#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/69/2226947.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226947_Fobs loop_ _publ_author_name 'Basu, Smita' 'Masharing, Cheerfulman' 'Das, Babulal' _publ_section_title ; {4-[(3-Formyl-4-hydroxyphenyl)diazenyl]benzoato}triphenyltin ; _journal_coeditor_code IS2569 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m927 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.262 _cell_angle_gamma 90.000 _cell_length_a 8.3751 _cell_length_b 48.8458 _cell_length_c 6.9742 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file is2569Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KMR-SBX-5-B in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 289.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4553.52 4510.24 68.10 o 2 0 0 744.50 685.83 22.04 o 3 0 0 11550.70 11579.06 245.14 o 4 0 0 599.50 655.78 32.52 o 5 0 0 6791.51 6812.74 100.98 o 6 0 0 354.43 450.76 71.36 o 7 0 0 3003.49 3164.17 199.83 o 8 0 0 832.13 816.14 186.96 o 9 0 0 32.43 113.40 110.34 o 1 1 0 34336.65 35519.54 421.16 o 2 1 0 378.17 371.03 11.55 o 3 1 0 4920.38 4725.12 51.42 o 4 1 0 8923.66 8778.66 73.12 o 5 1 0 451.29 471.02 22.59 o 6 1 0 4647.39 4422.26 154.59 o 7 1 0 874.30 957.84 109.15 o 8 1 0 128.88 153.56 78.41 o 9 1 0 516.02 501.03 121.45 o 1 2 0 3264.38 3218.22 37.48 o 2 2 0 585.35 598.04 14.25 o 3 2 0 4593.38 4567.95 58.14 o 4 2 0 68.86 97.62 11.27 o 5 2 0 4259.00 4196.65 54.34 o 6 2 0 166.64 219.84 43.83 o 7 2 0 798.26 725.49 71.36 o 8 2 0 246.90 193.37 83.36 o 9 2 0 16.79 10.02 68.01 o 1 3 0 2105.36 2241.42 34.30 o 2 3 0 5000.17 5081.15 59.12 o 3 3 0 517.96 533.56 15.93 o 4 3 0 363.02 386.57 15.80 o 5 3 0 420.21 475.04 23.36 o 6 3 0 226.06 197.65 39.07 o 7 3 0 86.06 86.66 41.97 o 8 3 0 25.26 76.02 69.81 o 9 3 0 50.78 14.35 69.30 o 0 4 0 6656.53 6358.71 109.07 o 1 4 0 1330.51 1326.99 16.82 o 2 4 0 2180.53 2237.59 25.60 o 3 4 0 292.33 296.82 14.11 o 4 4 0 515.71 537.46 17.98 o 5 4 0 6355.43 6525.50 71.16 o 6 4 0 483.24 535.41 52.39 o 7 4 0 1501.17 1499.12 93.91 o 8 4 0 291.34 235.58 88.78 o 9 4 0 6.20 -13.66 64.58 o 1 5 0 24816.33 25950.60 265.92 o 2 5 0 488.65 556.66 14.96 o 3 5 0 5135.93 5222.17 57.55 o 4 5 0 9289.34 9408.97 136.59 o 5 5 0 378.44 411.99 19.95 o 6 5 0 3812.10 3715.52 123.07 o 7 5 0 2952.42 2906.70 120.54 o 8 5 0 158.69 217.69 88.41 o 9 5 0 354.67 412.54 116.43 o 0 6 0 33153.76 30300.93 452.90 o 1 6 0 9065.24 9470.50 94.90 o 2 6 0 43829.11 45276.03 437.01 o 3 6 0 8519.34 8790.12 116.77 o 4 6 0 2432.27 2405.32 34.60 o 5 6 0 7179.17 6937.07 77.64 o 6 6 0 796.13 908.70 70.50 o 7 6 0 803.32 917.99 89.91 o 8 6 0 1401.41 1436.33 162.37 o 9 6 0 12.69 -16.99 66.37 o 1 7 0 22130.77 22688.82 271.60 o 2 7 0 83581.43 85902.36 914.08 o 3 7 0 5028.45 5050.01 68.20 o 4 7 0 8121.73 8080.30 91.10 o 5 7 0 9.65 33.71 11.45 o 6 7 0 2494.94 2643.84 106.13 o 7 7 0 805.54 879.09 87.86 o 8 7 0 308.62 406.03 106.50 o 9 7 0 851.04 728.66 139.70 o 0 8 0 4180.99 3797.37 65.31 o 1 8 0 1210.88 1251.29 17.16 o 2 8 0 13864.41 14442.23 162.83 o 3 8 0 8542.79 8608.27 65.52 o 4 8 0 169.45 230.28 14.45 o 5 8 0 1391.89 1428.33 32.60 o 6 8 0 0.33 40.14 32.55 o 7 8 0 488.88 483.59 73.10 o 8 8 0 168.83 154.91 69.11 o 9 8 0 14.33 26.61 73.80 o 1 9 0 916.54 967.02 15.45 o 2 9 0 12395.12 12967.69 133.94 o 3 9 0 1485.99 1555.93 26.46 o 4 9 0 97.13 105.26 11.47 o 5 9 0 70.91 73.16 12.87 o 6 9 0 46.70 34.93 28.34 o 7 9 0 74.96 72.84 47.48 o 8 9 0 20.30 31.68 53.95 o 9 9 0 33.98 14.94 68.77 o 0 10 0 2326.84 2171.43 44.95 o 1 10 0 12948.00 12812.46 99.22 o 2 10 0 5893.55 6122.84 63.67 o 3 10 0 9377.62 9471.97 80.17 o 4 10 0 6196.12 6411.71 64.05 o 5 10 0 980.86 978.59 29.85 o 6 10 0 521.07 588.58 54.35 o 7 10 0 179.44 220.27 58.48 o 8 10 0 491.42 484.75 91.91 o 9 10 0 101.08 75.81 77.70 o 1 11 0 18283.97 17460.89 121.92 o 2 11 0 6243.37 6335.69 68.76 o 3 11 0 6567.97 6731.30 66.96 o 4 11 0 10174.92 10120.45 116.46 o 5 11 0 102.05 113.82 15.84 o 6 11 0 4082.89 4197.45 161.31 o 7 11 0 2003.64 1961.98 116.52 o 8 11 0 184.21 211.54 72.59 o 9 11 0 1133.30 1020.37 156.96 o 0 12 0 198.71 165.89 11.98 o 1 12 0 850.65 890.40 17.21 o 2 12 0 17461.39 17604.19 196.21 o 3 12 0 8061.59 8226.77 87.34 o 4 12 0 4988.11 5118.01 60.02 o 5 12 0 6726.45 6657.35 77.14 o 6 12 0 1700.83 1693.49 80.04 o 7 12 0 1244.58 1307.00 118.88 o 8 12 0 874.96 968.01 115.33 o 9 12 0 0.07 86.96 80.55 o 1 13 0 15301.03 14757.97 125.76 o 2 13 0 8124.56 8137.71 72.36 o 3 13 0 9.62 33.02 8.69 o 4 13 0 10232.02 9894.09 108.07 o 5 13 0 196.83 229.28 21.99 o 6 13 0 2081.45 2037.74 86.53 o 7 13 0 440.67 537.16 89.52 o 8 13 0 500.16 426.98 89.69 o 9 13 0 295.50 270.99 103.33 o 0 14 0 318.73 316.68 16.62 o 1 14 0 1242.94 1244.56 21.25 o 2 14 0 2237.94 2135.30 29.18 o 3 14 0 1760.77 1741.96 30.27 o 4 14 0 1989.96 2048.18 39.55 o 5 14 0 1529.40 1550.85 45.38 o 6 14 0 77.37 66.09 31.13 o 7 14 0 623.77 613.32 93.81 o 8 14 0 213.93 228.15 74.99 o 9 14 0 35.73 42.06 75.00 o 1 15 0 3219.69 3307.41 34.33 o 2 15 0 2433.92 2497.20 31.46 o 3 15 0 592.80 591.99 19.46 o 4 15 0 5961.92 5965.39 70.53 o 5 15 0 543.58 549.62 32.67 o 6 15 0 290.20 282.55 44.77 o 7 15 0 311.28 262.65 72.92 o 8 15 0 55.15 40.40 58.18 o 9 15 0 37.56 48.60 77.38 o 0 16 0 4876.16 4667.40 63.30 o 1 16 0 506.11 494.20 15.35 o 2 16 0 5049.08 4992.14 48.90 o 3 16 0 7180.17 7260.85 59.80 o 4 16 0 85.75 89.73 14.16 o 5 16 0 5561.42 5452.06 85.41 o 6 16 0 1198.63 1204.53 72.75 o 7 16 0 119.63 153.59 64.18 o 8 16 0 598.06 575.54 100.89 o 9 16 0 14.08 79.99 65.82 o 1 17 0 16724.64 15570.16 129.31 o 2 17 0 10954.20 10957.84 98.09 o 3 17 0 316.04 382.13 17.58 o 4 17 0 1604.56 1674.31 37.37 o 5 17 0 586.42 594.20 35.06 o 6 17 0 3522.28 3355.81 111.41 o 7 17 0 887.85 1010.42 113.54 o 8 17 0 738.70 748.66 110.07 o 9 17 0 1040.49 1018.16 130.01 o 0 18 0 31210.62 29385.19 490.84 o 1 18 0 74.79 96.01 9.92 o 2 18 0 10446.53 10341.89 115.41 o 3 18 0 12998.10 12669.88 116.49 o 4 18 0 1677.78 1754.25 38.68 o 5 18 0 6062.54 5960.93 92.17 o 6 18 0 2062.39 2048.77 90.21 o 7 18 0 1798.05 1745.22 139.73 o 8 18 0 876.56 1025.01 123.85 o 9 18 0 14.83 118.24 71.79 o 1 19 0 2122.52 2005.14 28.76 o 2 19 0 94.66 97.43 10.31 o 3 19 0 2169.27 2193.10 37.47 o 4 19 0 8173.73 7864.66 80.87 o 5 19 0 230.26 247.03 27.35 o 6 19 0 1444.65 1490.28 81.09 o 7 19 0 364.93 407.31 85.56 o 8 19 0 198.22 197.34 74.09 o 9 19 0 298.32 381.04 96.23 o 0 20 0 3371.54 3300.96 52.97 o 1 20 0 326.11 372.84 15.10 o 2 20 0 173.95 185.19 12.35 o 3 20 0 2325.90 2308.24 38.17 o 4 20 0 389.51 423.75 24.03 o 5 20 0 11.76 32.12 18.53 o 6 20 0 23.34 34.15 31.07 o 7 20 0 187.30 152.54 63.91 o 8 20 0 16.72 -1.78 57.33 o 9 20 0 1.34 60.60 65.59 o 1 21 0 917.25 892.66 21.35 o 2 21 0 807.49 838.45 22.57 o 3 21 0 10.15 20.14 10.50 o 4 21 0 1007.99 1046.12 34.02 o 5 21 0 2.30 19.27 20.64 o 6 21 0 607.08 580.94 60.01 o 7 21 0 135.86 172.27 66.68 o 8 21 0 9.50 75.71 63.14 o 9 21 0 103.26 105.66 72.72 o 0 22 0 5697.12 5332.88 82.77 o 1 22 0 659.78 676.00 19.56 o 2 22 0 9356.42 8839.22 85.70 o 3 22 0 7899.47 7774.78 91.20 o 4 22 0 0.56 30.54 14.31 o 5 22 0 4897.18 4691.20 97.43 o 6 22 0 1932.12 1876.40 121.53 o 7 22 0 1018.53 990.92 116.06 o 8 22 0 1060.19 938.09 124.06 o 9 22 0 23.70 21.80 66.26 o 1 23 0 10084.12 9511.08 94.41 o 2 23 0 1455.35 1546.73 30.74 o 3 23 0 2248.35 2178.32 38.47 o 4 23 0 9829.70 9553.54 121.88 o 5 23 0 398.06 443.01 39.37 o 6 23 0 1198.43 1316.90 104.75 o 7 23 0 1461.82 1427.64 134.51 o 8 23 0 426.58 384.60 94.41 o 9 23 0 573.73 541.47 112.64 o 0 24 0 8222.33 7755.94 92.90 o 1 24 0 100.62 107.16 11.85 o 2 24 0 9554.39 9302.14 98.99 o 3 24 0 8722.52 8440.53 90.40 o 4 24 0 100.96 130.53 21.81 o 5 24 0 3961.29 3874.68 91.89 o 6 24 0 71.02 137.23 50.15 o 7 24 0 1043.62 1028.35 120.78 o 8 24 0 972.12 814.53 118.12 o 1 25 0 5355.40 4875.57 69.30 o 2 25 0 2001.00 1949.25 37.37 o 3 25 0 2709.28 2634.70 46.89 o 4 25 0 4516.83 4276.75 77.18 o 5 25 0 3.57 10.46 22.32 o 6 25 0 1536.74 1520.10 113.37 o 7 25 0 293.13 259.14 78.64 o 8 25 0 48.88 174.22 72.62 o 0 26 0 0.26 32.57 14.15 o 1 26 0 349.35 425.00 20.18 o 2 26 0 670.43 637.48 24.83 o 3 26 0 108.67 97.58 15.59 o 4 26 0 125.48 117.83 22.67 o 5 26 0 216.87 256.52 37.26 o 6 26 0 199.59 191.52 59.08 o 7 26 0 16.72 54.34 57.82 o 8 26 0 3.07 44.59 61.40 o 1 27 0 1251.99 1209.45 31.36 o 2 27 0 756.77 764.13 28.26 o 3 27 0 48.87 52.17 14.85 o 4 27 0 1069.45 1085.18 46.88 o 5 27 0 441.38 394.96 43.50 o 6 27 0 239.86 215.82 59.21 o 7 27 0 63.06 170.92 72.03 o 8 27 0 134.08 156.91 72.04 o 0 28 0 4440.81 4195.01 77.66 o 1 28 0 2224.84 2302.00 42.72 o 2 28 0 2309.41 2388.13 45.45 o 3 28 0 3793.67 3741.34 62.66 o 4 28 0 285.52 287.68 32.42 o 5 28 0 1135.46 1171.70 63.56 o 6 28 0 442.67 328.65 79.89 o 7 28 0 1397.53 1416.57 141.27 o 8 28 0 831.69 746.66 119.18 o 1 29 0 9810.25 9496.45 128.83 o 2 29 0 4000.17 3826.67 56.48 o 3 29 0 4200.06 4293.73 74.67 o 4 29 0 7976.00 7738.87 127.66 o 5 29 0 252.12 251.40 43.03 o 6 29 0 1596.56 1554.53 137.31 o 7 29 0 532.68 630.01 107.82 o 8 29 0 149.42 190.42 80.18 o 0 30 0 4734.08 4474.31 98.73 o 1 30 0 2097.04 2262.75 44.69 o 2 30 0 3946.54 3924.96 64.99 o 3 30 0 5399.24 5188.19 85.75 o 4 30 0 666.97 760.50 48.90 o 5 30 0 705.83 724.26 64.85 o 6 30 0 5.60 22.01 53.75 o 7 30 0 491.16 533.66 101.86 o 8 30 0 502.00 400.39 102.16 o 1 31 0 2682.74 2518.03 46.19 o 2 31 0 937.89 952.29 34.08 o 3 31 0 1475.57 1534.86 50.62 o 4 31 0 2137.66 1954.65 64.88 o 5 31 0 119.42 75.88 38.98 o 6 31 0 195.04 250.24 78.46 o 7 31 0 341.60 282.33 86.47 o 8 31 0 62.27 108.61 73.92 o 0 32 0 197.54 201.84 26.36 o 1 32 0 136.48 128.85 16.22 o 2 32 0 6.59 8.93 12.85 o 3 32 0 39.52 45.46 20.08 o 4 32 0 873.18 785.89 51.42 o 5 32 0 0.23 3.39 33.77 o 6 32 0 166.52 138.99 68.02 o 7 32 0 31.59 67.52 62.97 o 8 32 0 37.36 61.24 67.73 o 1 33 0 1103.34 1141.91 37.32 o 2 33 0 680.38 697.37 35.69 o 3 33 0 500.92 509.44 36.98 o 4 33 0 1380.38 1249.33 66.39 o 5 33 0 21.57 22.54 38.54 o 6 33 0 392.39 410.69 93.38 o 7 33 0 113.81 208.67 79.53 o 8 33 0 132.36 45.82 69.56 o 0 34 0 4338.96 4317.81 92.57 o 1 34 0 1003.72 984.07 36.81 o 2 34 0 2727.27 2668.19 66.87 o 3 34 0 4741.95 4728.01 90.21 o 4 34 0 8.39 24.41 30.63 o 5 34 0 661.10 644.36 79.80 o 6 34 0 4.92 25.09 55.76 o 7 34 0 480.86 311.42 89.87 o 8 34 0 416.54 340.06 97.43 o 1 35 0 4860.50 4822.58 75.97 o 2 35 0 2825.38 2766.14 74.55 o 3 35 0 2490.95 2450.12 73.20 o 4 35 0 2876.15 2775.79 107.53 o 5 35 0 71.95 -8.02 48.09 o 6 35 0 942.86 1038.14 128.02 o 7 35 0 294.03 340.78 93.33 o 0 36 0 6310.40 6267.83 157.37 o 1 36 0 981.85 1003.28 46.66 o 2 36 0 2030.33 2124.59 67.12 o 3 36 0 2626.09 2569.80 79.52 o 4 36 0 1158.63 967.18 88.53 o 5 36 0 417.64 492.65 93.45 o 6 36 0 258.23 282.16 84.42 o 7 36 0 337.22 262.52 87.90 o 1 37 0 1239.41 1254.44 53.61 o 2 37 0 618.08 636.41 44.25 o 3 37 0 55.65 109.17 34.59 o 4 37 0 12.47 22.67 38.26 o 5 37 0 64.59 73.66 60.45 o 6 37 0 191.93 241.64 82.04 o 7 37 0 90.39 114.49 72.75 o 0 38 0 26.61 61.77 37.02 o 1 38 0 60.34 90.76 25.61 o 2 38 0 77.28 71.03 27.29 o 3 38 0 126.75 143.10 37.74 o 4 38 0 6.40 -1.81 36.78 o 5 38 0 16.28 14.21 53.87 o 6 38 0 4.94 -7.44 54.23 o 7 38 0 21.19 46.52 81.40 o 1 39 0 984.05 992.44 58.27 o 2 39 0 1052.32 1099.44 61.60 o 3 39 0 605.50 569.49 73.70 o 4 39 0 316.58 299.79 96.96 o 5 39 0 7.83 26.22 70.83 o 6 39 0 203.08 125.32 104.64 o 7 39 0 56.80 4.93 75.93 o 0 40 0 4002.63 4014.09 145.88 o 1 40 0 280.23 357.16 42.34 o 2 40 0 4387.36 4295.06 142.22 o 3 40 0 1656.10 1586.13 167.67 o 4 40 0 16.10 50.42 65.44 o 5 40 0 2710.92 2584.40 215.27 o 6 40 0 131.41 101.95 82.80 o 7 40 0 169.69 106.11 88.47 o 1 41 0 5272.28 5506.09 122.52 o 2 41 0 448.63 630.54 69.31 o 3 41 0 284.56 307.14 94.80 o 4 41 0 1335.24 1408.79 302.77 o 5 41 0 35.62 56.85 76.15 o 6 41 0 916.06 934.62 159.16 o 0 42 0 4412.15 4253.13 174.58 o 1 42 0 17.48 114.09 35.27 o 2 42 0 1271.58 1367.58 93.04 o 3 42 0 232.63 253.00 89.93 o 4 42 0 24.72 54.95 79.25 o 5 42 0 1107.37 1106.08 163.29 o 6 42 0 155.21 200.61 99.18 o 1 43 0 232.21 274.46 54.50 o 2 43 0 44.32 40.54 43.49 o 3 43 0 12.85 14.18 65.78 o 4 43 0 162.06 138.27 86.27 o 5 43 0 1.73 59.83 74.42 o 6 43 0 270.33 171.05 97.48 o 0 44 0 181.33 186.57 65.87 o 1 44 0 42.98 67.45 40.16 o 2 44 0 1009.92 827.02 134.03 o 3 44 0 20.16 10.74 62.34 o 4 44 0 6.91 3.84 69.75 o 5 44 0 89.30 77.09 84.18 o 6 44 0 39.73 137.13 93.62 o 1 45 0 1900.97 1892.32 117.08 o 2 45 0 3.75 43.14 68.12 o 3 45 0 10.19 32.31 67.36 o 4 45 0 586.06 668.51 163.53 o 5 45 0 123.88 118.21 85.61 o 6 45 0 504.69 559.68 144.06 o 0 46 0 5956.17 5567.94 273.84 o 1 46 0 11.95 113.85 60.46 o 2 46 0 323.54 214.90 95.30 o 3 46 0 1190.71 1159.32 160.47 o 4 46 0 49.54 83.87 77.19 o 5 46 0 1447.58 1222.89 178.32 o 6 46 0 108.00 163.62 96.75 o 1 47 0 2805.06 2683.80 168.24 o 2 47 0 1825.43 1763.37 356.40 o 3 47 0 508.78 526.63 126.53 o 4 47 0 1151.57 1397.71 181.74 o 5 47 0 17.55 67.40 80.16 o 0 48 0 482.02 623.18 180.83 o 1 48 0 472.76 613.65 104.18 o 2 48 0 573.87 711.30 137.70 o 3 48 0 324.34 433.26 121.20 o 4 48 0 128.92 154.92 95.16 o 5 48 0 525.49 736.72 150.92 o 1 49 0 5.95 28.28 58.51 o 2 49 0 137.76 92.63 80.80 o 3 49 0 2.41 21.59 68.39 o 4 49 0 231.55 185.89 95.94 o 5 49 0 68.39 92.50 88.54 o 0 50 0 87.88 146.86 78.96 o 1 50 0 1.02 105.19 75.08 o 2 50 0 272.77 234.13 96.83 o 3 50 0 8.39 47.48 75.67 o 4 50 0 2.61 22.59 70.57 o 5 50 0 68.92 64.78 83.92 o 1 51 0 229.45 313.23 103.07 o 2 51 0 336.81 465.86 165.07 o 3 51 0 188.12 207.91 99.21 o 4 51 0 635.66 671.09 152.29 o 0 52 0 81.00 56.92 115.15 o 1 52 0 558.03 534.70 126.43 o 2 52 0 581.87 884.44 212.35 o 3 52 0 714.79 879.34 157.35 o 4 52 0 128.44 223.87 105.31 o 1 53 0 1132.24 1194.20 166.71 o 2 53 0 692.87 940.48 221.55 o 3 53 0 440.05 511.13 135.22 o 4 53 0 499.08 370.97 122.68 o 0 54 0 1824.10 1581.49 279.78 o 1 54 0 12.82 84.81 85.11 o 2 54 0 127.68 172.95 129.60 o 3 54 0 412.10 384.94 121.03 o 1 55 0 13.73 37.64 75.91 o 2 55 0 5.71 50.79 95.45 o 3 55 0 8.11 9.77 79.56 o 1 56 0 68.51 98.49 88.43 o 2 56 0 2.81 58.23 109.46 o 1 57 0 107.55 96.46 90.58 o -9 1 1 35.54 43.28 82.00 o -8 1 1 49.93 60.44 73.00 o -7 1 1 1660.99 1607.86 78.57 o -6 1 1 691.34 702.51 37.80 o -5 1 1 15.56 -2.37 12.14 o -4 1 1 535.33 515.90 21.61 o -3 1 1 3522.15 3614.46 40.87 o -2 1 1 17097.80 16980.15 184.64 o -1 1 1 15644.17 15138.03 163.49 o 0 1 1 9837.42 9406.47 98.84 o 1 1 1 4666.59 4675.17 73.27 o 2 1 1 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