#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/70/2227044.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2227044_Fobs loop_ _publ_author_name 'Han, Meng Ting' 'Zhang, Yuan' _publ_section_title ; Cyanomethanaminium tetrafluoroborate ; _journal_coeditor_code PV2302 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1941 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7900 _cell_length_b 10.2040 _cell_length_c 11.0574 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file pv2302Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4819.50 4678.34 77.06 o 4 0 0 410.29 393.35 8.17 o 6 0 0 2563.49 2608.86 82.87 o 8 0 0 136.54 137.53 9.97 o 10 0 0 129.19 126.72 8.35 o 2 1 0 1002.47 770.94 11.86 o 4 1 0 118.17 114.36 1.73 o 6 1 0 469.89 435.12 12.98 o 8 1 0 1.12 1.71 1.06 o 10 1 0 1.77 0.37 1.03 o 2 2 0 16052.53 15942.70 495.76 o 4 2 0 830.44 910.18 18.94 o 6 2 0 532.83 501.53 13.33 o 8 2 0 160.24 161.60 5.10 o 10 2 0 237.04 248.21 11.44 o 2 3 0 19.32 23.89 0.63 o 4 3 0 11.84 17.26 0.65 o 6 3 0 484.72 484.05 11.92 o 8 3 0 54.54 54.90 2.34 o 10 3 0 6.49 6.53 1.47 o 0 4 0 35669.47 30349.89 1738.56 o 2 4 0 731.33 695.23 30.03 o 4 4 0 72.44 62.83 1.65 o 6 4 0 64.79 52.48 1.61 o 8 4 0 26.51 23.29 1.78 o 10 4 0 272.19 273.35 12.69 o 2 5 0 1116.90 1135.78 29.29 o 4 5 0 1486.65 1598.66 109.38 o 6 5 0 1.51 2.62 0.59 o 8 5 0 16.08 20.11 1.48 o 10 5 0 11.14 9.61 1.45 o 0 6 0 7446.96 7327.34 334.56 o 2 6 0 2644.70 2708.81 84.92 o 4 6 0 100.57 81.94 3.26 o 6 6 0 28.60 20.14 1.08 o 8 6 0 5.41 8.50 1.09 o 10 6 0 40.41 45.42 3.96 o 2 7 0 466.18 441.48 12.26 o 4 7 0 82.66 70.12 2.15 o 6 7 0 99.43 84.66 3.10 o 8 7 0 25.54 31.88 2.94 o 0 8 0 5.80 3.33 1.17 o 2 8 0 138.48 128.23 5.98 o 4 8 0 364.01 353.36 9.95 o 6 8 0 499.78 461.97 16.48 o 8 8 0 158.19 183.87 8.57 o 2 9 0 360.14 366.88 10.75 o 4 9 0 669.74 624.14 19.57 o 6 9 0 65.98 63.97 3.22 o 0 10 0 866.78 853.86 40.22 o 2 10 0 100.81 92.79 3.25 o 4 10 0 35.93 28.82 2.25 o 6 10 0 11.02 11.75 1.65 o 2 11 0 59.52 61.55 3.16 o 4 11 0 0.16 0.35 0.86 o 0 12 0 0.11 0.00 2.83 o 1 1 1 309.09 275.86 2.67 o 2 1 1 0.51 3.57 0.26 o 3 1 1 455.82 481.31 6.07 o 4 1 1 3095.52 3177.27 58.22 o 5 1 1 3970.43 4055.01 79.42 o 6 1 1 895.44 875.16 14.68 o 7 1 1 36.97 42.63 1.10 o 8 1 1 6.64 7.29 0.68 o 9 1 1 389.81 391.02 11.59 o 10 1 1 1.13 1.28 0.77 o 11 1 1 7.78 8.51 1.12 o 0 2 1 1835.86 1825.54 51.47 o 1 2 1 1450.53 1579.88 14.67 o 2 2 1 3902.02 3853.37 54.85 o 3 2 1 1530.35 1475.46 23.36 o 4 2 1 33.29 28.36 0.49 o 5 2 1 944.03 980.60 17.50 o 6 2 1 307.59 316.90 5.75 o 7 2 1 61.67 68.84 1.43 o 8 2 1 130.94 147.42 3.75 o 9 2 1 37.22 38.71 1.75 o 10 2 1 0.79 1.20 0.77 o 11 2 1 46.89 49.03 2.44 o 1 3 1 0.69 1.91 0.15 o 2 3 1 7.75 4.94 0.34 o 3 3 1 2628.32 2554.98 42.36 o 4 3 1 1119.14 1101.02 16.44 o 5 3 1 1855.47 1734.29 35.76 o 6 3 1 1803.10 1820.28 40.73 o 7 3 1 3.97 4.68 0.65 o 8 3 1 0.61 1.18 0.58 o 9 3 1 5.63 4.45 0.68 o 10 3 1 59.46 59.04 2.58 o 11 3 1 4.34 3.62 0.96 o 0 4 1 513.04 564.26 9.88 o 1 4 1 5.07 5.86 0.40 o 2 4 1 686.91 719.87 9.63 o 3 4 1 1404.52 1497.64 23.91 o 4 4 1 99.53 96.68 2.67 o 5 4 1 650.36 622.29 10.17 o 6 4 1 38.46 37.77 1.11 o 7 4 1 87.23 94.76 2.12 o 8 4 1 103.46 90.78 2.35 o 9 4 1 8.04 6.28 0.95 o 10 4 1 0.03 0.17 0.71 o 1 5 1 150.88 148.49 2.23 o 2 5 1 11.46 10.69 0.83 o 3 5 1 12.77 11.36 0.53 o 4 5 1 1110.40 1067.75 18.91 o 5 5 1 1642.30 1610.01 34.87 o 6 5 1 87.82 92.31 1.90 o 7 5 1 111.39 103.97 2.42 o 8 5 1 1.63 1.23 0.56 o 9 5 1 339.30 339.80 9.74 o 10 5 1 34.71 35.14 2.00 o 0 6 1 1695.20 1644.82 42.67 o 1 6 1 863.36 893.55 16.95 o 2 6 1 1975.74 2156.43 56.91 o 3 6 1 460.51 454.73 7.61 o 4 6 1 0.03 0.39 0.33 o 5 6 1 552.68 538.22 10.56 o 6 6 1 321.67 337.47 6.72 o 7 6 1 44.17 55.64 1.78 o 8 6 1 87.21 95.63 2.78 o 9 6 1 25.04 31.77 1.45 o 10 6 1 3.78 4.51 0.97 o 1 7 1 4.81 5.45 0.42 o 2 7 1 4.05 4.64 0.41 o 3 7 1 341.55 351.87 6.34 o 4 7 1 230.90 222.79 4.28 o 5 7 1 425.00 404.47 8.42 o 6 7 1 305.12 299.90 6.63 o 7 7 1 4.99 5.87 0.79 o 8 7 1 13.53 16.14 1.19 o 9 7 1 2.44 2.46 0.82 o 0 8 1 514.74 554.26 17.88 o 1 8 1 88.06 114.96 3.25 o 2 8 1 0.95 1.91 0.53 o 3 8 1 83.29 74.35 1.70 o 4 8 1 56.42 54.59 1.39 o 5 8 1 6.19 8.80 0.69 o 6 8 1 7.24 8.27 0.70 o 7 8 1 35.04 40.06 1.75 o 8 8 1 0.49 1.06 0.71 o 1 9 1 2.35 3.33 0.51 o 2 9 1 2.80 4.05 0.54 o 3 9 1 68.62 66.05 1.82 o 4 9 1 26.40 27.25 1.14 o 5 9 1 152.84 148.46 4.10 o 6 9 1 123.41 110.81 3.21 o 7 9 1 23.16 25.20 1.60 o 0 10 1 12.68 15.28 1.13 o 1 10 1 7.74 6.91 0.64 o 2 10 1 4.94 6.11 0.71 o 3 10 1 89.20 87.06 3.83 o 4 10 1 56.15 59.01 2.03 o 5 10 1 70.88 58.31 2.12 o 6 10 1 10.90 11.20 1.09 o 1 11 1 0.15 0.89 0.56 o 2 11 1 1.96 3.05 0.62 o 3 11 1 0.21 0.60 0.62 o 4 11 1 51.71 54.21 2.61 o 0 12 1 100.42 113.46 10.65 o 1 12 1 20.95 24.23 1.75 o 0 0 2 21.48 24.76 0.43 o 1 0 2 7494.22 7123.14 156.89 o 2 0 2 3124.21 3097.62 57.32 o 3 0 2 15976.28 16427.30 532.49 o 4 0 2 1397.92 1461.72 28.86 o 5 0 2 162.47 136.19 4.03 o 6 0 2 26.84 28.69 1.15 o 7 0 2 1070.72 1111.28 34.64 o 8 0 2 27.09 28.99 1.63 o 9 0 2 88.89 100.41 4.79 o 10 0 2 3.28 6.20 1.46 o 11 0 2 0.63 2.99 1.93 o 1 1 2 976.19 783.23 8.82 o 2 1 2 241.27 228.93 2.93 o 3 1 2 625.96 619.05 7.24 o 4 1 2 196.85 212.10 3.09 o 5 1 2 40.07 52.09 1.05 o 6 1 2 18.27 17.10 0.59 o 7 1 2 5.07 3.08 0.45 o 8 1 2 34.54 33.53 1.17 o 9 1 2 61.91 60.49 2.33 o 10 1 2 29.27 31.70 1.72 o 11 1 2 41.82 44.45 2.35 o 0 2 2 2256.95 2259.54 26.57 o 1 2 2 8481.19 8805.72 122.66 o 2 2 2 2779.46 2814.30 44.46 o 3 2 2 12312.24 12421.11 238.32 o 4 2 2 35.47 32.23 0.85 o 5 2 2 8.99 11.47 0.91 o 6 2 2 253.04 279.35 7.13 o 7 2 2 158.38 158.21 3.58 o 8 2 2 5.07 5.27 0.64 o 9 2 2 138.16 141.04 3.84 o 10 2 2 2.32 3.45 0.93 o 11 2 2 48.74 52.72 2.62 o 1 3 2 635.31 612.60 8.29 o 2 3 2 675.41 661.12 12.16 o 3 3 2 136.01 140.72 2.43 o 4 3 2 0.07 0.98 0.28 o 5 3 2 39.40 43.33 0.85 o 6 3 2 52.63 50.18 1.23 o 7 3 2 58.62 60.78 1.69 o 8 3 2 0.66 0.40 0.48 o 9 3 2 2.49 4.35 0.69 o 10 3 2 36.80 32.20 1.82 o 11 3 2 5.41 9.54 1.20 o 0 4 2 35.97 44.84 0.92 o 1 4 2 1552.54 1628.43 51.98 o 2 4 2 407.83 406.81 5.15 o 3 4 2 93.08 91.24 1.77 o 4 4 2 895.48 936.06 15.27 o 5 4 2 208.10 221.18 5.63 o 6 4 2 3.80 4.22 0.47 o 7 4 2 99.45 96.10 2.38 o 8 4 2 10.27 9.26 0.75 o 9 4 2 0.12 0.86 0.62 o 10 4 2 3.84 7.28 1.00 o 1 5 2 530.46 532.31 9.08 o 2 5 2 1.61 1.17 0.24 o 3 5 2 66.56 69.40 2.65 o 4 5 2 244.37 233.20 3.74 o 5 5 2 4.21 4.63 0.39 o 6 5 2 2.20 1.48 0.44 o 7 5 2 5.55 4.22 0.53 o 8 5 2 77.93 69.95 2.10 o 9 5 2 46.41 50.54 2.04 o 10 5 2 0.38 0.24 0.77 o 0 6 2 723.45 808.14 26.54 o 1 6 2 1269.58 1351.26 24.62 o 2 6 2 28.65 31.60 0.70 o 3 6 2 6.39 7.92 0.41 o 4 6 2 11.09 8.52 0.62 o 5 6 2 20.57 22.84 0.74 o 6 6 2 41.26 39.68 1.14 o 7 6 2 70.24 70.49 2.83 o 8 6 2 21.65 21.93 1.61 o 9 6 2 28.09 37.72 1.81 o 1 7 2 1231.83 1260.60 25.99 o 2 7 2 140.84 140.35 2.42 o 3 7 2 1.20 1.20 0.41 o 4 7 2 3.98 4.56 0.53 o 5 7 2 275.91 254.18 5.56 o 6 7 2 195.20 186.44 4.38 o 7 7 2 86.35 83.10 2.47 o 8 7 2 8.97 7.69 0.91 o 9 7 2 26.05 36.05 3.05 o 0 8 2 26.69 25.18 2.61 o 1 8 2 55.30 63.72 1.63 o 2 8 2 11.82 10.37 0.64 o 3 8 2 1320.05 1240.93 28.81 o 4 8 2 93.41 88.53 2.25 o 5 8 2 439.54 437.91 10.20 o 6 8 2 21.19 21.63 1.07 o 7 8 2 43.92 45.71 2.01 o 8 8 2 66.18 68.19 2.75 o 1 9 2 161.22 163.69 5.49 o 2 9 2 21.35 19.61 0.85 o 3 9 2 0.31 0.42 0.49 o 4 9 2 73.16 70.90 2.03 o 5 9 2 0.64 0.57 0.53 o 6 9 2 1.27 2.60 0.70 o 7 9 2 25.99 19.24 1.33 o 0 10 2 71.23 68.55 3.20 o 1 10 2 35.24 33.53 1.26 o 2 10 2 6.69 10.97 0.80 o 3 10 2 34.27 32.54 1.27 o 4 10 2 7.65 9.49 0.79 o 5 10 2 0.31 2.14 0.67 o 6 10 2 5.48 6.24 1.00 o 1 11 2 130.97 137.64 4.73 o 2 11 2 13.09 13.10 1.19 o 3 11 2 0.51 0.00 0.63 o 4 11 2 4.30 5.91 1.06 o 1 1 3 269.42 283.10 2.90 o 2 1 3 1868.00 1912.65 36.71 o 3 1 3 1027.04 1046.81 14.63 o 4 1 3 41.58 37.37 0.68 o 5 1 3 0.04 1.37 0.57 o 6 1 3 76.20 69.97 1.48 o 7 1 3 2.92 5.60 0.53 o 8 1 3 494.53 478.12 12.12 o 9 1 3 24.05 23.22 1.23 o 10 1 3 87.62 75.12 2.89 o 11 1 3 13.20 14.08 1.31 o 0 2 3 5965.36 5989.17 149.57 o 1 2 3 831.46 819.47 8.28 o 2 2 3 574.96 560.83 7.37 o 3 2 3 18.40 14.88 0.37 o 4 2 3 59.29 57.49 1.16 o 5 2 3 449.33 485.14 8.34 o 6 2 3 576.89 562.10 11.18 o 7 2 3 2.50 2.75 0.45 o 8 2 3 351.71 349.20 8.12 o 9 2 3 6.92 6.23 0.73 o 10 2 3 7.22 6.29 0.96 o 11 2 3 10.40 11.28 1.28 o 1 3 3 1604.86 1604.98 20.78 o 2 3 3 4249.21 4301.50 79.14 o 3 3 3 111.62 105.06 1.77 o 4 3 3 7.73 9.63 0.49 o 5 3 3 13.37 13.86 0.49 o 6 3 3 337.07 330.50 6.64 o 7 3 3 86.05 83.90 1.97 o 8 3 3 529.79 510.99 11.27 o 9 3 3 43.26 45.74 1.79 o 10 3 3 61.06 56.92 2.47 o 0 4 3 4151.85 4410.76 88.98 o 1 4 3 0.68 0.77 0.23 o 2 4 3 691.86 716.67 10.87 o 3 4 3 24.95 27.04 0.72 o 4 4 3 185.82 192.99 2.87 o 5 4 3 201.00 214.07 4.05 o 6 4 3 16.81 14.95 0.70 o 7 4 3 63.11 57.06 1.48 o 8 4 3 61.07 56.46 1.65 o 9 4 3 6.10 12.19 0.99 o 10 4 3 13.65 15.33 1.51 o 1 5 3 19.70 14.19 0.54 o 2 5 3 172.54 135.45 2.27 o 3 5 3 441.54 437.21 7.57 o 4 5 3 1.05 2.78 0.55 o 5 5 3 2.66 3.91 0.45 o 6 5 3 220.86 220.86 7.04 o 7 5 3 87.95 76.46 2.74 o 8 5 3 43.53 47.50 1.62 o 9 5 3 59.95 60.87 2.68 o 10 5 3 24.57 19.49 1.71 o 0 6 3 2482.94 2660.17 69.40 o 1 6 3 546.51 531.52 7.74 o 2 6 3 9.63 7.86 0.79 o 3 6 3 67.14 56.37 1.97 o 4 6 3 37.53 30.70 1.26 o 5 6 3 323.59 309.42 6.43 o 6 6 3 375.25 380.99 9.45 o 7 6 3 0.90 0.37 0.59 o 8 6 3 437.23 478.86 14.05 o 9 6 3 2.79 2.34 0.85 o 1 7 3 101.08 108.12 2.78 o 2 7 3 321.68 326.47 10.32 o 3 7 3 62.14 61.57 1.47 o 4 7 3 1.06 1.78 0.48 o 5 7 3 7.90 9.75 0.67 o 6 7 3 187.67 187.94 7.05 o 7 7 3 20.47 18.08 1.12 o 8 7 3 112.73 113.36 3.67 o 9 7 3 29.12 31.21 1.79 o 0 8 3 212.07 189.09 4.77 o 1 8 3 44.07 43.31 1.26 o 2 8 3 5.92 5.68 0.53 o 3 8 3 0.00 0.00 0.47 o 4 8 3 111.61 123.47 4.32 o 5 8 3 0.02 0.41 0.49 o 6 8 3 55.21 52.92 1.94 o 7 8 3 9.49 7.69 0.91 o 8 8 3 0.40 0.41 0.70 o 1 9 3 43.83 46.42 1.60 o 2 9 3 43.32 46.92 1.75 o 3 9 3 3.86 5.21 0.66 o 4 9 3 23.34 24.12 1.09 o 5 9 3 4.12 5.74 0.79 o 6 9 3 0.20 1.17 0.74 o 7 9 3 3.82 5.38 0.98 o 0 10 3 25.90 26.59 2.12 o 1 10 3 0.97 1.86 0.72 o 2 10 3 369.42 361.29 10.11 o 3 10 3 0.82 0.65 0.63 o 4 10 3 38.67 41.90 1.94 o 5 10 3 17.71 18.43 1.49 o 6 10 3 18.98 16.49 1.57 o 1 11 3 5.67 6.93 0.97 o 2 11 3 1.60 1.70 0.83 o 3 11 3 42.95 42.54 2.13 o 4 11 3 1.77 2.06 0.84 o 0 0 4 5926.64 6433.89 303.27 o 1 0 4 1359.96 1420.38 44.48 o 2 0 4 624.48 679.51 23.71 o 3 0 4 348.17 415.69 8.21 o 4 0 4 922.50 1014.14 23.53 o 5 0 4 764.45 798.44 18.98 o 6 0 4 5722.37 5984.51 246.62 o 7 0 4 38.55 37.80 1.92 o 8 0 4 725.66 740.82 30.73 o 9 0 4 46.59 43.26 2.36 o 10 0 4 128.24 129.46 6.72 o 11 0 4 52.57 56.87 4.01 o 1 1 4 934.01 982.48 19.17 o 2 1 4 43.00 45.50 0.79 o 3 1 4 74.65 67.78 1.46 o 4 1 4 46.22 52.83 0.96 o 5 1 4 4.79 5.23 0.49 o 6 1 4 32.63 30.30 1.00 o 7 1 4 4.71 7.18 0.66 o 8 1 4 135.76 130.57 3.71 o 9 1 4 173.79 167.82 4.74 o 10 1 4 81.46 81.99 3.32 o 11 1 4 10.17 12.10 1.23 o 0 2 4 7637.42 9642.86 333.87 o 1 2 4 146.72 166.90 1.86 o 2 2 4 4299.88 4601.00 79.86 o 3 2 4 511.34 500.94 10.35 o 4 2 4 232.90 242.37 4.50 o 5 2 4 1162.97 1220.36 20.98 o 6 2 4 29.46 35.76 1.04 o 7 2 4 190.52 194.19 4.33 o 8 2 4 606.21 597.43 14.91 o 9 2 4 4.00 7.33 0.81 o 10 2 4 3.70 3.85 0.85 o 1 3 4 220.45 235.43 3.76 o 2 3 4 139.46 137.01 1.91 o 3 3 4 21.68 33.27 1.05 o 4 3 4 42.03 43.70 0.84 o 5 3 4 39.96 42.65 0.90 o 6 3 4 5.51 6.45 0.54 o 7 3 4 35.41 37.90 1.30 o 8 3 4 0.91 1.28 0.56 o 9 3 4 14.66 16.92 1.10 o 10 3 4 111.40 107.57 3.93 o 0 4 4 295.06 303.58 6.50 o 1 4 4 16.44 17.42 0.52 o 2 4 4 1239.54 1257.15 21.87 o 3 4 4 675.11 686.74 11.77 o 4 4 4 1305.08 1305.33 27.34 o 5 4 4 3.94 4.97 0.52 o 6 4 4 1287.49 1283.83 28.39 o 7 4 4 14.12 14.74 0.78 o 8 4 4 83.54 86.63 2.31 o 9 4 4 2.90 5.27 0.85 o 10 4 4 8.38 7.01 1.22 o 1 5 4 448.27 426.21 6.70 o 2 5 4 860.61 846.61 14.92 o 3 5 4 16.35 14.54 0.61 o 4 5 4 5.02 6.17 0.46 o 5 5 4 8.72 11.06 0.59 o 6 5 4 7.32 7.84 0.71 o 7 5 4 32.35 30.64 1.25 o 8 5 4 154.06 159.72 4.83 o 9 5 4 4.22 5.60 1.01 o 0 6 4 0.00 0.95 0.63 o 1 6 4 24.31 28.40 1.00 o 2 6 4 599.52 566.55 10.47 o 3 6 4 2.61 3.16 0.41 o 4 6 4 38.34 34.68 1.07 o 5 6 4 0.13 0.81 0.42 o 6 6 4 40.60 39.03 1.38 o 7 6 4 3.79 4.14 0.77 o 8 6 4 282.66 284.54 8.94 o 9 6 4 2.85 4.80 0.96 o 1 7 4 5.98 6.24 0.62 o 2 7 4 1.01 1.06 0.40 o 3 7 4 305.18 281.43 5.59 o 4 7 4 209.21 177.64 4.19 o 5 7 4 4.77 6.59 0.61 o 6 7 4 27.52 27.53 1.22 o 7 7 4 0.49 1.42 0.64 o 8 7 4 8.55 10.57 1.03 o 0 8 4 1549.68 1527.71 67.81 o 1 8 4 44.76 43.55 1.46 o 2 8 4 823.60 852.48 22.96 o 3 8 4 328.31 324.36 7.66 o 4 8 4 555.21 580.82 15.99 o 5 8 4 256.88 249.24 6.23 o 6 8 4 13.44 10.47 1.04 o 7 8 4 4.23 8.25 1.02 o 8 8 4 25.97 26.27 1.94 o 1 9 4 75.16 69.15 2.61 o 2 9 4 377.60 358.16 9.81 o 3 9 4 5.49 7.02 0.83 o 4 9 4 35.89 37.28 2.01 o 5 9 4 9.66 9.76 0.95 o 6 9 4 1.42 1.68 0.82 o 0 10 4 13.56 17.10 1.97 o 1 10 4 1.42 5.02 1.81 o 2 10 4 46.62 46.49 2.11 o 3 10 4 0.00 2.49 1.39 o 4 10 4 22.88 19.97 1.30 o 5 10 4 6.40 9.82 0.99 o 1 11 4 1.33 2.58 0.91 o 2 11 4 0.05 0.99 0.78 o 3 11 4 38.32 36.57 2.06 o 1 1 5 3552.67 3744.82 76.21 o 2 1 5 1339.70 1354.61 23.19 o 3 1 5 4540.93 4488.23 120.90 o 4 1 5 294.99 286.13 5.45 o 5 1 5 95.91 101.87 1.93 o 6 1 5 289.40 284.19 5.63 o 7 1 5 354.15 353.22 8.34 o 8 1 5 22.41 22.53 1.18 o 9 1 5 203.21 191.09 5.63 o 10 1 5 0.16 0.00 0.73 o 0 2 5 88.45 99.87 2.34 o 1 2 5 247.58 236.19 3.06 o 2 2 5 53.17 60.08 1.06 o 3 2 5 1497.45 1537.49 40.52 o 4 2 5 13.97 14.73 0.50 o 5 2 5 421.13 416.25 7.03 o 6 2 5 4.11 5.61 0.53 o 7 2 5 136.78 130.54 3.04 o 8 2 5 37.49 40.51 1.56 o 9 2 5 37.43 37.09 1.66 o 10 2 5 0.99 0.49 0.69 o 1 3 5 556.39 492.36 10.95 o 2 3 5 115.10 112.80 1.45 o 3 3 5 1114.59 1099.11 17.67 o 4 3 5 1391.12 1442.92 27.52 o 5 3 5 664.70 644.04 11.42 o 6 3 5 15.56 13.72 0.73 o 7 3 5 95.36 97.78 2.36 o 8 3 5 63.18 61.96 2.07 o 9 3 5 24.22 20.79 1.24 o 10 3 5 0.02 0.00 0.84 o 0 4 5 22.68 23.11 1.41 o 1 4 5 33.38 32.30 0.93 o 2 4 5 67.03 65.69 1.36 o 3 4 5 1919.47 1985.64 40.51 o 4 4 5 28.25 24.06 0.77 o 5 4 5 46.48 45.41 1.18 o 6 4 5 76.26 75.32 2.14 o 7 4 5 68.35 61.28 1.93 o 8 4 5 17.35 23.33 1.31 o 9 4 5 1.19 0.01 0.73 o 10 4 5 18.50 15.02 1.32 o 1 5 5 1516.77 1546.39 36.90 o 2 5 5 746.95 744.00 15.03 o 3 5 5 1924.59 1919.94 40.20 o 4 5 5 0.25 0.89 0.57 o 5 5 5 10.55 9.64 0.64 o 6 5 5 220.19 207.45 4.99 o 7 5 5 142.63 143.00 3.83 o 8 5 5 0.69 1.08 0.62 o 9 5 5 110.79 111.82 4.24 o 0 6 5 1.51 1.98 0.80 o 1 6 5 149.93 122.56 2.80 o 2 6 5 8.21 9.00 0.64 o 3 6 5 541.55 552.28 12.05 o 4 6 5 31.99 43.07 1.18 o 5 6 5 262.15 253.70 5.46 o 6 6 5 2.70 3.00 0.69 o 7 6 5 198.11 184.40 4.99 o 8 6 5 52.50 46.54 1.90 o 9 6 5 32.37 28.25 1.82 o 1 7 5 143.92 140.34 3.47 o 2 7 5 6.55 5.47 0.67 o 3 7 5 144.83 138.48 3.98 o 4 7 5 225.84 209.99 7.05 o 5 7 5 117.45 114.46 3.21 o 6 7 5 1.73 1.27 0.65 o 7 7 5 1.30 2.97 0.73 o 8 7 5 11.75 12.27 1.22 o 0 8 5 89.73 94.77 4.49 o 1 8 5 0.01 0.19 0.57 o 2 8 5 0.74 0.98 0.56 o 3 8 5 142.36 141.30 4.55 o 4 8 5 48.52 47.47 1.96 o 5 8 5 7.17 7.25 0.83 o 6 8 5 10.63 11.57 1.12 o 7 8 5 44.08 36.42 1.89 o 1 9 5 15.90 18.73 1.31 o 2 9 5 35.73 37.89 1.90 o 3 9 5 164.52 158.98 4.77 o 4 9 5 5.40 7.18 0.93 o 5 9 5 1.07 0.47 0.65 o 6 9 5 11.11 14.96 1.43 o 0 10 5 26.67 25.73 2.45 o 1 10 5 58.08 53.35 2.44 o 2 10 5 99.12 99.18 3.91 o 3 10 5 159.68 160.83 5.66 o 4 10 5 2.61 4.36 1.18 o 1 11 5 94.54 101.38 4.33 o 2 11 5 8.84 9.29 1.25 o 0 0 6 1713.44 1683.66 173.75 o 1 0 6 190.28 214.92 9.14 o 2 0 6 422.74 483.88 19.07 o 3 0 6 105.90 102.19 2.60 o 4 0 6 168.12 172.17 4.37 o 5 0 6 490.30 486.24 14.56 o 6 0 6 248.73 232.56 6.30 o 7 0 6 719.60 727.98 26.33 o 8 0 6 1293.97 1321.51 53.87 o 9 0 6 344.10 339.38 13.14 o 10 0 6 30.09 27.72 2.22 o 1 1 6 115.37 125.93 2.20 o 2 1 6 132.68 127.81 2.33 o 3 1 6 5.19 5.06 0.60 o 4 1 6 2.22 1.47 0.37 o 5 1 6 100.66 81.93 2.40 o 6 1 6 395.35 375.69 8.31 o 7 1 6 87.39 81.11 2.41 o 8 1 6 99.40 95.70 2.97 o 9 1 6 72.80 75.01 2.49 o 10 1 6 5.61 6.12 0.99 o 0 2 6 11.47 13.28 0.77 o 1 2 6 755.36 873.91 14.23 o 2 2 6 381.81 377.64 5.85 o 3 2 6 2636.73 2641.46 56.59 o 4 2 6 261.27 262.80 4.51 o 5 2 6 14.12 12.52 0.58 o 6 2 6 444.08 435.89 9.26 o 7 2 6 606.49 607.28 14.19 o 8 2 6 42.95 41.92 1.68 o 9 2 6 0.40 1.02 0.66 o 10 2 6 9.98 8.99 1.23 o 1 3 6 15.01 17.63 0.72 o 2 3 6 194.92 179.37 2.60 o 3 3 6 114.32 118.10 2.33 o 4 3 6 28.41 23.56 0.71 o 5 3 6 27.51 27.59 0.84 o 6 3 6 201.03 178.69 3.82 o 7 3 6 173.68 150.90 3.75 o 8 3 6 71.59 75.45 2.88 o 9 3 6 4.00 9.14 1.04 o 0 4 6 46.31 50.17 1.63 o 1 4 6 562.35 587.37 12.93 o 2 4 6 38.11 45.74 1.68 o 3 4 6 136.13 158.81 3.98 o 4 4 6 0.28 1.60 0.78 o 5 4 6 11.09 10.66 0.94 o 6 4 6 7.99 10.14 0.75 o 7 4 6 165.07 166.78 4.36 o 8 4 6 203.08 192.66 5.63 o 9 4 6 100.82 101.30 3.93 o 1 5 6 14.76 16.78 0.96 o 2 5 6 7.10 10.23 0.98 o 3 5 6 14.57 14.68 0.87 o 4 5 6 0.63 1.07 0.37 o 5 5 6 93.16 86.11 2.03 o 6 5 6 21.29 18.94 0.99 o 7 5 6 1.08 2.96 0.68 o 8 5 6 12.29 11.16 1.06 o 9 5 6 46.22 43.06 2.17 o 0 6 6 74.09 81.08 3.85 o 1 6 6 151.53 140.50 3.41 o 2 6 6 25.65 22.45 1.07 o 3 6 6 220.16 249.50 6.94 o 4 6 6 99.18 112.29 3.40 o 5 6 6 26.27 28.51 1.24 o 6 6 6 217.17 198.69 5.61 o 7 6 6 151.41 147.47 4.86 o 8 6 6 75.64 71.89 2.78 o 1 7 6 122.58 112.01 3.69 o 2 7 6 29.74 21.50 1.03 o 3 7 6 105.19 94.85 3.20 o 4 7 6 75.21 71.79 2.44 o 5 7 6 22.62 24.10 1.31 o 6 7 6 19.10 20.22 1.42 o 7 7 6 57.06 48.29 2.29 o 0 8 6 185.46 187.55 8.76 o 1 8 6 416.15 435.90 13.37 o 2 8 6 427.64 432.45 13.18 o 3 8 6 457.14 436.51 12.33 o 4 8 6 10.29 12.75 1.40 o 5 8 6 97.91 103.05 3.45 o 6 8 6 28.28 25.81 1.73 o 1 9 6 0.00 0.86 0.92 o 2 9 6 2.18 1.68 0.85 o 3 9 6 3.26 4.12 0.92 o 4 9 6 1.58 1.94 0.84 o 5 9 6 24.71 21.20 1.72 o 0 10 6 5.42 7.76 1.65 o 1 10 6 24.61 21.06 1.45 o 2 10 6 2.82 3.72 0.90 o 3 10 6 7.92 12.46 1.34 o 1 1 7 66.75 67.03 1.40 o 2 1 7 511.96 522.31 9.67 o 3 1 7 16.66 19.21 0.73 o 4 1 7 73.42 77.09 1.72 o 5 1 7 48.26 52.67 1.66 o 6 1 7 16.63 14.16 0.67 o 7 1 7 15.61 16.04 1.02 o 8 1 7 19.88 21.61 1.29 o 9 1 7 2.75 5.29 0.90 o 0 2 7 1857.91 1819.43 48.37 o 1 2 7 10.09 11.44 0.49 o 2 2 7 404.92 427.40 7.29 o 3 2 7 121.57 116.77 2.80 o 4 2 7 34.34 44.13 1.14 o 5 2 7 0.51 5.43 0.73 o 6 2 7 379.56 393.43 8.65 o 7 2 7 1.68 3.24 0.58 o 8 2 7 57.49 60.18 2.20 o 9 2 7 0.04 0.24 0.65 o 1 3 7 269.89 265.69 5.25 o 2 3 7 1825.95 1819.11 34.49 o 3 3 7 9.07 9.26 0.53 o 4 3 7 80.45 75.53 1.77 o 5 3 7 13.60 11.80 0.65 o 6 3 7 81.75 84.43 2.42 o 7 3 7 57.63 61.76 1.98 o 8 3 7 6.64 10.24 1.00 o 9 3 7 6.02 7.09 1.00 o 0 4 7 242.66 248.54 7.09 o 1 4 7 37.92 34.52 1.28 o 2 4 7 4.58 2.93 0.61 o 3 4 7 68.93 71.44 1.83 o 4 4 7 30.64 45.14 1.41 o 5 4 7 0.60 1.01 0.42 o 6 4 7 57.63 57.04 1.87 o 7 4 7 0.08 1.32 0.61 o 8 4 7 0.18 1.20 0.65 o 9 4 7 13.24 11.44 1.22 o 1 5 7 296.74 284.23 6.90 o 2 5 7 12.38 16.59 1.80 o 3 5 7 14.94 12.25 0.89 o 4 5 7 167.18 154.52 4.18 o 5 5 7 11.97 13.63 0.85 o 6 5 7 6.13 8.32 0.93 o 7 5 7 0.27 0.24 0.68 o 8 5 7 0.97 1.57 0.79 o 0 6 7 1420.31 1362.88 60.35 o 1 6 7 16.01 14.96 1.19 o 2 6 7 351.91 376.03 9.67 o 3 6 7 65.50 58.69 2.29 o 4 6 7 26.23 36.56 1.54 o 5 6 7 2.65 3.16 0.72 o 6 6 7 403.34 428.33 13.76 o 7 6 7 12.85 13.91 1.29 o 8 6 7 49.19 45.32 2.54 o 1 7 7 89.79 86.04 3.07 o 2 7 7 320.49 317.88 9.70 o 3 7 7 18.12 17.92 1.08 o 4 7 7 23.70 31.63 1.96 o 5 7 7 3.24 4.16 0.83 o 6 7 7 25.17 32.22 1.97 o 7 7 7 3.08 4.27 0.96 o 0 8 7 76.87 75.01 5.60 o 1 8 7 37.03 40.51 2.04 o 2 8 7 0.19 0.73 0.79 o 3 8 7 18.34 15.30 1.37 o 4 8 7 18.00 23.36 1.58 o 5 8 7 1.64 4.39 1.00 o 6 8 7 0.16 1.19 1.02 o 1 9 7 22.11 23.86 1.56 o 2 9 7 30.26 34.44 1.89 o 3 9 7 5.06 4.85 1.03 o 4 9 7 2.19 1.36 0.88 o 0 10 7 33.16 34.81 3.09 o 1 10 7 19.08 20.41 1.71 o 2 10 7 0.57 1.96 0.93 o 0 0 8 2671.37 2268.87 194.84 o 1 0 8 1525.53 1442.73 57.78 o 2 0 8 264.89 256.45 12.09 o 3 0 8 198.75 198.14 6.50 o 4 0 8 253.35 238.77 6.73 o 5 0 8 990.40 984.72 30.60 o 6 0 8 110.25 120.90 4.27 o 7 0 8 185.22 184.25 7.23 o 8 0 8 50.04 44.20 3.66 o 9 0 8 16.63 21.17 2.29 o 1 1 8 5.35 4.40 0.47 o 2 1 8 59.46 51.91 1.40 o 3 1 8 314.57 289.10 6.31 o 4 1 8 132.51 115.28 2.44 o 5 1 8 366.14 335.17 7.02 o 6 1 8 44.22 46.55 1.44 o 7 1 8 20.19 20.06 1.13 o 8 1 8 0.13 0.19 0.56 o 9 1 8 58.57 57.55 2.49 o 0 2 8 77.58 67.40 2.59 o 1 2 8 47.78 50.64 1.25 o 2 2 8 279.49 274.55 5.04 o 3 2 8 9.00 10.17 0.77 o 4 2 8 5.68 5.72 0.65 o 5 2 8 51.09 46.56 1.41 o 6 2 8 24.03 19.99 1.02 o 7 2 8 89.48 89.29 3.04 o 8 2 8 2.08 5.42 0.89 o 9 2 8 19.49 14.00 1.24 o 1 3 8 0.00 0.26 0.49 o 2 3 8 14.03 14.82 0.69 o 3 3 8 217.20 197.81 4.61 o 4 3 8 37.84 35.36 1.15 o 5 3 8 70.79 67.49 2.02 o 6 3 8 26.41 28.56 1.30 o 7 3 8 46.41 44.74 1.82 o 8 3 8 8.18 8.55 0.97 o 0 4 8 823.13 798.61 26.00 o 1 4 8 196.64 199.56 5.20 o 2 4 8 4.84 5.97 0.79 o 3 4 8 14.15 13.83 0.91 o 4 4 8 13.80 17.15 1.21 o 5 4 8 43.73 43.67 1.58 o 6 4 8 18.95 23.54 1.59 o 7 4 8 115.11 115.66 3.91 o 8 4 8 0.10 1.03 0.82 o 1 5 8 2.02 1.17 0.55 o 2 5 8 19.49 22.26 1.19 o 3 5 8 0.05 2.03 0.72 o 4 5 8 27.87 25.43 1.51 o 5 5 8 199.98 180.75 5.25 o 6 5 8 5.45 9.28 1.22 o 7 5 8 28.97 27.61 1.84 o 0 6 8 9.72 12.94 2.11 o 1 6 8 50.11 50.54 2.23 o 2 6 8 87.86 93.50 2.86 o 3 6 8 29.16 25.00 1.43 o 4 6 8 5.80 8.36 0.95 o 5 6 8 89.16 88.63 3.08 o 6 6 8 0.54 2.03 0.97 o 7 6 8 0.22 0.00 0.90 o 1 7 8 0.01 0.55 0.65 o 2 7 8 1.81 2.52 1.16 o 3 7 8 0.01 1.37 0.77 o 4 7 8 1.15 1.04 0.73 o 5 7 8 13.80 17.04 1.39 o 6 7 8 2.21 4.99 0.99 o 0 8 8 3.40 9.64 1.58 o 1 8 8 24.78 20.12 1.53 o 2 8 8 71.10 72.55 3.11 o 3 8 8 167.91 178.24 6.11 o 4 8 8 25.40 33.98 1.98 o 5 8 8 140.80 139.75 5.74 o 1 9 8 1.22 1.16 0.89 o 2 9 8 2.99 1.38 0.83 o 3 9 8 51.19 60.57 3.01 o 1 1 9 56.90 61.90 2.09 o 2 1 9 73.37 69.99 1.68 o 3 1 9 135.06 128.60 3.04 o 4 1 9 76.98 78.37 2.05 o 5 1 9 529.32 533.05 11.85 o 6 1 9 3.66 4.25 0.62 o 7 1 9 34.35 32.32 1.64 o 8 1 9 0.27 0.40 0.69 o 0 2 9 143.55 137.67 4.36 o 1 2 9 173.98 181.82 3.78 o 2 2 9 0.87 0.65 0.47 o 3 2 9 390.67 419.43 8.54 o 4 2 9 0.55 0.86 0.44 o 5 2 9 61.83 66.73 2.14 o 6 2 9 9.57 7.91 0.79 o 7 2 9 21.05 20.09 1.26 o 8 2 9 9.07 9.10 1.20 o 1 3 9 177.70 166.80 4.06 o 2 3 9 238.09 248.96 6.74 o 3 3 9 79.01 81.30 2.61 o 4 3 9 0.01 1.61 0.56 o 5 3 9 227.47 217.13 5.61 o 6 3 9 11.86 9.72 0.99 o 7 3 9 66.23 64.43 2.63 o 0 4 9 191.53 191.02 6.46 o 1 4 9 136.40 130.68 3.74 o 2 4 9 0.60 0.24 0.60 o 3 4 9 112.01 93.14 2.99 o 4 4 9 3.18 3.38 0.77 o 5 4 9 0.13 1.05 0.64 o 6 4 9 13.96 14.46 1.30 o 7 4 9 6.73 6.32 1.13 o 1 5 9 250.38 239.30 7.39 o 2 5 9 0.16 1.07 0.69 o 3 5 9 112.33 108.93 3.47 o 4 5 9 73.60 76.84 2.89 o 5 5 9 293.90 322.75 9.76 o 6 5 9 15.83 17.71 1.77 o 7 5 9 27.32 26.11 1.98 o 0 6 9 141.12 137.39 6.82 o 1 6 9 277.51 277.86 9.01 o 2 6 9 0.19 1.06 1.02 o 3 6 9 316.90 364.03 12.05 o 4 6 9 0.44 0.36 0.66 o 5 6 9 73.49 82.35 3.44 o 6 6 9 1.56 2.96 0.98 o 1 7 9 90.32 82.82 3.26 o 2 7 9 65.44 76.10 3.29 o 3 7 9 6.14 10.68 1.11 o 4 7 9 0.07 0.37 0.75 o 5 7 9 109.98 121.62 5.31 o 0 8 9 1.80 5.42 1.49 o 1 8 9 67.71 60.40 2.96 o 2 8 9 4.50 4.23 0.99 o 3 8 9 0.90 0.68 0.86 o 0 0 10 801.11 652.06 81.25 o 1 0 10 970.15 872.02 50.19 o 2 0 10 908.32 948.28 31.17 o 3 0 10 146.87 158.99 5.22 o 4 0 10 0.56 0.96 0.71 o 5 0 10 3.32 4.04 0.87 o 6 0 10 48.76 50.17 2.62 o 7 0 10 11.95 13.65 1.81 o 1 1 10 287.60 288.85 7.01 o 2 1 10 127.17 119.05 2.81 o 3 1 10 65.25 61.42 1.83 o 4 1 10 30.30 32.81 1.29 o 5 1 10 7.18 6.76 0.66 o 6 1 10 72.32 67.99 2.33 o 7 1 10 3.35 6.07 0.93 o 0 2 10 397.65 398.50 14.24 o 1 2 10 519.50 541.69 13.78 o 2 2 10 29.93 31.99 1.35 o 3 2 10 92.47 85.97 2.82 o 4 2 10 0.02 1.31 0.89 o 5 2 10 6.70 8.12 1.02 o 6 2 10 3.88 6.04 0.98 o 7 2 10 61.34 66.90 3.21 o 1 3 10 125.67 122.57 3.43 o 2 3 10 87.77 80.32 2.74 o 3 3 10 81.20 80.20 2.87 o 4 3 10 40.96 40.53 1.76 o 5 3 10 2.12 3.49 0.81 o 6 3 10 7.98 5.21 0.94 o 0 4 10 65.15 71.10 3.96 o 1 4 10 285.49 278.69 8.40 o 2 4 10 118.49 123.02 4.38 o 3 4 10 108.81 121.36 4.09 o 4 4 10 4.64 4.41 0.93 o 5 4 10 15.94 20.55 1.58 o 6 4 10 1.82 1.62 0.85 o 1 5 10 29.70 30.42 1.89 o 2 5 10 9.27 12.32 1.30 o 3 5 10 9.43 11.94 1.12 o 4 5 10 13.26 17.65 1.29 o 5 5 10 30.03 26.89 1.94 o 0 6 10 305.49 335.13 16.28 o 1 6 10 142.45 145.81 5.13 o 2 6 10 15.63 14.82 1.28 o 3 6 10 6.55 11.91 1.33 o 4 6 10 16.68 21.48 1.71 o 1 7 10 0.00 0.00 0.85 o 2 7 10 3.48 2.50 1.14 o 3 7 10 25.13 26.55 1.95 o 1 1 11 24.96 27.18 1.30 o 2 1 11 44.60 42.81 1.76 o 3 1 11 54.02 45.65 1.59 o 4 1 11 79.19 72.95 2.42 o 5 1 11 0.21 0.95 0.65 o 6 1 11 34.16 31.04 2.03 o 0 2 11 216.99 208.18 8.84 o 1 2 11 1.12 0.53 0.59 o 2 2 11 16.73 18.00 1.98 o 3 2 11 27.56 32.71 1.68 o 4 2 11 19.57 22.02 1.47 o 5 2 11 13.02 14.19 1.21 o 6 2 11 37.13 33.37 2.05 o 1 3 11 3.43 3.71 0.77 o 2 3 11 3.47 7.26 0.94 o 3 3 11 1.04 2.62 0.84 o 4 3 11 216.74 218.70 7.01 o 5 3 11 22.62 21.37 1.67 o 0 4 11 32.77 39.69 2.96 o 1 4 11 3.64 5.66 1.03 o 2 4 11 25.75 25.56 1.73 o 3 4 11 91.47 86.15 3.33 o 4 4 11 0.27 1.33 0.90 o 5 4 11 22.62 18.93 1.54 o 1 5 11 14.43 18.16 1.57 o 2 5 11 90.41 84.28 3.42 o 3 5 11 79.54 78.03 3.52 o 4 5 11 16.00 18.54 1.61 o 0 6 11 267.05 242.17 12.85 o 1 6 11 1.79 1.36 0.91 o 2 6 11 15.22 17.01 1.57 o 0 0 12 9.22 13.42 2.49 o 1 0 12 167.82 162.84 7.58 o 2 0 12 52.49 48.54 3.31 o 3 0 12 0.35 0.80 1.09 o 4 0 12 18.72 19.56 2.66 o 1 1 12 195.29 186.89 5.33 o 2 1 12 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