#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/71/2227134.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2227134_Fobs loop_ _publ_author_name 'Vafaee, Maryam' 'Amini, Mostafa M.' 'Ng, Seik Weng' _publ_section_title ; Bis(\m-quinolin-8-olato)-\k^3^N,O:O;\k^3^O:N,O-bis[chloridomethylphenyltin(IV)] ; _journal_coeditor_code XU2799 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m964 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.232 _cell_angle_gamma 90.000 _cell_length_a 7.9967 _cell_length_b 17.8081 _cell_length_c 10.1623 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file xu2799Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 75502.57 55338.83 6954.75 o 2 0 0 657.08 571.11 13.35 o 3 0 0 1391.02 1442.89 28.09 o 4 0 0 713.16 745.65 19.81 o 5 0 0 1963.88 1924.02 39.65 o 6 0 0 7309.28 7028.05 114.14 o 7 0 0 10096.80 10088.49 200.58 o 8 0 0 8180.05 8377.63 154.70 o 9 0 0 1736.62 1757.10 68.18 o 10 0 0 2.44 -5.74 14.94 o 1 1 0 548.68 648.16 10.05 o 2 1 0 4140.36 4180.49 44.86 o 3 1 0 352.79 332.43 15.35 o 4 1 0 2095.36 2149.22 28.60 o 5 1 0 1316.99 1324.68 21.77 o 6 1 0 2952.76 2938.93 40.09 o 7 1 0 1241.05 1211.25 23.26 o 8 1 0 1316.58 1380.92 36.50 o 9 1 0 1550.49 1478.58 45.73 o 10 1 0 1258.80 1372.90 43.90 o 0 2 0 14134.76 13576.74 212.07 o 1 2 0 13865.79 13664.92 170.06 o 2 2 0 2484.28 2433.23 27.73 o 3 2 0 3686.68 3767.67 42.70 o 4 2 0 858.44 828.67 14.84 o 5 2 0 6067.55 6057.75 69.25 o 6 2 0 627.11 572.58 14.91 o 7 2 0 1127.20 1131.85 22.43 o 8 2 0 1333.67 1306.38 30.19 o 9 2 0 773.82 756.43 30.08 o 10 2 0 1020.78 1040.55 38.06 o 1 3 0 7960.80 8173.14 82.85 o 2 3 0 202.89 142.24 6.68 o 3 3 0 26275.72 24791.69 256.14 o 4 3 0 30179.92 29221.32 300.21 o 5 3 0 8303.04 8005.83 88.30 o 6 3 0 710.72 687.90 15.99 o 7 3 0 254.35 255.16 13.85 o 8 3 0 435.01 438.56 17.33 o 9 3 0 1286.22 1329.31 41.07 o 10 3 0 3423.92 3635.05 79.82 o 0 4 0 3227.12 3175.91 48.44 o 1 4 0 11963.49 12208.54 123.66 o 2 4 0 13310.08 13595.63 137.43 o 3 4 0 6237.63 6597.90 70.79 o 4 4 0 8.41 4.31 2.90 o 5 4 0 3904.24 3819.34 47.00 o 6 4 0 2062.93 2036.79 44.95 o 7 4 0 547.74 561.88 15.37 o 8 4 0 419.59 479.63 31.69 o 9 4 0 774.58 788.62 31.35 o 10 4 0 385.13 429.39 37.28 o 1 5 0 10402.71 11131.42 121.76 o 2 5 0 3962.54 4040.44 44.66 o 3 5 0 4843.44 5048.88 56.10 o 4 5 0 7758.91 8154.59 88.11 o 5 5 0 777.74 758.09 19.70 o 6 5 0 28.15 24.95 5.06 o 7 5 0 221.56 232.11 13.35 o 8 5 0 262.24 279.66 26.36 o 9 5 0 1434.33 1427.98 42.89 o 10 5 0 796.72 854.39 34.91 o 0 6 0 21305.85 20782.91 303.94 o 1 6 0 10948.53 10748.33 117.79 o 2 6 0 5325.90 5394.59 58.60 o 3 6 0 2936.94 3200.74 43.70 o 4 6 0 10.42 28.27 4.46 o 5 6 0 900.56 895.39 17.09 o 6 6 0 4771.07 4760.56 58.70 o 7 6 0 9887.59 9908.00 111.67 o 8 6 0 5325.74 5409.32 81.00 o 9 6 0 2770.63 2886.16 66.53 o 1 7 0 1494.76 1472.26 20.73 o 2 7 0 4482.98 4492.00 50.46 o 3 7 0 4351.50 4216.04 48.72 o 4 7 0 2230.09 2121.22 29.15 o 5 7 0 2595.27 2549.40 34.92 o 6 7 0 384.48 394.51 13.38 o 7 7 0 264.13 269.34 11.49 o 8 7 0 290.87 320.82 16.19 o 9 7 0 337.97 375.87 32.89 o 0 8 0 3441.18 3576.42 58.60 o 1 8 0 515.04 446.76 9.56 o 2 8 0 300.25 261.08 7.44 o 3 8 0 85.78 97.31 9.13 o 4 8 0 81.83 101.44 6.23 o 5 8 0 121.88 117.59 7.49 o 6 8 0 707.49 716.77 16.54 o 7 8 0 920.79 942.97 30.07 o 8 8 0 1178.98 1228.45 62.31 o 9 8 0 206.08 187.96 14.35 o 1 9 0 5766.47 6108.15 67.30 o 2 9 0 11397.68 11682.73 122.38 o 3 9 0 7642.20 7617.01 83.50 o 4 9 0 9648.96 9660.62 120.34 o 5 9 0 6075.58 6194.75 72.48 o 6 9 0 1782.91 1862.83 29.96 o 7 9 0 76.53 89.54 9.52 o 8 9 0 1331.63 1264.89 32.45 o 9 9 0 1198.41 1223.88 49.38 o 0 10 0 10198.38 10336.70 154.43 o 1 10 0 6016.55 6260.42 69.60 o 2 10 0 1846.13 1918.76 26.82 o 3 10 0 1.59 12.26 3.33 o 4 10 0 0.22 2.38 3.13 o 5 10 0 26.80 39.16 5.16 o 6 10 0 3867.19 3766.25 50.17 o 7 10 0 5114.61 5106.39 76.92 o 8 10 0 2095.14 2141.96 43.13 o 9 10 0 614.01 637.88 29.71 o 1 11 0 395.08 385.26 12.14 o 2 11 0 2.79 10.90 3.16 o 3 11 0 1716.06 1773.96 26.58 o 4 11 0 1321.38 1312.49 22.45 o 5 11 0 1044.45 1051.02 20.62 o 6 11 0 4.88 14.54 4.65 o 7 11 0 535.77 501.09 20.58 o 8 11 0 17.12 5.90 6.56 o 9 11 0 6.47 6.45 10.00 o 0 12 0 6780.28 6998.28 110.69 o 1 12 0 11528.70 11491.50 122.69 o 2 12 0 9336.67 9230.94 101.00 o 3 12 0 1884.08 1841.53 38.61 o 4 12 0 246.21 257.26 9.90 o 5 12 0 4731.46 4766.13 60.17 o 6 12 0 6151.98 6013.45 100.38 o 7 12 0 3708.97 3626.11 60.73 o 8 12 0 1830.06 1891.28 40.81 o 1 13 0 484.59 504.53 12.70 o 2 13 0 1636.40 1621.82 25.75 o 3 13 0 7329.55 7342.81 84.10 o 4 13 0 9385.02 9444.60 105.72 o 5 13 0 2624.43 2699.30 39.76 o 6 13 0 45.98 56.75 6.87 o 7 13 0 108.70 113.23 14.36 o 8 13 0 8.12 5.90 8.93 o 0 14 0 4517.55 4586.07 122.03 o 1 14 0 2320.42 2265.81 32.99 o 2 14 0 0.33 2.72 3.60 o 3 14 0 184.67 175.30 9.02 o 4 14 0 523.40 531.13 20.14 o 5 14 0 548.72 540.95 15.47 o 6 14 0 504.58 493.38 24.32 o 7 14 0 1122.06 1113.19 37.26 o 8 14 0 495.78 545.55 28.32 o 1 15 0 2283.10 2263.51 33.74 o 2 15 0 8037.70 7859.20 90.31 o 3 15 0 7463.12 7501.12 131.44 o 4 15 0 4122.52 4117.52 54.41 o 5 15 0 4252.75 4221.16 64.53 o 6 15 0 2360.20 2414.45 48.59 o 7 15 0 64.39 77.14 13.38 o 0 16 0 14632.25 14254.55 306.63 o 1 16 0 4131.07 4009.23 52.50 o 2 16 0 8.60 31.58 9.51 o 3 16 0 20.35 30.80 6.48 o 4 16 0 14.55 19.91 5.24 o 5 16 0 276.00 290.10 16.37 o 6 16 0 700.93 699.51 22.67 o 7 16 0 2382.41 2332.36 60.87 o 1 17 0 592.75 599.38 15.88 o 2 17 0 37.36 40.62 5.68 o 3 17 0 834.99 819.73 19.26 o 4 17 0 1321.84 1323.23 26.02 o 5 17 0 641.72 685.37 20.98 o 6 17 0 45.37 54.26 9.04 o 7 17 0 365.98 366.69 24.84 o 0 18 0 10526.75 10524.27 169.06 o 1 18 0 7745.44 7614.45 90.58 o 2 18 0 4169.43 4080.20 55.38 o 3 18 0 866.30 871.43 20.53 o 4 18 0 199.99 205.66 12.63 o 5 18 0 2463.55 2450.53 47.77 o 6 18 0 2160.06 2186.93 58.64 o 1 19 0 961.79 1016.40 25.91 o 2 19 0 433.49 485.31 15.39 o 3 19 0 1741.40 1762.29 31.99 o 4 19 0 3317.97 3233.92 48.70 o 5 19 0 1047.63 1070.25 35.30 o 0 20 0 1877.56 1843.73 59.11 o 1 20 0 1333.60 1341.98 31.17 o 2 20 0 52.75 46.59 6.74 o 3 20 0 268.65 270.36 12.99 o 4 20 0 20.12 48.00 7.39 o 5 20 0 34.42 37.29 15.33 o 1 21 0 1120.92 1048.24 29.38 o 2 21 0 1190.85 1170.37 26.10 o 3 21 0 1144.22 1215.00 32.62 o 4 21 0 2770.12 2870.97 46.60 o 0 22 0 3719.78 3711.18 108.64 o 1 22 0 1723.15 1695.45 33.26 o 2 22 0 1676.85 1669.54 49.02 o 3 22 0 1214.10 1223.46 57.81 o 1 23 0 206.97 205.21 13.18 o -10 1 1 1478.86 1495.86 49.03 o -9 1 1 7456.05 7364.58 171.98 o -8 1 1 6155.30 6118.46 110.81 o -7 1 1 2595.47 2593.82 39.06 o -6 1 1 2750.05 2806.80 42.40 o -5 1 1 498.31 502.81 12.00 o -4 1 1 700.18 661.00 13.25 o -3 1 1 6284.08 6288.61 67.03 o -2 1 1 13509.93 13426.31 136.93 o -1 1 1 9587.03 9504.93 112.61 o 0 1 1 13512.30 13208.29 136.21 o 1 1 1 11465.89 11580.35 119.49 o 2 1 1 1601.89 1783.97 25.37 o 3 1 1 1264.92 1194.84 17.45 o 4 1 1 6315.01 6357.08 70.68 o 5 1 1 14430.20 14405.47 151.58 o 6 1 1 11657.42 11827.55 128.43 o 7 1 1 2761.83 2801.44 40.74 o 8 1 1 853.35 853.49 20.65 o 9 1 1 13.41 8.56 9.76 o 10 1 1 242.26 274.94 22.18 o -10 2 1 2584.02 2527.53 63.37 o -9 2 1 580.95 553.87 26.52 o -8 2 1 427.66 434.91 26.24 o -7 2 1 4522.69 4483.78 98.75 o -6 2 1 9160.04 9243.13 109.37 o -5 2 1 10212.98 10287.52 110.22 o -4 2 1 5728.96 5515.99 61.45 o -3 2 1 4511.69 4423.12 48.70 o -2 2 1 3309.52 3386.07 36.83 o -1 2 1 6559.94 6737.83 100.69 o 0 2 1 7820.92 7793.69 143.41 o 1 2 1 26326.42 25438.92 443.84 o 2 2 1 47918.50 41096.09 2124.48 o 3 2 1 12891.13 12259.03 367.66 o 4 2 1 8738.63 8828.32 94.68 o 5 2 1 4933.70 5155.46 70.18 o 6 2 1 942.35 958.52 19.74 o 7 2 1 717.98 707.51 17.70 o 8 2 1 5395.68 5567.31 70.59 o 9 2 1 4102.93 4248.04 138.09 o 10 2 1 2316.81 2302.34 84.43 o -10 3 1 52.23 33.60 13.25 o -9 3 1 3.11 5.79 10.04 o -8 3 1 52.40 62.36 12.00 o -7 3 1 12.20 9.07 5.91 o -6 3 1 225.09 236.06 9.89 o -5 3 1 199.40 179.52 8.22 o -4 3 1 1057.87 1187.49 18.17 o -3 3 1 284.88 293.62 6.90 o -2 3 1 420.69 429.76 7.69 o -1 3 1 1715.95 1926.50 21.88 o 0 3 1 6291.33 6699.02 78.75 o 1 3 1 10623.14 11026.02 112.39 o 2 3 1 20167.26 20186.01 206.84 o 3 3 1 3433.50 3707.77 49.60 o 4 3 1 272.82 280.70 14.53 o 5 3 1 136.46 180.25 11.62 o 6 3 1 352.71 343.12 11.87 o 7 3 1 49.08 44.09 6.53 o 8 3 1 89.22 102.65 9.39 o 9 3 1 148.57 132.22 12.42 o 10 3 1 37.44 64.63 21.62 o -10 4 1 428.27 373.13 25.59 o -9 4 1 130.24 156.04 17.34 o -8 4 1 379.47 363.57 21.15 o -7 4 1 367.21 387.75 15.16 o -6 4 1 5605.65 5703.01 67.30 o -5 4 1 14629.94 14269.02 149.38 o -4 4 1 10940.27 10702.55 112.43 o -3 4 1 5601.72 5616.22 60.91 o -2 4 1 5.57 12.23 2.69 o -1 4 1 73.26 95.53 4.51 o 0 4 1 5557.99 5515.14 57.29 o 1 4 1 29914.66 28440.33 296.57 o 2 4 1 38852.55 36866.32 557.22 o 3 4 1 26026.11 25395.84 359.22 o 4 4 1 4136.97 3938.27 46.65 o 5 4 1 685.19 742.21 20.75 o 6 4 1 1148.68 1107.05 21.10 o 7 4 1 1279.86 1274.08 30.20 o 8 4 1 358.78 370.38 14.12 o 9 4 1 2580.29 2651.04 49.55 o 10 4 1 2349.66 2448.72 90.70 o -10 5 1 3737.41 3885.38 85.16 o -9 5 1 2938.64 3059.64 69.70 o -8 5 1 2160.71 2117.69 62.19 o -7 5 1 2847.88 2872.55 48.44 o -6 5 1 3079.11 3162.90 42.09 o -5 5 1 875.69 905.69 16.79 o -4 5 1 4597.61 4513.85 52.03 o -3 5 1 17597.32 17439.32 176.99 o -2 5 1 21507.84 21054.71 246.07 o -1 5 1 3512.22 3360.37 37.28 o 0 5 1 282.17 214.64 5.26 o 1 5 1 14548.19 14400.56 168.00 o 2 5 1 604.95 755.91 20.25 o 3 5 1 5325.63 5408.62 69.42 o 4 5 1 6790.87 6302.36 70.18 o 5 5 1 10297.11 10212.16 110.45 o 6 5 1 3804.73 3824.99 49.46 o 7 5 1 2717.22 2702.66 39.79 o 8 5 1 871.08 844.64 23.99 o 9 5 1 156.61 195.66 14.64 o 10 5 1 41.65 48.90 21.42 o -10 6 1 74.03 85.77 16.18 o -9 6 1 104.53 125.25 21.11 o -8 6 1 85.69 91.09 9.99 o -7 6 1 562.24 539.95 17.84 o -6 6 1 207.27 205.36 9.22 o -5 6 1 896.87 894.86 16.87 o -4 6 1 1008.86 1046.84 17.32 o -3 6 1 193.08 203.91 6.92 o -2 6 1 5670.74 6170.77 66.26 o -1 6 1 2499.90 2769.22 32.12 o 0 6 1 4.44 16.22 8.64 o 1 6 1 459.26 487.82 25.50 o 2 6 1 47.18 28.46 4.11 o 3 6 1 4444.44 4794.88 63.07 o 4 6 1 680.09 744.72 14.35 o 5 6 1 2.62 2.63 3.61 o 6 6 1 361.05 365.60 13.95 o 7 6 1 4.78 3.85 4.98 o 8 6 1 216.90 243.94 14.44 o 9 6 1 139.35 151.29 16.88 o -9 7 1 4097.64 4116.89 118.03 o -8 7 1 5279.73 5307.97 80.35 o -7 7 1 3927.89 3943.06 62.06 o -6 7 1 342.22 359.25 12.11 o -5 7 1 1412.46 1421.12 22.92 o -4 7 1 319.86 324.27 9.09 o -3 7 1 3221.19 3324.42 39.98 o -2 7 1 21307.69 21502.67 216.63 o -1 7 1 30257.61 29605.03 540.08 o 0 7 1 12401.54 12611.55 148.90 o 1 7 1 64.76 106.71 4.65 o 2 7 1 256.71 252.28 19.51 o 3 7 1 1029.37 1059.17 23.36 o 4 7 1 132.28 119.81 11.95 o 5 7 1 1983.02 1900.05 37.10 o 6 7 1 11041.16 11109.51 121.95 o 7 7 1 5202.17 5239.09 66.02 o 8 7 1 546.20 549.31 25.99 o 9 7 1 387.24 396.26 23.15 o -9 8 1 209.24 235.12 21.10 o -8 8 1 2126.01 2119.33 42.26 o -7 8 1 6785.17 6614.25 93.72 o -6 8 1 3985.32 3963.47 50.98 o -5 8 1 4279.19 4230.95 52.14 o -4 8 1 6285.71 6210.89 70.36 o -3 8 1 6861.34 6688.73 84.35 o -2 8 1 736.28 628.98 11.91 o -1 8 1 3133.48 3336.03 39.15 o 0 8 1 7277.80 7282.62 89.59 o 1 8 1 31675.05 30788.15 319.46 o 2 8 1 24878.94 25336.55 257.19 o 3 8 1 2717.14 2741.69 34.86 o 4 8 1 3915.76 3915.14 47.67 o 5 8 1 2217.67 2281.71 32.80 o 6 8 1 0.87 1.78 4.04 o 7 8 1 1881.15 1949.96 32.40 o 8 8 1 5958.92 5852.57 86.79 o 9 8 1 3675.42 3777.66 81.60 o -9 9 1 498.26 467.34 25.32 o -8 9 1 705.27 747.06 23.40 o -7 9 1 333.50 344.88 15.27 o -6 9 1 427.29 412.96 15.45 o -5 9 1 656.53 700.43 23.27 o -4 9 1 556.06 553.22 12.82 o -3 9 1 582.42 578.47 12.52 o -2 9 1 69.39 57.14 7.99 o -1 9 1 1739.85 1684.43 23.33 o 0 9 1 1282.91 1270.35 21.62 o 1 9 1 195.93 224.65 8.11 o 2 9 1 296.85 228.06 7.57 o 3 9 1 55.30 73.48 5.26 o 4 9 1 594.02 564.08 13.03 o 5 9 1 4.38 9.45 3.92 o 6 9 1 958.23 945.02 19.62 o 7 9 1 896.95 924.26 20.79 o 8 9 1 218.79 258.74 33.62 o 9 9 1 59.75 70.22 13.43 o -9 10 1 433.38 451.10 26.52 o -8 10 1 693.04 617.92 21.71 o -7 10 1 1464.80 1435.55 32.13 o -6 10 1 4649.62 4615.71 69.35 o -5 10 1 5562.69 5590.69 66.85 o -4 10 1 5998.18 5812.31 67.80 o -3 10 1 703.66 676.87 13.97 o -2 10 1 1404.92 1508.33 22.58 o -1 10 1 1744.84 1796.97 25.12 o 0 10 1 1642.20 1600.65 26.35 o 1 10 1 3430.26 3454.58 41.95 o 2 10 1 9861.20 9893.42 105.87 o 3 10 1 8939.14 8702.18 95.10 o 4 10 1 2504.71 2480.58 34.39 o 5 10 1 114.98 124.15 9.80 o 6 10 1 578.98 614.02 15.86 o 7 10 1 775.76 803.71 19.49 o 8 10 1 634.25 616.16 44.38 o 9 10 1 2019.95 2077.98 90.93 o -9 11 1 2247.41 2327.96 60.65 o -8 11 1 3354.05 3498.00 60.80 o -7 11 1 3108.69 3089.32 53.77 o -6 11 1 4278.60 4168.77 64.70 o -5 11 1 512.05 470.20 13.05 o -4 11 1 1961.41 1927.12 33.39 o -3 11 1 12484.60 12647.96 134.32 o -2 11 1 21289.96 21649.38 221.52 o -1 11 1 6603.78 6569.19 73.40 o 0 11 1 6808.74 6922.89 76.90 o 1 11 1 9722.45 9850.70 105.75 o 2 11 1 1118.13 1122.95 19.14 o 3 11 1 1330.04 1401.50 34.38 o 4 11 1 5598.08 5581.06 79.32 o 5 11 1 6990.14 7135.67 83.35 o 6 11 1 4000.22 4012.82 53.51 o 7 11 1 2466.08 2498.44 39.27 o 8 11 1 1194.58 1214.68 40.14 o -8 12 1 2.25 3.09 6.40 o -7 12 1 17.72 24.03 7.04 o -6 12 1 113.35 100.41 9.79 o -5 12 1 440.14 391.55 16.35 o -4 12 1 921.85 906.49 20.78 o -3 12 1 83.53 96.66 9.14 o -2 12 1 106.38 126.63 9.10 o -1 12 1 450.12 494.24 11.99 o 0 12 1 42.49 42.77 4.50 o 1 12 1 258.13 262.80 8.82 o 2 12 1 797.53 788.61 15.90 o 3 12 1 452.90 462.45 12.29 o 4 12 1 720.54 708.37 16.12 o 5 12 1 21.00 17.04 5.11 o 6 12 1 438.61 423.64 13.90 o 7 12 1 66.71 68.64 15.90 o 8 12 1 21.64 15.17 11.01 o -8 13 1 1880.15 1876.90 57.87 o -7 13 1 1558.28 1572.86 35.64 o -6 13 1 233.18 222.37 13.96 o -5 13 1 451.05 409.31 12.95 o -4 13 1 23.07 43.06 6.41 o -3 13 1 3703.46 3732.32 48.06 o -2 13 1 5857.50 5735.19 67.45 o -1 13 1 8129.99 7986.17 103.16 o 0 13 1 5346.79 5424.80 63.89 o 1 13 1 1166.10 1160.38 20.45 o 2 13 1 183.84 216.50 8.78 o 3 13 1 576.79 602.91 14.65 o 4 13 1 921.55 949.09 19.34 o 5 13 1 3215.94 3191.02 50.96 o 6 13 1 4036.67 4085.50 55.52 o 7 13 1 2005.20 1956.87 62.59 o 8 13 1 333.00 317.20 22.70 o -8 14 1 424.08 397.23 18.75 o -7 14 1 1972.97 2005.68 42.08 o -6 14 1 4162.48 4088.09 66.16 o -5 14 1 6275.73 6214.85 76.14 o -4 14 1 4081.13 3928.47 51.54 o -3 14 1 4195.83 4132.40 52.92 o -2 14 1 634.22 621.94 14.95 o -1 14 1 272.13 304.66 15.16 o 0 14 1 2119.29 2115.68 31.37 o 1 14 1 10193.44 10167.86 111.79 o 2 14 1 12017.32 11842.41 128.62 o 3 14 1 6412.48 6356.70 92.40 o 4 14 1 2990.88 2975.79 42.09 o 5 14 1 1013.37 1041.72 24.70 o 6 14 1 7.12 3.72 5.40 o 7 14 1 638.61 655.14 28.89 o 8 14 1 2546.11 2472.59 63.74 o -7 15 1 272.78 256.55 16.43 o -6 15 1 109.15 116.89 11.03 o -5 15 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