 12 2 0 4768.29 4919.62 110.84 o 14 2 0 3735.96 3938.96 141.75 o 16 2 0 914.40 888.56 100.95 o 18 2 0 1443.94 1267.10 129.57 o 20 2 0 2362.85 2228.40 160.66 o 2 3 0 88.18 62.12 13.23 o 4 3 0 4994.06 5488.03 70.73 o 6 3 0 2789.55 2962.17 57.11 o 8 3 0 578.55 519.39 22.21 o 10 3 0 2503.31 2734.66 68.91 o 12 3 0 517.18 524.83 54.16 o 14 3 0 6081.90 5342.28 218.54 o 16 3 0 1.14 51.45 73.66 o 18 3 0 70.17 128.18 85.32 o 20 3 0 0.70 -91.65 91.65 o 0 4 0 28725.24 29020.78 394.98 o 2 4 0 2871.44 3365.99 52.95 o 4 4 0 18012.26 16778.38 190.04 o 6 4 0 68.44 27.74 20.11 o 8 4 0 18359.03 18814.81 273.92 o 10 4 0 3677.79 3786.59 104.07 o 12 4 0 9839.77 9318.11 420.99 o 14 4 0 331.25 289.14 103.33 o 16 4 0 8683.78 7988.65 304.05 o 18 4 0 17.72 46.59 85.41 o 20 4 0 5568.58 5775.48 259.58 o 2 5 0 41902.88 40865.20 406.75 o 4 5 0 2192.06 2536.76 55.57 o 6 5 0 34056.45 32619.94 393.67 o 8 5 0 14.82 92.14 36.60 o 10 5 0 9988.39 9941.72 267.79 o 12 5 0 366.28 333.77 84.09 o 14 5 0 10835.14 10631.34 680.38 o 16 5 0 57.75 116.25 97.43 o 18 5 0 3004.20 3155.64 410.10 o 0 6 0 36081.68 35534.50 539.88 o 2 6 0 77.77 55.50 23.76 o 4 6 0 24118.91 23622.31 284.94 o 6 6 0 253.80 295.61 39.93 o 8 6 0 11479.37 10919.63 232.72 o 10 6 0 140.95 26.21 69.64 o 12 6 0 12678.54 12515.06 421.25 o 14 6 0 588.41 656.71 125.14 o 16 6 0 6874.37 7121.35 314.59 o 18 6 0 314.52 604.73 148.98 o 2 7 0 237.42 268.52 40.02 o 4 7 0 111.43 72.62 47.09 o 6 7 0 2046.24 2016.30 131.65 o 8 7 0 21.01 94.44 92.64 o 10 7 0 478.24 451.33 115.28 o 12 7 0 111.65 239.01 111.66 o 14 7 0 1773.66 1851.35 215.11 o 16 7 0 1556.91 1395.16 183.08 o 0 8 0 2255.08 2355.39 169.15 o 2 8 0 1162.43 1090.58 84.38 o 4 8 0 1229.15 1169.43 85.88 o 6 8 0 217.86 210.11 85.87 o 8 8 0 50.49 3.25 161.56 o 10 8 0 154.09 115.62 109.24 o 12 8 0 1083.04 1412.18 253.93 o 14 8 0 23.15 107.37 122.95 o 2 9 0 8302.99 8633.94 243.07 o 4 9 0 0.92 9.54 76.90 o 6 9 0 8748.70 8761.97 362.29 o 8 9 0 20.27 151.68 118.94 o 10 9 0 3323.72 3169.45 244.47 o 12 9 0 515.75 708.06 232.19 o 0 10 0 7863.23 8313.02 487.73 o 2 10 0 201.74 198.43 128.56 o 4 10 0 7449.76 6854.86 461.85 o 6 10 0 97.73 -130.47 165.69 o 8 10 0 4935.46 5147.15 518.46 o 1 1 1 1725.27 1648.80 16.04 o 2 1 1 4426.48 4972.42 40.19 o 3 1 1 411.82 643.16 13.68 o 4 1 1 2082.49 2529.24 35.04 o 5 1 1 7456.86 7976.57 75.61 o 6 1 1 549.68 508.68 14.21 o 7 1 1 12751.50 13481.74 123.67 o 8 1 1 6350.99 7088.47 65.76 o 9 1 1 5236.51 5106.96 53.48 o 10 1 1 1309.55 1327.34 27.35 o 11 1 1 1808.66 1674.76 32.13 o 12 1 1 569.43 685.32 24.97 o 13 1 1 879.50 1051.47 40.66 o 14 1 1 868.87 788.60 35.51 o 15 1 1 839.13 915.10 41.43 o 16 1 1 1629.14 1615.30 55.92 o 17 1 1 5334.34 5331.15 183.65 o 18 1 1 1012.19 965.04 127.95 o 19 1 1 807.63 502.47 103.87 o 20 1 1 385.49 277.83 84.46 o 0 2 1 1579.81 1356.86 23.81 o 1 2 1 6267.20 5745.25 42.24 o 2 2 1 1305.65 1355.94 17.29 o 3 2 1 59375.90 62293.63 412.77 o 4 2 1 10018.77 10076.59 80.24 o 5 2 1 16071.83 15863.32 139.50 o 6 2 1 1855.09 1981.80 36.15 o 7 2 1 6439.37 5928.12 66.45 o 8 2 1 5093.93 5161.28 61.42 o 9 2 1 7527.12 7385.30 77.36 o 10 2 1 691.15 694.35 36.28 o 11 2 1 10753.75 11315.55 121.43 o 12 2 1 4063.02 4137.86 67.58 o 13 2 1 2139.64 2028.57 64.13 o 14 2 1 193.97 124.52 37.48 o 15 2 1 3979.56 3902.78 90.97 o 16 2 1 29.66 65.73 30.49 o 17 2 1 1272.87 1442.94 182.77 o 18 2 1 170.49 150.89 47.31 o 19 2 1 3039.98 3086.32 132.01 o 20 2 1 568.38 627.19 119.33 o 21 2 1 73.15 -1.44 86.98 o 1 3 1 17888.27 17577.71 119.93 o 2 3 1 9999.67 9939.20 76.93 o 3 3 1 50813.04 52427.39 345.51 o 4 3 1 746.40 877.29 19.78 o 5 3 1 13184.90 12626.05 110.56 o 6 3 1 9858.95 10179.32 94.89 o 7 3 1 15752.04 15657.96 140.72 o 8 3 1 3.40 -8.17 12.91 o 9 3 1 16007.64 15808.42 143.08 o 10 3 1 4904.00 5110.45 61.45 o 11 3 1 8821.62 9125.31 123.02 o 12 3 1 397.03 509.23 48.86 o 13 3 1 11030.83 10767.16 205.64 o 14 3 1 6408.45 6538.83 146.75 o 15 3 1 3202.73 3481.45 102.48 o 16 3 1 241.47 223.31 59.58 o 17 3 1 5605.08 5742.93 222.87 o 18 3 1 1921.12 1755.83 120.20 o 19 3 1 1313.35 1203.73 134.10 o 20 3 1 30.45 98.42 66.88 o 21 3 1 653.66 492.41 129.03 o 0 4 1 950.60 843.74 28.08 o 1 4 1 9523.15 9318.77 72.52 o 2 4 1 554.61 631.30 18.05 o 3 4 1 19935.50 20594.57 156.05 o 4 4 1 396.57 530.61 19.66 o 5 4 1 231.48 103.08 14.41 o 6 4 1 867.67 1038.78 27.28 o 7 4 1 5766.66 5486.68 78.53 o 8 4 1 3153.16 3174.17 50.68 o 9 4 1 1448.15 1493.88 42.41 o 10 4 1 277.75 350.68 28.61 o 11 4 1 9363.02 9248.56 135.90 o 12 4 1 225.05 208.89 50.25 o 13 4 1 32.95 -16.48 62.15 o 14 4 1 884.05 724.57 78.08 o 15 4 1 729.61 770.90 81.42 o 16 4 1 986.16 923.03 87.99 o 17 4 1 623.63 578.28 79.43 o 18 4 1 268.65 161.32 67.74 o 19 4 1 2853.01 2931.28 176.02 o 20 4 1 357.16 469.19 77.68 o 1 5 1 24.23 27.40 13.35 o 2 5 1 331.93 449.28 18.83 o 3 5 1 2.21 -5.44 13.17 o 4 5 1 47.04 2.42 14.65 o 5 5 1 214.29 167.93 18.05 o 6 5 1 856.27 923.69 29.90 o 7 5 1 259.46 265.57 27.99 o 8 5 1 203.80 228.09 30.63 o 9 5 1 88.53 82.12 28.90 o 10 5 1 830.35 834.17 44.91 o 11 5 1 1772.93 1683.51 67.31 o 12 5 1 49.91 40.39 44.61 o 13 5 1 56.36 78.86 60.55 o 14 5 1 162.48 17.79 64.55 o 15 5 1 168.84 140.80 79.58 o 16 5 1 406.93 428.14 117.56 o 17 5 1 183.20 111.07 72.15 o 18 5 1 55.25 153.14 72.80 o 19 5 1 102.21 67.57 72.70 o 0 6 1 37.40 8.60 22.68 o 1 6 1 216.34 151.21 18.14 o 2 6 1 221.47 190.34 19.62 o 3 6 1 4496.71 4362.75 57.87 o 4 6 1 171.88 184.33 22.64 o 5 6 1 1040.27 1011.94 38.06 o 6 6 1 84.99 41.40 22.98 o 7 6 1 1101.19 1058.27 48.82 o 8 6 1 1621.72 1673.74 59.20 o 9 6 1 78.75 106.77 36.51 o 10 6 1 42.01 10.95 37.84 o 11 6 1 126.78 101.51 49.59 o 12 6 1 530.65 445.98 78.38 o 13 6 1 989.12 1110.79 101.33 o 14 6 1 2.27 -48.87 63.27 o 15 6 1 360.52 395.56 84.29 o 16 6 1 206.55 188.37 81.16 o 17 6 1 553.48 618.16 98.05 o 18 6 1 88.51 126.98 77.09 o 1 7 1 1211.34 1152.54 39.06 o 2 7 1 1811.38 1886.47 62.90 o 3 7 1 9295.35 9037.39 120.09 o 4 7 1 1749.82 1727.22 51.26 o 5 7 1 6957.81 6666.10 99.76 o 6 7 1 4111.06 3907.75 95.99 o 7 7 1 4500.93 4569.89 146.93 o 8 7 1 605.39 568.38 79.53 o 9 7 1 3563.79 3666.21 152.50 o 10 7 1 460.62 440.97 81.11 o 11 7 1 7709.33 7041.68 217.52 o 12 7 1 107.69 90.52 71.89 o 13 7 1 2602.23 2748.62 146.63 o 14 7 1 334.50 357.80 89.79 o 15 7 1 623.76 684.17 103.64 o 16 7 1 113.96 67.76 91.36 o 0 8 1 1528.50 1732.97 97.58 o 1 8 1 5435.10 5393.69 116.92 o 2 8 1 61.14 78.48 37.89 o 3 8 1 3985.57 4035.57 97.25 o 4 8 1 231.63 194.54 44.85 o 5 8 1 4257.35 4416.83 119.57 o 6 8 1 54.44 69.97 50.08 o 7 8 1 3041.17 3083.46 146.73 o 8 8 1 2404.52 2430.92 138.82 o 9 8 1 2535.01 2682.33 161.54 o 10 8 1 0.72 2.88 71.25 o 11 8 1 4389.56 4828.30 198.17 o 12 8 1 897.65 1082.85 115.68 o 13 8 1 3343.91 3928.55 181.82 o 14 8 1 443.54 538.87 115.58 o 1 9 1 3609.86 3659.07 110.69 o 2 9 1 1805.35 1828.73 85.74 o 3 9 1 5119.19 5195.85 145.95 o 4 9 1 25.10 -56.26 56.26 o 5 9 1 3982.39 3770.25 191.82 o 6 9 1 755.54 849.34 107.00 o 7 9 1 580.48 580.63 99.75 o 8 9 1 24.25 15.49 79.01 o 9 9 1 3879.89 3862.12 237.49 o 10 9 1 745.84 678.90 105.92 o 11 9 1 600.98 952.63 152.11 o 12 9 1 149.50 229.53 140.01 o 0 10 1 956.72 693.52 185.46 o 1 10 1 188.95 228.86 101.47 o 2 10 1 170.60 196.31 114.11 o 3 10 1 222.41 303.28 126.37 o 4 10 1 228.44 232.16 126.65 o 5 10 1 120.32 134.82 125.40 o 6 10 1 1.45 -88.84 88.84 o 7 10 1 501.48 432.40 130.13 o 8 10 1 11.62 -86.42 86.42 o 0 0 2 41468.20 43911.56 610.88 o 1 0 2 17623.20 17889.96 202.83 o 2 0 2 975.22 945.16 18.38 o 3 0 2 19337.73 19929.03 235.53 o 4 0 2 31930.52 33226.07 371.30 o 5 0 2 25083.31 26080.47 315.00 o 6 0 2 6936.59 7780.61 127.37 o 7 0 2 1665.33 1412.26 48.75 o 8 0 2 18074.31 18329.69 334.87 o 9 0 2 796.15 651.65 27.84 o 10 0 2 804.41 797.93 41.79 o 11 0 2 14005.29 13941.60 230.68 o 12 0 2 12102.14 11755.11 230.02 o 13 0 2 982.31 1075.57 68.45 o 14 0 2 259.62 160.66 84.71 o 15 0 2 7341.64 6625.57 230.42 o 16 0 2 5874.81 5745.14 217.09 o 17 0 2 3452.54 3589.89 219.96 o 18 0 2 676.88 654.86 115.01 o 19 0 2 1393.54 1046.27 124.72 o 20 0 2 3125.09 3157.50 186.54 o 1 1 2 11330.55 12880.95 88.32 o 2 1 2 19802.53 20363.19 153.82 o 3 1 2 2699.96 2546.84 30.03 o 4 1 2 1023.75 1171.34 20.93 o 5 1 2 6664.68 6704.36 68.31 o 6 1 2 23863.48 23953.56 207.97 o 7 1 2 981.13 1349.50 25.41 o 8 1 2 709.13 745.58 19.21 o 9 1 2 269.08 141.31 13.67 o 10 1 2 13278.53 13261.31 137.89 o 11 1 2 763.13 688.95 24.14 o 12 1 2 244.40 211.02 19.54 o 13 1 2 4281.83 4276.22 76.35 o 14 1 2 4555.73 4573.30 101.71 o 15 1 2 1685.12 1687.70 65.50 o 16 1 2 101.64 179.48 45.49 o 17 1 2 8224.40 7686.03 220.13 o 18 1 2 1240.47 1230.51 136.58 o 19 1 2 422.53 453.63 67.68 o 20 1 2 350.35 409.74 108.54 o 21 1 2 2092.42 1935.12 156.35 o 0 2 2 18873.03 20193.79 191.42 o 1 2 2 1224.67 1543.00 19.40 o 2 2 2 257.81 270.39 10.58 o 3 2 2 781.42 840.06 18.08 o 4 2 2 877.36 710.79 17.68 o 5 2 2 23.90 19.10 10.35 o 6 2 2 114.06 141.33 14.91 o 7 2 2 4853.82 5018.21 65.89 o 8 2 2 11337.27 11598.81 120.45 o 9 2 2 865.17 896.50 27.17 o 10 2 2 536.84 625.05 27.17 o 11 2 2 1230.45 1192.81 31.24 o 12 2 2 1196.89 1358.73 36.59 o 13 2 2 159.78 92.69 28.00 o 14 2 2 1.94 26.86 42.40 o 15 2 2 1496.73 1415.66 76.42 o 16 2 2 812.24 1001.87 70.08 o 17 2 2 339.12 135.20 50.71 o 18 2 2 15.25 4.59 53.85 o 19 2 2 901.48 970.79 153.83 o 20 2 2 660.76 653.43 139.10 o 21 2 2 461.90 368.41 117.89 o 1 3 2 17.12 68.81 8.35 o 2 3 2 2896.81 3108.00 34.96 o 3 3 2 1687.59 1834.37 24.79 o 4 3 2 25.43 45.70 9.58 o 5 3 2 2785.19 3046.09 38.53 o 6 3 2 2855.06 3268.05 49.56 o 7 3 2 356.38 518.54 20.22 o 8 3 2 545.47 506.04 23.16 o 9 3 2 532.77 542.18 25.23 o 10 3 2 1380.69 1411.63 40.74 o 11 3 2 710.48 799.58 39.36 o 12 3 2 708.00 834.31 52.62 o 13 3 2 3254.04 3682.66 125.06 o 14 3 2 267.82 205.60 54.88 o 15 3 2 996.79 901.76 74.95 o 16 3 2 23.80 -12.92 50.01 o 17 3 2 1013.15 1101.77 83.24 o 18 3 2 7.06 4.81 54.19 o 19 3 2 69.60 98.67 54.86 o 20 3 2 109.83 131.19 118.25 o 21 3 2 536.55 584.06 145.57 o 0 4 2 14502.14 14370.27 150.89 o 1 4 2 328.82 434.52 15.19 o 2 4 2 25.41 14.86 10.70 o 3 4 2 7736.62 7669.77 70.56 o 4 4 2 6337.48 6155.33 65.06 o 5 4 2 175.07 137.12 13.59 o 6 4 2 252.67 291.86 17.23 o 7 4 2 4469.40 4324.09 62.51 o 8 4 2 16387.17 16655.57 171.94 o 9 4 2 2217.79 2130.96 56.29 o 10 4 2 1078.30 1158.84 49.25 o 11 4 2 8845.30 8451.63 153.88 o 12 4 2 5994.87 5994.04 152.99 o 13 4 2 913.41 842.30 101.89 o 14 4 2 930.71 844.49 79.53 o 15 4 2 4054.56 3879.36 144.09 o 16 4 2 3797.88 3777.39 170.63 o 17 4 2 18.50 33.92 60.51 o 18 4 2 28.74 -4.07 65.71 o 19 4 2 3672.04 3666.25 145.31 o 20 4 2 2417.37 2576.04 129.23 o 1 5 2 11053.32 10931.63 93.09 o 2 5 2 6939.28 6465.84 67.06 o 3 5 2 4250.79 3822.75 49.39 o 4 5 2 198.91 220.46 18.48 o 5 5 2 7762.94 7476.93 78.04 o 6 5 2 13511.78 13014.56 137.25 o 7 5 2 236.32 205.32 23.85 o 8 5 2 63.47 112.78 26.74 o 9 5 2 6792.82 6472.71 113.68 o 10 5 2 8269.22 8194.83 154.15 o 11 5 2 38.91 22.70 36.14 o 12 5 2 314.26 316.88 57.93 o 13 5 2 1975.68 1953.52 110.97 o 14 5 2 6740.84 6527.72 196.18 o 15 5 2 708.31 640.99 84.18 o 16 5 2 8.74 55.24 64.92 o 17 5 2 3340.10 3420.07 149.27 o 18 5 2 2014.19 2165.60 127.35 o 19 5 2 64.21 -40.78 93.43 o 0 6 2 9708.42 9187.90 125.65 o 1 6 2 11500.64 11231.73 103.39 o 2 6 2 132.17 123.66 18.65 o 3 6 2 5769.08 5578.38 70.01 o 4 6 2 9599.87 9234.78 103.94 o 5 6 2 4205.71 3994.38 62.50 o 6 6 2 3280.14 3093.66 58.61 o 7 6 2 3006.78 2971.34 73.04 o 8 6 2 4674.35 4757.98 106.84 o 9 6 2 2413.66 2342.06 83.05 o 10 6 2 195.87 139.38 50.31 o 11 6 2 12896.34 12306.81 363.85 o 12 6 2 2329.58 2237.07 124.47 o 13 6 2 1363.83 1544.13 112.69 o 14 6 2 1166.51 1144.16 105.79 o 15 6 2 3384.27 3512.90 158.65 o 16 6 2 1777.98 1990.12 186.35 o 17 6 2 879.28 1014.12 107.10 o 18 6 2 14.38 20.37 75.38 o 1 7 2 205.00 204.57 27.56 o 2 7 2 928.02 878.68 38.03 o 3 7 2 1713.69 1765.19 50.80 o 4 7 2 10.76 1.09 26.20 o 5 7 2 1184.57 1183.65 46.29 o 6 7 2 1055.55 1124.86 63.18 o 7 7 2 807.03 723.74 60.54 o 8 7 2 15.61 -7.04 60.01 o 9 7 2 1869.42 1821.02 116.42 o 10 7 2 404.55 427.13 81.65 o 11 7 2 1245.11 1324.02 127.93 o 12 7 2 104.11 122.12 74.20 o 13 7 2 875.15 843.41 101.53 o 14 7 2 890.98 950.35 116.21 o 15 7 2 241.76 357.85 92.13 o 16 7 2 285.82 403.14 95.96 o 0 8 2 417.12 447.42 69.17 o 1 8 2 932.83 934.89 59.32 o 2 8 2 125.12 151.25 43.44 o 3 8 2 2588.19 2635.05 79.99 o 4 8 2 294.15 320.53 48.71 o 5 8 2 2.00 -31.66 46.37 o 6 8 2 1201.16 1159.53 96.99 o 7 8 2 976.05 873.89 99.46 o 8 8 2 112.54 -14.93 64.94 o 9 8 2 348.01 299.11 82.69 o 10 8 2 21.09 -65.87 65.87 o 11 8 2 26.44 55.25 76.33 o 12 8 2 1.37 -51.67 74.34 o 13 8 2 211.70 158.25 85.74 o 14 8 2 19.96 -79.32 79.32 o 1 9 2 1115.36 1179.92 74.74 o 2 9 2 1007.37 948.53 72.61 o 3 9 2 129.74 171.06 73.41 o 4 9 2 11.05 0.76 65.31 o 5 9 2 250.72 265.35 76.46 o 6 9 2 3587.16 3665.21 169.38 o 7 9 2 103.93 15.63 75.29 o 8 9 2 126.34 261.25 87.12 o 9 9 2 1195.71 1156.49 120.43 o 10 9 2 1727.34 1775.92 166.06 o 11 9 2 75.03 94.51 86.83 o 12 9 2 24.93 102.33 131.35 o 0 10 2 4324.42 4531.77 338.75 o 1 10 2 1408.22 1701.62 149.06 o 2 10 2 29.06 53.16 113.19 o 3 10 2 1567.77 1586.19 183.98 o 4 10 2 2921.10 2719.91 216.66 o 5 10 2 815.69 852.57 182.91 o 6 10 2 104.97 -98.09 98.09 o 7 10 2 851.51 898.48 140.79 o 1 1 3 4343.05 5154.15 42.97 o 2 1 3 74632.54 81923.44 653.09 o 3 1 3 7583.04 8047.61 82.30 o 4 1 3 13593.10 14693.65 141.70 o 5 1 3 570.90 769.47 19.60 o 6 1 3 26243.76 27886.58 240.73 o 7 1 3 1280.73 1273.35 23.38 o 8 1 3 2681.21 3045.15 40.35 o 9 1 3 440.03 474.66 18.19 o 10 1 3 6414.35 6242.21 72.70 o 11 1 3 808.06 897.26 25.26 o 12 1 3 113.10 116.29 30.06 o 13 1 3 459.12 481.06 46.06 o 14 1 3 2091.99 2032.63 86.53 o 15 1 3 432.78 316.95 90.86 o 16 1 3 502.87 409.68 164.08 o 17 1 3 158.48 118.04 86.04 o 18 1 3 3203.67 3000.47 151.48 o 19 1 3 383.27 276.77 73.88 o 20 1 3 186.07 241.54 137.30 o 21 1 3 24.18 102.35 56.54 o 22 1 3 3707.01 3604.26 225.36 o 0 2 3 56531.42 56357.33 628.20 o 1 2 3 22.28 28.88 8.15 o 2 2 3 20583.46 22476.00 173.98 o 3 2 3 625.08 594.37 23.66 o 4 2 3 9733.46 8706.66 86.46 o 5 2 3 2593.17 2767.86 40.52 o 6 2 3 7.80 2.71 13.29 o 7 2 3 1534.46 1491.92 38.06 o 8 2 3 28409.99 28092.93 282.62 o 9 2 3 495.77 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