#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:45:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181192 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/71/2227100.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2227100_Fobs loop_ _publ_author_name 'Fujii, Kotaro' 'Toyota, Kazuyuki' 'Sekine, Akiko' 'Uekusa, Hidehiro' 'Nugrahani, Ilma' 'Asyarie, Sukmadjaja' 'Soewandhi, N. Sundani' 'Ibrahim, Slamet' _publ_section_title ; Potassium clavulanate ; _journal_coeditor_code TK2689 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m985 _journal_page_last m986 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.3453 _cell_length_b 7.8191 _cell_length_c 27.4913 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7704 _cod_data_source_file tk2689Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' irai_takigawa' _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 419.32 378.11 65.97 o 4 0 0 1303.10 1329.76 126.13 o 1 1 0 2862.42 2724.47 46.88 o 2 1 0 993.24 969.93 29.84 o 3 1 0 10.22 26.31 10.25 o 4 1 0 21.41 30.89 9.60 o 5 1 0 333.84 370.90 24.06 o 0 2 0 9574.12 9286.63 235.57 o 1 2 0 1.97 3.76 7.33 o 2 2 0 169.51 184.74 12.74 o 3 2 0 547.80 600.46 18.17 o 4 2 0 811.83 841.04 24.04 o 5 2 0 16.08 31.00 13.98 o 1 3 0 310.65 256.46 18.94 o 2 3 0 517.71 532.02 15.54 o 3 3 0 147.23 142.52 15.35 o 4 3 0 0.93 -2.51 7.59 o 5 3 0 244.39 296.68 26.30 o 0 4 0 3667.72 3845.05 99.00 o 1 4 0 1130.19 1097.71 30.37 o 2 4 0 155.38 170.02 18.06 o 3 4 0 64.93 92.31 17.29 o 4 4 0 169.05 188.20 18.39 o 5 4 0 4.64 20.70 14.26 o 1 5 0 46.99 44.49 13.37 o 2 5 0 460.87 436.65 26.08 o 3 5 0 88.41 72.03 19.65 o 4 5 0 39.12 -11.29 17.73 o 0 6 0 17.66 11.40 14.93 o 1 6 0 63.63 57.45 14.52 o 2 6 0 460.16 455.40 25.93 o 3 6 0 86.47 86.59 23.71 o 4 6 0 30.41 -7.64 21.83 o 1 7 0 1.34 -2.79 10.59 o 2 7 0 269.04 297.45 23.74 o 3 7 0 0.02 5.58 8.47 o 4 7 0 1.25 -18.90 20.71 o 0 8 0 732.31 820.98 47.61 o 1 8 0 31.69 0.15 8.46 o 2 8 0 6.25 -5.46 12.42 o 3 8 0 0.07 -1.04 8.65 o 1 9 0 49.32 20.41 20.63 o 2 9 0 364.91 448.89 30.82 o 0 10 0 75.78 76.96 37.71 o 1 0 1 701.51 686.25 33.08 o 2 0 1 6720.29 6357.58 141.10 o 3 0 1 16.18 29.82 17.95 o 4 0 1 8.15 -12.45 18.24 o 5 0 1 0.07 0.90 6.11 o -5 1 1 12.69 19.84 9.53 o -4 1 1 43.79 39.67 13.02 o -3 1 1 92.53 86.95 11.87 o -2 1 1 1.41 -2.92 6.31 o -1 1 1 1936.54 1941.65 35.85 o 1 1 1 1988.77 1975.38 34.62 o 2 1 1 0.92 1.50 6.64 o 3 1 1 103.03 108.70 12.86 o 4 1 1 41.49 45.84 11.06 o 5 1 1 13.38 4.82 14.18 o -5 2 1 29.00 14.16 21.26 o -4 2 1 7.43 6.44 9.70 o -3 2 1 122.99 120.95 15.24 o -2 2 1 3983.81 3920.08 60.93 o -1 2 1 2659.82 2808.46 42.93 o 0 2 1 85.56 25.81 22.01 o 1 2 1 2702.07 3015.03 134.62 o 2 2 1 4006.99 3945.57 65.47 o 3 2 1 116.83 116.46 12.66 o 4 2 1 7.91 8.41 8.92 o 5 2 1 31.17 17.63 19.39 o -5 3 1 23.16 33.10 17.61 o -4 3 1 64.56 62.10 13.87 o -3 3 1 617.94 653.90 24.47 o -2 3 1 219.56 227.09 13.83 o -1 3 1 886.59 891.55 28.69 o 0 3 1 40.90 29.93 17.61 o 1 3 1 898.05 890.59 25.00 o 2 3 1 217.71 248.56 11.07 o 3 3 1 585.37 708.14 56.91 o 4 3 1 58.00 65.77 12.96 o 5 3 1 25.07 16.52 10.30 o -5 4 1 83.14 72.36 24.92 o -4 4 1 23.82 30.24 8.61 o -3 4 1 212.36 201.33 18.52 o -2 4 1 450.63 440.86 18.46 o -1 4 1 117.55 101.85 13.46 o 0 4 1 86.65 64.89 19.72 o 1 4 1 110.53 105.96 13.92 o 2 4 1 452.93 433.20 17.99 o 3 4 1 219.71 202.00 17.55 o 4 4 1 22.28 12.57 11.31 o 5 4 1 87.26 73.42 22.81 o -4 5 1 85.73 56.97 43.11 o -3 5 1 791.82 876.76 41.48 o -2 5 1 132.68 113.97 17.23 o -1 5 1 683.33 680.35 27.45 o 0 5 1 343.52 372.85 22.93 o 1 5 1 699.08 687.82 26.19 o 2 5 1 131.00 132.96 15.92 o 3 5 1 804.10 842.13 48.45 o 4 5 1 77.36 22.28 10.87 o -4 6 1 11.18 4.82 22.44 o -3 6 1 93.63 93.81 18.89 o -2 6 1 579.34 608.93 28.62 o -1 6 1 221.65 234.65 20.32 o 0 6 1 32.67 15.78 12.56 o 1 6 1 234.90 236.61 22.38 o 2 6 1 564.70 606.50 33.70 o 3 6 1 94.88 75.40 13.65 o 4 6 1 10.69 -8.94 15.12 o -4 7 1 99.58 70.63 43.17 o -3 7 1 26.72 25.07 9.78 o -2 7 1 121.62 110.63 18.29 o -1 7 1 13.23 12.86 11.56 o 0 7 1 1058.42 1145.30 38.35 o 1 7 1 15.64 1.84 12.54 o 2 7 1 119.72 117.18 23.77 o 3 7 1 29.29 20.26 10.93 o 4 7 1 96.27 37.47 38.85 o -3 8 1 73.54 66.94 19.08 o -2 8 1 162.50 124.04 35.98 o -1 8 1 76.95 67.42 16.66 o 0 8 1 75.09 68.44 16.81 o 1 8 1 86.21 110.85 21.59 o 2 8 1 159.76 171.96 44.29 o 3 8 1 77.65 63.92 19.69 o -2 9 1 48.24 39.05 18.06 o -1 9 1 32.51 26.92 15.49 o 0 9 1 597.97 785.14 35.61 o 1 9 1 33.77 30.37 19.38 o 2 9 1 48.61 12.74 15.92 o 0 10 1 1.28 17.96 18.54 o 1 0 2 3632.86 3559.64 70.97 o 2 0 2 35.06 31.57 12.97 o 3 0 2 64.94 61.50 25.56 o 4 0 2 1145.61 1173.33 66.03 o 5 0 2 38.67 31.74 10.27 o -5 1 2 167.39 210.34 69.48 o -4 1 2 118.76 121.72 16.54 o -3 1 2 324.31 336.58 14.15 o -2 1 2 88.57 95.77 12.09 o -1 1 2 2873.23 2690.53 41.61 o 0 1 2 1725.01 1655.09 21.98 o 1 1 2 2878.47 2772.00 36.79 o 2 1 2 89.29 96.33 12.74 o 3 1 2 326.89 340.85 19.82 o 4 1 2 118.03 150.68 16.81 o 5 1 2 168.41 206.84 32.27 o -5 2 2 147.11 176.73 62.74 o -4 2 2 273.78 288.07 16.43 o -3 2 2 123.40 152.73 11.45 o -2 2 2 676.97 657.58 17.92 o -1 2 2 741.87 739.28 22.22 o 0 2 2 6895.52 6808.82 103.48 o 1 2 2 766.51 794.10 25.33 o 2 2 2 686.93 695.04 20.11 o 3 2 2 130.21 146.83 13.35 o 4 2 2 275.33 305.95 20.27 o 5 2 2 152.10 157.88 28.12 o -5 3 2 222.06 259.39 27.64 o -4 3 2 275.20 287.87 23.53 o -3 3 2 271.36 317.30 26.82 o -2 3 2 1257.47 1265.10 25.57 o -1 3 2 1887.74 1904.25 41.03 o 0 3 2 2.15 -2.23 8.67 o 1 3 2 1860.65 1855.47 32.57 o 2 3 2 1247.95 1204.12 24.72 o 3 3 2 267.16 300.26 19.80 o 4 3 2 274.31 314.61 16.27 o 5 3 2 220.47 223.26 21.70 o -5 4 2 42.21 32.06 26.24 o -4 4 2 1.00 -3.75 6.98 o -3 4 2 290.11 321.71 43.21 o -2 4 2 245.54 246.01 14.36 o -1 4 2 1507.91 1507.38 34.59 o 0 4 2 115.19 122.03 25.96 o 1 4 2 1477.30 1454.69 33.03 o 2 4 2 245.38 244.41 15.02 o 3 4 2 293.60 343.24 27.55 o 4 4 2 2.09 -5.85 7.31 o 5 4 2 45.52 24.55 17.26 o -4 5 2 3.72 2.34 20.29 o -3 5 2 241.73 257.24 26.69 o -2 5 2 60.69 74.25 11.96 o -1 5 2 273.22 311.74 21.06 o 0 5 2 43.85 44.78 16.02 o 1 5 2 273.05 308.93 21.14 o 2 5 2 54.11 63.87 14.95 o 3 5 2 238.75 240.99 17.02 o 4 5 2 4.48 3.65 7.31 o -4 6 2 2.54 -0.15 18.32 o -3 6 2 531.56 521.47 49.46 o -2 6 2 323.78 338.77 21.10 o -1 6 2 113.48 107.25 26.02 o 0 6 2 211.76 239.53 27.49 o 1 6 2 118.36 142.50 18.23 o 2 6 2 326.03 328.46 21.09 o 3 6 2 540.68 549.32 53.94 o 4 6 2 2.40 -3.23 14.93 o -4 7 2 50.16 -8.34 21.13 o -3 7 2 13.04 12.44 9.60 o -2 7 2 170.02 194.04 36.63 o -1 7 2 30.44 19.67 13.51 o 0 7 2 1.14 -7.42 12.17 o 1 7 2 34.72 29.02 12.82 o 2 7 2 159.12 182.57 27.31 o 3 7 2 13.82 15.89 10.52 o 4 7 2 52.39 24.51 18.42 o -3 8 2 63.35 -1.41 18.75 o -2 8 2 53.64 19.11 14.27 o -1 8 2 85.74 72.23 16.15 o 0 8 2 0.52 -9.82 13.48 o 1 8 2 78.40 62.14 21.38 o 2 8 2 52.81 14.97 13.03 o 3 8 2 65.24 48.27 17.65 o -2 9 2 103.21 45.28 29.01 o -1 9 2 59.48 61.98 20.02 o 0 9 2 18.32 46.41 20.44 o 1 9 2 58.49 53.75 21.42 o 2 9 2 97.02 50.66 19.68 o 0 10 2 49.48 30.01 14.36 o 1 0 3 94.37 93.31 21.24 o 2 0 3 1982.82 1916.29 54.48 o 3 0 3 160.32 148.06 28.58 o 4 0 3 124.06 152.69 28.61 o 5 0 3 30.20 28.04 10.79 o -5 1 3 108.31 103.18 37.25 o -4 1 3 191.32 192.07 17.41 o -3 1 3 281.87 275.72 16.87 o -2 1 3 2319.56 2324.28 42.38 o -1 1 3 5674.48 5550.92 111.90 o 0 1 3 313.43 280.08 11.70 o 1 1 3 5767.93 5676.84 67.93 o 2 1 3 2323.98 2341.91 47.41 o 3 1 3 269.59 268.68 16.54 o 4 1 3 191.40 188.36 18.66 o 5 1 3 116.46 120.01 32.22 o -5 2 3 0.46 -13.38 13.38 o -4 2 3 3.40 14.55 6.44 o -3 2 3 16.13 11.30 8.55 o -2 2 3 365.66 383.28 18.66 o -1 2 3 431.57 430.05 25.26 o 0 2 3 65.97 49.08 13.14 o 1 2 3 454.54 436.25 14.43 o 2 2 3 315.38 329.14 16.61 o 3 2 3 20.00 13.41 8.32 o 4 2 3 4.32 7.91 11.49 o 5 2 3 0.87 7.82 6.92 o -5 3 3 125.30 129.81 52.26 o -4 3 3 132.75 141.33 14.87 o -3 3 3 1108.98 1176.69 36.50 o -2 3 3 384.18 423.01 19.64 o -1 3 3 2981.88 3068.44 53.92 o 0 3 3 1755.10 1742.93 39.74 o 1 3 3 3030.15 3061.81 43.47 o 2 3 3 368.56 398.65 19.45 o 3 3 3 1109.37 1188.60 58.95 o 4 3 3 125.27 153.79 15.92 o 5 3 3 122.07 104.43 16.99 o -5 4 3 26.88 23.81 21.86 o -4 4 3 199.27 214.63 47.14 o -3 4 3 20.68 12.11 21.68 o -2 4 3 358.43 375.24 16.71 o -1 4 3 285.31 251.87 16.11 o 0 4 3 3.97 -6.32 10.17 o 1 4 3 286.16 259.57 15.05 o 2 4 3 368.38 365.62 19.85 o 3 4 3 23.95 22.18 10.98 o 4 4 3 196.77 229.82 16.37 o 5 4 3 24.37 25.54 11.96 o -4 5 3 97.51 25.18 29.53 o -3 5 3 121.53 135.83 20.86 o -2 5 3 345.47 314.58 18.07 o -1 5 3 595.23 610.25 29.15 o 0 5 3 214.65 224.08 21.85 o 1 5 3 597.03 600.60 26.14 o 2 5 3 358.33 339.11 22.24 o 3 5 3 123.04 123.36 13.37 o 4 5 3 94.89 79.42 15.44 o -4 6 3 99.03 47.88 32.29 o -3 6 3 18.25 33.17 14.94 o -2 6 3 5.07 4.32 6.98 o -1 6 3 487.35 485.73 27.91 o 0 6 3 55.70 63.71 20.81 o 1 6 3 476.29 486.08 26.34 o 2 6 3 5.18 -2.29 8.14 o 3 6 3 18.57 24.20 10.04 o 4 6 3 99.77 53.35 39.03 o -4 7 3 43.81 9.68 23.01 o -3 7 3 97.46 51.25 16.81 o -2 7 3 30.12 14.20 15.66 o -1 7 3 372.09 365.36 25.94 o 0 7 3 111.08 151.11 17.89 o 1 7 3 358.92 363.07 23.81 o 2 7 3 30.90 27.81 12.96 o 3 7 3 103.97 36.66 17.22 o 4 7 3 43.72 20.83 19.24 o -3 8 3 0.79 3.79 7.81 o -2 8 3 12.52 23.97 17.42 o -1 8 3 340.58 409.37 30.44 o 0 8 3 184.24 202.59 24.31 o 1 8 3 344.00 427.45 30.73 o 2 8 3 12.32 6.67 14.55 o 3 8 3 0.27 3.96 9.36 o -2 9 3 30.09 16.10 15.27 o -1 9 3 0.36 12.59 13.97 o 0 9 3 95.07 136.99 22.08 o 1 9 3 0.65 -10.17 10.17 o 2 9 3 31.06 -0.52 14.77 o 0 10 3 16.45 5.62 11.99 o 1 0 4 4056.25 4016.62 107.09 o 2 0 4 13.02 8.89 9.73 o 3 0 4 31.50 26.28 22.31 o 4 0 4 519.39 503.59 46.74 o 5 0 4 67.08 56.24 16.64 o -5 1 4 44.17 33.62 18.11 o -4 1 4 66.16 72.71 11.85 o -3 1 4 339.69 307.32 18.29 o -2 1 4 623.52 607.87 26.27 o -1 1 4 3801.78 3615.23 90.77 o 0 1 4 2678.77 2411.22 43.93 o 1 1 4 3853.93 3801.08 97.93 o 2 1 4 629.02 574.89 20.69 o 3 1 4 347.61 362.79 23.22 o 4 1 4 59.92 66.33 16.46 o 5 1 4 40.36 46.75 21.98 o -5 2 4 5.20 11.90 15.37 o -4 2 4 429.20 447.63 18.96 o -3 2 4 30.95 23.43 10.05 o -2 2 4 1089.50 1144.69 22.43 o -1 2 4 2005.70 1920.42 35.61 o 0 2 4 1204.59 1180.95 29.52 o 1 2 4 1971.79 1867.69 28.28 o 2 2 4 1098.96 1116.51 24.47 o 3 2 4 35.47 38.81 12.29 o 4 2 4 414.68 408.17 21.18 o 5 2 4 3.49 -5.30 7.27 o -5 3 4 53.34 59.66 23.85 o -4 3 4 267.91 296.61 23.61 o -3 3 4 374.07 402.91 36.65 o -2 3 4 399.80 367.92 20.16 o -1 3 4 2506.76 2471.87 45.66 o 0 3 4 55.32 60.03 12.47 o 1 3 4 2479.92 2392.24 39.80 o 2 3 4 389.77 349.73 11.17 o 3 3 4 391.15 447.76 22.05 o 4 3 4 274.66 258.92 15.44 o 5 3 4 53.49 60.66 14.33 o -5 4 4 3.47 38.81 21.47 o -4 4 4 144.02 99.98 38.68 o -3 4 4 400.86 438.44 45.18 o -2 4 4 219.47 219.83 15.82 o -1 4 4 9.85 5.09 8.05 o 0 4 4 20.57 16.09 12.29 o 1 4 4 14.21 16.84 9.14 o 2 4 4 217.34 236.49 13.55 o 3 4 4 403.03 438.93 30.54 o 4 4 4 148.66 164.46 16.07 o 5 4 4 3.37 11.80 9.52 o -4 5 4 206.41 82.08 60.29 o -3 5 4 207.36 221.15 24.22 o -2 5 4 365.16 382.95 17.88 o -1 5 4 1128.84 1224.45 37.85 o 0 5 4 331.15 342.62 27.18 o 1 5 4 1134.20 1174.18 37.68 o 2 5 4 372.40 378.67 18.20 o 3 5 4 193.50 161.47 21.27 o 4 5 4 210.56 205.10 33.95 o -4 6 4 81.99 46.68 30.14 o -3 6 4 41.81 21.43 14.87 o -2 6 4 320.29 326.41 20.37 o -1 6 4 1068.45 1175.27 38.36 o 0 6 4 5.44 -0.98 8.43 o 1 6 4 1041.39 1101.33 34.04 o 2 6 4 321.67 334.95 19.28 o 3 6 4 39.64 27.69 9.01 o 4 6 4 85.49 20.23 26.25 o -4 7 4 10.22 -1.75 25.13 o -3 7 4 16.89 6.46 15.01 o -2 7 4 66.33 46.09 13.62 o -1 7 4 101.84 113.08 19.60 o 0 7 4 22.79 10.32 14.40 o 1 7 4 100.07 108.14 19.94 o 2 7 4 68.43 44.53 17.27 o 3 7 4 15.46 -3.55 8.37 o 4 7 4 9.12 -3.13 18.97 o -3 8 4 151.45 154.97 67.45 o -2 8 4 138.53 55.66 29.43 o -1 8 4 127.75 141.00 33.67 o 0 8 4 51.90 43.86 16.76 o 1 8 4 133.94 109.92 24.88 o 2 8 4 137.92 70.80 22.17 o 3 8 4 153.54 124.89 35.66 o -2 9 4 105.20 51.65 23.25 o -1 9 4 28.73 12.73 15.41 o 0 9 4 13.74 25.42 17.95 o 1 9 4 28.82 24.28 14.71 o 2 9 4 104.97 55.68 25.20 o 0 10 4 21.29 15.73 13.78 o 1 0 5 4374.34 3803.39 324.58 o 2 0 5 695.73 665.33 27.27 o 3 0 5 1231.49 1225.49 48.15 o 4 0 5 77.58 75.07 9.93 o 5 0 5 119.80 75.22 21.88 o -5 1 5 106.25 79.86 28.94 o -4 1 5 3.78 4.45 6.56 o -3 1 5 913.13 894.88 23.03 o -2 1 5 581.80 540.74 26.07 o -1 1 5 1671.88 1500.99 42.44 o 0 1 5 8.48 10.07 7.21 o 1 1 5 1675.43 1591.52 32.70 o 2 1 5 573.25 531.25 22.73 o 3 1 5 886.73 871.68 31.77 o 4 1 5 3.19 -4.01 10.29 o 5 1 5 107.44 115.00 22.14 o -5 2 5 37.26 21.13 31.38 o -4 2 5 1.80 -8.81 11.70 o -3 2 5 317.70 336.73 20.21 o -2 2 5 1336.82 1378.21 49.36 o -1 2 5 1505.11 1414.53 27.41 o 0 2 5 152.08 164.89 14.80 o 1 2 5 1486.70 1379.37 25.92 o 2 2 5 1338.67 1355.44 26.47 o 3 2 5 305.76 332.53 17.71 o 4 2 5 2.60 7.47 8.56 o 5 2 5 39.97 34.40 14.27 o -5 3 5 98.14 97.93 31.31 o -4 3 5 535.31 559.05 32.24 o -3 3 5 668.48 727.94 50.83 o -2 3 5 768.57 796.97 30.31 o -1 3 5 3787.79 3787.66 61.43 o 0 3 5 2095.19 2105.93 43.46 o 1 3 5 3862.01 3845.95 63.61 o 2 3 5 803.51 826.85 20.75 o 3 3 5 650.25 686.47 20.58 o 4 3 5 537.25 500.85 20.18 o 5 3 5 103.34 105.62 18.91 o -5 4 5 18.88 24.55 22.91 o -4 4 5 2.36 12.17 17.66 o -3 4 5 68.35 60.44 31.79 o -2 4 5 72.54 74.15 12.69 o -1 4 5 231.87 218.32 14.38 o 0 4 5 0.62 -0.25 8.78 o 1 4 5 233.12 229.09 12.12 o 2 4 5 85.07 91.05 13.51 o 3 4 5 60.12 63.14 15.64 o 4 4 5 2.43 7.15 9.83 o 5 4 5 20.51 5.98 10.80 o -4 5 5 44.65 26.91 37.98 o -3 5 5 258.54 266.91 22.58 o -2 5 5 37.73 35.27 9.18 o -1 5 5 334.34 372.97 27.66 o 0 5 5 2.37 -10.76 10.76 o 1 5 5 321.43 346.99 19.28 o 2 5 5 31.51 42.85 11.68 o 3 5 5 246.95 239.25 19.33 o 4 5 5 45.38 41.77 11.48 o -4 6 5 51.27 30.03 25.88 o -3 6 5 149.84 138.70 25.51 o -2 6 5 165.99 138.10 21.21 o -1 6 5 726.74 733.66 34.93 o 0 6 5 109.04 157.89 21.35 o 1 6 5 718.69 748.90 36.56 o 2 6 5 175.67 166.17 19.62 o 3 6 5 152.73 92.33 26.61 o 4 6 5 50.60 33.46 11.94 o -4 7 5 87.77 27.12 60.86 o -3 7 5 68.94 37.15 21.47 o -2 7 5 17.73 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