#------------------------------------------------------------------------------ #$Date: 2010-11-03 10:57:48 +0200 (Wed, 03 Nov 2010) $ #$Revision: 1704 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2226969.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2226969_Fobs loop_ _publ_author_name 'Ng, Seik Weng' _publ_section_title ; (Quinoline-2-carboxylato-\kO)(quinoline-2-carboxylic acid-\kO)bis(quinoline-2-carboxylic acid-\k^2^N,O)potassium ; _journal_coeditor_code JH2182 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m948 _journal_volume 66 _journal_year 2010 _space_group_IT_number 73 _symmetry_space_group_name_Hall '-I 2b 2c' _symmetry_space_group_name_H-M 'I b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.8679 _cell_length_b 18.3617 _cell_length_c 20.5162 _exptl_crystal_F_000 3024.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file jh2182Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ibca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 513.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-x+1/2, y+1, -z+1' 'x+1, -y+1, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'x+1/2, -y, z' '-x, y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3881.44 3940.12 115.73 o 4 0 0 1074.47 966.16 58.96 o 6 0 0 9056.07 8146.82 255.70 o 8 0 0 255.66 284.69 61.39 o 10 0 0 1732.08 1634.73 125.12 o 12 0 0 52454.17 54634.78 1273.52 o 14 0 0 4112.98 4510.94 166.10 o 16 0 0 2703.69 2715.40 144.71 o 18 0 0 3096.77 3188.71 239.76 o 20 0 0 1485.84 1229.99 164.77 o 22 0 0 1807.30 1837.46 448.86 o 0 2 0 22577.04 22806.75 518.21 o 2 2 0 81029.83 81600.08 1390.89 o 4 2 0 134808.19 139302.23 2225.28 o 6 2 0 13212.10 12978.97 225.14 o 8 2 0 879.77 880.47 40.67 o 10 2 0 2322.82 2540.17 79.74 o 12 2 0 151.45 328.58 51.64 o 14 2 0 28.05 -20.56 40.37 o 16 2 0 672.60 813.78 70.78 o 18 2 0 8396.59 8290.32 278.34 o 20 2 0 4296.47 4409.37 287.67 o 22 2 0 1849.30 1627.52 288.21 o 0 4 0 32736.88 31956.96 727.57 o 2 4 0 263473.38 244777.45 4340.00 o 4 4 0 155324.53 161002.27 2744.87 o 6 4 0 14793.18 15319.32 261.97 o 8 4 0 0.57 53.04 24.64 o 10 4 0 19124.91 21205.06 395.30 o 12 4 0 11577.67 11712.76 223.19 o 14 4 0 25488.82 25763.42 516.93 o 16 4 0 325.20 312.46 101.35 o 18 4 0 11218.47 11223.58 363.84 o 20 4 0 342.37 436.73 89.13 o 22 4 0 767.97 821.90 248.92 o 0 6 0 260442.16 251653.11 5650.38 o 2 6 0 43494.35 42091.13 750.95 o 4 6 0 6123.21 5569.32 108.60 o 6 6 0 12289.28 12274.58 217.23 o 8 6 0 13941.63 15471.51 293.57 o 10 6 0 1793.42 1788.66 72.58 o 12 6 0 603.69 684.71 56.76 o 14 6 0 667.16 617.09 61.08 o 16 6 0 1889.44 1685.22 95.85 o 18 6 0 163.99 129.39 79.08 o 20 6 0 3211.17 3330.84 179.92 o 22 6 0 331.73 119.46 95.90 o 0 8 0 3381.58 2497.44 121.96 o 2 8 0 2624.03 2133.90 67.37 o 4 8 0 1188.96 1775.58 61.78 o 6 8 0 4108.19 4199.93 93.69 o 8 8 0 5310.64 5476.83 132.54 o 10 8 0 15375.48 16245.13 316.89 o 12 8 0 951.07 1002.64 71.34 o 14 8 0 68.21 91.22 47.65 o 16 8 0 2425.33 2120.06 133.99 o 18 8 0 470.13 585.33 99.43 o 20 8 0 2296.11 2454.06 245.45 o 0 10 0 3531.87 3404.95 117.87 o 2 10 0 33437.62 33769.55 618.13 o 4 10 0 290.99 374.17 37.67 o 6 10 0 1466.09 1407.87 62.59 o 8 10 0 10.34 59.14 30.37 o 10 10 0 1542.05 1600.97 75.43 o 12 10 0 17935.52 18284.09 411.91 o 14 10 0 15718.70 16027.27 440.66 o 16 10 0 4782.92 4858.99 249.16 o 18 10 0 762.59 618.74 185.12 o 20 10 0 220.93 47.00 92.34 o 0 12 0 49983.83 52435.70 1343.51 o 2 12 0 3869.62 4550.43 124.42 o 4 12 0 3342.82 3220.27 99.45 o 6 12 0 199.87 270.66 52.85 o 8 12 0 3621.28 3636.17 132.75 o 10 12 0 7516.71 7402.33 212.07 o 12 12 0 37538.76 37491.51 834.00 o 14 12 0 2638.93 2662.49 224.66 o 16 12 0 584.59 543.52 96.03 o 18 12 0 475.20 357.91 143.65 o 20 12 0 1564.75 1763.53 155.67 o 0 14 0 12615.68 13210.35 451.66 o 2 14 0 1882.00 1949.65 106.65 o 4 14 0 1628.64 1566.67 74.94 o 6 14 0 531.42 609.43 67.54 o 8 14 0 1135.83 1088.90 84.02 o 10 14 0 14.10 -74.72 56.63 o 12 14 0 165.03 137.33 66.83 o 14 14 0 4164.13 4075.85 294.51 o 16 14 0 517.96 622.62 100.15 o 18 14 0 1303.28 1432.89 370.78 o 0 16 0 183.52 -1.39 105.81 o 2 16 0 14792.27 14409.46 377.77 o 4 16 0 7211.43 6938.72 209.29 o 6 16 0 5248.97 5409.09 219.65 o 8 16 0 5691.84 5803.86 187.18 o 10 16 0 5821.19 6165.12 200.20 o 12 16 0 4116.56 4394.09 174.38 o 14 16 0 11481.37 11056.20 511.53 o 16 16 0 566.59 283.98 142.85 o 0 18 0 4312.37 3966.54 305.95 o 2 18 0 1116.92 1495.77 134.26 o 4 18 0 1426.76 1347.51 141.30 o 6 18 0 133.06 19.99 90.53 o 8 18 0 2408.35 2531.12 191.95 o 10 18 0 2.88 10.71 97.47 o 12 18 0 3686.39 3971.49 466.57 o 14 18 0 1946.14 1970.38 330.01 o 0 20 0 1945.02 1899.31 216.84 o 2 20 0 2945.07 2824.46 173.92 o 4 20 0 6318.19 6519.60 257.37 o 6 20 0 2823.33 2609.33 192.89 o 8 20 0 3880.23 3679.52 225.97 o 10 20 0 199.41 75.66 128.39 o 12 20 0 155.43 33.32 127.46 o 0 22 0 2.44 -203.37 230.59 o 2 22 0 2099.55 2484.61 183.60 o 4 22 0 1976.59 2311.85 278.93 o 6 22 0 1.87 101.03 113.39 o 8 22 0 147.78 222.81 123.67 o 2 1 1 42.15 -12.73 8.49 o 4 1 1 6847.32 6218.07 81.31 o 6 1 1 1197.14 752.22 27.19 o 8 1 1 13693.01 12494.15 157.37 o 10 1 1 28248.52 26287.06 314.03 o 12 1 1 77.28 87.29 29.97 o 14 1 1 0.75 2.72 23.89 o 16 1 1 100.99 65.52 25.70 o 18 1 1 730.05 823.62 110.09 o 20 1 1 49.77 -71.84 93.91 o 22 1 1 4540.29 4622.71 377.35 o 1 2 1 4665.56 4216.08 57.34 o 3 2 1 105.44 163.59 14.19 o 5 2 1 7364.69 7922.61 103.75 o 7 2 1 3.58 78.50 35.09 o 9 2 1 2936.47 2911.98 55.80 o 11 2 1 3620.31 3791.49 69.08 o 13 2 1 3393.57 3488.61 70.46 o 15 2 1 1257.14 1425.09 54.32 o 17 2 1 56.87 72.27 32.41 o 19 2 1 177.64 146.68 59.89 o 21 2 1 250.46 209.70 91.67 o 23 2 1 223.71 75.15 68.85 o 2 3 1 82783.74 81500.02 977.19 o 4 3 1 18744.91 16271.75 199.37 o 6 3 1 3081.83 2453.87 45.01 o 8 3 1 13995.60 12135.93 153.71 o 10 3 1 20490.70 20037.70 244.97 o 12 3 1 14157.94 14647.63 190.05 o 14 3 1 1437.15 1522.99 53.50 o 16 3 1 597.79 639.81 57.27 o 18 3 1 981.86 1011.29 83.82 o 20 3 1 246.09 296.72 57.11 o 22 3 1 1556.55 1239.45 128.53 o 1 4 1 9987.34 9372.77 119.50 o 3 4 1 130649.22 131770.41 1480.94 o 5 4 1 120864.46 126580.78 1478.40 o 7 4 1 20212.01 21487.04 265.72 o 9 4 1 14513.84 15458.21 195.86 o 11 4 1 7.20 -15.15 19.75 o 13 4 1 117.31 151.83 29.52 o 15 4 1 385.43 395.90 41.40 o 17 4 1 561.50 633.99 66.23 o 19 4 1 568.47 576.25 57.03 o 21 4 1 425.01 374.43 82.16 o 2 5 1 64929.77 63995.02 878.89 o 4 5 1 15864.96 13238.33 172.00 o 6 5 1 15005.19 14113.50 179.11 o 8 5 1 5761.02 5184.74 83.17 o 10 5 1 20923.56 20792.56 277.73 o 12 5 1 1293.25 1184.46 44.38 o 14 5 1 81.92 111.81 33.96 o 16 5 1 2398.40 2411.33 77.75 o 18 5 1 252.77 196.42 45.79 o 20 5 1 224.39 163.75 47.51 o 22 5 1 4355.25 4828.41 175.35 o 1 6 1 974.08 1220.28 29.60 o 3 6 1 27799.62 27889.24 357.20 o 5 6 1 1021.02 1010.63 32.56 o 7 6 1 2740.27 2896.87 56.46 o 9 6 1 3484.72 3791.01 70.78 o 11 6 1 2990.14 3305.48 70.51 o 13 6 1 564.79 606.66 40.92 o 15 6 1 1467.88 1618.20 81.39 o 17 6 1 110.15 45.30 38.30 o 19 6 1 15.39 -45.27 40.55 o 21 6 1 385.72 353.60 58.68 o 2 7 1 1153.29 1195.56 34.89 o 4 7 1 15950.05 15694.00 211.22 o 6 7 1 27414.10 26296.57 320.75 o 8 7 1 21.63 81.70 23.50 o 10 7 1 122.14 49.16 23.25 o 12 7 1 1111.16 1053.78 47.66 o 14 7 1 6666.29 6768.94 126.83 o 16 7 1 134.86 69.63 54.22 o 18 7 1 3821.63 3628.70 123.47 o 20 7 1 944.47 978.61 89.18 o 22 7 1 1014.12 1027.94 128.54 o 1 8 1 2779.75 3142.87 54.92 o 3 8 1 13783.38 14859.56 201.77 o 5 8 1 24472.27 26329.15 344.74 o 7 8 1 79392.88 84919.67 1003.36 o 9 8 1 13331.92 13899.16 185.68 o 11 8 1 1759.95 1818.35 56.33 o 13 8 1 373.52 361.72 40.47 o 15 8 1 36.97 -34.51 33.56 o 17 8 1 668.72 766.22 72.95 o 19 8 1 345.23 250.29 65.21 o 21 8 1 1273.19 1218.11 111.08 o 2 9 1 15580.11 17984.91 248.42 o 4 9 1 487.81 337.81 25.86 o 6 9 1 16137.94 15362.15 189.78 o 8 9 1 10390.04 9648.97 136.19 o 10 9 1 3.18 61.72 25.94 o 12 9 1 7058.67 6983.91 122.30 o 14 9 1 5970.74 5949.76 122.01 o 16 9 1 43.55 4.27 90.66 o 18 9 1 1487.62 1403.90 89.28 o 20 9 1 0.58 -29.62 57.48 o 1 10 1 1789.22 1998.68 43.29 o 3 10 1 8864.17 9664.73 142.78 o 5 10 1 2042.60 2642.22 63.08 o 7 10 1 8787.40 9239.71 133.17 o 9 10 1 4015.67 4366.93 85.35 o 11 10 1 2577.87 2861.21 114.43 o 13 10 1 920.65 1088.57 132.04 o 15 10 1 1054.56 1062.15 81.70 o 17 10 1 37.27 -49.61 48.98 o 19 10 1 6.02 68.31 57.54 o 21 10 1 32.57 -50.06 86.66 o 2 11 1 1443.50 1648.47 46.09 o 4 11 1 3210.98 3537.71 73.31 o 6 11 1 4653.26 4247.52 84.28 o 8 11 1 5710.17 5335.51 116.21 o 10 11 1 3503.80 3476.30 94.71 o 12 11 1 1091.89 1056.73 76.38 o 14 11 1 1695.93 1911.86 108.81 o 16 11 1 3284.22 3180.36 169.17 o 18 11 1 29.35 43.22 56.30 o 20 11 1 1503.84 1942.87 176.91 o 1 12 1 3480.20 4075.80 81.62 o 3 12 1 3905.32 4374.64 84.88 o 5 12 1 567.92 683.79 35.64 o 7 12 1 93.49 118.67 34.38 o 9 12 1 921.47 991.11 56.30 o 11 12 1 30142.30 29834.80 461.90 o 13 12 1 193.38 330.90 53.44 o 15 12 1 2390.78 2360.27 139.44 o 17 12 1 243.64 228.35 98.54 o 19 12 1 7.45 5.26 57.89 o 2 13 1 6476.59 6570.32 114.55 o 4 13 1 957.05 936.52 40.83 o 6 13 1 6090.47 5549.02 167.87 o 8 13 1 6.58 -19.63 40.48 o 10 13 1 229.32 231.02 57.47 o 12 13 1 4170.58 4303.99 114.48 o 14 13 1 5518.65 5650.58 148.85 o 16 13 1 2110.98 2168.72 196.24 o 18 13 1 52.21 -34.10 80.33 o 1 14 1 162.07 294.62 41.18 o 3 14 1 4618.54 4829.93 96.85 o 5 14 1 128.19 127.16 29.17 o 7 14 1 6446.21 5763.65 325.41 o 9 14 1 2770.17 2897.95 88.37 o 11 14 1 2013.39 2179.33 98.46 o 13 14 1 403.76 344.51 78.57 o 15 14 1 5287.25 4927.87 159.00 o 17 14 1 0.04 -57.73 55.48 o 2 15 1 8011.36 7932.87 158.19 o 4 15 1 592.89 440.67 48.99 o 6 15 1 3231.64 3257.50 89.41 o 8 15 1 11924.35 11650.20 223.06 o 10 15 1 847.73 800.12 60.10 o 12 15 1 243.25 221.80 69.63 o 14 15 1 0.48 -70.28 48.56 o 16 15 1 108.94 43.00 78.70 o 18 15 1 1.80 19.87 90.53 o 1 16 1 2201.73 2049.44 81.37 o 3 16 1 1129.42 1459.33 69.14 o 5 16 1 1072.39 865.95 79.62 o 7 16 1 223.66 198.38 50.14 o 9 16 1 364.08 341.56 47.53 o 11 16 1 152.46 113.81 59.41 o 13 16 1 6232.43 5724.02 152.60 o 15 16 1 1575.08 1062.40 164.94 o 17 16 1 787.95 605.28 130.20 o 2 17 1 4677.30 4707.39 126.08 o 4 17 1 273.50 384.33 68.78 o 6 17 1 13.10 46.69 63.92 o 8 17 1 3355.29 3531.41 130.61 o 10 17 1 985.58 984.18 95.03 o 12 17 1 3143.16 3422.85 169.75 o 14 17 1 1231.65 1055.01 81.55 o 16 17 1 344.75 348.44 89.54 o 1 18 1 545.24 455.27 55.50 o 3 18 1 1121.55 1025.31 85.81 o 5 18 1 317.97 289.02 70.65 o 7 18 1 90.41 32.29 65.73 o 9 18 1 98.02 18.29 68.02 o 11 18 1 15.01 -10.99 69.71 o 13 18 1 276.85 224.83 98.84 o 15 18 1 142.91 111.82 153.20 o 2 19 1 404.72 483.85 73.37 o 4 19 1 291.19 211.19 74.58 o 6 19 1 9024.92 8867.22 237.72 o 8 19 1 76.43 46.06 69.78 o 10 19 1 111.92 163.10 81.38 o 12 19 1 50.51 102.41 84.17 o 14 19 1 252.31 224.56 118.32 o 1 20 1 133.27 75.20 56.14 o 3 20 1 819.29 702.96 85.57 o 5 20 1 292.59 326.75 94.37 o 7 20 1 1575.81 1567.59 111.28 o 9 20 1 9.62 -8.39 75.84 o 11 20 1 467.48 518.99 101.55 o 2 21 1 87.40 -42.18 66.88 o 4 21 1 1646.23 1848.65 112.38 o 6 21 1 4872.88 5296.03 223.43 o 8 21 1 2.40 -0.30 77.14 o 10 21 1 467.12 376.37 103.59 o 1 22 1 158.78 121.98 88.24 o 3 22 1 47.43 -15.57 72.19 o 5 22 1 391.91 380.33 83.27 o 7 22 1 1.31 67.16 79.63 o 2 23 1 775.88 1032.84 118.82 o 4 23 1 1262.16 1265.24 109.31 o 6 23 1 465.18 415.94 91.69 o 0 0 2 61538.55 60876.73 1957.02 o 2 0 2 152344.03 153006.34 3659.84 o 4 0 2 78052.40 83900.84 1646.05 o 6 0 2 49.78 34.87 21.97 o 8 0 2 183.41 263.66 28.58 o 10 0 2 14424.88 15912.48 281.69 o 12 0 2 2100.24 2899.51 94.15 o 14 0 2 1146.49 1170.31 70.32 o 16 0 2 31.46 -0.45 49.04 o 18 0 2 7266.51 6923.37 239.85 o 20 0 2 1186.54 1074.11 283.03 o 22 0 2 702.82 641.15 107.96 o 1 1 2 28.30 5.05 9.28 o 3 1 2 904.70 1163.49 52.08 o 5 1 2 18699.87 19755.01 247.51 o 7 1 2 668.32 594.77 24.69 o 9 1 2 5471.66 5534.83 87.56 o 11 1 2 1185.21 1178.61 45.23 o 13 1 2 1503.04 1551.00 47.41 o 15 1 2 1674.58 1658.49 55.41 o 17 1 2 1113.10 1193.83 63.23 o 19 1 2 83.81 46.70 49.45 o 21 1 2 1648.79 1592.90 122.78 o 23 1 2 624.38 524.40 116.24 o 0 2 2 17945.90 18411.12 418.96 o 2 2 2 11248.29 10339.90 129.58 o 4 2 2 111296.66 108401.25 1257.49 o 6 2 2 15165.82 14547.86 185.91 o 8 2 2 17454.16 18553.86 235.38 o 10 2 2 2237.93 2245.33 50.50 o 12 2 2 134.83 321.73 28.12 o 14 2 2 2294.84 2323.00 60.76 o 16 2 2 3410.90 3531.21 95.86 o 18 2 2 7138.79 7007.60 158.86 o 20 2 2 2309.15 2113.10 128.74 o 22 2 2 191.78 117.23 67.64 o 1 3 2 10085.42 10118.01 133.54 o 3 3 2 449.56 413.60 18.31 o 5 3 2 17997.42 18264.26 224.36 o 7 3 2 201.34 164.81 17.36 o 9 3 2 3523.61 3960.59 78.34 o 11 3 2 19.45 -29.06 19.38 o 13 3 2 3945.54 3981.29 83.29 o 15 3 2 256.18 267.12 39.23 o 17 3 2 690.01 636.44 50.71 o 19 3 2 41.76 -32.52 43.83 o 21 3 2 1254.78 1143.33 158.54 o 0 4 2 32380.71 31559.63 511.21 o 2 4 2 5640.70 6674.28 88.62 o 4 4 2 55966.28 54959.77 647.16 o 6 4 2 3831.29 3745.58 63.26 o 8 4 2 6977.87 7714.25 113.36 o 10 4 2 7.46 9.82 19.71 o 12 4 2 6496.01 6130.18 97.16 o 14 4 2 217.15 212.62 35.39 o 16 4 2 1041.26 1004.80 55.41 o 18 4 2 2452.82 2424.50 137.68 o 20 4 2 411.37 351.73 62.61 o 22 4 2 2588.29 2391.86 176.22 o 1 5 2 8744.08 9231.80 119.24 o 3 5 2 322.42 468.29 19.37 o 5 5 2 6165.94 6391.54 90.72 o 7 5 2 0.90 -0.49 17.95 o 9 5 2 11069.80 12350.38 169.39 o 11 5 2 340.21 363.32 33.73 o 13 5 2 121.68 92.66 35.27 o 15 5 2 117.58 82.61 43.82 o 17 5 2 2572.71 2602.04 92.42 o 19 5 2 2618.08 2706.72 156.11 o 21 5 2 11.39 -69.57 51.11 o 0 6 2 29394.75 26849.46 437.96 o 2 6 2 3573.70 2875.32 54.39 o 4 6 2 32601.28 32980.60 393.88 o 6 6 2 183.63 215.84 20.07 o 8 6 2 19540.88 21300.04 267.02 o 10 6 2 2367.34 2775.59 61.14 o 12 6 2 9.81 28.67 27.91 o 14 6 2 3270.22 3252.61 82.07 o 16 6 2 3650.72 3784.08 95.68 o 18 6 2 2298.10 2512.31 87.99 o 20 6 2 2987.08 3167.33 102.70 o 22 6 2 316.55 283.88 74.52 o 1 7 2 1666.92 1881.84 38.56 o 3 7 2 6642.54 5948.60 94.36 o 5 7 2 6845.44 7633.76 106.57 o 7 7 2 1023.37 1041.64 33.71 o 9 7 2 661.97 713.19 32.33 o 11 7 2 50.23 93.01 29.71 o 13 7 2 1396.76 1513.47 58.87 o 15 7 2 1195.46 1336.75 62.73 o 17 7 2 441.87 468.21 63.10 o 19 7 2 74.30 -11.21 55.70 o 21 7 2 3.56 -95.30 63.53 o 0 8 2 18736.00 17479.00 294.96 o 2 8 2 649.64 614.84 23.53 o 4 8 2 18920.21 18836.49 251.06 o 6 8 2 14715.99 14354.68 185.67 o 8 8 2 25365.94 26543.46 342.52 o 10 8 2 3108.36 3115.38 69.76 o 12 8 2 47.44 55.86 30.73 o 14 8 2 52.45 76.08 35.36 o 16 8 2 1673.23 1896.23 81.21 o 18 8 2 6387.55 6467.66 166.15 o 20 8 2 38.12 65.00 69.66 o 1 9 2 2446.40 2482.25 48.49 o 3 9 2 6978.75 6580.12 99.33 o 5 9 2 16984.98 18233.92 233.22 o 7 9 2 13413.14 13614.49 179.73 o 9 9 2 104.07 136.50 22.82 o 11 9 2 2124.99 2208.09 61.52 o 13 9 2 815.66 916.91 51.11 o 15 9 2 704.44 838.64 92.77 o 17 9 2 1009.45 778.74 72.77 o 19 9 2 3.97 -18.58 53.60 o 21 9 2 871.37 831.01 89.65 o 0 10 2 5802.16 6999.53 134.92 o 2 10 2 7508.99 7206.05 107.45 o 4 10 2 9263.63 9324.32 138.61 o 6 10 2 2664.49 2503.51 52.76 o 8 10 2 22.58 65.83 20.40 o 10 10 2 616.03 561.15 41.27 o 12 10 2 59.79 77.45 41.71 o 14 10 2 7276.25 7711.53 170.94 o 16 10 2 2905.90 3149.33 242.48 o 18 10 2 753.40 720.66 75.94 o 20 10 2 55.50 35.19 65.24 o 1 11 2 106.10 40.67 20.08 o 3 11 2 1388.81 1528.49 47.11 o 5 11 2 1535.52 1650.73 53.24 o 7 11 2 7054.96 6782.20 123.67 o 9 11 2 297.48 315.06 42.03 o 11 11 2 2457.19 2415.22 82.04 o 13 11 2 1522.83 1368.29 82.07 o 15 11 2 2610.17 2679.43 110.60 o 17 11 2 355.61 286.35 63.99 o 19 11 2 1069.37 1141.54 100.73 o 0 12 2 81.34 248.16 33.79 o 2 12 2 17201.02 17559.19 249.31 o 4 12 2 897.52 739.83 37.02 o 6 12 2 1871.89 1961.46 66.77 o 8 12 2 4990.64 4999.07 115.05 o 10 12 2 14514.19 14905.93 246.49 o 12 12 2 3424.78 3220.01 115.09 o 14 12 2 107.87 134.70 51.18 o 16 12 2 64.50 61.61 54.99 o 18 12 2 3306.26 3838.60 168.43 o 1 13 2 17.35 25.34 21.24 o 3 13 2 2465.40 2410.59 62.37 o 5 13 2 590.21 769.56 39.59 o 7 13 2 911.43 849.41 50.17 o 9 13 2 154.23 209.61 42.70 o 11 13 2 404.02 447.62 59.88 o 13 13 2 1116.34 1016.55 85.27 o 15 13 2 193.83 153.81 71.14 o 17 13 2 129.80 39.67 87.39 o 19 13 2 19.77 77.24 64.57 o 0 14 2 625.91 766.51 72.99 o 2 14 2 2883.53 2729.06 73.14 o 4 14 2 3815.94 3707.11 82.51 o 6 14 2 179.24 220.00 38.85 o 8 14 2 43.50 49.05 36.44 o 10 14 2 1127.91 1124.24 65.35 o 12 14 2 10.88 -12.23 43.75 o 14 14 2 1251.06 1095.71 130.96 o 16 14 2 7076.42 7325.07 192.08 o 18 14 2 979.72 1144.45 126.19 o 1 15 2 318.39 305.95 46.85 o 3 15 2 612.30 640.62 52.00 o 5 15 2 76.46 3.52 36.60 o 7 15 2 2494.32 2408.92 88.74 o 9 15 2 569.55 613.66 54.41 o 11 15 2 4477.97 4524.98 121.26 o 13 15 2 716.08 628.85 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