#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/68/2226866.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226866_Fobs loop_ _publ_author_name 'Safaei-Ghomi, Javad' 'Motieiyan, Elham' 'Manteghi, Faranak' 'Ghadermazi, Mohammad' 'Aghabozorg, Hossein' _publ_section_title ; Hexaaquanickel(II) tetraaquabis(\m-pyridine-2,6-dicarboxylato)bis(pyridine-2,6-dicarboxylato)trinickelate(II) octahydrate ; _journal_coeditor_code GK2279 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1016 _journal_page_last m1017 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.942 _cell_angle_gamma 90.000 _cell_length_a 20.4561 _cell_length_b 12.7587 _cell_length_c 8.8582 _exptl_crystal_F_000 1256.00 _reflns_d_resolution_high 0.7330 _[local]_cod_data_source_file gk2279Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6868.79 6385.49 153.86 o 4 0 0 43099.04 36339.36 1070.17 o 5 0 0 661.95 546.23 24.70 o 6 0 0 4709.95 4446.48 142.67 o 7 0 0 42.57 86.75 15.19 o 10 0 0 2225.25 2092.35 63.40 o 11 0 0 19377.39 18733.34 497.40 o 12 0 0 11159.05 10483.09 152.88 o 13 0 0 32350.27 30483.85 355.99 o 14 0 0 10438.90 10072.07 162.52 o 15 0 0 2547.06 2538.26 88.02 o 16 0 0 5394.28 5198.69 130.45 o 17 0 0 6015.61 5876.06 140.54 o 18 0 0 6351.79 6280.27 150.93 o 19 0 0 797.73 826.11 66.25 o 20 0 0 137.31 193.04 45.18 o 21 0 0 239.44 247.77 50.49 o 22 0 0 68.66 52.89 39.26 o 23 0 0 69.61 76.98 42.14 o 24 0 0 102.81 207.63 53.75 o 25 0 0 5.47 48.24 43.34 o 26 0 0 3760.08 4835.65 289.48 o 27 0 0 26.93 -4.05 80.46 o 1 1 0 1632.04 1735.64 61.14 o 2 1 0 252.84 264.11 7.07 o 3 1 0 192.11 202.77 8.78 o 4 1 0 223.52 175.86 9.74 o 5 1 0 3367.11 3014.63 38.76 o 6 1 0 1468.08 1474.86 29.24 o 7 1 0 2018.50 1665.62 33.50 o 8 1 0 179.65 152.86 14.01 o 9 1 0 4301.34 3878.06 56.64 o 10 1 0 0.30 10.49 10.61 o 11 1 0 4594.80 4797.23 90.07 o 12 1 0 118.81 114.17 18.88 o 13 1 0 559.42 572.14 31.30 o 14 1 0 481.62 476.75 30.19 o 15 1 0 195.08 172.25 23.67 o 16 1 0 248.39 225.19 26.60 o 17 1 0 83.02 73.45 21.71 o 18 1 0 26.74 40.52 21.16 o 19 1 0 1533.09 1528.39 59.52 o 20 1 0 689.76 776.75 47.26 o 21 1 0 219.58 227.18 33.95 o 22 1 0 3.25 -1.93 23.63 o 23 1 0 1.73 -0.53 26.37 o 24 1 0 227.21 232.85 38.79 o 25 1 0 60.34 71.72 31.44 o 26 1 0 255.16 299.77 56.76 o 27 1 0 82.45 145.16 56.80 o 0 2 0 26216.29 26965.13 1104.52 o 1 2 0 24.97 36.59 4.12 o 2 2 0 9823.55 10369.67 175.63 o 3 2 0 202.46 215.10 11.84 o 4 2 0 16040.93 16075.51 318.63 o 5 2 0 113.88 97.78 9.55 o 9 2 0 22.70 24.91 10.37 o 10 2 0 3586.01 3394.20 57.08 o 11 2 0 4525.56 4026.88 65.61 o 12 2 0 5145.10 4650.20 73.38 o 13 2 0 5569.54 5067.82 79.46 o 14 2 0 11462.30 10788.53 138.99 o 15 2 0 5146.51 4606.22 82.54 o 16 2 0 3209.41 3136.00 71.76 o 17 2 0 1233.15 1300.21 51.40 o 18 2 0 4169.78 4185.01 97.44 o 19 2 0 966.50 994.39 50.75 o 20 2 0 205.41 237.52 33.64 o 21 2 0 197.78 218.94 34.15 o 22 2 0 3381.37 3769.67 96.85 o 23 2 0 424.53 452.84 43.76 o 24 2 0 359.13 370.76 48.39 o 25 2 0 13.57 24.33 32.15 o 26 2 0 5083.40 6024.26 169.07 o 27 2 0 9.66 49.69 49.87 o 1 3 0 847.42 897.46 22.25 o 5 3 0 645.53 561.12 22.61 o 6 3 0 1060.59 1079.61 26.75 o 7 3 0 491.77 522.38 21.28 o 9 3 0 8309.08 8603.59 149.87 o 10 3 0 21.06 18.11 13.11 o 11 3 0 2701.27 2686.13 70.89 o 12 3 0 119.39 108.28 18.29 o 13 3 0 2373.38 2426.23 57.13 o 14 3 0 1553.55 1481.65 47.63 o 15 3 0 745.38 721.47 37.71 o 16 3 0 269.14 249.94 27.65 o 17 3 0 562.64 596.88 43.96 o 18 3 0 32.78 38.45 21.27 o 19 3 0 317.24 358.02 36.07 o 20 3 0 1573.87 1613.63 63.61 o 21 3 0 201.40 220.10 33.84 o 22 3 0 2802.02 2982.46 98.48 o 23 3 0 429.48 467.54 51.01 o 24 3 0 32.71 22.39 31.17 o 25 3 0 190.92 155.86 42.28 o 26 3 0 10.84 23.76 46.96 o 27 3 0 60.74 50.33 66.53 o 0 4 0 211.51 257.86 19.95 o 1 4 0 5978.25 6447.24 117.24 o 3 4 0 1644.97 1703.03 33.65 o 4 4 0 14722.76 15127.86 401.94 o 5 4 0 1207.54 1474.50 30.91 o 6 4 0 4189.45 4550.25 119.73 o 7 4 0 85.33 140.87 13.97 o 8 4 0 19134.58 18270.13 349.24 o 9 4 0 11763.74 12031.82 303.97 o 10 4 0 1609.02 1516.33 42.30 o 11 4 0 11424.51 11291.58 173.58 o 12 4 0 2057.40 1980.59 50.23 o 13 4 0 2766.99 2753.14 60.65 o 14 4 0 6851.50 6685.79 107.79 o 15 4 0 4588.21 4453.82 96.90 o 16 4 0 2395.88 2299.16 63.54 o 17 4 0 1560.35 1496.83 55.02 o 18 4 0 1433.91 1467.96 56.60 o 19 4 0 642.70 679.06 43.56 o 20 4 0 2152.50 2263.03 72.04 o 21 4 0 249.94 275.81 41.88 o 22 4 0 10050.97 10597.80 190.89 o 23 4 0 81.36 109.47 35.92 o 24 4 0 36.48 45.41 32.96 o 25 4 0 44.01 9.09 45.99 o 26 4 0 4364.84 4998.76 188.55 o 1 5 0 7413.47 7747.75 139.00 o 2 5 0 1101.61 1358.78 36.59 o 3 5 0 1195.87 1102.56 31.09 o 4 5 0 6056.24 6671.08 116.26 o 5 5 0 4.32 11.25 8.22 o 6 5 0 1950.43 2004.88 39.81 o 7 5 0 341.37 328.45 20.07 o 8 5 0 110.90 113.42 16.43 o 9 5 0 911.42 1037.43 63.54 o 10 5 0 6507.52 6436.96 208.33 o 11 5 0 308.22 275.34 22.69 o 12 5 0 207.26 189.32 20.78 o 13 5 0 233.65 276.53 24.51 o 14 5 0 1078.97 1064.46 42.78 o 15 5 0 166.42 165.07 23.64 o 16 5 0 732.03 724.06 39.36 o 17 5 0 649.61 620.42 39.12 o 18 5 0 428.22 437.88 43.27 o 19 5 0 372.76 422.42 43.53 o 20 5 0 93.97 114.09 32.95 o 21 5 0 47.28 59.41 30.38 o 22 5 0 123.41 104.38 34.42 o 23 5 0 122.53 161.70 45.55 o 24 5 0 4.05 -26.70 33.66 o 25 5 0 185.99 287.35 68.13 o 26 5 0 13.86 49.74 50.25 o 0 6 0 18186.93 18070.07 759.28 o 1 6 0 2163.84 2408.21 51.85 o 2 6 0 6064.12 7045.33 138.92 o 3 6 0 12.91 8.60 9.18 o 4 6 0 34741.10 35261.90 715.43 o 5 6 0 729.98 681.51 29.22 o 6 6 0 9722.79 9752.53 147.47 o 7 6 0 1058.96 985.75 40.90 o 8 6 0 17125.17 16889.63 507.29 o 9 6 0 1262.20 1158.51 44.03 o 10 6 0 2730.58 2689.48 54.53 o 11 6 0 1613.06 1548.14 44.30 o 12 6 0 6815.42 7014.36 152.00 o 13 6 0 6095.85 5986.10 164.94 o 14 6 0 159.19 195.33 23.67 o 15 6 0 3759.96 3816.19 98.33 o 16 6 0 178.09 193.20 32.26 o 17 6 0 1023.29 1058.13 57.23 o 18 6 0 1268.97 1343.22 63.98 o 19 6 0 164.54 153.42 34.06 o 20 6 0 4186.35 4065.74 129.60 o 21 6 0 1533.92 1443.08 86.70 o 22 6 0 4896.36 5425.16 154.99 o 23 6 0 8.44 13.40 35.67 o 24 6 0 73.69 49.91 40.98 o 25 6 0 0.61 40.04 51.45 o 26 6 0 3298.62 3677.34 172.89 o 1 7 0 1285.19 1216.40 38.41 o 2 7 0 81.59 105.41 17.13 o 3 7 0 1454.67 1358.31 43.02 o 4 7 0 3711.94 3568.55 96.96 o 5 7 0 6183.50 6285.25 118.95 o 6 7 0 112.52 75.05 15.03 o 7 7 0 2619.70 2634.24 57.29 o 8 7 0 379.88 365.14 23.97 o 9 7 0 13.54 1.45 14.63 o 10 7 0 2766.27 2772.87 73.51 o 11 7 0 298.66 302.26 24.30 o 12 7 0 3067.63 3224.18 75.08 o 13 7 0 134.94 158.05 21.38 o 14 7 0 3113.49 3190.39 84.37 o 15 7 0 178.86 187.11 31.05 o 16 7 0 1034.15 1130.23 79.02 o 17 7 0 107.81 118.70 30.11 o 18 7 0 116.42 117.87 38.26 o 19 7 0 55.89 76.82 38.22 o 20 7 0 162.85 179.96 46.65 o 21 7 0 134.21 113.24 43.26 o 22 7 0 2.71 -16.70 32.85 o 23 7 0 1164.23 1233.71 88.44 o 24 7 0 1.01 -16.60 47.07 o 25 7 0 1324.16 1337.08 117.22 o 0 8 0 9195.89 8939.83 307.45 o 1 8 0 285.51 303.46 23.95 o 2 8 0 355.07 369.72 25.53 o 3 8 0 1287.58 1293.25 41.38 o 4 8 0 3345.26 3181.85 65.21 o 5 8 0 884.27 882.38 35.24 o 6 8 0 660.54 693.47 31.87 o 7 8 0 535.45 570.19 29.94 o 8 8 0 11051.28 10931.59 230.72 o 9 8 0 120.93 117.42 18.26 o 10 8 0 7449.13 7427.38 188.09 o 11 8 0 2038.63 2094.66 52.38 o 12 8 0 182.20 173.98 28.11 o 13 8 0 741.17 809.49 56.89 o 14 8 0 3963.67 4053.47 122.78 o 15 8 0 6.11 39.25 24.39 o 16 8 0 102.96 152.23 40.37 o 17 8 0 149.75 156.55 41.10 o 18 8 0 3248.07 3220.43 117.47 o 19 8 0 495.75 502.54 60.65 o 20 8 0 589.72 580.84 64.53 o 21 8 0 190.36 202.41 49.47 o 22 8 0 3581.14 3678.32 137.51 o 23 8 0 20.09 63.72 42.90 o 24 8 0 62.70 48.86 54.90 o 1 9 0 3794.26 3816.90 93.68 o 2 9 0 173.96 180.28 22.14 o 3 9 0 3491.01 3396.32 79.09 o 4 9 0 1235.63 1177.55 42.52 o 5 9 0 1468.91 1547.02 47.54 o 6 9 0 637.71 614.67 35.24 o 7 9 0 11011.22 10791.11 279.49 o 8 9 0 7480.19 7468.12 178.37 o 9 9 0 3271.09 3203.49 79.77 o 10 9 0 5332.95 5448.22 198.58 o 11 9 0 776.14 763.19 50.79 o 12 9 0 1788.60 1814.14 67.29 o 13 9 0 512.75 491.84 53.33 o 14 9 0 188.08 158.14 39.98 o 15 9 0 37.47 4.29 30.73 o 16 9 0 1628.68 1643.34 87.42 o 17 9 0 599.77 617.75 63.20 o 18 9 0 901.37 872.75 72.76 o 19 9 0 860.97 871.84 75.58 o 20 9 0 3216.18 3320.01 130.04 o 21 9 0 2533.32 2621.84 120.47 o 22 9 0 486.67 567.40 71.38 o 23 9 0 313.11 275.20 60.31 o 0 10 0 15758.50 15176.95 716.96 o 1 10 0 106.89 138.07 22.48 o 2 10 0 3616.44 3668.58 118.99 o 3 10 0 566.00 488.29 32.35 o 4 10 0 6725.34 6238.99 113.45 o 5 10 0 56.13 78.37 19.52 o 6 10 0 5409.31 5257.21 124.63 o 7 10 0 9.15 18.09 15.77 o 8 10 0 3564.11 3614.05 94.53 o 9 10 0 250.65 274.21 33.35 o 10 10 0 659.51 680.92 46.01 o 11 10 0 63.14 64.34 32.75 o 12 10 0 7508.46 7027.17 159.98 o 13 10 0 1146.19 1165.11 76.33 o 14 10 0 1203.71 1194.57 78.38 o 15 10 0 40.30 46.58 35.69 o 16 10 0 910.14 833.08 71.60 o 17 10 0 77.74 60.50 39.45 o 18 10 0 1762.06 1765.31 105.86 o 19 10 0 39.24 53.65 41.33 o 20 10 0 628.48 663.69 73.50 o 21 10 0 251.23 257.70 56.84 o 22 10 0 426.26 420.59 66.98 o 1 11 0 2664.51 2697.24 68.78 o 2 11 0 131.09 149.71 25.15 o 3 11 0 2650.97 2746.50 69.41 o 4 11 0 3.73 5.64 16.51 o 5 11 0 49.02 25.36 17.80 o 6 11 0 65.31 121.35 22.93 o 7 11 0 217.65 159.71 29.88 o 8 11 0 78.46 101.30 27.35 o 9 11 0 511.46 503.03 54.34 o 10 11 0 197.87 177.41 41.20 o 11 11 0 166.79 183.36 44.20 o 12 11 0 1631.41 1545.28 85.76 o 13 11 0 173.10 221.29 48.82 o 14 11 0 2086.57 2177.78 106.44 o 15 11 0 183.53 194.51 48.15 o 16 11 0 795.37 836.71 74.40 o 17 11 0 291.22 276.80 54.75 o 18 11 0 346.11 418.95 62.78 o 19 11 0 283.77 268.86 56.80 o 20 11 0 250.10 229.02 56.82 o 21 11 0 634.82 719.80 80.05 o 0 12 0 3277.55 3332.98 189.85 o 1 12 0 2149.94 1951.80 64.10 o 2 12 0 3414.72 3253.14 108.09 o 3 12 0 2877.53 2603.47 71.86 o 4 12 0 1101.66 1141.23 51.04 o 5 12 0 71.35 33.90 20.26 o 6 12 0 3497.94 3418.43 101.94 o 7 12 0 30.01 45.82 32.77 o 8 12 0 3204.93 3182.06 112.75 o 9 12 0 61.11 42.92 35.74 o 10 12 0 12.97 -7.51 30.58 o 11 12 0 19.02 37.51 35.17 o 12 12 0 3561.18 3454.63 125.25 o 13 12 0 155.04 176.58 46.42 o 14 12 0 1299.61 1272.18 86.38 o 15 12 0 7.71 6.45 36.06 o 16 12 0 1006.96 982.41 82.47 o 17 12 0 145.01 71.32 44.87 o 18 12 0 1034.88 1108.99 89.85 o 19 12 0 38.97 16.57 44.06 o 20 12 0 53.37 67.61 46.93 o 1 13 0 5743.35 5450.29 105.73 o 2 13 0 1164.29 1210.56 55.87 o 3 13 0 2859.28 2660.74 118.01 o 4 13 0 283.99 305.84 48.38 o 5 13 0 1622.86 1423.28 92.40 o 6 13 0 786.84 727.92 65.16 o 7 13 0 452.22 410.74 55.41 o 8 13 0 1379.12 1317.91 83.69 o 9 13 0 1592.85 1501.98 89.04 o 10 13 0 1773.46 1743.52 94.92 o 11 13 0 119.63 114.81 43.91 o 12 13 0 4573.79 4492.75 147.73 o 13 13 0 134.53 93.75 44.12 o 14 13 0 1230.23 1232.81 90.35 o 15 13 0 166.05 170.90 50.98 o 16 13 0 548.93 602.27 73.78 o 17 13 0 82.68 63.08 45.31 o 18 13 0 1153.19 1143.31 94.13 o 0 14 0 23.10 30.12 32.36 o 1 14 0 147.32 186.82 32.07 o 2 14 0 1739.80 1708.16 87.14 o 3 14 0 3.85 10.81 32.93 o 4 14 0 416.54 476.94 57.92 o 5 14 0 99.76 80.88 38.71 o 6 14 0 715.62 776.71 69.29 o 7 14 0 90.94 104.35 41.74 o 8 14 0 1008.32 1020.28 84.37 o 9 14 0 89.23 120.63 44.38 o 10 14 0 1632.30 1646.81 97.03 o 11 14 0 22.68 14.46 36.28 o 12 14 0 392.96 379.60 61.80 o 13 14 0 22.71 30.02 38.92 o 14 14 0 1776.73 1844.81 109.17 o 15 14 0 5.94 12.66 40.70 o 16 14 0 1112.11 1116.59 94.10 o 1 15 0 1626.80 1623.59 87.86 o 2 15 0 103.12 110.07 39.53 o 3 15 0 1081.29 1127.99 79.28 o 4 15 0 4.27 -10.88 36.43 o 5 15 0 1213.44 1219.98 84.83 o 6 15 0 2014.04 2106.87 105.45 o 7 15 0 322.17 394.70 60.42 o 8 15 0 619.36 647.76 71.30 o 9 15 0 2.52 13.80 37.38 o 10 15 0 810.85 808.83 79.75 o 11 15 0 945.25 1019.80 87.45 o 12 15 0 2585.14 2552.26 124.91 o 13 15 0 10.88 14.46 42.64 o 14 15 0 1977.19 2187.53 121.38 o 0 16 0 1369.43 1502.31 207.43 o 1 16 0 240.28 329.79 86.57 o 2 16 0 1747.59 1912.99 157.14 o 3 16 0 221.57 251.01 62.26 o 4 16 0 129.26 86.63 42.58 o 5 16 0 36.22 43.17 39.67 o 6 16 0 985.35 1034.84 84.51 o 7 16 0 93.62 100.04 46.38 o 8 16 0 1130.97 1172.65 91.56 o 9 16 0 21.10 -4.22 39.99 o 10 16 0 1548.39 1629.93 105.86 o 1 17 0 1366.88 1439.23 149.82 o 2 17 0 639.24 672.49 117.51 o 3 17 0 29.00 28.99 62.46 o 4 17 0 45.94 109.42 72.42 o 5 17 0 25.23 4.00 46.75 o -27 1 1 61.23 4.17 35.13 o -26 1 1 67.90 116.60 44.19 o -25 1 1 2379.09 2896.41 104.09 o -24 1 1 36.97 53.27 29.14 o -23 1 1 165.96 158.84 34.03 o -22 1 1 1.44 33.55 25.66 o -21 1 1 2752.99 2904.98 83.78 o -20 1 1 82.87 111.55 27.69 o -19 1 1 444.99 447.17 37.45 o -18 1 1 1128.57 1123.33 50.98 o -17 1 1 3562.77 3383.73 76.97 o -16 1 1 2815.32 2826.11 68.35 o -15 1 1 3820.70 3654.50 73.15 o -14 1 1 11710.05 10944.00 128.82 o -13 1 1 12515.14 11723.07 181.93 o -12 1 1 1600.79 1517.99 44.21 o -10 1 1 11918.76 11057.46 186.57 o -9 1 1 920.27 798.62 28.20 o -8 1 1 10155.12 9378.59 149.35 o -7 1 1 3999.24 3479.11 72.11 o -5 1 1 3511.66 3294.57 92.41 o -4 1 1 71.49 97.06 6.84 o -3 1 1 60111.79 58896.45 1729.26 o -2 1 1 7999.54 8417.38 232.31 o 1 1 1 87974.30 86786.84 2039.47 o 3 1 1 79.42 107.80 6.55 o 4 1 1 4341.36 4387.58 72.29 o 5 1 1 17634.07 16971.13 281.32 o 7 1 1 478.98 484.35 20.69 o 8 1 1 934.30 929.94 30.82 o 10 1 1 15076.57 14024.29 113.73 o 11 1 1 269.04 198.86 20.81 o 12 1 1 7974.01 7395.16 91.53 o 13 1 1 12319.16 11232.84 116.96 o 14 1 1 5822.61 5415.32 85.91 o 15 1 1 11208.87 10759.96 124.16 o 16 1 1 2882.62 2765.69 68.17 o 17 1 1 1647.77 1647.28 61.19 o 18 1 1 752.71 765.39 43.64 o 19 1 1 1241.29 1300.98 56.63 o 20 1 1 52.90 51.81 24.79 o 21 1 1 954.60 953.31 53.42 o 22 1 1 136.65 141.87 32.34 o 23 1 1 1119.43 1400.44 66.35 o 24 1 1 134.11 195.80 49.06 o 25 1 1 27.09 29.83 42.62 o 26 1 1 111.63 214.39 53.39 o 27 1 1 5060.66 6135.93 209.24 o -27 2 1 4.87 3.92 38.79 o -26 2 1 1129.19 1230.82 76.93 o -25 2 1 42.54 22.02 33.37 o -24 2 1 32.11 -11.23 29.62 o -23 2 1 22.82 40.24 35.25 o -22 2 1 924.30 944.97 54.15 o -21 2 1 489.13 517.45 43.08 o -20 2 1 853.41 811.22 48.27 o -19 2 1 942.65 925.83 49.27 o -18 2 1 14.52 17.23 20.15 o -17 2 1 554.23 557.38 36.69 o -16 2 1 27.75 24.11 17.41 o -15 2 1 2483.16 2456.02 66.65 o -14 2 1 638.84 663.18 34.30 o -13 2 1 737.99 755.03 35.17 o -12 2 1 1773.58 1708.15 46.55 o -11 2 1 1.58 -1.89 12.87 o -10 2 1 18.32 24.63 11.50 o -9 2 1 119.55 127.89 14.13 o -8 2 1 974.53 1030.06 28.29 o -7 2 1 6345.15 6252.63 91.62 o -6 2 1 141.63 153.47 10.80 o -5 2 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